#------------------------------------------------------------------------------ #$Date: 2009-05-03 21:56:13 +0300 (Sun, 03 May 2009) $ #$Revision: 691 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2217787.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2217787_Fobs loop_ _publ_author_name 'Luo, Wei' 'Liu, Rui' 'Li, Yu-Hao' 'Chen, Wei' 'Zhu, Hong-Jun' _publ_section_title ; 4-Iodo-2-methylaniline ; _journal_coeditor_code HK2418 _journal_issue 3 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o591 _journal_volume 64 _journal_year 2008 _space_group_IT_number 19 _symmetry_space_group_name_Hall 'P 2ac 2ab' _symmetry_space_group_name_H-M 'P 21 21 21' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 5.5910 _cell_length_b 8.9410 _cell_length_c 15.6740 _exptl_crystal_F_000 440.00 _reflns_d_resolution_high 0.8117 _[local]_cod_data_source_file hk2418Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' X in P2(1)2(1)2(1)' _shelx_refln_list_code 4 _shelx_F_calc_maximum 170.28 _shelx_F_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 28565.21 26934.89 531.20 o 4 0 0 1617.09 1696.46 43.54 o 6 0 0 265.67 280.86 26.57 o 1 1 0 3725.83 4048.93 24.82 o 2 1 0 1730.97 1825.56 4.16 o 3 1 0 227.12 268.10 5.80 o 4 1 0 221.46 209.59 14.37 o 5 1 0 55.25 9.27 11.19 o 6 1 0 28.20 34.12 13.53 o 0 2 0 6632.40 6486.84 35.40 o 1 2 0 1593.19 1905.85 24.61 o 2 2 0 7912.64 7829.17 3.89 o 3 2 0 2447.97 2622.49 5.91 o 4 2 0 1594.66 1337.58 27.16 o 5 2 0 177.87 174.33 14.80 o 6 2 0 54.96 58.02 12.55 o 1 3 0 67.95 78.91 6.46 o 2 3 0 25.26 5.36 5.36 o 3 3 0 111.07 112.15 9.85 o 4 3 0 14.94 6.98 7.49 o 5 3 0 47.47 33.47 10.04 o 6 3 0 0.03 1.48 10.26 o 0 4 0 1289.11 1327.90 21.39 o 1 4 0 11193.63 10626.49 7.59 o 2 4 0 985.69 975.25 23.02 o 3 4 0 3594.28 3190.51 42.05 o 4 4 0 257.07 252.21 9.31 o 5 4 0 425.51 434.82 10.68 o 6 4 0 9.33 42.92 9.63 o 1 5 0 13.99 26.75 6.47 o 2 5 0 90.02 84.02 10.53 o 3 5 0 70.58 78.32 10.48 o 4 5 0 29.07 22.00 10.72 o 5 5 0 23.88 8.15 11.78 o 6 5 0 0.02 10.58 12.93 o 0 6 0 1269.70 1183.48 25.42 o 1 6 0 4141.03 4066.24 48.00 o 2 6 0 498.53 480.41 19.80 o 3 6 0 1733.63 1461.24 35.17 o 4 6 0 40.38 17.25 12.64 o 5 6 0 172.64 173.66 17.71 o 1 7 0 17.23 15.79 9.66 o 2 7 0 319.41 296.25 18.88 o 3 7 0 60.60 5.55 11.09 o 4 7 0 21.13 23.79 14.06 o 5 7 0 18.42 17.48 17.48 o 0 8 0 1092.96 982.14 29.53 o 1 8 0 1583.03 1585.65 38.83 o 2 8 0 339.28 403.08 21.54 o 3 8 0 102.07 112.38 17.68 o 4 8 0 35.77 3.06 13.41 o 1 9 0 37.61 37.27 15.50 o 2 9 0 36.11 73.67 14.53 o 3 9 0 1.96 15.47 15.47 o 0 10 0 139.53 146.76 18.14 o 1 10 0 22.41 51.11 16.36 o 2 10 0 265.85 274.40 23.75 o 1 0 1 27494.38 25481.77 335.53 o 2 0 1 360.71 406.15 14.54 o 3 0 1 7145.94 7369.85 64.97 o 4 0 1 0.61 0.78 10.13 o 5 0 1 735.70 771.39 13.58 o 6 0 1 5.25 2.38 15.04 o 0 1 1 307.75 313.43 12.40 o 1 1 1 896.65 696.36 10.58 o 2 1 1 307.86 399.09 11.63 o 3 1 1 515.87 524.36 15.85 o 4 1 1 73.95 51.00 9.20 o 5 1 1 34.91 11.10 11.10 o 6 1 1 15.50 32.42 12.50 o 0 2 1 4650.99 4439.12 35.68 o 1 2 1 25760.21 24887.78 5.02 o 2 2 1 4841.93 4578.24 5.73 o 3 2 1 4087.03 4071.07 6.36 o 4 2 1 983.77 1034.98 7.10 o 5 2 1 418.31 425.57 7.02 o 6 2 1 39.09 3.46 10.30 o 0 3 1 15.96 11.29 3.88 o 1 3 1 316.84 380.99 12.83 o 2 3 1 9.52 9.03 5.42 o 3 3 1 66.62 51.36 7.79 o 4 3 1 115.09 133.98 7.84 o 5 3 1 36.95 9.58 9.58 o 6 3 1 14.03 14.33 10.87 o 0 4 1 11720.67 10248.63 58.82 o 1 4 1 553.77 591.72 17.35 o 2 4 1 6545.06 6152.55 55.59 o 3 4 1 395.50 350.28 16.10 o 4 4 1 1083.83 1126.34 9.17 o 5 4 1 32.94 30.93 11.19 o 6 4 1 80.64 7.37 11.74 o 0 5 1 2.57 6.46 5.60 o 1 5 1 93.94 112.63 9.04 o 2 5 1 68.63 79.06 9.55 o 3 5 1 81.26 90.70 11.45 o 4 5 1 136.93 97.76 13.94 o 5 5 1 8.03 4.15 10.57 o 6 5 1 33.08 10.01 10.90 o 0 6 1 6680.99 6210.44 56.43 o 1 6 1 584.13 553.01 20.04 o 2 6 1 3394.54 3140.35 47.55 o 3 6 1 12.04 1.44 10.48 o 4 6 1 619.65 636.28 27.94 o 5 6 1 9.27 34.09 12.81 o 0 7 1 0.07 0.00 8.50 o 1 7 1 86.77 94.30 13.10 o 2 7 1 94.35 84.42 13.81 o 3 7 1 27.66 3.34 10.21 o 4 7 1 1.08 3.80 12.53 o 5 7 1 18.97 31.21 13.35 o 0 8 1 676.26 688.50 27.11 o 1 8 1 767.78 812.00 29.10 o 2 8 1 356.52 391.95 25.28 o 3 8 1 357.69 383.50 24.51 o 4 8 1 68.73 52.51 16.82 o 0 9 1 0.15 6.14 11.98 o 1 9 1 18.57 17.33 14.84 o 2 9 1 0.49 5.23 14.23 o 3 9 1 17.94 17.37 17.37 o 0 10 1 13.13 25.23 14.67 o 1 10 1 282.26 305.62 24.70 o 2 10 1 1.94 10.78 16.67 o 0 11 1 8.32 24.03 13.30 o 0 0 2 10795.08 11781.26 167.07 o 1 0 2 1451.20 1349.73 26.40 o 2 0 2 12293.70 12968.07 69.14 o 3 0 2 194.85 223.95 12.62 o 4 0 2 2675.44 2553.27 43.44 o 5 0 2 0.07 6.95 11.93 o 6 0 2 132.21 140.64 19.28 o 0 1 2 933.78 891.41 17.74 o 1 1 2 2212.41 2155.92 21.93 o 2 1 2 97.41 137.10 7.56 o 3 1 2 393.43 393.48 6.73 o 4 1 2 180.43 136.66 11.86 o 5 1 2 45.24 33.30 11.52 o 6 1 2 21.43 22.88 12.12 o 0 2 2 27875.39 23358.10 350.49 o 1 2 2 16772.14 13542.11 259.78 o 2 2 2 9014.46 8381.34 48.32 o 3 2 2 1699.88 1552.75 25.48 o 4 2 2 1376.68 1326.04 7.14 o 5 2 2 143.15 156.64 14.70 o 6 2 2 139.38 136.50 9.87 o 0 3 2 140.95 175.63 9.08 o 1 3 2 36.23 61.92 6.51 o 2 3 2 683.02 802.39 18.69 o 3 3 2 320.61 322.77 6.03 o 4 3 2 18.21 0.48 8.39 o 5 3 2 128.27 146.09 9.02 o 6 3 2 7.37 4.24 10.22 o 0 4 2 1137.50 1282.30 23.28 o 1 4 2 9160.26 9118.69 64.72 o 2 4 2 1113.52 1135.62 25.57 o 3 4 2 4099.42 4082.65 9.14 o 4 4 2 217.44 200.41 14.92 o 5 4 2 248.38 293.85 19.89 o 6 4 2 8.90 1.68 11.51 o 0 5 2 526.04 493.68 16.17 o 1 5 2 195.16 205.25 12.41 o 2 5 2 326.07 311.30 16.15 o 3 5 2 158.17 178.64 9.82 o 4 5 2 51.03 60.15 12.64 o 5 5 2 24.14 32.73 12.73 o 6 5 2 9.59 22.56 11.94 o 0 6 2 62.70 60.23 10.74 o 1 6 2 5115.97 5040.58 55.95 o 2 6 2 79.30 72.69 13.52 o 3 6 2 875.69 884.18 28.74 o 4 6 2 47.40 16.49 10.65 o 5 6 2 161.34 159.50 18.43 o 0 7 2 40.70 49.27 11.16 o 1 7 2 59.71 74.46 12.40 o 2 7 2 27.24 12.36 12.25 o 3 7 2 2.05 29.50 11.80 o 4 7 2 47.37 0.95 14.42 o 5 7 2 0.23 16.51 16.51 o 0 8 2 1014.03 1030.31 32.59 o 1 8 2 267.17 274.74 19.99 o 2 8 2 778.34 783.03 32.92 o 3 8 2 238.97 272.14 21.26 o 4 8 2 143.16 161.88 21.08 o 0 9 2 12.79 13.90 13.90 o 1 9 2 15.44 31.25 13.76 o 2 9 2 49.77 56.59 15.96 o 3 9 2 23.92 15.14 16.72 o 0 10 2 581.62 642.18 33.14 o 1 10 2 20.06 45.30 16.50 o 2 10 2 226.93 222.64 26.06 o 1 0 3 28996.76 25694.75 344.70 o 2 0 3 57.11 69.12 8.24 o 3 0 3 7318.07 7109.61 58.59 o 4 0 3 12.42 11.93 9.90 o 5 0 3 738.82 733.78 29.01 o 6 0 3 6.24 1.14 13.48 o 0 1 3 6030.61 5938.69 140.75 o 1 1 3 771.41 942.59 14.18 o 2 1 3 695.43 783.37 16.37 o 3 1 3 217.85 176.55 10.85 o 4 1 3 61.95 45.53 10.43 o 5 1 3 56.11 34.11 12.18 o 6 1 3 16.52 41.76 11.09 o 0 2 3 12502.92 13237.15 276.74 o 1 2 3 7803.52 8130.54 47.71 o 2 2 3 5433.73 5308.20 5.58 o 3 2 3 3209.58 3245.09 6.46 o 4 2 3 606.50 582.44 8.22 o 5 2 3 321.06 301.15 19.27 o 6 2 3 42.57 39.63 13.27 o 0 3 3 10.55 14.25 5.29 o 1 3 3 9.42 3.12 5.88 o 2 3 3 1276.81 1333.09 23.28 o 3 3 3 460.41 500.42 6.59 o 4 3 3 282.79 288.75 8.20 o 5 3 3 99.97 149.18 10.87 o 6 3 3 33.38 31.43 13.32 o 0 4 3 17516.11 16132.76 83.23 o 1 4 3 3860.97 4321.20 46.96 o 2 4 3 6856.87 6644.01 57.62 o 3 4 3 756.87 744.57 8.93 o 4 4 3 923.67 948.42 8.68 o 5 4 3 80.49 12.87 12.87 o 6 4 3 68.80 76.92 14.91 o 0 5 3 161.73 194.28 11.92 o 1 5 3 392.11 432.91 17.03 o 2 5 3 97.45 96.32 11.25 o 3 5 3 166.78 171.99 14.08 o 4 5 3 36.72 5.24 11.25 o 5 5 3 15.11 7.15 11.57 o 6 5 3 5.94 3.90 12.31 o 0 6 3 2713.95 2689.71 41.54 o 1 6 3 260.02 267.28 16.85 o 2 6 3 1953.61 1855.83 38.94 o 3 6 3 222.54 247.93 17.92 o 4 6 3 394.38 422.86 13.36 o 5 6 3 17.35 7.19 12.98 o 0 7 3 123.49 124.77 13.58 o 1 7 3 174.82 179.01 15.68 o 2 7 3 29.29 53.67 12.54 o 3 7 3 43.96 41.99 15.85 o 4 7 3 22.56 31.49 14.09 o 5 7 3 20.28 0.00 13.56 o 0 8 3 607.07 670.45 27.98 o 1 8 3 871.26 878.44 33.26 o 2 8 3 405.65 377.64 25.92 o 3 8 3 220.99 271.68 22.06 o 4 8 3 112.72 119.28 20.94 o 0 9 3 92.79 108.97 17.01 o 1 9 3 15.78 54.31 13.48 o 2 9 3 52.55 39.08 17.45 o 3 9 3 25.27 58.31 15.97 o 0 10 3 0.56 10.07 14.11 o 1 10 3 403.69 403.69 31.52 o 2 10 3 7.39 7.68 18.15 o 0 0 4 25807.17 21319.31 295.18 o 1 0 4 100.14 144.11 8.16 o 2 0 4 11136.98 11724.50 66.09 o 3 0 4 15.71 12.48 9.21 o 4 0 4 1708.01 1548.11 34.02 o 5 0 4 19.26 17.22 13.25 o 6 0 4 98.41 81.23 17.21 o 0 1 4 14.27 21.49 3.46 o 1 1 4 1626.41 1798.27 20.60 o 2 1 4 425.15 377.05 4.90 o 3 1 4 409.55 470.87 16.26 o 4 1 4 226.57 193.03 14.98 o 5 1 4 66.79 94.69 14.35 o 6 1 4 15.26 3.22 14.14 o 0 2 4 15033.73 13417.28 276.10 o 1 2 4 5406.46 5293.74 5.20 o 2 2 4 9793.82 9017.20 54.03 o 3 2 4 1896.77 1812.26 29.32 o 4 2 4 1421.46 1416.43 30.42 o 5 2 4 192.78 205.56 17.40 o 6 2 4 37.10 42.72 15.42 o 0 3 4 892.84 883.96 22.39 o 1 3 4 1463.40 1592.55 25.55 o 2 3 4 1433.24 1365.86 24.12 o 3 3 4 115.53 140.87 7.53 o 4 3 4 448.84 455.03 9.43 o 5 3 4 15.48 20.94 10.96 o 6 3 4 28.11 14.48 14.48 o 0 4 4 1699.30 1645.69 32.30 o 1 4 4 8682.54 8952.90 65.63 o 2 4 4 668.90 612.13 19.71 o 3 4 4 1404.19 1420.27 30.04 o 4 4 4 73.11 63.62 11.92 o 5 4 4 297.83 290.91 20.79 o 6 4 4 34.82 4.77 11.87 o 0 5 4 696.39 677.48 7.55 o 1 5 4 113.35 118.21 11.53 o 2 5 4 251.96 253.00 15.74 o 3 5 4 174.82 137.50 13.93 o 4 5 4 131.04 143.43 14.90 o 5 5 4 56.71 3.65 14.01 o 0 6 4 262.03 289.40 16.82 o 1 6 4 3107.05 3070.87 10.50 o 2 6 4 213.27 225.02 16.88 o 3 6 4 1713.02 1752.92 41.60 o 4 6 4 7.88 9.22 12.35 o 5 6 4 105.42 15.33 15.33 o 0 7 4 153.93 160.75 14.65 o 1 7 4 196.68 187.91 15.05 o 2 7 4 151.62 171.56 17.44 o 3 7 4 104.90 104.04 15.98 o 4 7 4 17.28 15.61 15.39 o 5 7 4 11.87 41.43 13.23 o 0 8 4 984.80 1003.70 33.50 o 1 8 4 502.40 549.72 26.92 o 2 8 4 448.37 453.80 26.54 o 3 8 4 130.65 119.21 20.05 o 4 8 4 82.80 3.45 15.42 o 0 9 4 2.84 15.23 15.23 o 1 9 4 72.00 78.79 17.56 o 2 9 4 11.55 11.36 15.06 o 3 9 4 44.81 52.99 16.81 o 0 10 4 244.60 277.88 25.09 o 1 10 4 8.57 23.23 16.76 o 2 10 4 177.24 181.17 23.82 o 1 0 5 21751.23 19237.49 323.82 o 2 0 5 5.84 18.43 7.01 o 3 0 5 5369.78 5536.88 52.95 o 4 0 5 64.58 83.50 13.22 o 5 0 5 232.05 189.04 20.38 o 6 0 5 0.88 11.67 14.46 o 0 1 5 2179.91 2251.52 23.22 o 1 1 5 702.78 836.49 15.24 o 2 1 5 1247.45 1382.71 22.41 o 3 1 5 423.37 455.38 16.23 o 4 1 5 236.25 228.11 16.15 o 5 1 5 238.94 230.75 18.99 o 6 1 5 19.25 2.19 15.94 o 0 2 5 5627.15 5851.47 43.27 o 1 2 5 11465.02 10829.03 57.25 o 2 2 5 1389.58 1349.41 23.01 o 3 2 5 3272.40 3110.03 38.04 o 4 2 5 269.42 293.47 8.88 o 5 2 5 379.65 392.43 22.15 o 6 2 5 74.30 93.01 17.30 o 0 3 5 351.75 383.38 13.86 o 1 3 5 3041.13 3201.83 36.06 o 2 3 5 387.73 419.28 14.45 o 3 3 5 467.45 507.31 17.90 o 4 3 5 165.15 178.40 14.09 o 5 3 5 8.90 22.24 10.80 o 6 3 5 18.09 45.88 12.61 o 0 4 5 5525.26 5627.31 52.16 o 1 4 5 455.76 478.69 17.24 o 2 4 5 4383.71 4348.99 47.49 o 3 4 5 248.23 207.16 14.47 o 4 4 5 874.37 902.79 27.98 o 5 4 5 29.55 18.82 12.85 o 6 4 5 35.38 5.96 11.92 o 0 5 5 89.70 102.05 10.44 o 1 5 5 772.58 709.65 22.35 o 2 5 5 118.65 130.09 13.28 o 3 5 5 424.41 418.42 20.40 o 4 5 5 70.08 71.32 14.47 o 5 5 5 57.61 8.61 13.41 o 0 6 5 4535.68 4186.67 54.53 o 1 6 5 158.87 132.25 14.67 o 2 6 5 2272.61 2308.04 44.19 o 3 6 5 119.20 140.13 16.63 o 4 6 5 446.52 489.98 11.74 o 5 6 5 1.81 0.00 14.25 o 0 7 5 292.05 268.11 18.03 o 1 7 5 109.32 105.05 14.38 o 2 7 5 183.10 209.17 19.05 o 3 7 5 69.16 109.23 15.29 o 4 7 5 45.06 56.70 17.21 o 5 7 5 24.49 11.71 17.31 o 0 8 5 497.68 544.84 26.12 o 1 8 5 526.08 539.02 26.63 o 2 8 5 380.51 390.40 24.95 o 3 8 5 145.96 156.47 21.58 o 4 8 5 56.35 44.78 19.91 o 0 9 5 107.32 137.49 16.63 o 1 9 5 1.93 37.53 14.33 o 2 9 5 71.71 75.06 17.77 o 3 9 5 6.32 21.79 17.34 o 0 10 5 0.16 0.00 17.71 o 1 10 5 214.49 190.76 25.07 o 2 10 5 2.18 48.66 16.41 o 0 0 6 14676.18 14391.60 279.52 o 1 0 6 0.16 23.54 6.58 o 2 0 6 13490.87 13294.55 73.81 o 3 0 6 11.27 5.67 8.10 o 4 0 6 2728.39 2803.51 47.48 o 5 0 6 1.74 13.99 13.99 o 6 0 6 53.44 87.97 19.35 o 0 1 6 815.86 880.14 16.01 o 1 1 6 3080.98 3381.40 32.04 o 2 1 6 693.47 721.44 17.94 o 3 1 6 1184.09 1233.37 26.40 o 4 1 6 200.33 210.84 17.15 o 5 1 6 170.44 198.73 18.56 o 6 1 6 22.87 22.12 17.18 o 0 2 6 8931.47 8211.64 52.11 o 1 2 6 2959.02 3067.46 32.61 o 2 2 6 3106.58 3104.38 35.69 o 3 2 6 576.48 594.49 18.76 o 4 2 6 463.25 441.66 19.42 o 5 2 6 107.30 137.45 15.85 o 6 2 6 62.61 75.65 16.89 o 0 3 6 3310.91 3469.19 38.79 o 1 3 6 681.58 650.47 17.53 o 2 3 6 671.93 658.45 18.84 o 3 3 6 432.99 454.61 17.18 o 4 3 6 48.35 56.31 11.51 o 5 3 6 47.82 14.37 15.31 o 6 3 6 23.78 20.99 13.13 o 0 4 6 1244.50 1286.96 26.94 o 1 4 6 6571.48 6482.25 56.95 o 2 4 6 829.42 812.09 23.46 o 3 4 6 1664.34 1656.83 34.53 o 4 4 6 108.67 127.76 15.29 o 5 4 6 150.79 219.58 20.78 o 6 4 6 9.81 23.93 11.92 o 0 5 6 1753.77 1708.46 32.37 o 1 5 6 15.68 20.99 9.51 o 2 5 6 1015.62 1086.96 28.82 o 3 5 6 227.87 274.88 18.35 o 4 5 6 182.27 208.80 17.92 o 5 5 6 27.63 23.08 15.93 o 0 6 6 259.16 268.66 16.09 o 1 6 6 2696.46 2668.37 44.92 o 2 6 6 163.46 201.06 16.00 o 3 6 6 764.79 753.01 30.29 o 4 6 6 47.16 32.52 16.15 o 5 6 6 100.99 99.99 19.45 o 0 7 6 70.04 84.67 12.43 o 1 7 6 161.53 172.05 14.64 o 2 7 6 138.74 155.28 16.07 o 3 7 6 45.70 43.15 16.66 o 4 7 6 85.97 69.38 17.80 o 0 8 6 217.19 248.99 20.31 o 1 8 6 332.11 374.94 23.23 o 2 8 6 207.49 204.82 20.18 o 3 8 6 324.04 334.11 25.51 o 4 8 6 50.52 19.14 19.14 o 0 9 6 0.06 11.15 14.58 o 1 9 6 177.22 190.32 20.53 o 2 9 6 43.21 47.70 16.20 o 3 9 6 48.93 37.57 17.10 o 0 10 6 344.09 340.13 27.87 o 1 10 6 0.80 6.03 16.01 o 1 0 7 7353.71 7942.33 55.73 o 2 0 7 37.79 72.50 9.33 o 3 0 7 2085.29 2046.14 36.23 o 4 0 7 20.50 42.02 13.48 o 5 0 7 463.11 532.66 27.42 o 6 0 7 16.42 16.60 16.60 o 0 1 7 4113.81 4153.56 36.17 o 1 1 7 122.73 113.67 8.58 o 2 1 7 3118.92 3159.30 36.88 o 3 1 7 32.87 41.22 9.55 o 4 1 7 830.36 837.90 26.97 o 5 1 7 34.94 60.14 12.60 o 6 1 7 24.84 29.16 18.57 o 0 2 7 5600.31 5222.28 43.75 o 1 2 7 6322.85 6164.16 47.75 o 2 2 7 2178.60 2195.02 31.74 o 3 2 7 2496.65 2494.31 38.70 o 4 2 7 209.34 215.70 15.62 o 5 2 7 147.81 203.12 19.37 o 6 2 7 5.61 11.49 14.56 o 0 3 7 1050.01 1022.39 22.40 o 1 3 7 1903.46 1719.87 28.28 o 2 3 7 526.88 567.83 18.34 o 3 3 7 541.69 580.77 21.30 o 4 3 7 27.12 44.88 12.07 o 5 3 7 137.11 124.11 17.71 o 6 3 7 8.91 0.00 13.97 o 0 4 7 5011.33 4970.50 50.57 o 1 4 7 658.12 685.56 9.90 o 2 4 7 2346.94 2300.55 38.30 o 3 4 7 182.38 197.32 14.37 o 4 4 7 486.78 514.33 24.14 o 5 4 7 37.96 44.97 14.93 o 0 5 7 75.78 79.56 11.11 o 1 5 7 1372.18 1372.59 30.73 o 2 5 7 260.27 249.83 16.83 o 3 5 7 315.61 345.33 21.58 o 4 5 7 62.39 58.36 15.87 o 5 5 7 41.10 66.04 15.26 o 0 6 7 2308.76 2124.21 40.09 o 1 6 7 9.01 1.30 11.34 o 2 6 7 1562.00 1566.92 38.59 o 3 6 7 97.58 101.43 15.62 o 4 6 7 254.96 245.11 23.90 o 5 6 7 11.30 24.00 14.67 o 0 7 7 184.80 179.82 16.02 o 1 7 7 297.13 288.12 19.49 o 2 7 7 190.06 184.69 18.63 o 3 7 7 270.14 298.09 22.89 o 4 7 7 71.68 86.31 18.15 o 0 8 7 253.93 307.38 21.65 o 1 8 7 439.82 357.95 24.94 o 2 8 7 150.54 182.98 19.62 o 3 8 7 71.36 80.93 20.34 o 4 8 7 62.07 70.57 19.26 o 0 9 7 169.47 139.99 18.69 o 1 9 7 6.27 15.60 15.60 o 2 9 7 51.09 86.04 16.54 o 3 9 7 27.09 31.52 17.20 o 0 10 7 7.51 19.08 15.55 o 1 10 7 170.21 187.32 21.25 o 0 0 8 8774.61 9328.66 59.91 o 1 0 8 128.16 142.74 11.19 o 2 0 8 3643.82 3704.72 42.93 o 3 0 8 121.28 134.11 12.86 o 4 0 8 433.26 428.62 22.71 o 5 0 8 155.02 166.01 21.11 o 6 0 8 25.54 17.19 19.12 o 0 1 8 1373.02 1537.22 24.07 o 1 1 8 4408.71 4200.27 40.98 o 2 1 8 242.66 236.00 13.00 o 3 1 8 1426.17 1397.04 30.18 o 4 1 8 50.49 45.69 12.88 o 5 1 8 77.34 125.07 17.14 o 6 1 8 55.48 88.45 17.44 o 0 2 8 4740.16 4347.43 42.90 o 1 2 8 2045.05 2170.43 30.72 o 2 2 8 3119.34 2955.83 39.02 o 3 2 8 970.79 1033.33 26.39 o 4 2 8 674.70 706.36 26.39 o 5 2 8 88.30 97.62 17.55 o 6 2 8 50.24 64.53 18.95 o 0 3 8 1486.31 1362.65 26.39 o 1 3 8 724.80 696.63 19.85 o 2 3 8 1094.78 1069.73 26.34 o 3 3 8 338.67 400.46 18.86 o 4 3 8 254.40 352.67 20.41 o 5 3 8 113.95 103.49 17.38 o 0 4 8 1065.01 974.49 25.59 o 1 4 8 3593.03 3524.07 45.41 o 2 4 8 476.10 418.04 19.69 o 3 4 8 761.77 735.17 26.81 o 4 4 8 76.47 84.81 15.04 o 5 4 8 83.69 67.84 16.46 o 0 5 8 1487.00 1293.58 29.64 o 1 5 8 54.76 55.93 12.86 o 2 5 8 939.76 908.71 28.48 o 3 5 8 22.22 11.40 12.64 o 4 5 8 238.93 282.20 22.87 o 5 5 8 13.98 26.25 14.91 o 0 6 8 82.27 70.11 12.63 o 1 6 8 1127.34 1119.38 31.12 o 2 6 8 15.91 0.81 14.18 o 3 6 8 541.76 596.26 29.79 o 4 6 8 2.35 9.71 15.93 o 5 6 8 65.02 54.14 19.45 o 0 7 8 470.04 423.33 22.05 o 1 7 8 262.95 278.08 20.37 o 2 7 8 280.91 272.77 21.59 o 3 7 8 172.77 169.48 21.47 o 4 7 8 43.44 67.91 17.36 o 0 8 8 387.50 359.46 22.09 o 1 8 8 319.96 370.69 22.52 o 2 8 8 228.93 242.01 21.77 o 3 8 8 53.16 33.95 17.93 o 0 9 8 1.34 6.91 14.51 o 1 9 8 154.57 175.92 19.36 o 2 9 8 12.44 2.28 14.72 o 0 10 8 98.11 69.76 18.22 o 1 0 9 7493.88 8202.28 63.65 o 2 0 9 141.11 174.72 11.96 o 3 0 9 1651.06 1619.22 34.78 o 4 0 9 2.78 10.59 10.91 o 5 0 9 75.81 66.10 20.06 o 6 0 9 7.53 23.28 15.68 o 0 1 9 2991.07 2751.80 34.40 o 1 1 9 764.09 750.83 22.45 o 2 1 9 2079.69 2023.87 33.36 o 3 1 9 646.99 672.94 23.30 o 4 1 9 384.64 456.73 23.03 o 5 1 9 67.34 55.77 19.21 o 6 1 9 28.28 16.96 19.82 o 0 2 9 1025.49 1009.34 22.51 o 1 2 9 2783.98 2759.52 37.09 o 2 2 9 795.03 822.80 23.40 o 3 2 9 557.82 520.68 21.41 o 4 2 9 302.90 321.22 21.36 o 5 2 9 108.53 107.78 18.62 o 0 3 9 1420.20 1421.03 27.91 o 1 3 9 2141.16 2024.84 34.19 o 2 3 9 562.51 515.70 20.01 o 3 3 9 415.31 481.56 21.94 o 4 3 9 209.89 239.26 20.33 o 5 3 9 73.09 105.01 15.83 o 0 4 9 2012.94 1933.87 34.49 o 1 4 9 624.48 543.72 21.47 o 2 4 9 1740.99 1722.80 37.12 o 3 4 9 422.35 456.93 23.39 o 4 4 9 329.72 394.97 24.07 o 5 4 9 37.41 23.59 16.14 o 0 5 9 17.89 19.28 9.87 o 1 5 9 1673.26 1535.34 34.37 o 2 5 9 26.32 37.34 12.65 o 3 5 9 472.38 544.38 25.77 o 4 5 9 22.73 42.07 16.87 o 5 5 9 52.18 59.40 19.53 o 0 6 9 1265.79 1083.97 30.08 o 1 6 9 123.29 142.47 14.74 o 2 6 9 470.23 482.95 24.31 o 3 6 9 0.20 2.92 13.75 o 4 6 9 103.24 170.16 21.08 o 0 7 9 330.78 290.88 20.30 o 1 7 9 153.71 129.13 16.55 o 2 7 9 208.01 227.57 20.38 o 3 7 9 144.24 171.08 21.03 o 4 7 9 19.36 27.71 15.85 o 0 8 9 429.75 384.14 23.55 o 1 8 9 145.86 159.59 18.60 o 2 8 9 204.17 214.45 23.94 o 3 8 9 86.15 103.83 18.91 o 0 9 9 167.87 184.51 19.24 o 1 9 9 9.69 0.00 15.24 o 2 9 9 145.49 158.40 21.94 o 0 0 10 4746.57 4698.82 47.61 o 1 0 10 17.45 5.04 9.30 o 2 0 10 1902.76 1821.24 32.96 o 3 0 10 0.17 9.23 10.97 o 4 0 10 300.11 308.66 21.04 o 5 0 10 0.36 7.89 14.96 o 0 1 10 193.17 160.39 12.24 o 1 1 10 2786.24 2738.98 38.79 o 2 1 10 393.67 398.45 17.74 o 3 1 10 780.28 785.88 26.27 o 4 1 10 65.58 62.70 16.75 o 5 1 10 155.81 179.95 22.14 o 0 2 10 3582.43 3555.29 44.61 o 1 2 10 725.46 731.81 21.94 o 2 2 10 1606.30 1703.34 33.78 o 3 2 10 306.62 269.36 19.39 o 4 2 10 260.52 292.13 21.71 o 5 2 10 18.87 35.28 17.53 o 0 3 10 4140.25 4134.02 50.26 o 1 3 10 549.98 505.72 19.27 o 2 3 10 1803.55 1823.86 36.91 o 3 3 10 495.89 543.76 23.79 o 4 3 10 302.46 308.97 21.82 o 5 3 10 41.39 29.21 17.88 o 0 4 10 71.43 66.66 12.57 o 1 4 10 984.25 944.53 27.01 o 2 4 10 304.57 326.24 20.74 o 3 4 10 659.67 715.12 28.95 o 4 4 10 97.87 94.02 18.12 o 5 4 10 71.59 50.74 19.22 o 0 5 10 1046.21 942.47 26.95 o 1 5 10 75.35 73.39 13.36 o 2 5 10 848.49 893.27 30.41 o 3 5 10 98.73 138.91 16.94 o 4 5 10 144.91 187.16 20.60 o 0 6 10 12.00 17.69 11.55 o 1 6 10 1233.88 1218.54 33.83 o 2 6 10 13.51 2.56 14.59 o 3 6 10 215.30 244.47 22.20 o 4 6 10 5.50 24.74 16.50 o 0 7 10 274.06 201.73 18.38 o 1 7 10 371.14 395.36 23.00 o 2 7 10 164.83 179.71 20.56 o 3 7 10 78.01 83.56 19.78 o 0 8 10 109.40 76.62 16.11 o 1 8 10 159.77 133.33 17.78 o 2 8 10 57.55 60.80 16.15 o 3 8 10 41.61 54.11 18.14 o 0 9 10 2.58 12.28 13.65 o 1 9 10 158.27 155.43 18.60 o 1 0 11 2256.75 2415.99 38.49 o 2 0 11 15.46 17.22 9.84 o 3 0 11 645.74 725.73 27.10 o 4 0 11 10.55 33.97 12.57 o 5 0 11 150.80 174.13 21.57 o 0 1 11 3399.50 3168.87 43.04 o 1 1 11 520.30 465.86 23.34 o 2 1 11 1823.30 1713.99 34.50 o 3 1 11 162.55 193.59 16.25 o 4 1 11 360.03 401.71 23.73 o 5 1 11 20.67 34.42 15.44 o 0 2 11 210.09 239.54 16.74 o 1 2 11 1675.67 1677.95 34.07 o 2 2 11 397.57 406.12 19.49 o 3 2 11 512.98 506.85 24.18 o 4 2 11 56.07 61.70 15.61 o 5 2 11 50.02 21.47 16.63 o 0 3 11 980.72 869.51 26.29 o 1 3 11 1526.07 1404.70 32.68 o 2 3 11 454.72 449.41 22.10 o 3 3 11 742.33 764.46 29.77 o 4 3 11 109.35 128.09 19.09 o 5 3 11 62.76 87.10 18.38 o 0 4 11 1472.26 1456.84 34.48 o 1 4 11 159.35 153.05 14.37 o 2 4 11 536.10 488.07 24.28 o 3 4 11 62.39 58.64 17.27 o 4 4 11 76.79 72.13 17.93 o 5 4 11 27.43 29.57 17.85 o 0 5 11 59.57 42.55 13.50 o 1 5 11 1296.31 1255.72 34.35 o 2 5 11 14.49 4.30 16.23 o 3 5 11 367.89 348.38 24.43 o 4 5 11 18.95 14.92 17.92 o 0 6 11 689.38 669.04 25.68 o 1 6 11 12.63 20.83 14.30 o 2 6 11 514.45 515.40 26.66 o 3 6 11 5.62 30.63 14.33 o 4 6 11 94.45 111.37 20.35 o 0 7 11 220.87 197.06 17.97 o 1 7 11 234.41 215.92 19.49 o 2 7 11 177.63 183.12 21.57 o 3 7 11 67.12 62.50 18.38 o 0 8 11 152.06 138.69 16.83 o 1 8 11 37.30 25.53 14.76 o 2 8 11 67.87 56.80 19.29 o 0 9 11 176.18 150.65 17.88 o 0 0 12 2550.94 2446.41 39.04 o 1 0 12 5.18 19.51 10.22 o 2 0 12 1129.32 1110.29 29.60 o 3 0 12 42.62 75.80 12.78 o 4 0 12 174.45 121.92 19.07 o 5 0 12 5.99 8.66 17.90 o 0 1 12 615.19 519.41 21.84 o 1 1 12 3021.93 2860.86 45.77 o 2 1 12 229.38 238.44 16.63 o 3 1 12 793.33 753.45 28.54 o 4 1 12 74.19 95.03 15.96 o 5 1 12 97.53 108.23 20.80 o 0 2 12 649.90 715.57 24.89 o 1 2 12 404.88 422.82 20.78 o 2 2 12 475.09 545.06 23.13 o 3 2 12 63.95 100.86 13.29 o 4 2 12 138.92 155.49 18.15 o 5 2 12 2.15 4.74 15.49 o 0 3 12 492.40 486.17 22.29 o 1 3 12 770.41 748.35 27.30 o 2 3 12 735.41 726.32 28.06 o 3 3 12 201.13 229.11 20.31 o 4 3 12 224.85 260.79 23.58 o 5 3 12 27.47 55.39 13.69 o 0 4 12 313.84 309.45 20.45 o 1 4 12 612.54 600.62 24.94 o 2 4 12 210.24 143.14 19.61 o 3 4 12 254.34 256.18 22.54 o 4 4 12 36.60 3.42 17.50 o 0 5 12 1552.79 1471.30 36.99 o 1 5 12 192.28 228.52 20.25 o 2 5 12 873.15 890.83 34.19 o 3 5 12 23.89 1.12 17.04 o 4 5 12 174.83 219.21 23.58 o 0 6 12 0.42 12.13 12.38 o 1 6 12 332.97 322.46 22.56 o 2 6 12 54.66 52.96 17.90 o 3 6 12 121.71 125.85 21.22 o 0 7 12 395.98 332.61 21.26 o 1 7 12 115.64 155.57 17.15 o 2 7 12 144.82 129.55 21.64 o 3 7 12 66.86 86.24 18.56 o 0 8 12 38.87 29.92 14.01 o 1 8 12 141.66 128.96 18.50 o 2 8 12 13.09 10.90 15.55 o 1 0 13 617.51 641.34 23.78 o 2 0 13 146.62 166.33 16.55 o 3 0 13 372.15 314.15 21.97 o 4 0 13 10.96 19.67 16.70 o 5 0 13 11.00 12.73 17.20 o 0 1 13 3529.54 3261.73 50.61 o 1 1 13 25.08 18.88 18.88 o 2 1 13 1538.76 1438.04 36.67 o 3 1 13 103.84 104.84 15.70 o 4 1 13 209.03 230.88 23.74 o 5 1 13 12.73 33.78 17.71 o 0 2 13 244.42 286.34 18.90 o 1 2 13 689.39 778.61 29.16 o 2 2 13 101.13 110.17 14.93 o 3 2 13 158.88 186.66 19.16 o 4 2 13 28.39 26.88 17.46 o 0 3 13 205.53 223.08 20.66 o 1 3 13 1234.06 1258.34 35.39 o 2 3 13 311.64 349.92 22.84 o 3 3 13 477.77 486.15 29.53 o 4 3 13 111.64 116.67 20.96 o 0 4 13 386.77 416.43 24.89 o 1 4 13 218.92 194.30 20.18 o 2 4 13 204.24 235.59 20.45 o 3 4 13 55.18 73.45 18.22 o 4 4 13 16.83 8.40 17.70 o 0 5 13 3.35 13.67 15.86 o 1 5 13 716.32 669.10 29.86 o 2 5 13 9.49 2.07 16.97 o 3 5 13 317.74 363.80 27.81 o 4 5 13 18.58 26.56 17.67 o 0 6 13 219.97 229.43 18.45 o 1 6 13 0.79 5.47 13.34 o 2 6 13 156.33 164.07 21.49 o 3 6 13 5.94 3.63 17.48 o 0 7 13 346.25 261.06 20.56 o 1 7 13 364.35 380.87 25.23 o 2 7 13 112.66 119.75 19.42 o 0 8 13 62.01 43.82 14.22 o 0 0 14 330.61 349.93 18.56 o 1 0 14 93.46 82.08 13.64 o 2 0 14 185.37 165.71 16.64 o 3 0 14 25.76 34.89 15.28 o 4 0 14 32.62 32.83 16.79 o 0 1 14 53.31 29.06 17.18 o 1 1 14 1616.71 1536.40 38.73 o 2 1 14 210.28 230.62 12.75 o 3 1 14 519.74 488.55 27.49 o 4 1 14 86.15 108.79 19.14 o 0 2 14 368.99 460.11 24.50 o 1 2 14 147.70 149.00 17.91 o 2 2 14 296.26 278.31 21.86 o 3 2 14 17.85 45.89 15.44 o 4 2 14 66.65 74.67 17.80 o 0 3 14 1384.67 1630.86 44.65 o 1 3 14 428.47 413.17 27.83 o 2 3 14 638.53 642.23 30.62 o 3 3 14 182.88 161.03 22.77 o 4 3 14 95.16 49.40 19.94 o 0 4 14 160.04 172.42 20.00 o 1 4 14 178.72 204.85 20.81 o 2 4 14 78.95 100.06 18.00 o 3 4 14 34.82 60.49 16.83 o 4 4 14 24.42 2.53 20.00 o 0 5 14 886.56 979.73 36.54 o 1 5 14 4.01 7.71 16.26 o 2 5 14 500.83 508.00 28.86 o 3 5 14 8.14 19.65 16.94 o 0 6 14 30.88 36.93 13.48 o 1 6 14 103.94 108.33 18.75 o 2 6 14 4.55 35.03 13.89 o 0 7 14 137.02 108.19 15.81 o 1 7 14 179.21 125.27 20.94 o 1 0 15 159.75 147.87 16.51 o 2 0 15 42.76 14.47 12.65 o 3 0 15 110.63 91.40 17.45 o 4 0 15 8.04 33.24 14.55 o 0 1 15 1135.19 1050.96 34.55 o 1 1 15 540.56 448.08 29.15 o 2 1 15 765.06 829.45 13.10 o 3 1 15 32.36 49.65 16.68 o 4 1 15 189.05 143.03 25.46 o 0 2 15 108.80 126.08 19.97 o 1 2 15 152.34 150.55 20.64 o 2 2 15 65.74 87.18 18.77 o 3 2 15 78.86 72.69 18.47 o 4 2 15 0.87 2.47 16.22 o 0 3 15 577.71 628.90 33.71 o 1 3 15 660.54 690.26 34.36 o 2 3 15 309.55 286.35 26.24 o 3 3 15 279.08 280.03 25.68 o 0 4 15 128.98 187.84 22.25 o 1 4 15 100.38 111.72 20.64 o 2 4 15 36.24 41.97 19.05 o 3 4 15 37.00 61.96 18.53 o 0 5 15 2.87 19.93 18.24 o 1 5 15 623.26 640.63 32.09 o 2 5 15 17.89 17.47 17.47 o 0 6 15 75.82 43.45 17.93 o 1 6 15 25.46 24.18 15.38 o 2 6 15 61.49 64.01 18.81 o 0 0 16 49.88 61.85 13.17 o 1 0 16 1.72 12.64 12.64 o 2 0 16 125.94 105.22 15.93 o 3 0 16 7.55 29.74 14.77 o 0 1 16 139.64 83.86 20.94 o 1 1 16 864.54 794.26 34.55 o 2 1 16 36.19 31.10 15.65 o 3 1 16 416.10 377.74 27.14 o 0 2 16 106.33 154.87 21.36 o 1 2 16 10.04 13.06 16.80 o 2 2 16 80.00 83.72 19.29 o 3 2 16 3.15 18.63 17.98 o 0 3 16 842.62 1020.51 41.84 o 1 3 16 348.21 322.81 28.33 o 2 3 16 486.14 503.07 31.68 o 3 3 16 57.95 44.71 19.45 o 0 4 16 73.23 53.58 26.73 o 1 4 16 50.15 53.95 18.65 o 2 4 16 28.11 52.33 16.38 o 0 5 16 464.96 496.19 33.44 o 1 5 16 1.30 17.49 17.49 o 2 5 16 230.37 219.55 24.72 o 0 6 16 9.59 17.08 17.08 o 1 0 17 97.46 93.20 15.85 o 2 0 17 16.72 40.44 13.31 o 3 0 17 3.34 1.05 13.88 o 0 1 17 874.19 806.84 36.76 o 1 1 17 50.58 34.33 18.95 o 2 1 17 529.99 455.49 28.44 o 3 1 17 46.64 21.92 19.57 o 0 2 17 0.29 11.03 17.35 o 1 2 17 29.12 43.79 18.83 o 2 2 17 2.62 9.30 16.52 o 3 2 17 34.77 56.68 18.71 o 0 3 17 143.28 102.40 27.73 o 1 3 17 445.70 518.57 32.34 o 2 3 17 152.73 154.07 23.34 o 0 4 17 4.52 56.43 19.21 o 1 4 17 35.77 52.55 20.48 o 2 4 17 8.53 21.89 17.18 o 0 5 17 12.15 6.83 20.02 o 0 0 18 26.79 18.47 14.74 o 1 0 18 2.21 9.74 12.51 o 2 0 18 3.56 12.08 13.08 o 0 1 18 73.17 32.17 22.63 o 1 1 18 541.77 450.90 30.81 o 2 1 18 64.71 43.17 18.60 o 0 2 18 28.57 29.22 20.27 o 1 2 18 7.31 7.59 17.05 o 2 2 18 16.52 20.88 17.97 o 0 3 18 302.67 371.63 33.54 o 1 3 18 124.61 208.73 26.64 o 1 0 19 1.49 15.54 12.41 o 0 1 19 355.67 368.11 27.76 o 1 1 19 25.06 0.00 18.05 o