#------------------------------------------------------------------------------ #$Date: 2009-05-03 21:56:13 +0300 (Sun, 03 May 2009) $ #$Revision: 691 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2217884.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2217884_Fobs loop_ _publ_author_name 'Natarajan, S.' 'Vijitha, K. V.' 'Dhas, S. A. Martin Britto' 'Suresh, J.' 'Lakshman, P. L. Nilantha' _publ_section_title ; Hexaaquazinc(II) dipicrate ; _journal_coeditor_code CI2563 _journal_issue 4 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m581 _journal_volume 64 _journal_year 2008 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 89.835 _cell_angle_beta 83.097 _cell_angle_gamma 72.837 _cell_length_a 7.8571 _cell_length_b 8.3311 _cell_length_c 8.9897 _exptl_crystal_F_000 320.00 _reflns_d_resolution_high 0.8420 _[local]_cod_data_source_file ci2563Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' piczncl in P -1' _shelx_refln_list_code 4 _shelx_F_calc_maximum 131.65 _shelx_F_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 9.23 12.41 0.23 o 2 0 0 2.59 4.03 0.34 o 3 0 0 5303.82 5235.91 9.06 o 4 0 0 1169.92 1177.12 4.91 o 5 0 0 216.18 215.59 2.49 o 6 0 0 93.04 90.79 1.99 o 7 0 0 541.64 531.78 4.82 o 8 0 0 68.82 72.13 1.93 o -8 1 0 490.86 446.72 5.09 o -7 1 0 3.66 3.26 0.81 o -6 1 0 79.35 82.04 1.95 o -5 1 0 95.81 95.24 1.85 o -4 1 0 1314.89 1230.80 5.31 o -3 1 0 1492.85 1428.13 4.92 o -2 1 0 156.64 155.97 1.42 o -1 1 0 3937.23 3769.63 42.82 o 0 1 0 109.19 97.49 0.49 o 1 1 0 3251.60 3094.21 5.65 o 2 1 0 2694.04 2535.48 4.95 o 3 1 0 1295.50 1244.06 4.23 o 4 1 0 2946.40 3017.50 7.72 o 5 1 0 634.01 600.99 3.93 o 6 1 0 203.66 198.45 2.68 o 7 1 0 304.86 289.92 3.53 o 8 1 0 18.09 16.25 0.99 o 9 1 0 50.26 48.79 1.37 o -8 2 0 1.87 1.14 1.36 o -7 2 0 675.32 614.54 5.61 o -6 2 0 108.77 96.51 2.24 o -5 2 0 27.27 27.62 0.87 o -4 2 0 901.44 904.84 4.86 o -3 2 0 464.26 456.71 3.07 o -2 2 0 60.53 54.68 1.03 o -1 2 0 652.82 651.98 3.01 o 0 2 0 207.17 221.20 1.64 o 1 2 0 1956.90 1779.08 9.86 o 2 2 0 2496.01 2401.45 5.22 o 3 2 0 59.43 55.12 1.02 o 4 2 0 49.40 33.81 0.93 o 5 2 0 787.62 778.49 4.47 o 6 2 0 168.58 180.96 2.53 o 7 2 0 99.81 96.76 2.17 o 8 2 0 269.87 263.16 3.69 o 9 2 0 40.43 41.12 1.31 o -7 3 0 44.47 39.75 1.26 o -6 3 0 372.27 339.25 4.03 o -5 3 0 173.40 169.52 2.71 o -4 3 0 4.70 3.12 0.62 o -3 3 0 2258.34 2313.01 7.56 o -2 3 0 4226.44 4119.59 9.21 o -1 3 0 482.13 477.80 5.83 o 0 3 0 716.12 725.12 4.47 o 1 3 0 3173.79 3000.75 19.82 o 2 3 0 69.68 72.89 1.11 o 3 3 0 38.17 29.16 0.85 o 4 3 0 1148.54 1125.02 4.90 o 5 3 0 390.72 361.68 3.13 o 6 3 0 305.89 291.01 3.17 o 7 3 0 4.72 4.47 0.66 o 8 3 0 161.76 168.60 3.01 o 9 3 0 173.74 163.95 3.27 o -6 4 0 206.36 199.52 3.35 o -5 4 0 258.85 245.21 3.36 o -4 4 0 237.65 242.61 3.08 o -3 4 0 168.08 158.57 2.33 o -2 4 0 1950.88 1977.95 7.04 o -1 4 0 131.59 119.52 2.12 o 0 4 0 1203.64 1144.04 13.87 o 1 4 0 6571.85 6399.45 33.97 o 2 4 0 1180.50 1057.55 4.43 o 3 4 0 818.38 810.67 4.09 o 4 4 0 1138.49 1079.31 5.09 o 5 4 0 508.20 513.07 3.85 o 6 4 0 120.58 117.40 2.16 o 7 4 0 49.81 49.91 1.47 o 8 4 0 264.62 268.20 3.77 o 9 4 0 40.39 42.04 1.30 o -6 5 0 135.33 128.96 3.03 o -5 5 0 36.46 33.33 1.14 o -4 5 0 37.33 32.26 1.01 o -3 5 0 297.14 284.21 3.34 o -2 5 0 279.99 271.57 3.00 o -1 5 0 105.34 97.17 1.83 o 0 5 0 636.51 606.73 2.75 o 1 5 0 334.49 310.61 2.96 o 2 5 0 885.22 883.69 4.55 o 3 5 0 181.38 174.24 2.16 o 4 5 0 27.92 30.48 0.93 o 5 5 0 2371.95 2380.88 8.76 o 6 5 0 17.02 17.09 0.81 o 7 5 0 242.00 237.80 3.35 o 8 5 0 107.71 112.31 2.63 o 9 5 0 15.13 18.94 1.07 o -5 6 0 68.74 63.14 1.98 o -4 6 0 52.92 53.14 1.72 o -3 6 0 480.83 497.46 4.70 o -2 6 0 5.07 5.21 0.71 o -1 6 0 203.07 204.13 1.94 o 0 6 0 66.80 68.46 1.18 o 1 6 0 6.34 3.98 0.81 o 2 6 0 215.77 223.22 2.64 o 3 6 0 427.95 428.50 3.65 o 4 6 0 388.00 360.27 3.50 o 5 6 0 188.86 199.47 2.81 o 6 6 0 572.94 589.83 4.97 o 7 6 0 112.94 123.63 2.63 o 8 6 0 3.99 3.86 0.82 o -4 7 0 73.23 80.30 2.13 o -3 7 0 18.60 16.78 0.96 o -2 7 0 775.98 769.09 5.98 o -1 7 0 410.01 405.47 2.95 o 0 7 0 114.90 118.28 1.62 o 1 7 0 109.76 115.02 2.08 o 2 7 0 551.60 551.96 4.50 o 3 7 0 214.43 204.61 2.87 o 4 7 0 1.63 0.14 0.96 o 5 7 0 109.79 117.85 2.39 o 6 7 0 173.33 185.68 3.06 o 7 7 0 69.05 69.30 1.91 o 8 7 0 26.05 26.30 1.13 o -2 8 0 33.20 34.65 1.21 o -1 8 0 421.81 436.25 3.37 o 0 8 0 85.94 88.96 1.61 o 1 8 0 54.90 55.53 2.19 o 2 8 0 492.94 456.97 4.53 o 3 8 0 227.28 234.95 3.31 o 4 8 0 110.74 117.80 2.52 o 5 8 0 351.78 357.26 4.24 o 6 8 0 124.49 131.38 2.85 o 7 8 0 0.45 0.24 1.19 o -1 9 0 15.24 15.70 0.72 o 0 9 0 72.16 67.52 1.37 o 1 9 0 252.99 246.71 2.67 o 2 9 0 2.29 4.88 0.79 o 3 9 0 80.74 83.69 2.36 o 4 9 0 106.53 106.06 2.58 o 5 9 0 53.03 59.71 1.87 o 6 9 0 33.34 40.24 1.26 o -5 -9 1 43.27 46.33 1.48 o -4 -9 1 4.36 5.60 0.82 o -3 -9 1 99.87 93.14 2.53 o -2 -9 1 149.57 142.79 2.91 o -1 -9 1 70.44 67.77 1.36 o 0 -9 1 9.32 9.53 0.63 o 1 -9 1 37.93 38.63 0.89 o -7 -8 1 18.01 18.94 1.01 o -6 -8 1 341.77 369.06 4.55 o -5 -8 1 115.04 118.88 2.59 o -4 -8 1 46.64 42.96 1.33 o -3 -8 1 113.40 122.53 2.49 o -2 -8 1 249.26 239.17 3.36 o -1 -8 1 73.83 75.19 1.49 o 0 -8 1 70.23 70.05 1.37 o 1 -8 1 76.17 74.56 2.59 o 2 -8 1 374.12 368.88 4.59 o 3 -8 1 68.19 68.13 2.04 o -8 -7 1 68.77 76.53 2.15 o -7 -7 1 31.40 32.35 1.09 o -6 -7 1 116.42 122.69 2.61 o -5 -7 1 70.46 69.55 2.00 o -4 -7 1 162.49 157.44 2.66 o -3 -7 1 132.66 128.02 2.36 o -2 -7 1 159.35 207.18 2.85 o -1 -7 1 441.79 429.72 2.88 o 0 -7 1 216.83 217.85 2.40 o 1 -7 1 172.74 172.53 2.01 o 2 -7 1 31.08 29.19 1.04 o 3 -7 1 312.70 323.42 4.22 o 4 -7 1 96.64 97.89 2.64 o -8 -6 1 14.12 13.46 0.96 o -7 -6 1 0.61 -1.12 1.12 o -6 -6 1 1.10 1.83 1.06 o -5 -6 1 327.41 314.20 3.49 o -4 -6 1 474.39 475.10 4.03 o -3 -6 1 2.84 3.87 0.57 o -2 -6 1 68.73 55.60 1.51 o -1 -6 1 535.63 539.70 6.96 o 0 -6 1 89.08 102.13 1.36 o 1 -6 1 4.63 4.14 0.47 o 2 -6 1 448.72 464.44 4.27 o 3 -6 1 43.95 46.32 1.37 o 4 -6 1 6.54 6.80 0.83 o 5 -6 1 133.06 129.75 3.01 o -8 -5 1 83.46 86.21 2.41 o -7 -5 1 117.72 126.45 2.55 o -6 -5 1 60.26 65.74 1.92 o -5 -5 1 221.70 229.22 2.84 o -4 -5 1 71.48 80.25 1.69 o -3 -5 1 13.62 11.93 0.58 o -2 -5 1 265.53 216.65 2.36 o -1 -5 1 531.34 559.61 2.95 o 0 -5 1 397.86 394.16 2.24 o 1 -5 1 400.51 394.52 2.35 o 2 -5 1 391.16 389.41 3.54 o 3 -5 1 179.03 182.92 2.71 o 4 -5 1 42.86 44.99 1.32 o 5 -5 1 14.33 14.10 0.94 o 6 -5 1 267.55 250.04 3.96 o -9 -4 1 29.35 25.68 1.17 o -8 -4 1 149.55 150.08 2.96 o -7 -4 1 178.96 179.62 2.91 o -6 -4 1 93.85 94.04 2.04 o -5 -4 1 676.13 672.31 4.48 o -4 -4 1 417.17 391.73 3.16 o -3 -4 1 910.76 859.31 4.31 o -2 -4 1 2427.81 2496.09 6.97 o -1 -4 1 37.93 56.89 0.81 o 0 -4 1 656.63 678.96 2.56 o 1 -4 1 363.94 374.34 2.03 o 2 -4 1 399.65 432.53 3.34 o 3 -4 1 738.08 774.73 4.83 o 4 -4 1 710.52 735.64 5.17 o 5 -4 1 279.01 272.31 3.53 o 6 -4 1 36.13 39.24 1.30 o 7 -4 1 237.52 236.14 3.94 o -9 -3 1 0.70 0.05 1.29 o -8 -3 1 153.48 163.46 3.04 o -7 -3 1 41.87 41.15 1.25 o -6 -3 1 292.86 292.26 3.23 o -5 -3 1 262.06 270.20 2.80 o -4 -3 1 515.72 500.91 3.36 o -3 -3 1 1327.15 1332.66 4.91 o -2 -3 1 392.38 443.95 2.61 o -1 -3 1 4321.95 4239.12 14.49 o 0 -3 1 1757.58 1792.01 3.58 o 1 -3 1 170.30 192.68 1.94 o 2 -3 1 195.82 194.09 2.03 o 3 -3 1 524.22 574.93 3.77 o 4 -3 1 159.31 161.50 2.34 o 5 -3 1 104.11 112.41 2.26 o 6 -3 1 154.24 155.59 2.83 o 7 -3 1 170.46 163.98 3.20 o -9 -2 1 94.50 92.50 2.69 o -8 -2 1 21.83 21.15 1.03 o -7 -2 1 16.98 15.71 0.84 o -6 -2 1 16.45 14.18 0.73 o -5 -2 1 9.81 14.75 0.64 o -4 -2 1 99.62 92.46 1.50 o -3 -2 1 710.34 699.16 3.35 o -2 -2 1 197.08 198.72 1.59 o -1 -2 1 771.46 805.03 1.99 o 0 -2 1 523.71 564.14 9.98 o 1 -2 1 363.30 438.33 1.74 o 2 -2 1 267.39 278.16 2.11 o 3 -2 1 7.99 13.24 0.51 o 4 -2 1 377.66 422.78 3.36 o 5 -2 1 162.88 177.80 2.52 o 6 -2 1 203.25 216.49 3.12 o 7 -2 1 11.23 9.88 0.97 o 8 -2 1 64.20 60.66 1.77 o -8 -1 1 59.95 61.59 1.84 o -7 -1 1 362.94 369.51 4.05 o -6 -1 1 158.14 164.84 2.52 o -5 -1 1 17.54 24.08 0.72 o -4 -1 1 2938.63 3035.26 7.98 o -3 -1 1 14.13 18.64 0.56 o -2 -1 1 30.02 32.94 0.76 o -1 -1 1 53.03 49.30 0.48 o 0 -1 1 878.99 873.15 1.60 o 1 -1 1 4058.59 4744.20 15.70 o 2 -1 1 724.70 881.15 3.25 o 3 -1 1 1270.21 1477.70 5.01 o 4 -1 1 490.21 531.13 3.50 o 5 -1 1 58.09 61.10 1.61 o 6 -1 1 87.38 95.29 2.13 o 7 -1 1 353.94 360.86 4.12 o 8 -1 1 0.85 1.56 1.28 o -8 0 1 120.94 117.18 2.80 o -7 0 1 288.57 284.82 3.64 o -6 0 1 111.82 105.83 2.17 o -5 0 1 744.23 746.79 4.59 o -4 0 1 109.18 100.53 1.61 o -3 0 1 1227.49 1182.11 4.34 o -2 0 1 4748.01 4829.40 7.52 o -1 0 1 963.42 960.35 6.71 o 0 0 1 1044.52 1037.21 2.62 o 1 0 1 417.51 416.71 2.28 o 2 0 1 476.34 494.72 2.23 o 3 0 1 2628.91 2660.40 6.31 o 4 0 1 287.61 310.85 2.55 o 5 0 1 668.69 649.94 4.16 o 6 0 1 748.73 737.03 5.01 o 7 0 1 354.27 344.59 3.88 o 8 0 1 212.48 200.10 3.40 o -8 1 1 32.08 33.06 1.17 o -7 1 1 15.85 15.32 0.94 o -6 1 1 147.52 142.46 2.56 o -5 1 1 470.68 469.30 3.84 o -4 1 1 40.86 44.38 1.21 o -3 1 1 1151.70 1163.84 4.57 o -2 1 1 936.86 954.03 3.53 o -1 1 1 948.15 878.78 7.81 o 0 1 1 1221.49 1090.09 11.06 o 1 1 1 7.36 6.83 0.18 o 2 1 1 756.32 683.44 2.58 o 3 1 1 2842.22 2630.56 6.16 o 4 1 1 82.36 64.71 1.24 o 5 1 1 301.26 277.69 2.71 o 6 1 1 39.28 38.75 1.18 o 7 1 1 189.72 176.76 2.83 o 8 1 1 190.76 173.60 3.06 o 9 1 1 98.40 89.67 2.60 o -7 2 1 62.35 60.37 1.81 o -6 2 1 121.76 113.95 2.40 o -5 2 1 3.11 4.30 0.64 o -4 2 1 4.02 4.28 0.55 o -3 2 1 268.12 274.15 2.46 o -2 2 1 110.41 114.47 1.44 o -1 2 1 866.15 812.28 4.40 o 0 2 1 2869.60 2630.70 16.53 o 1 2 1 603.68 549.94 2.46 o 2 2 1 489.28 446.71 2.28 o 3 2 1 1011.94 979.82 3.83 o 4 2 1 2138.31 2124.02 6.47 o 5 2 1 40.88 34.41 0.98 o 6 2 1 1.75 4.59 0.60 o 7 2 1 159.74 157.62 2.63 o 8 2 1 120.26 112.94 2.58 o 9 2 1 11.46 11.61 0.96 o -7 3 1 24.65 21.53 1.09 o -6 3 1 57.42 56.31 1.69 o -5 3 1 53.14 52.53 1.49 o -4 3 1 826.93 791.36 5.04 o -3 3 1 136.50 130.33 1.93 o -2 3 1 79.92 76.19 1.39 o -1 3 1 152.41 157.73 1.20 o 0 3 1 333.88 324.74 1.94 o 1 3 1 463.43 396.01 2.10 o 2 3 1 193.10 174.40 1.65 o 3 3 1 1286.34 1192.93 4.57 o 4 3 1 1048.35 937.62 4.46 o 5 3 1 330.58 310.72 2.91 o 6 3 1 239.19 224.68 2.77 o 7 3 1 76.17 66.25 1.85 o 8 3 1 3.73 6.72 0.78 o 9 3 1 87.91 77.85 2.10 o -6 4 1 120.92 108.59 2.70 o -5 4 1 158.25 145.80 2.73 o -4 4 1 130.19 120.24 2.32 o -3 4 1 395.22 388.90 3.54 o -2 4 1 825.62 797.31 4.56 o -1 4 1 187.60 183.63 1.59 o 0 4 1 17.71 12.03 0.32 o 1 4 1 4551.85 4259.00 32.11 o 2 4 1 77.40 70.33 1.26 o 3 4 1 289.33 278.36 2.43 o 4 4 1 297.96 276.95 2.63 o 5 4 1 366.03 355.53 3.25 o 6 4 1 470.33 463.47 4.04 o 7 4 1 87.53 87.51 2.12 o 8 4 1 443.88 413.87 4.54 o 9 4 1 97.22 103.41 2.67 o -6 5 1 13.63 13.64 1.00 o -5 5 1 20.76 18.72 0.98 o -4 5 1 23.85 22.46 0.95 o -3 5 1 334.14 319.08 3.53 o -2 5 1 364.41 341.86 3.39 o -1 5 1 86.78 84.13 1.21 o 0 5 1 1081.44 1082.67 3.70 o 1 5 1 2.78 5.63 0.35 o 2 5 1 195.44 193.49 2.23 o 3 5 1 245.80 243.17 2.54 o 4 5 1 190.14 192.28 2.40 o 5 5 1 620.54 601.71 4.41 o 6 5 1 25.76 26.43 0.89 o 7 5 1 38.88 36.99 1.16 o 8 5 1 184.51 191.40 3.27 o 9 5 1 30.56 27.88 1.21 o -5 6 1 28.18 25.43 1.14 o -4 6 1 7.42 7.82 0.82 o -3 6 1 25.17 27.12 0.99 o -2 6 1 11.49 12.56 0.77 o -1 6 1 59.81 58.17 1.43 o 0 6 1 114.53 105.99 1.40 o 1 6 1 201.09 207.18 1.83 o 2 6 1 317.42 317.96 3.12 o 3 6 1 84.47 81.20 1.73 o 4 6 1 86.64 86.99 1.87 o 5 6 1 58.33 62.13 1.81 o 6 6 1 7.07 8.49 0.75 o 7 6 1 45.77 50.38 1.45 o 8 6 1 20.73 25.46 1.12 o -4 7 1 93.39 89.81 2.61 o -3 7 1 0.69 -0.53 1.27 o -2 7 1 196.44 197.61 3.24 o -1 7 1 120.82 119.31 2.06 o 0 7 1 6.76 9.78 0.63 o 1 7 1 148.94 160.59 2.33 o 2 7 1 273.52 273.00 3.27 o 3 7 1 3.67 4.03 0.64 o 4 7 1 33.28 36.81 1.16 o 5 7 1 337.44 339.94 3.86 o 6 7 1 231.74 231.95 3.36 o 7 7 1 53.72 54.80 1.57 o 8 7 1 17.10 24.15 1.11 o -2 8 1 34.45 38.55 1.24 o -1 8 1 56.13 56.01 1.55 o 0 8 1 22.65 21.78 0.68 o 1 8 1 217.24 203.73 2.25 o 2 8 1 170.94 168.20 2.92 o 3 8 1 138.72 142.90 2.66 o 4 8 1 79.00 84.36 2.21 o 5 8 1 63.71 64.45 1.77 o 6 8 1 150.67 156.16 3.08 o 7 8 1 12.85 14.42 0.96 o 0 9 1 56.02 54.48 1.47 o 1 9 1 11.05 11.70 0.69 o 2 9 1 84.34 82.37 2.38 o 3 9 1 74.00 78.36 2.00 o 4 9 1 15.62 17.00 0.95 o 5 9 1 3.69 2.88 0.80 o 6 9 1 142.69 165.01 3.37 o -5 -9 2 46.95 48.26 1.42 o -4 -9 2 22.69 19.43 1.02 o -3 -9 2 46.79 49.76 1.55 o -2 -9 2 119.72 112.02 2.66 o -1 -9 2 1.45 2.45 0.89 o 0 -9 2 7.26 7.77 0.61 o -6 -8 2 174.74 176.66 3.27 o -5 -8 2 7.89 9.67 0.89 o -4 -8 2 24.94 25.89 1.03 o -3 -8 2 527.02 490.24 4.85 o -2 -8 2 0.89 1.56 1.07 o -1 -8 2 76.41 70.23 1.46 o 0 -8 2 303.96 290.36 2.70 o 1 -8 2 185.20 183.75 2.29 o 2 -8 2 76.60 76.13 2.04 o -7 -7 2 19.92 17.93 1.02 o -6 -7 2 11.01 12.62 0.86 o -5 -7 2 18.11 20.31 0.90 o -4 -7 2 95.80 87.25 2.09 o -3 -7 2 67.17 77.64 1.96 o -2 -7 2 250.19 233.55 3.07 o -1 -7 2 128.16 126.44 1.90 o 0 -7 2 1.33 1.47 0.64 o 1 -7 2 465.07 476.04 6.20 o 2 -7 2 29.88 32.29 1.09 o 3 -7 2 156.86 162.60 3.16 o 4 -7 2 64.94 58.84 1.73 o -8 -6 2 13.41 13.84 0.98 o -7 -6 2 72.79 65.47 1.87 o -6 -6 2 4.81 5.97 0.77 o -5 -6 2 263.53 256.83 3.27 o -4 -6 2 51.92 56.15 1.64 o -3 -6 2 110.59 102.32 1.97 o -2 -6 2 70.39 70.44 1.70 o -1 -6 2 169.71 170.28 1.70 o 0 -6 2 18.42 15.26 0.51 o 1 -6 2 184.18 193.97 1.94 o 2 -6 2 1066.92 1085.09 6.53 o 3 -6 2 55.62 56.85 1.62 o 4 -6 2 16.76 16.68 0.99 o 5 -6 2 34.90 37.81 1.27 o -8 -5 2 31.61 31.56 1.15 o -7 -5 2 28.51 28.45 1.06 o -6 -5 2 599.11 637.14 5.12 o -5 -5 2 30.19 28.17 0.88 o -4 -5 2 35.53 30.91 0.90 o -3 -5 2 26.93 21.24 0.71 o -2 -5 2 858.00 870.22 4.73 o -1 -5 2 464.06 479.66 2.47 o 0 -5 2 6.35 6.69 0.39 o 1 -5 2 27.11 26.46 0.58 o 2 -5 2 6.85 7.84 0.66 o 3 -5 2 104.08 111.89 2.22 o 4 -5 2 2.16 0.48 1.12 o 5 -5 2 132.34 126.16 2.72 o 6 -5 2 33.88 31.94 1.24 o -8 -4 2 43.16 44.93 1.35 o -7 -4 2 123.81 126.17 2.60 o -6 -4 2 97.41 99.69 2.21 o -5 -4 2 1543.60 1533.65 7.02 o -4 -4 2 224.72 239.54 2.61 o -3 -4 2 1.39 1.94 0.46 o -2 -4 2 1252.89 1301.83 5.24 o -1 -4 2 406.23 417.83 2.06 o 0 -4 2 426.35 427.17 3.19 o 1 -4 2 613.56 655.51 2.74 o 2 -4 2 531.00 587.56 3.93 o 3 -4 2 362.00 383.81 3.48 o 4 -4 2 205.52 220.03 2.98 o 5 -4 2 16.25 15.62 0.90 o 6 -4 2 38.45 39.45 1.23 o 7 -4 2 107.95 112.07 2.87 o -8 -3 2 114.32 122.45 2.76 o -7 -3 2 38.62 39.85 1.21 o -6 -3 2 85.49 78.17 1.91 o -5 -3 2 40.85 43.39 1.20 o -4 -3 2 9.31 9.18 0.52 o -3 -3 2 268.02 265.09 2.35 o -2 -3 2 120.18 178.64 1.79 o -1 -3 2 582.30 640.09 2.24 o 0 -3 2 1216.09 1368.50 3.30 o 1 -3 2 64.02 61.31 1.71 o 2 -3 2 981.68 1165.58 4.94 o 3 -3 2 96.96 81.43 1.59 o 4 -3 2 355.83 408.58 3.63 o 5 -3 2 73.54 75.58 1.99 o 6 -3 2 191.67 196.96 3.18 o 7 -3 2 184.97 197.97 3.40 o -8 -2 2 65.35 61.94 1.81 o -7 -2 2 18.38 18.95 0.90 o -6 -2 2 130.24 139.35 2.40 o -5 -2 2 25.51 24.04 0.74 o -4 -2 2 495.25 502.83 3.41 o -3 -2 2 836.59 801.60 3.81 o -2 -2 2 1008.52 1031.20 3.86 o -1 -2 2 258.29 236.53 1.23 o 0 -2 2 452.14 508.95 2.89 o 1 -2 2 1753.59 2033.65 4.33 o 2 -2 2 1213.11 1603.07 5.17 o 3 -2 2 2773.69 3419.14 8.57 o 4 -2 2 304.09 337.58 3.08 o 5 -2 2 132.68 152.41 2.41 o 6 -2 2 251.28 273.03 3.47 o 7 -2 2 55.75 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