#------------------------------------------------------------------------------ #$Date: 2016-04-03 01:48:09 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181098 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/78/2217808.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2217808_Fobs loop_ _publ_author_name 'Soares-Sobrinho, Jos\'e Lamartine' 'Cunha-Filho, Marc\'ilio S. S.' 'Rolim Neto, Pedro Jos\'e' 'Torres-Labandeira, Juan J.' 'Dacunha-Marinho, Bruno' _publ_section_title ; Benznidazole ; _journal_coeditor_code OM2213 _journal_issue 3 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o634 _journal_volume 64 _journal_year 2008 _space_group_IT_number 4 _symmetry_space_group_name_Hall 'P 2yb' _symmetry_space_group_name_H-M 'P 1 21 1' _cell_angle_alpha 90.000 _cell_angle_beta 90.668 _cell_angle_gamma 90.000 _cell_length_a 4.6556 _cell_length_b 10.9113 _cell_length_c 11.7681 _exptl_crystal_F_000 272.00 _reflns_d_resolution_high 0.7993 _cod_data_source_file om2213Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' bzd_n in P 21' _shelx_refln_list_code 4 _shelx_f_calc_maximum 91.00 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 67.07 44.17 0.48 o 2 0 0 775.97 761.86 5.08 o 3 0 0 539.67 555.35 4.44 o 4 0 0 14.33 11.57 0.94 o 5 0 0 24.59 25.42 1.39 o 1 1 0 3061.52 2854.28 14.89 o 2 1 0 95.55 87.09 0.72 o 3 1 0 82.96 92.64 1.00 o 4 1 0 135.46 136.11 2.28 o 5 1 0 38.61 37.50 1.65 o 0 2 0 887.77 870.98 5.76 o 1 2 0 1956.27 1858.15 11.32 o 2 2 0 39.62 42.14 0.67 o 3 2 0 12.33 12.48 0.60 o 4 2 0 11.49 11.74 0.99 o 5 2 0 76.46 74.02 2.66 o 1 3 0 8.96 7.52 0.45 o 2 3 0 25.21 30.91 0.93 o 3 3 0 176.40 181.45 3.15 o 4 3 0 2.13 0.37 0.67 o 5 3 0 47.16 46.98 4.94 o 0 4 0 347.81 359.43 2.78 o 1 4 0 94.99 93.35 0.99 o 2 4 0 98.70 91.84 1.60 o 3 4 0 2.70 1.58 0.60 o 4 4 0 31.31 29.40 1.30 o 5 4 0 62.25 55.40 3.41 o 1 5 0 23.23 25.04 1.05 o 2 5 0 9.18 12.12 0.82 o 3 5 0 8.44 9.44 0.94 o 4 5 0 79.12 73.59 4.09 o 5 5 0 6.94 7.63 1.53 o 0 6 0 510.57 542.05 4.13 o 1 6 0 116.48 116.71 1.31 o 2 6 0 97.47 107.36 5.87 o 3 6 0 221.23 228.19 6.13 o 4 6 0 17.41 16.92 1.92 o 5 6 0 3.73 2.91 1.50 o 1 7 0 610.72 651.58 4.79 o 2 7 0 243.07 240.75 2.40 o 3 7 0 95.77 94.80 2.44 o 4 7 0 77.08 84.57 2.79 o 5 7 0 25.90 24.87 3.67 o 0 8 0 86.13 100.67 1.54 o 1 8 0 464.21 475.64 3.82 o 2 8 0 56.99 55.72 1.19 o 3 8 0 14.97 14.10 1.81 o 4 8 0 27.03 27.33 1.95 o 1 9 0 42.37 43.52 1.74 o 2 9 0 76.91 76.59 1.61 o 3 9 0 118.75 120.70 3.29 o 4 9 0 64.97 71.09 4.71 o 0 10 0 130.36 130.79 2.66 o 1 10 0 230.13 220.95 3.08 o 2 10 0 169.97 169.38 3.08 o 3 10 0 37.41 35.55 2.98 o 1 11 0 3.76 3.64 0.90 o 2 11 0 35.93 33.98 3.08 o 3 11 0 50.31 45.17 2.38 o 0 12 0 38.70 36.77 1.78 o 1 12 0 18.56 18.22 1.41 o 2 12 0 1.84 0.87 1.09 o 1 13 0 1.61 2.95 1.17 o -5 0 1 9.97 9.55 1.34 o -4 0 1 170.99 163.94 3.15 o -3 0 1 0.85 2.49 0.48 o -2 0 1 19.75 21.08 0.48 o -1 0 1 846.55 794.46 4.33 o 0 0 1 399.04 365.97 2.46 o 1 0 1 632.16 535.26 3.60 o 2 0 1 117.98 111.11 1.22 o 3 0 1 30.05 27.87 0.82 o 4 0 1 0.02 0.48 0.67 o 5 0 1 37.06 35.96 1.73 o -5 1 1 61.01 56.61 1.90 o -4 1 1 78.05 72.02 1.50 o -3 1 1 12.06 13.76 0.52 o -2 1 1 113.60 125.99 1.03 o -1 1 1 288.18 247.80 1.50 o 0 1 1 568.63 544.64 2.28 o 1 1 1 54.21 48.09 0.45 o 2 1 1 202.28 200.75 1.34 o 3 1 1 47.01 47.81 0.76 o 4 1 1 55.02 53.05 1.48 o 5 1 1 18.97 18.20 1.34 o -5 2 1 0.38 0.47 1.13 o -4 2 1 10.39 11.03 0.85 o -3 2 1 268.54 290.62 4.16 o -2 2 1 303.35 309.76 2.29 o -1 2 1 2261.12 2254.08 12.00 o 0 2 1 59.47 60.65 0.83 o 1 2 1 1180.09 1161.62 6.00 o 2 2 1 903.86 912.75 9.31 o 3 2 1 53.46 55.24 1.08 o 4 2 1 27.27 28.88 2.38 o 5 2 1 79.43 83.50 6.18 o -5 3 1 20.58 19.87 2.03 o -4 3 1 48.80 47.91 2.69 o -3 3 1 29.10 30.18 1.64 o -2 3 1 40.15 39.83 1.36 o -1 3 1 112.32 116.16 1.68 o 0 3 1 1593.43 1596.35 6.72 o 1 3 1 602.50 611.52 3.70 o 2 3 1 382.00 393.52 3.96 o 3 3 1 731.13 779.30 5.91 o 4 3 1 10.44 10.08 2.01 o 5 3 1 81.09 79.15 2.83 o -5 4 1 54.56 52.23 1.96 o -4 4 1 192.80 198.45 3.13 o -3 4 1 7.09 10.02 1.85 o -2 4 1 678.83 687.33 7.38 o -1 4 1 85.80 84.01 1.19 o 0 4 1 110.09 109.64 0.79 o 1 4 1 20.66 22.47 0.85 o 2 4 1 331.68 339.25 2.96 o 3 4 1 10.50 11.30 0.72 o 4 4 1 70.41 72.43 1.91 o 5 4 1 4.21 1.96 2.18 o -5 5 1 17.43 17.27 1.36 o -4 5 1 26.87 28.57 2.57 o -3 5 1 174.92 172.14 2.76 o -2 5 1 143.37 143.78 2.14 o -1 5 1 252.76 243.36 2.10 o 0 5 1 244.56 273.32 1.63 o 1 5 1 619.58 648.13 4.16 o 2 5 1 103.13 109.26 1.44 o 3 5 1 36.18 39.95 1.79 o 4 5 1 140.07 130.19 2.56 o 5 5 1 31.55 29.66 1.65 o -5 6 1 19.99 15.64 1.91 o -4 6 1 7.11 6.42 1.27 o -3 6 1 151.76 156.18 3.00 o -2 6 1 104.43 109.45 1.95 o -1 6 1 181.19 179.96 1.93 o 0 6 1 81.75 84.61 0.83 o 1 6 1 9.91 14.23 1.09 o 2 6 1 45.24 48.31 1.03 o 3 6 1 128.74 121.48 2.13 o 4 6 1 26.95 30.21 2.57 o 5 6 1 6.37 3.87 1.17 o -4 7 1 105.36 105.99 4.53 o -3 7 1 180.05 171.84 3.27 o -2 7 1 241.24 241.80 4.66 o -1 7 1 36.78 36.91 0.93 o 0 7 1 178.59 187.45 1.43 o 1 7 1 178.28 181.68 1.76 o 2 7 1 48.72 53.97 2.36 o 3 7 1 239.25 247.09 4.01 o 4 7 1 60.55 60.95 3.21 o -4 8 1 134.94 137.34 3.63 o -3 8 1 78.14 80.80 2.38 o -2 8 1 40.32 43.27 1.05 o -1 8 1 43.33 45.07 1.91 o 0 8 1 36.25 41.36 0.69 o 1 8 1 18.53 17.98 0.74 o 2 8 1 267.18 262.13 2.60 o 3 8 1 13.79 13.60 1.31 o 4 8 1 37.58 41.56 5.80 o -4 9 1 54.52 66.62 3.18 o -3 9 1 92.62 89.98 2.62 o -2 9 1 15.68 16.80 0.89 o -1 9 1 115.91 111.55 1.79 o 0 9 1 76.32 74.35 1.14 o 1 9 1 82.23 76.61 1.61 o 2 9 1 73.55 79.43 3.59 o 3 9 1 231.44 250.73 4.80 o 4 9 1 53.27 50.77 2.87 o -3 10 1 97.44 95.44 3.07 o -2 10 1 8.17 8.89 1.04 o -1 10 1 18.73 16.71 1.07 o 0 10 1 334.45 324.82 3.30 o 1 10 1 59.31 60.95 1.65 o 2 10 1 43.06 42.23 1.91 o 3 10 1 2.87 5.07 1.82 o -3 11 1 43.37 46.63 2.44 o -2 11 1 1.72 0.63 0.88 o -1 11 1 183.96 172.35 3.04 o 0 11 1 15.97 16.42 0.86 o 1 11 1 8.60 9.00 1.32 o 2 11 1 35.48 37.05 1.67 o 3 11 1 20.41 19.73 1.37 o -2 12 1 10.36 15.97 3.95 o -1 12 1 27.48 26.81 1.46 o 0 12 1 153.83 148.09 2.14 o 1 12 1 1.11 1.19 0.89 o 2 12 1 32.67 32.95 1.89 o -1 13 1 1.99 1.58 1.18 o 0 13 1 18.92 20.65 1.51 o 1 13 1 17.95 20.68 1.46 o -5 0 2 24.99 21.52 1.58 o -4 0 2 55.32 55.95 1.81 o -3 0 2 93.86 102.90 1.43 o -2 0 2 333.27 343.46 2.40 o -1 0 2 8280.75 7716.31 42.04 o 0 0 2 338.66 299.93 1.93 o 1 0 2 257.96 235.07 1.83 o 2 0 2 17.81 17.29 0.58 o 3 0 2 12.96 15.89 0.67 o 4 0 2 6.54 6.60 0.84 o 5 0 2 3.46 3.91 1.09 o -5 1 2 13.85 11.94 1.15 o -4 1 2 111.63 106.76 2.00 o -3 1 2 5.10 5.63 0.32 o -2 1 2 134.39 128.22 0.89 o -1 1 2 4185.86 4020.69 17.19 o 0 1 2 2210.74 2105.09 8.76 o 1 1 2 286.94 251.14 1.38 o 2 1 2 90.21 90.67 0.85 o 3 1 2 55.07 53.84 0.84 o 4 1 2 17.85 17.65 0.80 o 5 1 2 218.58 221.70 4.68 o -5 2 2 42.67 38.17 2.01 o -4 2 2 23.70 23.91 0.93 o -3 2 2 67.96 65.03 0.90 o -2 2 2 65.41 59.31 0.95 o -1 2 2 829.51 815.13 4.17 o 0 2 2 3337.50 3341.45 13.15 o 1 2 2 750.78 738.94 3.41 o 2 2 2 75.26 78.20 0.85 o 3 2 2 315.46 325.42 3.37 o 4 2 2 69.29 70.47 2.12 o 5 2 2 15.89 14.68 1.99 o -5 3 2 40.23 36.59 2.00 o -4 3 2 6.78 6.40 0.71 o -3 3 2 23.10 24.71 0.65 o -2 3 2 425.32 430.10 3.61 o -1 3 2 367.53 387.09 2.43 o 0 3 2 1218.40 1229.27 5.91 o 1 3 2 83.44 75.50 1.51 o 2 3 2 353.69 369.22 4.32 o 3 3 2 3.60 5.45 1.43 o 4 3 2 89.22 89.89 2.86 o 5 3 2 41.85 41.95 2.64 o -5 4 2 18.21 19.65 1.67 o -4 4 2 7.18 8.73 1.06 o -3 4 2 133.51 137.39 2.59 o -2 4 2 230.37 239.29 2.87 o -1 4 2 125.36 129.56 1.21 o 0 4 2 1198.14 1252.26 7.99 o 1 4 2 414.79 457.93 2.46 o 2 4 2 25.30 23.53 0.74 o 3 4 2 207.12 219.48 2.30 o 4 4 2 130.31 125.25 2.50 o 5 4 2 34.55 36.49 5.40 o -5 5 2 0.16 0.00 0.90 o -4 5 2 256.77 269.73 4.65 o -3 5 2 137.06 139.62 2.50 o -2 5 2 177.32 179.32 3.51 o -1 5 2 217.20 237.80 1.89 o 0 5 2 7.28 9.65 0.31 o 1 5 2 727.58 799.85 12.04 o 2 5 2 53.21 56.26 0.91 o 3 5 2 46.42 41.82 4.07 o 4 5 2 111.23 121.91 2.80 o 5 5 2 47.63 41.57 1.95 o -5 6 2 8.59 8.19 1.71 o -4 6 2 67.50 68.12 2.47 o -3 6 2 141.46 140.99 2.86 o -2 6 2 126.69 131.44 2.16 o -1 6 2 648.11 670.36 5.41 o 0 6 2 91.41 103.18 0.93 o 1 6 2 244.49 241.31 3.10 o 2 6 2 102.91 110.35 2.97 o 3 6 2 52.28 53.07 1.89 o 4 6 2 13.27 11.75 1.10 o 5 6 2 13.72 13.58 2.41 o -4 7 2 70.37 66.71 2.58 o -3 7 2 147.88 151.52 3.26 o -2 7 2 0.15 0.58 0.75 o -1 7 2 9.03 8.62 0.53 o 0 7 2 269.12 285.94 1.98 o 1 7 2 31.93 37.61 1.28 o 2 7 2 75.60 78.90 1.96 o 3 7 2 2.10 1.47 0.63 o 4 7 2 26.42 25.56 1.40 o -4 8 2 13.95 12.02 1.61 o -3 8 2 88.81 93.10 4.14 o -2 8 2 416.18 408.37 8.22 o -1 8 2 34.23 33.63 2.14 o 0 8 2 18.36 19.12 0.56 o 1 8 2 171.22 171.93 1.67 o 2 8 2 151.23 156.57 2.30 o 3 8 2 27.57 27.43 3.09 o 4 8 2 12.40 13.23 1.20 o -4 9 2 32.98 33.23 2.66 o -3 9 2 0.29 0.28 1.04 o -2 9 2 80.88 77.31 1.58 o -1 9 2 168.96 164.98 2.36 o 0 9 2 17.71 21.43 0.71 o 1 9 2 36.77 36.16 1.03 o 2 9 2 115.53 111.76 2.12 o 3 9 2 11.14 11.66 1.11 o 4 9 2 2.38 0.41 1.40 o -3 10 2 54.61 58.17 2.55 o -2 10 2 13.27 13.26 1.39 o -1 10 2 118.65 115.96 2.99 o 0 10 2 10.20 9.86 1.15 o 1 10 2 161.67 166.62 3.55 o 2 10 2 65.49 64.92 2.95 o 3 10 2 39.97 30.90 1.58 o -3 11 2 20.83 18.04 1.82 o -2 11 2 20.22 17.97 2.29 o -1 11 2 69.93 73.37 3.18 o 0 11 2 152.39 144.91 2.35 o 1 11 2 42.53 42.50 1.73 o 2 11 2 16.32 17.73 1.35 o 3 11 2 15.06 15.69 1.34 o -2 12 2 2.18 2.01 1.68 o -1 12 2 100.11 103.89 4.20 o 0 12 2 245.18 250.04 2.92 o 1 12 2 29.71 29.17 1.51 o 2 12 2 41.35 39.87 1.99 o -1 13 2 93.32 89.28 2.82 o 0 13 2 18.19 17.56 1.02 o 1 13 2 9.49 8.13 1.18 o -5 0 3 11.90 10.37 2.62 o -4 0 3 32.28 28.54 1.15 o -3 0 3 161.28 167.53 1.91 o -2 0 3 93.75 96.64 1.02 o -1 0 3 677.07 607.26 3.62 o 0 0 3 169.96 148.75 1.19 o 1 0 3 19.73 19.94 0.58 o 2 0 3 40.06 41.40 0.93 o 3 0 3 0.47 0.38 0.49 o 4 0 3 23.30 24.69 1.10 o 5 0 3 115.40 119.95 3.08 o -5 1 3 111.91 108.23 2.50 o -4 1 3 53.86 53.22 1.90 o -3 1 3 2.83 2.64 0.32 o -2 1 3 576.55 554.96 2.86 o -1 1 3 1620.97 1576.28 7.92 o 0 1 3 338.72 325.26 1.58 o 1 1 3 41.79 44.08 0.71 o 2 1 3 441.38 446.64 2.84 o 3 1 3 11.55 11.87 0.76 o 4 1 3 178.59 176.81 3.17 o 5 1 3 12.04 12.32 0.97 o -5 2 3 50.92 47.73 2.22 o -4 2 3 178.13 171.73 2.01 o -3 2 3 239.38 238.02 1.91 o -2 2 3 869.35 876.40 6.75 o -1 2 3 1849.98 1797.32 8.42 o 0 2 3 536.60 521.93 2.35 o 1 2 3 200.46 196.60 1.28 o 2 2 3 266.91 284.75 1.85 o 3 2 3 88.16 95.87 1.19 o 4 2 3 60.86 66.47 1.44 o 5 2 3 178.16 190.93 4.45 o -5 3 3 0.84 0.28 1.12 o -4 3 3 40.47 42.16 1.13 o -3 3 3 52.74 47.57 0.81 o -2 3 3 222.65 224.19 2.05 o -1 3 3 1733.92 1770.98 9.03 o 0 3 3 270.44 269.81 1.44 o 1 3 3 1684.42 1729.04 14.75 o 2 3 3 1017.03 1100.25 6.07 o 3 3 3 76.00 72.19 1.27 o 4 3 3 139.69 144.83 2.70 o 5 3 3 10.65 12.08 5.02 o -5 4 3 114.89 112.47 8.24 o -4 4 3 57.35 57.08 4.60 o -3 4 3 20.97 20.82 0.69 o -2 4 3 241.75 251.99 2.19 o -1 4 3 198.61 198.15 1.49 o 0 4 3 661.47 706.13 5.64 o 1 4 3 194.16 212.13 1.38 o 2 4 3 207.84 222.18 2.42 o 3 4 3 63.35 60.58 2.21 o 4 4 3 35.64 36.01 4.62 o 5 4 3 2.92 1.25 1.09 o -5 5 3 6.19 5.37 1.11 o -4 5 3 91.34 92.36 1.78 o -3 5 3 57.89 58.09 1.60 o -2 5 3 311.38 323.27 3.38 o -1 5 3 10.98 14.82 1.03 o 0 5 3 2.76 2.31 0.61 o 1 5 3 200.31 210.73 1.54 o 2 5 3 26.73 28.52 0.76 o 3 5 3 382.66 378.74 4.46 o 4 5 3 163.21 159.03 2.98 o 5 5 3 61.06 59.03 5.64 o -5 6 3 32.43 31.11 2.32 o -4 6 3 6.23 5.71 1.24 o -3 6 3 498.04 488.44 9.44 o -2 6 3 25.22 26.01 1.05 o -1 6 3 68.16 69.16 1.09 o 0 6 3 91.28 96.91 1.45 o 1 6 3 115.51 110.86 1.14 o 2 6 3 5.72 6.84 0.55 o 3 6 3 61.17 52.12 1.41 o 4 6 3 17.97 18.16 1.29 o 5 6 3 39.70 42.04 3.58 o -4 7 3 123.12 122.19 10.83 o -3 7 3 51.53 52.71 1.98 o -2 7 3 148.55 147.32 1.97 o -1 7 3 0.62 0.87 0.46 o 0 7 3 221.96 234.68 1.79 o 1 7 3 100.40 97.53 1.12 o 2 7 3 138.32 138.26 1.85 o 3 7 3 26.50 27.45 1.42 o 4 7 3 15.86 13.48 1.26 o -4 8 3 111.75 118.76 4.20 o -3 8 3 60.55 61.64 2.20 o -2 8 3 129.44 128.86 3.72 o -1 8 3 33.73 36.88 1.05 o 0 8 3 3.03 3.15 0.44 o 1 8 3 150.86 146.90 2.63 o 2 8 3 3.21 4.61 1.19 o 3 8 3 70.31 69.90 2.57 o 4 8 3 19.10 19.74 2.19 o -4 9 3 0.44 0.89 1.51 o -3 9 3 9.76 8.34 1.42 o -2 9 3 60.53 62.00 2.69 o -1 9 3 39.36 41.24 1.37 o 0 9 3 51.53 51.60 1.11 o 1 9 3 220.45 220.38 2.39 o 2 9 3 304.45 289.24 3.75 o 3 9 3 5.78 5.72 1.03 o 4 9 3 22.76 23.42 1.60 o -3 10 3 100.02 103.15 6.96 o -2 10 3 18.11 16.82 1.24 o -1 10 3 152.32 145.13 2.49 o 0 10 3 100.50 102.74 1.71 o 1 10 3 81.30 80.41 1.97 o 2 10 3 5.01 5.80 0.92 o 3 10 3 45.93 50.57 1.92 o -3 11 3 4.91 5.16 1.50 o -2 11 3 1.71 2.07 0.97 o -1 11 3 37.30 38.86 1.59 o 0 11 3 143.48 143.36 2.88 o 1 11 3 10.89 9.96 0.99 o 2 11 3 37.34 41.50 1.78 o 3 11 3 35.25 34.00 1.73 o -2 12 3 16.72 17.61 1.57 o -1 12 3 77.43 81.17 3.49 o 0 12 3 1.36 0.64 0.71 o 1 12 3 45.36 47.07 3.55 o 2 12 3 3.67 0.90 1.27 o -1 13 3 33.23 35.76 2.03 o 0 13 3 30.04 30.42 2.23 o 1 13 3 18.20 16.44 1.40 o -5 0 4 0.19 1.01 2.03 o -4 0 4 2.97 2.41 0.64 o -3 0 4 11.77 12.16 0.63 o -2 0 4 293.98 283.94 2.09 o -1 0 4 49.38 59.23 0.80 o 0 0 4 278.21 277.31 2.09 o 1 0 4 609.84 595.86 4.45 o 2 0 4 183.29 208.11 2.53 o 3 0 4 39.94 43.81 1.25 o 4 0 4 902.23 906.04 9.25 o 5 0 4 109.48 116.34 3.40 o -5 1 4 11.62 11.98 1.07 o -4 1 4 3.49 3.37 0.72 o -3 1 4 23.57 24.73 0.91 o -2 1 4 434.27 430.72 2.61 o -1 1 4 565.47 540.80 2.76 o 0 1 4 646.55 602.41 3.04 o 1 1 4 898.81 913.68 9.33 o 2 1 4 48.40 51.37 0.88 o 3 1 4 167.45 159.79 1.61 o 4 1 4 133.46 138.05 1.98 o 5 1 4 28.93 28.25 1.42 o -5 2 4 65.87 66.32 2.58 o -4 2 4 48.12 47.79 1.09 o -3 2 4 3.31 2.94 0.45 o -2 2 4 229.60 215.30 2.14 o -1 2 4 341.80 354.08 1.89 o 0 2 4 21.72 23.61 0.39 o 1 2 4 416.42 431.69 2.37 o 2 2 4 104.63 108.76 1.05 o 3 2 4 159.78 161.47 2.00 o 4 2 4 12.01 12.50 2.02 o 5 2 4 79.65 77.73 3.41 o -5 3 4 1.25 1.21 1.22 o -4 3 4 132.80 140.02 1.86 o -3 3 4 65.66 64.03 1.09 o -2 3 4 314.99 306.27 2.32 o -1 3 4 46.42 52.98 0.63 o 0 3 4 51.90 48.54 1.01 o 1 3 4 190.40 192.03 1.44 o 2 3 4 153.48 168.99 2.63 o 3 3 4 21.19 21.23 0.69 o 4 3 4 51.05 51.41 1.65 o 5 3 4 19.09 18.70 1.90 o -5 4 4 1.20 0.00 1.13 o -4 4 4 195.68 202.14 3.46 o -3 4 4 270.53 260.95 2.09 o -2 4 4 84.59 89.44 1.05 o -1 4 4 636.09 675.49 3.78 o 0 4 4 57.75 56.75 0.66 o 1 4 4 127.72 131.18 1.07 o 2 4 4 25.76 28.71 0.66 o 3 4 4 55.21 57.98 2.13 o 4 4 4 10.94 10.91 1.11 o 5 4 4 8.17 7.75 1.32 o -5 5 4 58.12 58.77 2.61 o -4 5 4 69.34 72.13 2.25 o -3 5 4 272.40 266.12 4.69 o -2 5 4 95.89 100.43 1.94 o -1 5 4 91.24 92.74 2.97 o 0 5 4 541.23 590.98 3.28 o 1 5 4 208.01 224.01 1.63 o 2 5 4 5.55 7.96 0.43 o 3 5 4 99.87 95.74 1.83 o 4 5 4 8.95 4.46 1.21 o 5 5 4 2.88 2.48 1.23 o -5 6 4 11.94 12.80 3.40 o -4 6 4 39.86 39.21 2.02 o -3 6 4 8.76 6.87 1.01 o -2 6 4 38.97 39.42 1.07 o -1 6 4 70.73 69.77 1.59 o 0 6 4 329.98 348.83 2.35 o 1 6 4 683.28 692.44 4.47 o 2 6 4 7.70 8.89 0.61 o 3 6 4 138.90 143.98 3.19 o 4 6 4 24.76 23.68 1.58 o -4 7 4 32.44 29.14 3.36 o -3 7 4 21.19 20.23 2.44 o -2 7 4 99.97 103.56 1.79 o -1 7 4 4.50 3.97 1.04 o 0 7 4 45.28 44.26 1.29 o 1 7 4 52.76 54.90 0.90 o 2 7 4 236.29 229.91 2.94 o 3 7 4 30.29 25.59 1.14 o 4 7 4 43.42 41.52 4.84 o -4 8 4 20.88 22.24 1.91 o -3 8 4 2.70 4.50 1.14 o -2 8 4 77.73 75.81 1.56 o -1 8 4 83.88 77.45 1.45 o 0 8 4 44.54 45.47 0.83 o 1 8 4 64.94 64.90 1.11 o 2 8 4 118.85 127.29 4.88 o 3 8 4 30.77 27.38 2.84 o 4 8 4 14.54 15.64 2.57 o -4 9 4 6.00 2.34 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