#------------------------------------------------------------------------------ #$Date: 2009-05-05 17:46:52 +0300 (Tue, 05 May 2009) $ #$Revision: 697 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2217842.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2217842_Fobs loop_ _publ_author_name 'Dong, Yan' _publ_section_title ; (4-Formyl-2-methoxyphenolato)tris(2-methyl-2-phenylpropyl)tin(IV) ; _journal_coeditor_code WN2240 _journal_issue 3 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m450 _journal_volume 64 _journal_year 2008 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 92.873 _cell_angle_gamma 90.000 _cell_length_a 9.7900 _cell_length_b 33.7613 _cell_length_c 10.3073 _exptl_crystal_F_000 1392.00 _reflns_d_resolution_high 0.8107 _[local]_cod_data_source_file wn2240Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' A in P2(1)/n' _shelx_refln_list_code 4 _shelx_F_calc_maximum 316.65 _shelx_F_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 7871.80 7506.71 261.58 o 4 0 0 71291.13 74831.15 2507.27 o 6 0 0 223.30 320.33 45.36 o 8 0 0 4433.02 4300.02 175.88 o 10 0 0 706.13 923.82 99.43 o 12 0 0 338.20 364.62 116.96 o 1 1 0 3639.49 4104.49 99.74 o 2 1 0 5122.22 5205.38 128.36 o 3 1 0 28959.63 30479.56 726.19 o 4 1 0 1304.31 1457.55 45.68 o 5 1 0 85.30 125.39 14.86 o 6 1 0 3329.50 3002.40 96.39 o 7 1 0 2786.17 2615.14 81.19 o 8 1 0 405.03 548.38 36.40 o 9 1 0 116.74 109.33 33.23 o 10 1 0 179.43 272.24 48.75 o 11 1 0 1019.46 1227.74 250.14 o 12 1 0 175.72 257.76 73.49 o 0 2 0 10.55 -6.86 6.86 o 1 2 0 32841.07 34052.38 877.31 o 2 2 0 96.14 80.78 7.80 o 3 2 0 7595.32 7766.98 191.47 o 4 2 0 15.34 44.70 9.68 o 5 2 0 15058.81 15629.81 382.73 o 6 2 0 5.96 4.53 10.66 o 7 2 0 792.61 874.87 48.22 o 8 2 0 9.76 35.88 16.55 o 9 2 0 1643.83 1883.85 109.98 o 10 2 0 96.21 38.09 56.00 o 11 2 0 355.97 399.24 76.60 o 12 2 0 11.30 -29.32 55.74 o 1 3 0 14576.69 15681.53 373.14 o 2 3 0 16017.21 16856.34 403.16 o 3 3 0 8086.10 8318.74 204.68 o 4 3 0 2880.09 3021.15 82.67 o 5 3 0 4325.55 4611.52 123.17 o 6 3 0 7488.28 7110.85 184.78 o 7 3 0 1426.04 1420.70 53.92 o 8 3 0 399.64 437.06 41.60 o 9 3 0 8.14 62.49 28.41 o 10 3 0 1256.96 1237.92 93.92 o 11 3 0 684.62 821.01 104.11 o 12 3 0 100.96 283.92 76.92 o 0 4 0 86854.73 78051.33 2605.74 o 1 4 0 14828.92 15635.87 372.57 o 2 4 0 980.85 920.14 28.08 o 3 4 0 6.98 14.01 6.07 o 4 4 0 14753.48 14846.27 361.25 o 5 4 0 1660.63 1767.22 55.71 o 6 4 0 351.72 435.06 27.48 o 7 4 0 37.96 51.29 14.73 o 8 4 0 2647.01 2447.21 88.16 o 9 4 0 693.14 637.40 92.23 o 10 4 0 563.11 642.10 81.34 o 11 4 0 113.47 231.10 65.99 o 12 4 0 208.87 206.52 79.20 o 1 5 0 38074.74 39997.77 1046.03 o 2 5 0 1023.19 1009.17 30.64 o 3 5 0 8821.15 8618.39 212.31 o 4 5 0 265.43 341.65 20.54 o 5 5 0 5590.28 5521.11 144.49 o 6 5 0 1453.93 1454.85 57.19 o 7 5 0 3538.19 3390.74 100.07 o 8 5 0 118.42 105.23 24.58 o 9 5 0 109.68 138.34 30.05 o 10 5 0 113.49 221.77 55.07 o 11 5 0 907.56 987.99 112.89 o 0 6 0 9937.28 10526.94 359.68 o 1 6 0 9531.94 10348.80 276.03 o 2 6 0 769.82 768.70 27.35 o 3 6 0 1010.16 938.06 31.28 o 4 6 0 1472.85 1389.86 44.41 o 5 6 0 12228.89 11767.52 291.76 o 6 6 0 653.16 760.22 53.90 o 7 6 0 799.37 909.96 70.95 o 8 6 0 157.91 201.71 56.04 o 9 6 0 1833.77 1816.21 80.97 o 10 6 0 177.85 151.27 57.24 o 11 6 0 2.56 76.63 43.45 o 1 7 0 15992.23 16534.41 437.43 o 2 7 0 4384.74 4235.82 107.66 o 3 7 0 3324.24 3418.08 90.56 o 4 7 0 2166.25 2467.82 70.25 o 5 7 0 2774.72 2875.66 82.61 o 6 7 0 8649.95 8394.01 215.87 o 7 7 0 339.90 344.05 27.47 o 8 7 0 366.31 531.91 45.26 o 9 7 0 69.43 103.24 24.98 o 10 7 0 1694.10 1841.73 142.15 o 11 7 0 221.46 206.38 65.05 o 0 8 0 1387.35 1423.13 56.49 o 1 8 0 333.27 322.54 18.52 o 2 8 0 490.99 530.50 28.91 o 3 8 0 1.91 6.92 6.40 o 4 8 0 2031.60 1944.77 58.36 o 5 8 0 1052.14 1074.03 41.99 o 6 8 0 900.34 970.16 43.27 o 7 8 0 165.87 219.22 25.03 o 8 8 0 1650.06 1651.65 75.29 o 9 8 0 335.45 319.41 35.53 o 10 8 0 448.98 537.43 77.75 o 11 8 0 1.33 -41.69 41.69 o 1 9 0 38355.02 38951.15 1022.24 o 2 9 0 74.01 62.73 8.74 o 3 9 0 18463.98 19065.77 509.11 o 4 9 0 61.76 70.61 11.39 o 5 9 0 2254.04 2280.62 68.99 o 6 9 0 1055.10 1141.90 69.32 o 7 9 0 1762.70 1718.06 84.90 o 8 9 0 156.00 89.15 22.27 o 9 9 0 161.78 170.78 29.13 o 10 9 0 165.21 182.78 73.77 o 11 9 0 871.90 873.23 108.69 o 0 10 0 2033.01 1984.92 98.09 o 1 10 0 9913.71 9851.01 266.59 o 2 10 0 1408.16 1483.46 44.12 o 3 10 0 731.73 706.19 41.16 o 4 10 0 5280.92 4958.40 145.29 o 5 10 0 4631.89 4407.64 133.25 o 6 10 0 456.88 522.53 35.16 o 7 10 0 198.68 227.13 29.36 o 8 10 0 502.66 536.48 41.59 o 9 10 0 1652.94 1649.57 91.35 o 10 10 0 43.50 71.09 65.92 o 11 10 0 7.42 111.94 55.40 o 1 11 0 3931.93 4250.40 122.02 o 2 11 0 10949.33 10570.41 288.39 o 3 11 0 383.51 451.35 23.80 o 4 11 0 3528.25 3653.79 99.91 o 5 11 0 0.61 22.61 11.48 o 6 11 0 5773.61 5681.72 152.99 o 7 11 0 23.42 36.66 15.06 o 8 11 0 943.13 1066.77 59.52 o 9 11 0 46.67 91.35 30.39 o 10 11 0 963.84 1209.59 169.55 o 11 11 0 1.52 57.14 79.76 o 0 12 0 45836.73 46170.05 1869.78 o 1 12 0 4020.43 3969.45 116.21 o 2 12 0 0.17 23.26 9.45 o 3 12 0 3511.00 3579.12 96.30 o 4 12 0 8015.37 8036.76 203.86 o 5 12 0 4969.98 4862.47 131.35 o 6 12 0 194.99 199.83 21.70 o 7 12 0 447.25 419.84 37.97 o 8 12 0 1017.95 1187.57 84.62 o 9 12 0 520.39 577.43 200.81 o 11 12 0 20.89 44.22 49.34 o 1 13 0 9780.40 9331.61 256.67 o 2 13 0 3937.43 4036.73 120.21 o 3 13 0 9704.84 9595.82 238.22 o 4 13 0 234.70 306.29 21.40 o 5 13 0 481.44 493.14 29.19 o 6 13 0 9.25 27.04 16.95 o 7 13 0 2927.96 2909.78 115.17 o 8 13 0 20.98 -13.02 19.50 o 9 13 0 591.36 671.92 67.46 o 10 13 0 11.43 14.26 51.25 o 11 13 0 849.84 905.21 110.57 o 0 14 0 38921.87 39661.93 1336.53 o 1 14 0 3996.07 4180.00 123.68 o 2 14 0 333.39 386.33 65.06 o 3 14 0 358.51 371.76 20.45 o 4 14 0 9348.90 9423.28 237.78 o 5 14 0 3584.24 3537.23 100.98 o 6 14 0 77.83 97.55 18.53 o 7 14 0 2.75 -7.98 16.85 o 8 14 0 507.28 506.22 57.34 o 9 14 0 645.13 750.47 88.92 o 10 14 0 282.57 302.22 84.41 o 11 14 0 36.67 75.70 52.56 o 1 15 0 1010.94 1039.05 44.18 o 2 15 0 9226.41 8827.93 246.68 o 3 15 0 128.62 111.63 21.61 o 4 15 0 635.29 628.32 30.56 o 5 15 0 4.70 21.03 16.30 o 6 15 0 3915.39 3803.19 123.44 o 7 15 0 597.48 575.23 48.98 o 8 15 0 866.59 783.47 85.48 o 9 15 0 150.69 166.58 40.12 o 10 15 0 464.99 432.21 91.08 o 11 15 0 1.51 95.75 54.55 o 0 16 0 4169.31 4291.14 208.50 o 1 16 0 2863.04 2586.80 83.77 o 2 16 0 2981.97 3180.76 100.45 o 3 16 0 1802.72 1825.65 65.92 o 4 16 0 2737.03 2572.22 87.56 o 5 16 0 3490.54 3257.94 107.67 o 6 16 0 166.37 170.93 23.63 o 7 16 0 276.67 339.28 38.39 o 8 16 0 589.89 604.47 54.17 o 9 16 0 871.20 1122.89 216.46 o 10 16 0 85.51 107.11 40.31 o 11 16 0 155.75 129.63 60.08 o 1 17 0 11306.27 11439.21 315.07 o 2 17 0 417.96 360.93 40.74 o 3 17 0 5442.12 5212.46 155.86 o 4 17 0 40.90 37.00 14.04 o 5 17 0 1876.75 1777.09 71.84 o 6 17 0 797.15 822.18 49.77 o 7 17 0 2938.53 2715.73 112.62 o 8 17 0 8.07 35.72 23.55 o 9 17 0 85.87 194.28 54.73 o 10 17 0 154.22 212.17 50.92 o 11 17 0 814.73 681.12 100.87 o 0 18 0 24316.90 24237.88 826.51 o 1 18 0 1101.98 1174.63 59.42 o 2 18 0 696.61 726.96 71.76 o 3 18 0 311.64 294.71 26.04 o 4 18 0 7115.55 6593.25 194.91 o 5 18 0 890.64 812.22 47.91 o 6 18 0 1141.11 1164.26 60.80 o 7 18 0 81.38 95.13 27.01 o 8 18 0 1086.30 1171.91 77.64 o 9 18 0 243.88 188.54 75.11 o 10 18 0 322.13 403.19 77.27 o 1 19 0 47.87 93.27 15.84 o 2 19 0 4045.88 3774.37 146.58 o 3 19 0 312.87 330.18 28.34 o 4 19 0 95.76 111.37 22.40 o 5 19 0 108.90 105.90 20.20 o 6 19 0 3297.69 3157.94 112.26 o 7 19 0 533.51 578.87 51.57 o 8 19 0 430.21 563.75 56.82 o 9 19 0 171.12 183.68 53.63 o 10 19 0 666.95 721.48 83.24 o 0 20 0 4098.77 4184.87 161.45 o 1 20 0 5188.75 5134.74 178.03 o 2 20 0 2205.65 2254.85 82.29 o 3 20 0 1082.59 1117.01 76.44 o 4 20 0 759.45 736.59 45.31 o 5 20 0 5653.02 5350.22 165.84 o 6 20 0 89.15 74.69 28.45 o 7 20 0 368.99 403.77 66.69 o 8 20 0 522.50 623.18 68.05 o 9 20 0 974.31 952.34 107.65 o 10 20 0 3.15 47.68 42.44 o 1 21 0 3722.44 3511.31 130.92 o 2 21 0 7718.65 7422.48 216.41 o 3 21 0 2899.60 2874.71 98.19 o 4 21 0 25.67 35.54 16.82 o 5 21 0 522.71 588.69 42.78 o 6 21 0 1396.09 1369.78 69.42 o 7 21 0 1363.19 1224.17 77.73 o 8 21 0 16.86 84.69 91.44 o 9 21 0 6.81 58.48 36.43 o 10 21 0 214.74 214.23 53.83 o 0 22 0 8195.62 8083.71 596.99 o 1 22 0 1446.09 1678.72 66.99 o 2 22 0 1132.53 1114.45 66.94 o 3 22 0 619.65 723.36 44.92 o 4 22 0 3447.85 3300.11 124.43 o 5 22 0 65.44 123.38 23.24 o 6 22 0 739.89 842.74 62.40 o 7 22 0 86.43 57.08 26.32 o 8 22 0 798.67 1040.92 160.61 o 9 22 0 8.67 31.51 36.94 o 10 22 0 213.70 146.91 49.67 o 1 23 0 5038.62 4626.81 147.11 o 2 23 0 3787.85 3631.58 137.26 o 3 23 0 3057.39 2907.88 131.01 o 4 23 0 362.28 445.33 37.75 o 5 23 0 623.88 683.50 47.24 o 6 23 0 1301.03 1350.42 130.13 o 7 23 0 225.92 209.11 51.61 o 8 23 0 115.38 94.62 46.88 o 9 23 0 24.44 23.15 38.59 o 10 23 0 500.50 534.09 103.85 o 0 24 0 205.83 291.15 50.18 o 1 24 0 6174.28 5773.65 202.10 o 2 24 0 4.17 39.79 19.11 o 3 24 0 1368.32 1498.60 82.64 o 4 24 0 85.80 97.47 22.42 o 5 24 0 4531.40 4289.26 157.32 o 6 24 0 3.90 11.42 21.78 o 7 24 0 55.28 68.83 30.13 o 8 24 0 16.60 13.93 34.98 o 9 24 0 854.00 774.57 84.18 o 1 25 0 854.26 882.99 61.83 o 2 25 0 1038.99 1022.96 55.30 o 3 25 0 2635.85 2505.00 106.46 o 4 25 0 228.56 285.51 37.10 o 5 25 0 538.10 617.31 52.82 o 6 25 0 746.19 823.01 158.19 o 7 25 0 1624.40 1559.04 109.97 o 8 25 0 6.65 -31.55 31.55 o 9 25 0 99.05 128.35 48.13 o 0 26 0 5704.23 5466.68 276.57 o 1 26 0 2.63 11.94 18.91 o 2 26 0 247.81 203.16 31.14 o 3 26 0 148.84 143.42 23.72 o 4 26 0 2960.52 2830.34 118.21 o 5 26 0 80.66 92.24 35.23 o 6 26 0 153.16 168.54 40.83 o 7 26 0 64.63 48.13 29.55 o 8 26 0 589.59 525.49 67.05 o 9 26 0 0.01 -5.79 37.50 o 1 27 0 603.00 639.70 89.27 o 2 27 0 4601.52 4187.21 159.45 o 3 27 0 1121.08 1157.66 75.30 o 4 27 0 0.73 -4.41 17.63 o 5 27 0 526.74 589.31 47.31 o 6 27 0 1444.72 1434.94 93.07 o 7 27 0 241.15 236.26 39.84 o 8 27 0 39.41 122.88 40.73 o 9 27 0 6.09 33.68 42.79 o 0 28 0 99.19 179.69 44.72 o 1 28 0 862.22 931.36 67.14 o 2 28 0 417.78 488.20 80.74 o 3 28 0 1560.60 1674.21 93.16 o 4 28 0 64.08 71.25 22.23 o 5 28 0 1834.43 1758.59 132.64 o 6 28 0 6.29 -12.28 23.88 o 7 28 0 36.72 85.93 37.39 o 8 28 0 0.17 12.44 39.98 o 1 29 0 1166.83 1200.85 94.53 o 2 29 0 1578.38 1748.02 97.05 o 3 29 0 2465.19 2150.72 131.33 o 4 29 0 107.89 80.85 33.60 o 5 29 0 297.67 282.51 35.27 o 6 29 0 1221.64 1129.21 78.73 o 7 29 0 295.47 297.01 53.81 o 8 29 0 222.01 298.64 79.28 o 0 30 0 5411.09 5498.86 292.92 o 1 30 0 1.98 48.53 23.71 o 2 30 0 1.96 8.38 22.31 o 3 30 0 82.13 152.86 34.08 o 4 30 0 2460.85 2402.47 117.32 o 5 30 0 18.80 20.25 31.58 o 6 30 0 110.03 150.41 35.36 o 7 30 0 76.61 71.71 62.13 o 8 30 0 778.34 743.04 82.84 o 1 31 0 1058.07 1160.66 80.59 o 2 31 0 1779.08 1840.34 170.29 o 3 31 0 761.18 910.82 71.26 o 4 31 0 76.95 72.87 32.05 o 5 31 0 203.69 111.34 39.35 o 6 31 0 295.72 250.28 49.02 o 7 31 0 322.83 242.23 50.64 o 8 31 0 84.47 86.29 45.79 o 0 32 0 23.86 51.48 59.98 o 1 32 0 2079.68 1969.33 123.44 o 2 32 0 0.25 39.94 34.51 o 3 32 0 869.74 828.27 68.04 o 4 32 0 80.99 87.54 31.81 o 5 32 0 1299.11 1266.25 105.57 o 6 32 0 64.47 32.09 47.62 o 7 32 0 139.24 125.38 57.20 o 1 33 0 51.86 91.80 30.99 o 2 33 0 3158.68 3101.36 134.87 o 3 33 0 34.89 59.23 27.92 o 4 33 0 112.44 142.11 41.44 o 5 33 0 38.49 93.57 40.37 o 6 33 0 905.46 910.06 98.80 o 7 33 0 0.68 24.00 48.35 o 0 34 0 1442.42 1646.46 270.86 o 1 34 0 175.90 252.98 41.71 o 2 34 0 66.31 144.83 34.59 o 3 34 0 28.59 8.03 26.49 o 4 34 0 1294.18 1280.63 90.69 o 5 34 0 233.12 292.68 95.16 o 6 34 0 172.99 201.81 72.07 o 1 35 0 996.57 990.49 100.77 o 2 35 0 2.82 -4.32 29.68 o 3 35 0 695.83 781.75 70.08 o 4 35 0 26.04 55.45 32.34 o 5 35 0 248.45 265.95 53.10 o 6 35 0 10.38 -25.29 43.49 o 0 36 0 453.08 551.04 85.95 o 1 36 0 1498.80 1274.49 99.58 o 2 36 0 47.34 86.33 32.28 o 3 36 0 712.81 747.61 87.26 o 4 36 0 427.40 574.51 61.83 o 5 36 0 507.78 421.65 65.16 o 6 36 0 129.76 158.12 93.45 o 1 37 0 12.19 62.89 33.41 o 2 37 0 797.74 892.56 105.76 o 3 37 0 29.63 52.94 32.63 o 4 37 0 63.32 72.82 41.29 o 5 37 0 5.08 -35.51 35.51 o 0 38 0 577.90 752.99 100.07 o 1 38 0 388.11 380.72 51.88 o 2 38 0 0.10 26.25 28.01 o 3 38 0 181.20 156.10 38.31 o 4 38 0 323.27 344.88 62.89 o 1 39 0 330.17 370.29 52.72 o 2 39 0 23.57 -41.90 42.10 o 3 39 0 446.93 413.98 54.28 o 4 39 0 15.33 44.60 44.19 o 0 40 0 546.86 554.48 187.58 o 1 40 0 281.84 283.35 51.44 o 2 40 0 3.04 40.60 34.40 o 3 40 0 111.34 133.49 40.73 o 1 41 0 9.62 33.86 37.07 o 2 41 0 794.42 626.82 81.87 o -11 0 1 138.54 167.48 78.73 o -9 0 1 3102.62 2971.66 135.87 o -7 0 1 937.76 1027.85 67.62 o -5 0 1 3873.90 3676.37 142.97 o -3 0 1 221.77 336.27 93.76 o -1 0 1 24626.61 26404.57 886.70 o 1 0 1 27517.18 28839.03 1180.94 o 3 0 1 386.22 378.13 24.97 o 5 0 1 13756.05 13678.92 476.34 o 7 0 1 994.68 1031.97 67.21 o 9 0 1 4125.14 3906.47 355.53 o 11 0 1 191.08 227.08 84.83 o -12 1 1 172.92 258.90 74.15 o -11 1 1 880.26 766.52 95.49 o -10 1 1 565.29 508.26 75.11 o -9 1 1 188.89 216.13 26.61 o -8 1 1 469.22 643.97 39.33 o -7 1 1 3534.49 3435.24 101.16 o -6 1 1 4520.42 4192.59 116.07 o -5 1 1 3744.75 3722.26 101.95 o -4 1 1 1123.53 1099.34 37.24 o -3 1 1 27996.44 29079.46 693.50 o -2 1 1 8238.90 8201.64 199.27 o -1 1 1 15262.45 16514.72 428.40 o 0 1 1 262.29 197.15 8.06 o 1 1 1 66.11 79.06 6.54 o 2 1 1 35761.29 37965.51 979.66 o 3 1 1 26608.94 28042.41 668.35 o 4 1 1 3821.15 4204.69 121.63 o 5 1 1 542.97 555.82 30.29 o 6 1 1 4043.19 4007.96 111.44 o 7 1 1 4934.51 5061.05 154.16 o 8 1 1 42.22 133.37 27.50 o 9 1 1 206.90 228.00 36.87 o 10 1 1 725.35 733.70 63.57 o 11 1 1 501.11 552.75 61.26 o -12 2 1 477.40 688.02 146.82 o -11 2 1 1.48 -41.54 61.79 o -10 2 1 199.07 291.00 128.64 o -9 2 1 102.24 89.99 24.55 o -8 2 1 3489.50 3304.56 100.88 o -7 2 1 4.21 16.20 13.25 o -6 2 1 24.77 68.84 15.18 o -5 2 1 726.18 825.02 35.22 o -4 2 1 27263.68 27762.68 665.37 o -3 2 1 37.39 73.73 15.26 o -2 2 1 40221.50 43166.67 1128.67 o -1 2 1 76.13 96.60 8.21 o 0 2 1 67726.79 68365.17 1614.43 o 1 2 1 1204.36 1154.88 38.50 o 2 2 1 4057.02 4233.30 106.34 o 3 2 1 0.61 1.35 9.46 o 4 2 1 19204.71 19434.34 516.86 o 5 2 1 63.94 86.30 19.49 o 6 2 1 2403.35 2396.85 79.45 o 7 2 1 2.01 10.77 12.49 o 8 2 1 3976.39 4022.08 148.52 o 9 2 1 11.69 58.37 27.04 o 10 2 1 732.99 871.91 70.23 o 11 2 1 8.43 20.16 33.32 o -12 3 1 157.52 231.65 104.25 o -11 3 1 558.84 437.98 111.07 o -10 3 1 263.70 263.96 123.26 o -9 3 1 196.41 152.14 35.70 o -8 3 1 559.73 661.89 39.98 o -7 3 1 2997.27 2923.00 88.71 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24.73 o -6 22 2 91.36 144.51 29.48 o -5 22 2 78.13 110.01 22.45 o -4 22 2 1191.05 1168.32 87.45 o -3 22 2 1074.05 1076.10 67.36 o -2 22 2 9.38 44.35 15.87 o -1 22 2 70.74 81.83 18.13 o 0 22 2 5664.33 5104.86 223.92 o 1 22 2 643.98 792.37 45.81 o 2 22 2 642.58 683.16 43.28 o 3 22 2 754.79 894.10 51.32 o 4 22 2 2206.61 2286.02 100.15 o 5 22 2 380.05 422.45 43.74 o 6 22 2 26.27 15.07 21.67 o 7 22 2 527.70 534.57 56.58 o 8 22 2 543.02 576.67 75.35 o 9 22 2 57.43 12.88 38.00 o -9 23 2 43.30 16.55 40.94 o -8 23 2 3.45 23.91 31.62 o -7 23 2 73.47 137.24 32.37 o -6 23 2 1030.54 1138.96 86.24 o -5 23 2 512.62 548.21 43.57 o -4 23 2 8.16 6.76 16.47 o -3 23 2 2082.38 2043.55 86.47 o -2 23 2 4368.48 4428.94 141.06 o -1 23 2 2266.40 2148.15 78.79 o 0 23 2 284.35 301.25 34.86 o 1 23 2 892.14 974.67 51.93 o 2 23 2 5083.18 4972.59 154.08 o 3 23 2 900.87 1047.94 69.82 o 4 23 2 365.51 382.60 67.54 o 5 23 2 610.50 763.13 86.60 o 6 23 2 2921.45 2687.09 115.79 o 7 23 2 434.73 441.59 50.47 o 8 23 2 429.64 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