#------------------------------------------------------------------------------ #$Date: 2009-05-05 17:46:52 +0300 (Tue, 05 May 2009) $ #$Revision: 697 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2217898.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2217898_Fobs loop_ _publ_author_name 'Cadiau, A.' 'Hemon-Ribaud, A.' 'Leblanc, M.' 'Maisonneuve, V.' _publ_section_title ; 2,4,6-Triamino-1,3,5-triazine-1,3-diium aquapentafluoridoaluminate ; _journal_coeditor_code DN2317 _journal_issue 4 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m523 _journal_page_last m524 _journal_volume 64 _journal_year 2008 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 105.530 _cell_angle_gamma 90.000 _cell_length_a 7.5707 _cell_length_b 8.8227 _cell_length_c 13.4840 _exptl_crystal_F_000 555.78 _reflns_d_resolution_high 0.7100 _[local]_cod_data_source_file dn2317Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' CAMW11B 28/02/2007 P21/c PARAMETRES DB LIST SANS ABS' _shelx_refln_list_code 4 _shelx_F_calc_maximum 137.55 _shelx_F_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 7.32 10.67 6.50 o 5 0 0 1415.94 1266.36 30.05 o 6 0 0 2.39 33.67 15.25 o 8 0 0 0.07 6.52 20.48 o 9 0 0 130.91 132.74 20.14 o 10 0 0 0.07 0.02 24.01 o 1 1 0 639.96 797.95 13.07 o 2 1 0 3456.75 3381.55 29.50 o 3 1 0 303.45 332.95 16.01 o 4 1 0 63.26 52.71 11.78 o 5 1 0 0.13 24.23 15.54 o 7 1 0 12.27 0.02 18.15 o 8 1 0 9.26 0.02 20.65 o 9 1 0 0.01 43.39 19.33 o 10 1 0 3.06 0.02 25.24 o 0 2 0 4452.09 4879.36 29.90 o 1 2 0 109.90 95.43 10.65 o 2 2 0 840.78 900.41 19.63 o 3 2 0 737.96 702.50 20.08 o 4 2 0 22.17 3.69 14.12 o 5 2 0 46.70 52.96 14.21 o 6 2 0 1.36 0.02 17.92 o 7 2 0 9.41 0.02 18.66 o 8 2 0 20.42 51.21 18.00 o 9 2 0 152.91 119.44 21.81 o 10 2 0 66.20 48.33 26.07 o 1 3 0 420.53 469.15 16.14 o 2 3 0 3206.51 3275.87 34.16 o 3 3 0 5025.14 5146.93 46.87 o 4 3 0 131.01 72.58 13.68 o 5 3 0 12.19 13.64 17.83 o 6 3 0 1085.87 1119.98 33.31 o 7 3 0 10.51 57.43 16.75 o 8 3 0 44.17 60.88 18.32 o 9 3 0 220.09 260.34 24.44 o 0 4 0 26.54 32.83 9.89 o 1 4 0 456.90 436.96 17.35 o 2 4 0 911.89 902.89 22.79 o 3 4 0 6622.30 6840.42 57.62 o 4 4 0 0.22 6.21 15.78 o 5 4 0 308.21 298.18 22.32 o 6 4 0 66.31 59.49 16.31 o 7 4 0 83.06 74.46 18.21 o 8 4 0 42.96 36.98 22.75 o 9 4 0 88.54 66.18 21.50 o 1 5 0 1378.59 1407.63 27.43 o 2 5 0 940.10 947.23 25.56 o 3 5 0 454.00 501.74 22.58 o 4 5 0 0.19 0.02 17.17 o 5 5 0 95.86 115.55 16.75 o 6 5 0 8.51 22.19 20.78 o 7 5 0 21.63 0.02 21.11 o 8 5 0 66.10 86.28 20.35 o 9 5 0 13.54 0.02 25.18 o 0 6 0 4268.20 4136.26 47.99 o 1 6 0 4.40 0.02 13.13 o 2 6 0 6.46 29.63 12.96 o 3 6 0 85.83 68.19 15.76 o 4 6 0 420.49 459.17 24.65 o 5 6 0 105.99 104.17 17.58 o 6 6 0 0.81 0.02 21.24 o 7 6 0 137.36 142.80 20.52 o 8 6 0 6.77 0.02 24.54 o 1 7 0 0.42 0.02 14.02 o 2 7 0 450.21 541.07 25.05 o 3 7 0 409.67 398.01 24.90 o 4 7 0 371.82 374.93 25.52 o 6 7 0 322.24 365.14 26.58 o 7 7 0 0.33 0.02 22.30 o 8 7 0 2.72 0.02 25.27 o 0 8 0 763.92 666.27 26.45 o 1 8 0 45.03 25.98 12.81 o 2 8 0 31.86 29.58 17.26 o 3 8 0 73.63 86.26 16.79 o 4 8 0 175.40 155.65 19.80 o 5 8 0 7.36 0.02 20.52 o 6 8 0 108.13 129.04 21.01 o 7 8 0 16.72 14.76 24.95 o 1 9 0 238.02 236.41 19.72 o 2 9 0 353.81 375.86 25.41 o 3 9 0 0.64 0.02 19.72 o 4 9 0 76.38 54.32 18.51 o 5 9 0 34.07 34.20 22.60 o 6 9 0 6.29 0.02 24.48 o 7 9 0 30.60 44.52 26.35 o 0 10 0 17.63 30.54 13.60 o 1 10 0 120.45 157.31 16.43 o 2 10 0 52.74 29.58 18.85 o 3 10 0 53.73 97.12 19.25 o 4 10 0 0.02 31.94 23.04 o 5 10 0 0.89 0.02 25.05 o 6 10 0 1.74 0.02 25.67 o 1 11 0 2.73 5.19 17.32 o 2 11 0 79.18 73.06 19.15 o 3 11 0 5.99 0.02 24.29 o 4 11 0 3.38 32.87 25.69 o 0 12 0 195.07 164.06 19.97 o 1 12 0 1.85 10.70 18.15 o 2 12 0 198.12 212.90 23.70 o -10 1 1 50.12 37.25 25.71 o -9 1 1 1.15 21.20 17.49 o -8 1 1 133.51 139.62 19.14 o -7 1 1 27.99 9.91 18.26 o -6 1 1 0.43 32.63 14.68 o -5 1 1 137.29 152.69 14.57 o -4 1 1 51.44 20.92 13.70 o -3 1 1 581.66 606.93 17.89 o -2 1 1 4.55 5.76 12.35 o -1 1 1 74.06 73.61 7.48 o 1 1 1 383.38 377.79 12.49 o 2 1 1 12.04 0.42 10.69 o 3 1 1 1.08 8.01 12.45 o 4 1 1 14.60 0.02 14.19 o 5 1 1 200.37 186.68 15.99 o 6 1 1 59.98 69.74 15.90 o 7 1 1 11.83 9.51 19.44 o 8 1 1 26.90 37.57 20.42 o 9 1 1 15.21 0.02 21.79 o 10 1 1 14.93 0.02 23.59 o -10 2 1 0.05 48.01 19.69 o -9 2 1 17.36 21.79 21.41 o -8 2 1 2.93 0.02 19.42 o -7 2 1 19.62 26.17 15.71 o -6 2 1 150.10 179.08 17.13 o -5 2 1 12.40 0.02 15.65 o -4 2 1 96.93 83.84 12.43 o -3 2 1 361.05 403.92 16.48 o -2 2 1 621.04 639.77 17.53 o -1 2 1 17.75 41.13 10.08 o 0 2 1 294.54 387.47 13.57 o 1 2 1 8.67 0.02 12.56 o 2 2 1 197.08 180.75 14.21 o 3 2 1 58.92 60.21 11.44 o 4 2 1 12.08 41.27 12.30 o 5 2 1 7.88 0.02 16.50 o 6 2 1 1.39 16.43 17.85 o 7 2 1 36.17 14.00 19.95 o 8 2 1 17.27 0.02 22.39 o 9 2 1 6.28 37.63 19.61 o -10 3 1 0.68 25.18 23.82 o -9 3 1 113.59 121.12 21.11 o -8 3 1 41.14 49.41 17.81 o -7 3 1 86.57 71.56 16.98 o -6 3 1 60.11 19.46 19.23 o -5 3 1 248.51 243.61 18.68 o -4 3 1 1707.52 1636.77 31.77 o -3 3 1 1000.13 1001.85 23.53 o -2 3 1 1565.73 1523.09 25.12 o -1 3 1 2005.75 2048.40 25.98 o 0 3 1 106.39 102.78 10.82 o 1 3 1 0.92 1.00 12.18 o 2 3 1 361.12 350.62 16.48 o 3 3 1 143.06 128.15 12.96 o 4 3 1 101.49 97.25 14.12 o 5 3 1 105.16 124.82 16.20 o 6 3 1 125.49 112.88 17.32 o 7 3 1 24.39 0.02 20.50 o 8 3 1 7.01 33.97 18.30 o 9 3 1 103.76 116.39 22.02 o -9 4 1 0.12 0.02 22.79 o -8 4 1 46.34 26.54 21.14 o -7 4 1 2.42 0.02 18.91 o -6 4 1 19.26 35.28 15.25 o -5 4 1 21.37 0.02 17.15 o -4 4 1 0.00 7.82 15.37 o -3 4 1 3150.30 3130.68 40.37 o -2 4 1 732.00 665.55 20.67 o -1 4 1 830.74 852.10 21.03 o 0 4 1 796.38 940.98 21.33 o 1 4 1 1319.43 1434.87 25.54 o 2 4 1 1629.71 1719.62 29.16 o 3 4 1 66.49 54.38 13.24 o 4 4 1 361.86 389.50 21.69 o 5 4 1 46.48 49.62 16.28 o 6 4 1 2.07 0.02 18.40 o 7 4 1 27.46 2.80 20.73 o 8 4 1 3.57 23.36 22.07 o 9 4 1 139.62 126.26 23.30 o -9 5 1 7.18 0.02 21.83 o -8 5 1 81.42 81.87 19.46 o -7 5 1 0.17 0.02 19.63 o -6 5 1 22.74 22.60 18.49 o -5 5 1 22.89 11.29 17.28 o -4 5 1 264.55 255.27 19.82 o -3 5 1 939.82 894.27 26.53 o -2 5 1 652.99 585.67 21.73 o -1 5 1 1947.82 1989.74 31.77 o 0 5 1 1107.53 1092.21 24.29 o 1 5 1 466.04 469.53 19.59 o 2 5 1 441.17 398.18 20.20 o 3 5 1 35.78 0.02 17.03 o 4 5 1 16.16 21.58 18.38 o 5 5 1 22.78 0.02 17.70 o 6 5 1 53.34 54.43 17.18 o 7 5 1 31.76 67.98 18.66 o 8 5 1 104.64 124.31 21.81 o 9 5 1 32.42 76.60 21.98 o -9 6 1 0.71 0.02 23.10 o -8 6 1 6.65 32.68 19.02 o -7 6 1 73.11 74.80 18.30 o -6 6 1 76.26 80.73 17.15 o -5 6 1 216.68 224.38 18.25 o -4 6 1 345.70 350.43 22.94 o -3 6 1 50.64 49.66 14.42 o -2 6 1 419.93 385.83 21.69 o -1 6 1 1297.56 1251.15 29.67 o 0 6 1 2458.33 2431.04 37.53 o 1 6 1 2.93 9.36 14.66 o 2 6 1 171.63 149.53 15.35 o 3 6 1 89.51 101.10 16.22 o 4 6 1 0.05 0.02 17.22 o 5 6 1 21.28 0.02 19.23 o 6 6 1 2.35 24.73 20.97 o 7 6 1 284.73 263.98 23.89 o 8 6 1 6.23 0.02 23.66 o -8 7 1 1.76 7.67 22.79 o -7 7 1 1.91 0.02 19.17 o -6 7 1 428.10 427.93 28.53 o -5 7 1 94.55 92.78 17.64 o -4 7 1 1.84 1.17 17.35 o -3 7 1 49.04 29.69 17.77 o -2 7 1 121.66 120.48 16.39 o -1 7 1 2114.99 2058.00 39.69 o 0 7 1 14.08 38.29 11.54 o 1 7 1 1980.64 2023.35 38.99 o 2 7 1 433.02 433.86 24.23 o 3 7 1 263.07 259.60 19.72 o 4 7 1 194.96 237.42 19.27 o 5 7 1 137.33 159.76 19.33 o 6 7 1 959.57 990.29 38.35 o 7 7 1 26.23 38.76 20.84 o 8 7 1 44.10 39.03 27.34 o -7 8 1 61.32 77.68 20.56 o -6 8 1 175.18 182.44 21.11 o -5 8 1 594.35 565.95 30.03 o -4 8 1 0.07 18.70 18.40 o -3 8 1 686.55 710.68 29.33 o -2 8 1 3.36 27.02 14.85 o -1 8 1 2483.70 2313.97 44.88 o 0 8 1 634.22 607.84 25.22 o 1 8 1 617.13 639.58 26.71 o 2 8 1 91.60 114.55 16.16 o 3 8 1 713.15 688.74 30.84 o 4 8 1 110.61 169.15 19.53 o 5 8 1 10.79 0.02 21.24 o 6 8 1 31.25 32.61 19.70 o 7 8 1 18.20 0.02 26.07 o -7 9 1 26.95 27.43 20.46 o -6 9 1 31.50 0.02 21.75 o -5 9 1 7.73 27.02 20.54 o -4 9 1 529.36 575.88 30.41 o -3 9 1 41.31 34.80 20.88 o -2 9 1 73.82 101.91 16.94 o -1 9 1 261.74 227.79 18.72 o 0 9 1 12.27 1.29 14.82 o 1 9 1 145.71 147.59 16.22 o 2 9 1 71.99 95.13 17.17 o 3 9 1 200.33 235.39 20.95 o 4 9 1 376.23 379.23 29.04 o 5 9 1 72.17 78.25 19.95 o 6 9 1 21.07 3.35 26.15 o -6 10 1 1.20 32.15 20.46 o -5 10 1 0.07 35.41 18.85 o -4 10 1 7.12 28.82 21.90 o -3 10 1 701.22 695.58 34.50 o -2 10 1 268.25 227.64 21.03 o -1 10 1 2.03 0.02 17.62 o 0 10 1 30.22 2.33 15.65 o 1 10 1 143.86 172.15 17.89 o 2 10 1 523.12 558.43 30.37 o 3 10 1 290.46 301.14 24.61 o 4 10 1 191.84 231.47 24.33 o 5 10 1 19.87 47.65 21.60 o -3 11 1 80.80 70.75 20.92 o -2 11 1 168.73 129.21 21.07 o -1 11 1 180.09 200.07 20.20 o 0 11 1 7.31 0.02 16.05 o 1 11 1 38.49 33.06 18.95 o 2 11 1 0.00 34.03 20.90 o 3 11 1 141.55 146.15 23.49 o 4 11 1 113.18 144.20 23.55 o -2 12 1 0.21 6.25 19.19 o -1 12 1 0.37 0.02 21.22 o 0 12 1 17.99 29.37 18.93 o 1 12 1 97.83 120.16 19.12 o 2 12 1 206.58 202.61 22.96 o -10 0 2 39.84 36.47 25.81 o -9 0 2 13.81 0.02 22.36 o -7 0 2 45.27 39.05 15.65 o -6 0 2 995.03 1050.92 30.79 o -5 0 2 1693.50 1704.05 33.16 o -4 0 2 20.17 8.09 13.45 o -3 0 2 2296.79 2276.93 28.40 o -2 0 2 304.02 310.15 14.02 o -1 0 2 7749.26 7389.56 31.72 o 0 0 2 79.81 114.80 7.84 o 1 0 2 1415.10 1536.26 19.14 o 3 0 2 812.08 776.62 20.44 o 4 0 2 8139.93 8274.42 63.24 o 5 0 2 1857.69 1849.25 36.45 o 6 0 2 198.71 196.04 17.60 o 7 0 2 1022.88 1018.30 34.08 o 8 0 2 7.61 0.02 20.67 o -10 1 2 3.04 46.74 26.17 o -9 1 2 56.31 21.41 21.58 o -8 1 2 213.14 205.23 20.22 o -7 1 2 382.17 358.26 23.89 o -6 1 2 1804.44 1732.13 37.78 o -5 1 2 1294.38 1265.95 29.78 o -4 1 2 2765.43 2742.54 35.52 o -3 1 2 286.97 276.96 15.48 o -2 1 2 2134.19 2331.42 25.29 o -1 1 2 3717.69 3942.76 26.17 o 0 1 2 883.18 1035.05 14.68 o 1 1 2 15561.79 15228.42 55.72 o 2 1 2 5.29 0.02 12.22 o 3 1 2 58.34 54.79 11.35 o 4 1 2 1213.54 1277.14 27.66 o 5 1 2 650.46 653.63 25.58 o 6 1 2 750.11 783.11 29.06 o 7 1 2 103.90 140.64 18.04 o 8 1 2 275.16 278.00 23.87 o 9 1 2 3.36 25.90 23.29 o -10 2 2 31.18 45.30 21.56 o -9 2 2 5.56 0.02 21.64 o -8 2 2 52.91 90.79 17.68 o -7 2 2 0.69 9.11 18.09 o -6 2 2 33.81 35.73 18.30 o -5 2 2 954.67 906.44 26.41 o -4 2 2 220.04 173.47 13.70 o -3 2 2 7856.13 7460.18 51.59 o -2 2 2 3403.19 3404.44 31.83 o -1 2 2 2232.77 2311.07 24.88 o 0 2 2 1076.51 1225.00 19.48 o 1 2 2 767.41 769.95 18.04 o 2 2 2 26.37 62.09 10.91 o 3 2 2 171.18 183.99 12.96 o 4 2 2 644.56 592.15 22.85 o 5 2 2 155.23 178.25 16.50 o 6 2 2 274.41 259.53 20.69 o 7 2 2 87.86 78.57 17.92 o 8 2 2 5.46 0.02 21.77 o 9 2 2 125.85 161.73 22.66 o -10 3 2 31.97 60.33 21.22 o -9 3 2 220.19 215.44 22.51 o -8 3 2 16.94 63.57 17.20 o -7 3 2 0.46 0.02 18.11 o -5 3 2 43.61 18.87 17.90 o -4 3 2 8069.02 8242.00 64.53 o -3 3 2 375.55 337.10 17.24 o -2 3 2 18921.30 18944.59 79.63 o -1 3 2 348.71 301.31 15.27 o 0 3 2 1957.86 1876.14 25.43 o 1 3 2 1759.55 1678.71 25.56 o 2 3 2 61.07 40.85 11.16 o 3 3 2 2784.88 2819.27 37.91 o 4 3 2 28.57 37.55 13.89 o 5 3 2 5.25 12.50 17.68 o 6 3 2 8.73 18.00 18.13 o 7 3 2 13.86 0.02 19.72 o 8 3 2 613.65 594.03 33.12 o 9 3 2 0.24 0.02 24.35 o -9 4 2 11.79 44.52 22.66 o -8 4 2 134.56 144.77 19.63 o -7 4 2 2.93 38.61 19.51 o -6 4 2 44.46 26.87 18.66 o -5 4 2 3.64 6.16 16.65 o -4 4 2 113.54 133.14 14.30 o -3 4 2 2007.68 1846.32 31.64 o -2 4 2 1759.61 1700.48 28.80 o -1 4 2 1046.36 1179.40 23.89 o 0 4 2 46.63 38.44 10.74 o 1 4 2 974.86 1060.62 23.78 o 2 4 2 590.18 590.81 20.86 o 3 4 2 38.98 74.71 13.15 o 4 4 2 948.63 926.27 29.27 o 5 4 2 268.93 257.82 21.14 o 6 4 2 75.77 72.58 17.43 o 7 4 2 74.84 21.60 21.60 o 8 4 2 0.02 0.02 23.34 o 9 4 2 82.77 103.71 22.66 o -9 5 2 26.45 39.45 24.04 o -8 5 2 65.53 34.18 22.30 o -7 5 2 134.75 178.10 19.23 o -6 5 2 43.93 30.09 19.38 o -5 5 2 112.67 108.13 16.20 o -4 5 2 703.85 730.60 26.62 o -3 5 2 268.67 293.06 19.46 o -2 5 2 1932.96 2036.71 33.86 o -1 5 2 9.72 5.49 11.27 o 0 5 2 189.34 184.37 15.80 o 1 5 2 47.07 30.22 12.20 o 2 5 2 90.39 100.38 14.00 o 3 5 2 30.63 14.74 16.18 o 4 5 2 5.74 0.02 19.74 o 5 5 2 4.31 0.02 18.47 o 6 5 2 102.17 124.55 18.51 o 7 5 2 2.90 0.02 20.63 o 8 5 2 280.27 298.03 25.24 o 9 5 2 19.22 0.02 25.77 o -9 6 2 0.65 27.70 19.44 o -7 6 2 19.98 0.02 20.82 o -6 6 2 323.30 316.99 25.01 o -5 6 2 171.95 191.42 18.36 o -4 6 2 107.58 63.94 15.84 o -3 6 2 10.63 19.72 17.43 o -2 6 2 508.25 505.51 23.00 o -1 6 2 420.95 420.23 20.82 o 0 6 2 2057.62 2089.68 36.23 o 1 6 2 197.04 183.08 15.90 o 2 6 2 178.26 184.08 16.62 o 3 6 2 11.74 32.30 15.88 o 4 6 2 16.68 28.67 17.90 o 5 6 2 179.50 194.30 19.57 o 6 6 2 371.65 403.18 28.70 o 7 6 2 127.57 126.22 21.43 o 8 6 2 28.88 34.24 26.41 o -8 7 2 49.76 60.86 20.84 o -7 7 2 15.18 11.92 18.06 o -6 7 2 106.69 113.41 18.74 o -5 7 2 260.85 240.98 21.31 o -4 7 2 12.62 31.70 18.47 o -3 7 2 41.42 63.47 15.16 o -2 7 2 469.40 474.59 24.57 o -1 7 2 1581.29 1531.79 35.96 o 0 7 2 149.07 169.67 16.54 o 1 7 2 1463.50 1468.56 35.34 o 2 7 2 31.67 20.69 18.72 o 3 7 2 50.91 1.63 19.38 o 4 7 2 331.09 369.63 26.22 o 5 7 2 131.97 124.99 19.70 o 6 7 2 7.13 0.02 22.09 o 7 7 2 34.83 8.00 24.99 o 8 7 2 6.89 35.71 25.77 o -8 8 2 0.25 34.35 23.89 o -7 8 2 70.78 66.56 20.77 o -6 8 2 38.85 44.24 17.85 o -5 8 2 0.03 32.80 20.18 o -4 8 2 13.81 7.62 18.34 o -3 8 2 57.12 28.25 15.71 o -2 8 2 465.62 401.27 24.29 o -1 8 2 120.61 143.06 16.31 o 0 8 2 40.65 61.75 14.72 o 1 8 2 78.31 93.44 15.06 o 2 8 2 233.43 258.88 20.25 o 3 8 2 43.40 47.12 17.15 o 4 8 2 9.38 30.88 21.26 o 5 8 2 139.44 120.73 20.73 o 6 8 2 118.10 140.60 22.53 o 7 8 2 15.16 29.08 26.49 o -7 9 2 36.63 37.89 25.20 o -6 9 2 28.49 0.02 23.00 o -5 9 2 161.46 166.98 20.61 o -4 9 2 13.44 28.97 20.50 o -3 9 2 9.56 11.39 19.31 o -2 9 2 18.90 7.67 18.81 o -1 9 2 0.12 0.02 17.39 o 0 9 2 284.45 267.71 20.08 o 1 9 2 141.12 122.51 16.16 o 2 9 2 91.11 78.10 17.47 o 3 9 2 207.76 233.50 21.71 o 4 9 2 87.13 86.17 20.08 o 5 9 2 29.25 59.59 20.58 o 6 9 2 40.23 41.04 21.81 o -6 10 2 33.70 63.68 20.56 o -5 10 2 43.99 0.02 24.33 o -4 10 2 6.67 0.02 20.52 o -3 10 2 11.45 21.14 20.78 o -2 10 2 1.54 0.02 19.55 o -1 10 2 15.35 23.99 18.59 o 1 10 2 193.49 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