#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/79/2217951.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2217951_Fobs loop_ _publ_author_name 'Sato, Kazuyuki' 'Shibata, Hiroki' 'Mizuguchi, Jin' _publ_section_title ; Poly[tris{\m~2~-4-[4-(dimethylamino)phenyldiazenyl]benzenesulfonato}tridioxanetrisodium(I)] ; _journal_coeditor_code IS2280 _journal_issue 4 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m586 _journal_page_last m587 _journal_volume 64 _journal_year 2008 _space_group_IT_number 19 _symmetry_space_group_name_Hall 'P 2ac 2ab' _symmetry_space_group_name_H-M 'P 21 21 21' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 8.4471 _cell_length_b 15.5153 _cell_length_c 44.4881 _exptl_crystal_F_000 2616.00 _reflns_d_resolution_high 0.8301 _[local]_cod_data_source_file is2280Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' MONa_08' _shelx_refln_list_code 4 _shelx_F_calc_maximum 906.13 _shelx_F_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' 'x+1/2, -y+1/2, -z' '-x, y+1/2, -z+1/2' '-x+1/2, -y, z+1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 5386.26 5443.23 113.81 o 6 0 0 6950.86 6934.66 183.17 o 1 1 0 1018.23 998.00 14.30 o 2 1 0 1809.98 1732.61 56.93 o 3 1 0 1281.99 1338.57 33.03 o 4 1 0 1703.77 1678.39 39.86 o 5 1 0 2104.78 2220.91 79.50 o 6 1 0 6.95 13.57 90.20 o 7 1 0 64.08 178.20 192.41 o 8 1 0 78.84 102.87 175.83 o 0 2 0 117.15 97.67 20.43 o 1 2 0 3911.15 3912.94 38.37 o 2 2 0 10456.02 10220.31 148.30 o 3 2 0 258.87 276.87 26.04 o 4 2 0 5.41 -4.42 27.25 o 5 2 0 224.15 171.23 57.27 o 6 2 0 456.32 414.58 109.45 o 7 2 0 3386.78 3402.67 387.94 o 8 2 0 105.34 169.04 192.64 o 1 3 0 821077.56 717631.50 3929.10 o 2 3 0 275297.41 268265.28 3372.33 o 3 3 0 131566.47 127967.09 1813.31 o 4 3 0 15008.51 15541.03 242.59 o 5 3 0 21094.39 19204.68 558.84 o 6 3 0 1043.51 967.46 271.41 o 7 3 0 13246.21 12323.04 337.08 o 8 3 0 2653.48 2405.63 244.07 o 9 3 0 1782.73 1203.38 143.25 o 0 4 0 25907.40 25147.47 534.46 o 1 4 0 578.36 507.40 27.02 o 2 4 0 697.56 684.87 22.17 o 3 4 0 1713.63 1780.74 37.88 o 4 4 0 256.62 280.26 42.48 o 5 4 0 154.34 193.61 76.01 o 6 4 0 468.46 364.53 284.84 o 7 4 0 217.08 120.39 307.89 o 8 4 0 472.65 585.70 213.52 o 9 4 0 522.56 382.42 144.92 o 1 5 0 364.34 355.65 29.14 o 2 5 0 426.43 409.61 36.65 o 3 5 0 3822.70 3818.44 125.20 o 4 5 0 86.02 118.95 59.23 o 5 5 0 125.93 253.71 92.65 o 6 5 0 1323.66 857.56 330.78 o 7 5 0 383.11 288.49 318.38 o 8 5 0 2408.02 1869.11 287.42 o 9 5 0 53.95 31.44 144.79 o 0 6 0 1196.18 894.74 75.91 o 1 6 0 4041.00 3698.40 140.62 o 2 6 0 18209.36 18841.15 514.14 o 3 6 0 40038.39 39688.23 1310.67 o 4 6 0 68475.72 66519.53 2783.53 o 5 6 0 5012.49 4923.54 229.44 o 6 6 0 42252.88 34041.77 4306.12 o 7 6 0 2338.05 2050.21 333.33 o 8 6 0 4664.96 3594.64 293.41 o 9 6 0 177.66 179.04 393.75 o 1 7 0 1016.57 921.50 49.37 o 2 7 0 14067.21 14877.10 371.74 o 3 7 0 2622.49 2579.82 101.89 o 4 7 0 78.26 148.67 113.61 o 5 7 0 1.87 57.02 154.97 o 6 7 0 591.36 500.10 222.57 o 7 7 0 10.00 -79.90 337.36 o 9 7 0 27.97 -2.59 191.44 o 0 8 0 1711.46 1689.86 85.65 o 1 8 0 957.42 1012.97 63.07 o 2 8 0 2769.08 3082.76 74.55 o 3 8 0 1207.52 1084.94 108.61 o 4 8 0 1.33 -38.18 159.67 o 5 8 0 1125.71 851.49 178.74 o 6 8 0 516.55 408.89 234.41 o 7 8 0 1583.68 1376.26 338.67 o 8 8 0 0.08 -51.18 549.38 o 9 8 0 969.70 702.03 183.68 o 1 9 0 1575.50 1656.84 72.74 o 2 9 0 3558.85 3601.95 97.21 o 3 9 0 7214.75 7371.90 269.80 o 4 9 0 501.94 447.57 177.77 o 5 9 0 43425.26 41634.86 2225.53 o 6 9 0 9488.04 9870.48 1703.78 o 7 9 0 8954.71 8012.09 359.64 o 0 10 0 746.34 647.43 112.07 o 1 10 0 67.79 11.22 64.27 o 2 10 0 303.73 322.17 85.15 o 3 10 0 546.10 701.24 131.41 o 4 10 0 114.27 -40.35 168.00 o 5 10 0 52.85 118.30 195.36 o 6 10 0 541.58 333.45 253.45 o 7 10 0 40.99 218.68 205.53 o 8 10 0 479.86 634.42 242.97 o 1 11 0 3142.73 2764.84 137.88 o 2 11 0 2839.22 2689.47 140.30 o 3 11 0 47.11 89.00 141.62 o 4 11 0 2740.26 2628.47 216.50 o 5 11 0 19.61 -175.27 175.27 o 6 11 0 1502.18 1439.66 329.82 o 7 11 0 303.65 390.84 197.57 o 8 11 0 755.02 1165.03 222.64 o 0 12 0 3678.62 3380.17 179.55 o 1 12 0 2873.74 2791.93 156.10 o 2 12 0 2604.23 2460.99 193.89 o 3 12 0 2082.93 1564.98 146.17 o 4 12 0 46.13 14.08 165.40 o 5 12 0 427.31 513.51 168.53 o 6 12 0 1367.77 1484.33 310.11 o 7 12 0 1500.09 1324.53 472.25 o 1 13 0 2111.58 1982.27 229.14 o 2 13 0 104.51 380.23 197.27 o 3 13 0 531.91 603.25 177.24 o 4 13 0 139.87 290.03 186.51 o 5 13 0 672.12 672.57 177.00 o 6 13 0 154.07 309.64 156.76 o 7 13 0 166.82 246.66 243.11 o 0 14 0 4419.11 4422.06 282.76 o 1 14 0 969.60 1416.49 221.50 o 2 14 0 1124.63 903.92 182.18 o 3 14 0 1029.68 928.54 179.01 o 4 14 0 41.86 244.88 203.48 o 5 14 0 224.91 174.40 192.03 o 6 14 0 7.29 3.96 126.97 o 1 15 0 5155.33 5093.51 236.08 o 2 15 0 507.72 364.86 172.63 o 3 15 0 15.35 -124.26 267.02 o 4 15 0 162.81 145.67 183.55 o 5 15 0 13.23 23.79 103.56 o 0 16 0 8.00 179.12 292.17 o 1 16 0 292.88 318.10 220.94 o 2 16 0 271.31 107.98 189.57 o 3 16 0 1.45 2.15 135.74 o 4 16 0 82.09 325.91 181.07 o 5 16 0 12.00 113.37 256.71 o 1 17 0 1152.51 906.76 317.99 o 2 17 0 102.07 10.54 180.68 o 3 17 0 153.41 109.36 169.99 o 4 17 0 17.85 -71.19 223.81 o 0 18 0 1019.83 826.67 268.51 o 1 18 0 625.26 798.94 133.65 o 2 18 0 391.68 135.04 133.97 o 1 0 1 41.56 64.81 10.92 o 2 0 1 627.05 703.09 60.64 o 3 0 1 1560.87 1581.86 32.09 o 4 0 1 2206.81 2309.84 49.76 o 5 0 1 342.39 417.04 80.80 o 6 0 1 3144.89 3131.74 102.29 o 7 0 1 76.65 79.46 126.51 o -8 1 1 173.14 171.91 173.62 o -7 1 1 364.21 300.51 195.40 o -6 1 1 3571.77 3411.52 99.40 o -5 1 1 461.00 406.08 84.74 o -4 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180.52 242.55 274.78 o -5 3 1 1866.06 1786.62 80.37 o -4 3 1 686.18 656.63 28.82 o -3 3 1 5186.85 5385.30 70.46 o -2 3 1 1693.77 1879.23 29.22 o -1 3 1 6834.87 7180.00 261.88 o 0 3 1 95.90 99.12 30.97 o 1 3 1 6993.36 7328.81 170.62 o 2 3 1 1639.91 1902.75 67.71 o 3 3 1 5148.97 5287.00 92.48 o 4 3 1 673.11 700.10 38.83 o 5 3 1 1762.44 1770.56 65.17 o 6 3 1 179.38 244.25 264.93 o 7 3 1 348.73 480.23 253.72 o 8 3 1 261.91 262.89 204.10 o 9 3 1 815.82 748.70 159.38 o -9 4 1 118.41 192.75 197.03 o -8 4 1 143.58 -7.90 232.29 o -7 4 1 783.16 548.17 314.23 o -6 4 1 848.09 754.84 289.19 o -5 4 1 575.63 506.66 80.48 o -4 4 1 965.34 972.57 50.66 o -3 4 1 4172.40 4288.87 81.58 o -2 4 1 1298.00 1368.95 50.75 o -1 4 1 1151.04 1154.04 36.73 o 0 4 1 503.24 587.83 45.32 o 1 4 1 1013.77 906.79 37.24 o 2 4 1 1243.44 1285.25 34.24 o 3 4 1 3993.58 3957.71 75.61 o 4 4 1 939.65 912.81 37.84 o 5 4 1 508.47 442.60 73.45 o 6 4 1 862.26 846.26 302.37 o 7 4 1 727.71 646.78 305.66 o 8 4 1 132.40 -81.18 229.74 o 9 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