#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/79/2217955.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2217955_Fobs loop_ _publ_author_name 'Portalone, Gustavo' _publ_section_title ; Biguanidinium dichloride ; _journal_coeditor_code KP2161 _journal_issue 4 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o683 _journal_volume 64 _journal_year 2008 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 98.688 _cell_angle_gamma 90.000 _cell_length_a 6.4369 _cell_length_b 16.9342 _cell_length_c 6.6526 _exptl_crystal_F_000 360.00 _reflns_d_resolution_high 0.6707 _[local]_cod_data_source_file kp2161Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title 'Biguanidinium dihydrochloride: exp_123 in P 2(1)/c' _shelx_refln_list_code 4 _shelx_F_calc_maximum 83.14 _shelx_F_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 282.07 286.00 1.07 o 2 0 0 781.09 764.82 1.30 o 3 0 0 561.46 590.04 1.47 o 4 0 0 6912.52 6482.99 30.57 o 5 0 0 277.18 274.62 1.15 o 6 0 0 209.18 199.53 0.90 o 7 0 0 1.48 0.61 0.59 o 8 0 0 612.22 648.05 3.01 o 9 0 0 0.00 0.18 0.75 o 1 1 0 463.64 423.35 1.15 o 2 1 0 6200.27 5181.48 44.21 o 3 1 0 43.62 61.25 0.19 o 4 1 0 17.46 17.43 0.22 o 5 1 0 22.91 25.67 0.33 o 6 1 0 686.92 691.85 1.83 o 7 1 0 73.87 66.52 0.50 o 8 1 0 0.01 4.88 0.40 o 9 1 0 0.01 0.36 0.53 o 2 2 0 5.79 7.22 0.13 o 3 2 0 902.72 857.67 2.63 o 4 2 0 18.23 23.73 0.19 o 5 2 0 22.92 18.56 0.22 o 6 2 0 1.48 2.18 0.26 o 7 2 0 221.18 217.89 0.74 o 8 2 0 1.61 1.96 0.39 o 9 2 0 0.53 1.15 0.45 o 1 3 0 782.91 900.44 2.42 o 2 3 0 16.31 15.54 0.11 o 3 3 0 306.15 299.28 0.53 o 4 3 0 191.27 189.01 0.51 o 5 3 0 94.72 81.26 0.33 o 6 3 0 84.70 76.40 0.42 o 7 3 0 8.92 7.89 0.34 o 8 3 0 4.65 3.08 0.40 o 9 3 0 47.59 44.16 0.57 o 0 4 0 313.12 301.57 0.87 o 1 4 0 446.26 481.68 0.84 o 2 4 0 277.87 300.27 0.47 o 3 4 0 654.62 714.92 0.93 o 4 4 0 193.91 200.56 0.47 o 5 4 0 270.83 279.45 0.66 o 6 4 0 83.90 77.41 0.48 o 7 4 0 1.76 3.01 0.31 o 8 4 0 5.05 3.53 0.40 o 9 4 0 2.49 3.71 1.22 o 1 5 0 2785.01 2872.92 14.56 o 2 5 0 1144.36 1218.58 3.10 o 3 5 0 1814.60 1832.89 3.57 o 4 5 0 79.90 91.90 0.30 o 5 5 0 212.76 221.59 0.58 o 6 5 0 88.06 92.38 0.46 o 7 5 0 188.12 185.28 0.72 o 8 5 0 13.71 12.96 0.44 o 9 5 0 2.18 2.18 1.71 o 0 6 0 3.07 3.33 0.11 o 1 6 0 1189.94 1183.21 2.01 o 2 6 0 251.61 307.11 0.56 o 3 6 0 1045.54 1134.87 1.47 o 4 6 0 109.23 109.59 0.32 o 5 6 0 263.50 261.53 0.61 o 6 6 0 60.84 53.96 0.39 o 7 6 0 102.71 104.35 0.55 o 8 6 0 31.97 33.28 0.52 o 9 6 0 17.15 20.98 2.86 o 1 7 0 447.23 495.60 0.69 o 2 7 0 838.82 765.21 0.94 o 3 7 0 9.64 13.12 0.41 o 4 7 0 32.87 31.12 0.29 o 5 7 0 314.89 311.45 0.89 o 6 7 0 158.38 154.04 0.70 o 7 7 0 1.58 1.21 0.34 o 8 7 0 40.33 38.28 0.55 o 0 8 0 5523.83 5444.91 23.04 o 1 8 0 872.13 976.89 1.12 o 2 8 0 665.42 693.73 0.78 o 3 8 0 44.04 47.86 0.23 o 4 8 0 3129.41 3085.87 7.71 o 5 8 0 47.85 45.47 0.34 o 6 8 0 63.73 60.00 0.43 o 7 8 0 2.74 3.94 0.37 o 8 8 0 151.23 159.04 1.14 o 1 9 0 1002.49 1049.63 1.22 o 2 9 0 1109.36 1121.04 1.31 o 3 9 0 709.05 735.31 1.01 o 4 9 0 165.09 166.72 0.66 o 5 9 0 289.35 292.95 1.06 o 6 9 0 391.27 394.19 1.38 o 7 9 0 188.83 196.40 1.07 o 8 9 0 9.23 10.71 0.49 o 0 10 0 503.39 564.46 0.98 o 1 10 0 1780.95 1850.83 2.48 o 2 10 0 5.95 7.43 0.14 o 3 10 0 425.48 397.47 0.84 o 4 10 0 208.52 215.51 0.65 o 5 10 0 148.24 161.46 0.53 o 6 10 0 5.55 7.52 0.34 o 7 10 0 116.36 114.41 0.66 o 8 10 0 10.85 10.83 0.46 o 1 11 0 536.34 566.27 0.89 o 2 11 0 207.60 197.78 0.38 o 3 11 0 88.66 98.24 0.35 o 4 11 0 70.00 70.78 0.35 o 5 11 0 281.86 265.39 0.83 o 6 11 0 17.96 14.53 0.35 o 7 11 0 0.23 1.81 0.38 o 8 11 0 23.94 24.98 0.52 o 0 12 0 0.16 0.37 0.19 o 1 12 0 543.47 546.77 0.73 o 2 12 0 1.18 0.96 0.14 o 3 12 0 47.57 39.55 0.26 o 4 12 0 37.77 27.37 0.29 o 5 12 0 1.69 1.94 0.30 o 6 12 0 32.30 32.72 0.41 o 7 12 0 97.72 102.14 0.65 o 8 12 0 5.03 5.55 1.23 o 1 13 0 281.82 285.44 0.67 o 2 13 0 29.58 24.05 0.22 o 3 13 0 142.45 162.95 0.49 o 4 13 0 44.34 49.01 0.36 o 5 13 0 190.44 188.74 0.73 o 6 13 0 11.66 9.79 0.34 o 7 13 0 94.20 100.83 0.76 o 8 13 0 69.97 70.68 2.78 o 0 14 0 1203.17 1167.15 3.21 o 1 14 0 207.54 213.38 0.60 o 2 14 0 2.28 1.73 0.17 o 3 14 0 55.71 57.11 0.37 o 4 14 0 498.22 489.13 1.52 o 5 14 0 20.36 21.16 0.35 o 6 14 0 3.05 3.14 0.36 o 7 14 0 26.40 24.69 0.50 o 1 15 0 187.73 191.98 0.56 o 2 15 0 1441.11 1405.08 2.83 o 3 15 0 75.62 67.02 0.40 o 4 15 0 10.87 9.45 0.30 o 5 15 0 53.58 56.79 0.43 o 6 15 0 225.26 226.55 1.29 o 7 15 0 2.24 2.12 0.44 o 0 16 0 777.36 760.58 2.54 o 1 16 0 369.90 357.57 0.77 o 2 16 0 1.88 6.83 0.32 o 3 16 0 10.70 8.02 0.26 o 4 16 0 233.91 231.12 0.83 o 5 16 0 0.95 2.42 0.32 o 6 16 0 47.23 43.59 0.53 o 7 16 0 20.35 21.99 0.96 o 1 17 0 298.74 305.22 0.90 o 2 17 0 249.63 229.86 0.63 o 3 17 0 158.04 158.13 0.64 o 4 17 0 0.20 0.90 0.30 o 5 17 0 116.05 114.38 0.68 o 6 17 0 15.13 13.64 0.44 o 7 17 0 8.39 9.38 2.60 o 0 18 0 51.93 52.80 0.47 o 1 18 0 104.96 108.53 0.48 o 2 18 0 15.96 17.23 0.28 o 3 18 0 210.07 203.24 0.71 o 4 18 0 43.90 42.24 0.41 o 5 18 0 27.77 30.79 0.44 o 6 18 0 4.90 5.55 0.44 o 1 19 0 12.51 12.97 0.28 o 2 19 0 0.33 0.43 0.27 o 3 19 0 26.61 25.56 0.36 o 4 19 0 23.50 20.45 0.39 o 5 19 0 88.41 85.58 0.61 o 6 19 0 6.33 6.91 1.02 o 0 20 0 67.76 59.62 0.59 o 1 20 0 42.09 42.51 0.37 o 2 20 0 2.03 1.43 0.29 o 3 20 0 182.11 182.49 0.76 o 4 20 0 40.09 37.96 0.45 o 5 20 0 103.90 116.87 0.72 o 1 21 0 89.79 83.90 0.48 o 2 21 0 8.76 9.27 0.35 o 3 21 0 67.68 71.68 0.52 o 4 21 0 2.70 2.32 0.39 o 5 21 0 25.44 21.59 1.02 o 0 22 0 296.99 315.10 1.70 o 1 22 0 8.72 9.27 0.37 o 2 22 0 6.29 7.66 0.39 o 3 22 0 2.31 2.83 0.36 o 4 22 0 86.48 94.56 1.17 o 1 23 0 8.38 8.24 0.38 o 2 23 0 371.64 392.20 1.72 o 3 23 0 1.23 2.07 0.70 o 0 24 0 0.87 1.00 0.58 o 1 24 0 0.16 1.24 0.42 o 2 24 0 14.77 19.40 1.05 o 1 25 0 66.78 64.26 3.87 o -9 1 1 0.68 1.02 0.58 o -8 1 1 7.45 6.51 0.41 o -7 1 1 9.81 8.85 0.32 o -6 1 1 283.02 284.46 0.65 o -5 1 1 267.11 273.98 0.74 o -4 1 1 5.66 6.59 0.14 o -3 1 1 231.30 243.37 0.34 o -2 1 1 6151.46 6171.18 49.30 o -1 1 1 48.11 31.53 0.14 o 0 1 1 83.90 74.20 0.30 o 1 1 1 41.33 51.65 0.24 o 3 1 1 0.14 2.97 0.11 o 4 1 1 4.28 5.35 0.16 o 5 1 1 47.99 51.82 0.35 o 6 1 1 328.35 342.99 0.88 o 7 1 1 17.53 13.97 0.35 o 8 1 1 21.75 18.87 0.43 o 9 1 1 0.71 1.08 1.78 o -9 2 1 56.72 54.79 0.62 o -8 2 1 51.79 48.25 0.52 o -7 2 1 6.35 6.45 0.32 o -6 2 1 50.67 42.13 0.34 o -5 2 1 5.88 6.21 0.20 o -4 2 1 619.39 595.30 0.85 o -3 2 1 974.16 959.39 1.29 o -2 2 1 474.85 460.05 0.77 o -1 2 1 8.55 12.81 0.11 o 0 2 1 606.74 503.33 1.06 o 1 2 1 478.27 516.18 1.05 o 2 2 1 1192.98 1214.61 3.37 o 3 2 1 97.28 125.01 0.36 o 4 2 1 751.39 718.94 1.29 o 5 2 1 177.63 180.76 0.52 o 6 2 1 10.32 7.04 0.26 o 7 2 1 10.74 11.21 0.35 o 8 2 1 2.39 2.43 0.37 o 9 2 1 3.85 6.13 1.37 o -9 3 1 64.72 71.45 0.64 o -8 3 1 40.61 35.91 0.50 o -7 3 1 20.03 18.82 0.38 o -6 3 1 7.98 8.65 0.26 o -5 3 1 403.76 410.81 0.94 o -4 3 1 131.79 119.62 0.32 o -3 3 1 1392.83 1388.87 2.11 o -2 3 1 3.14 2.44 0.12 o -1 3 1 3920.79 3922.68 20.03 o 0 3 1 560.27 623.52 1.12 o 1 3 1 4009.66 3974.04 13.69 o 2 3 1 27.62 30.91 0.22 o 3 3 1 289.74 317.19 0.51 o 4 3 1 147.26 152.91 0.37 o 5 3 1 1281.33 1225.65 2.02 o 6 3 1 1.99 0.77 0.26 o 7 3 1 0.07 1.79 0.32 o 8 3 1 33.88 33.78 0.47 o 9 3 1 166.21 186.20 3.04 o -9 4 1 60.84 63.51 0.74 o -8 4 1 0.06 0.23 0.48 o -7 4 1 64.08 62.50 0.48 o -6 4 1 1117.16 1097.49 2.28 o -5 4 1 1484.74 1497.95 2.82 o -4 4 1 25.52 31.51 0.24 o -3 4 1 546.33 513.62 0.86 o 0 4 1 73.64 88.39 0.24 o 1 4 1 859.28 946.80 1.79 o 2 4 1 1473.81 1444.23 3.05 o 3 4 1 4638.33 4391.96 23.51 o 4 4 1 222.46 231.32 0.49 o 5 4 1 25.83 30.71 0.61 o 6 4 1 46.82 53.66 0.50 o 7 4 1 640.01 636.16 1.94 o 8 4 1 6.17 7.80 0.41 o 9 4 1 0.31 3.25 2.70 o -9 5 1 4.48 6.02 0.51 o -8 5 1 80.77 79.57 0.66 o -7 5 1 218.83 228.45 1.01 o -6 5 1 179.07 182.01 0.55 o -5 5 1 289.32 298.88 0.72 o -4 5 1 449.42 450.08 0.79 o -3 5 1 1040.66 1024.03 2.03 o -2 5 1 666.81 671.11 1.01 o -1 5 1 0.59 2.89 0.11 o 0 5 1 2307.65 2416.43 6.54 o 2 5 1 606.36 628.81 1.10 o 3 5 1 0.08 1.43 0.12 o 4 5 1 645.10 648.75 1.26 o 5 5 1 1347.55 1341.79 3.14 o 6 5 1 167.59 166.58 0.65 o 7 5 1 0.25 2.56 0.34 o 8 5 1 19.38 20.22 0.46 o 9 5 1 83.77 88.17 7.09 o -9 6 1 3.79 3.80 1.44 o -8 6 1 122.81 128.34 0.77 o -7 6 1 55.60 54.10 0.46 o -6 6 1 19.24 16.67 0.29 o -5 6 1 43.90 48.43 0.36 o -4 6 1 337.13 330.25 0.73 o -3 6 1 172.37 159.10 0.36 o -2 6 1 391.52 412.10 0.68 o -1 6 1 681.08 698.07 0.95 o 0 6 1 4295.70 4448.77 12.90 o 1 6 1 2554.52 2590.42 6.94 o 2 6 1 13.83 17.89 0.16 o 3 6 1 6.98 11.94 0.22 o 4 6 1 144.87 146.31 0.45 o 5 6 1 171.15 167.52 0.52 o 6 6 1 244.42 241.25 0.94 o 7 6 1 10.01 8.51 0.37 o 8 6 1 71.39 70.21 0.59 o 9 6 1 69.53 81.26 2.86 o -9 7 1 3.60 4.05 2.04 o -8 7 1 15.58 15.12 0.46 o -7 7 1 0.11 1.11 0.38 o -6 7 1 82.58 75.59 0.44 o -5 7 1 112.58 113.15 0.39 o -4 7 1 0.01 1.24 0.14 o -3 7 1 18.37 12.45 0.15 o -2 7 1 1384.68 1403.20 2.71 o -1 7 1 743.25 756.31 1.05 o 0 7 1 151.33 143.64 0.38 o 1 7 1 324.66 334.41 0.59 o 2 7 1 451.76 416.90 0.95 o 3 7 1 208.52 207.03 0.56 o 4 7 1 0.62 1.11 0.18 o 5 7 1 207.67 197.11 0.53 o 6 7 1 25.45 22.08 0.34 o 7 7 1 55.15 55.56 0.49 o 8 7 1 3.52 3.27 0.41 o -8 8 1 2.99 2.48 0.44 o -7 8 1 119.82 128.88 0.83 o -6 8 1 104.28 98.82 0.49 o -5 8 1 17.19 15.88 0.24 o -4 8 1 0.04 1.09 0.17 o -3 8 1 670.41 724.86 0.99 o -2 8 1 310.86 338.78 0.65 o -1 8 1 52.02 62.02 0.18 o 0 8 1 0.92 5.20 0.11 o 1 8 1 123.54 121.68 0.25 o 2 8 1 3.16 2.94 0.11 o 3 8 1 176.90 194.80 0.52 o 4 8 1 9.25 8.01 0.20 o 5 8 1 105.42 107.17 0.50 o 6 8 1 11.05 12.90 0.34 o 7 8 1 5.03 5.64 0.37 o 8 8 1 0.53 1.71 0.43 o -8 9 1 0.22 1.22 0.48 o -7 9 1 45.52 43.14 0.47 o -6 9 1 228.10 230.93 0.85 o -5 9 1 21.33 26.12 0.27 o -4 9 1 0.44 0.85 0.20 o -3 9 1 23.96 20.43 0.19 o -2 9 1 1635.33 1673.86 2.66 o -1 9 1 205.34 184.49 0.33 o 0 9 1 113.20 118.88 0.35 o 1 9 1 269.05 315.04 0.57 o 2 9 1 2150.96 2227.75 3.24 o 3 9 1 17.72 18.64 0.18 o 4 9 1 189.87 192.50 0.66 o 5 9 1 52.03 49.22 0.35 o 6 9 1 569.64 579.97 2.05 o 7 9 1 3.31 3.02 0.38 o 8 9 1 16.65 15.86 0.49 o -8 10 1 46.29 46.59 0.57 o -7 10 1 8.59 9.25 0.39 o -6 10 1 31.93 31.14 0.38 o -5 10 1 411.76 414.57 1.11 o -4 10 1 6.46 9.60 0.21 o -3 10 1 20.59 22.59 0.21 o -2 10 1 545.02 550.34 0.76 o -1 10 1 231.15 218.68 0.39 o 0 10 1 183.94 172.87 0.37 o 1 10 1 87.51 96.01 0.27 o 2 10 1 55.40 48.46 0.24 o 3 10 1 454.43 439.79 0.73 o 4 10 1 5.66 7.25 0.23 o 5 10 1 55.62 55.42 0.40 o 6 10 1 55.41 51.79 0.45 o 7 10 1 1.61 2.52 0.40 o 8 10 1 36.84 36.24 0.56 o -8 11 1 2.89 4.56 0.47 o -7 11 1 28.70 26.20 0.44 o -6 11 1 96.82 94.94 0.52 o -5 11 1 366.34 354.73 1.08 o -4 11 1 213.14 214.59 0.76 o -3 11 1 700.59 676.18 0.95 o -2 11 1 180.62 185.23 0.43 o -1 11 1 1446.35 1430.03 2.09 o 0 11 1 23.94 17.08 0.19 o 1 11 1 1459.75 1430.43 2.34 o 2 11 1 454.41 464.73 0.83 o 3 11 1 514.27 487.39 1.04 o 4 11 1 15.73 14.16 0.25 o 5 11 1 441.51 428.66 1.68 o 6 11 1 84.81 81.51 0.51 o 7 11 1 0.31 2.27 0.42 o 8 11 1 15.91 13.06 1.10 o -8 12 1 2.99 3.78 0.60 o -7 12 1 128.58 128.37 0.68 o -6 12 1 90.64 92.42 0.61 o -5 12 1 258.96 254.00 0.95 o -4 12 1 82.85 72.31 0.39 o -3 12 1 715.70 711.00 1.27 o -2 12 1 321.31 328.06 0.67 o -1 12 1 1077.35 1068.55 1.45 o 0 12 1 428.57 401.23 0.68 o 1 12 1 336.10 328.97 0.61 o 2 12 1 279.02 260.13 0.49 o 3 12 1 1521.21 1503.73 2.42 o 4 12 1 67.79 58.05 0.35 o 5 12 1 102.00 98.69 0.50 o 6 12 1 11.77 10.27 0.34 o 7 12 1 205.83 212.33 1.06 o 8 12 1 0.63 0.03 3.08 o -8 13 1 44.10 47.46 1.30 o -7 13 1 70.55 70.00 0.58 o -6 13 1 100.68 106.84 0.57 o -5 13 1 1.58 2.63 0.29 o -4 13 1 172.66 168.99 0.63 o -3 13 1 520.25 497.24 1.12 o -2 13 1 173.64 180.83 0.52 o -1 13 1 0.01 2.13 0.15 o 0 13 1 457.59 464.37 0.78 o 1 13 1 535.15 524.97 0.87 o 2 13 1 193.79 206.00 0.53 o 3 13 1 13.77 15.91 0.23 o 4 13 1 151.58 138.11 0.51 o 5 13 1 166.59 168.56 0.75 o 6 13 1 38.66 44.10 0.44 o 7 13 1 5.87 6.79 0.45 o -7 14 1 0.19 1.40 0.45 o -6 14 1 2.48 1.84 0.35 o -5 14 1 1.04 0.82 0.30 o -4 14 1 582.54 567.22 1.63 o -3 14 1 158.81 179.15 0.52 o -2 14 1 22.34 20.27 0.38 o -1 14 1 136.94 128.96 0.40 o 0 14 1 720.36 730.60 1.21 o 1 14 1 2.21 3.06 0.17 o 2 14 1 179.89 172.06 0.44 o 3 14 1 36.75 35.78 0.32 o 4 14 1 423.68 423.64 1.21 o 5 14 1 198.64 206.20 0.83 o 6 14 1 102.27 95.40 0.57 o 7 14 1 18.87 19.64 0.50 o -7 15 1 13.37 12.46 0.46 o -6 15 1 29.43 27.29 0.44 o -5 15 1 6.61 5.45 0.31 o -4 15 1 55.55 46.43 0.38 o -3 15 1 2.30 1.36 0.23 o -2 15 1 28.24 24.82 0.25 o -1 15 1 144.32 149.16 0.40 o 0 15 1 39.31 43.41 0.27 o 1 15 1 69.30 73.88 0.31 o 2 15 1 16.68 11.33 0.22 o 3 15 1 141.58 128.10 0.46 o 4 15 1 63.08 53.59 0.40 o 5 15 1 30.88 27.35 0.38 o 6 15 1 7.07 8.37 0.39 o 7 15 1 6.00 5.79 0.64 o -7 16 1 67.81 74.14 1.37 o -6 16 1 24.37 25.47 0.46 o -5 16 1 1.72 2.09 0.32 o -4 16 1 53.50 53.29 0.40 o -3 16 1 262.82 266.31 0.83 o -2 16 1 43.09 48.45 0.31 o -1 16 1 118.95 121.33 0.38 o 0 16 1 199.62 197.72 0.59 o 1 16 1 432.24 428.58 1.04 o 2 16 1 0.01 0.74 0.24 o 3 16 1 22.91 22.50 0.30 o 4 16 1 97.67 102.29 0.50 o 5 16 1 36.55 35.61 0.41 o 6 16 1 0.27 1.68 0.41 o 7 16 1 5.87 5.47 1.94 o -7 17 1 2.02 1.77 1.55 o -6 17 1 92.02 93.95 0.62 o -5 17 1 61.57 60.60 0.52 o -4 17 1 0.54 1.21 0.30 o -3 17 1 0.18 0.80 0.28 o -2 17 1 275.16 274.94 0.81 o -1 17 1 227.77 226.85 0.58 o 0 17 1 43.70 40.84 0.29 o 1 17 1 1.58 4.73 0.23 o 2 17 1 497.57 513.86 1.11 o 3 17 1 107.62 104.96 0.50 o 4 17 1 31.66 24.46 0.37 o 5 17 1 20.30 19.99 0.41 o 6 17 1 163.70 170.95 1.05 o -6 18 1 139.05 151.26 1.03 o 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