#------------------------------------------------------------------------------ #$Date: 2009-05-05 17:46:52 +0300 (Tue, 05 May 2009) $ #$Revision: 697 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2217979.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2217979_Fobs loop_ _publ_author_name 'Li, Jun-Hua' 'Nie, Jing-Jing' 'Su, Jian-Rong' 'Xu, Duan-Jun' _publ_section_title ; cyclo-Tetra-\m-malato-\k^16^O,O',O'':O'''-tetrakis[bis(1H-benzimidazole-\kN^3^)cobalt(II)] eicosahydrate ; _journal_coeditor_code NG2434 _journal_issue 4 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m538 _journal_page_last m539 _journal_volume 64 _journal_year 2008 _space_group_IT_number 85 _symmetry_space_group_name_Hall '-P 4a' _symmetry_space_group_name_H-M 'P 4/n :2' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 20.2303 _cell_length_b 20.2303 _cell_length_c 11.6203 _exptl_crystal_F_000 2152.00 _reflns_d_resolution_high 0.8409 _[local]_cod_data_source_file ng2434Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' su-24 in' _shelx_refln_list_code 4 _shelx_F_calc_maximum 505.29 _shelx_F_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y+1/2, z' '-y+1/2, x, z' 'y, -x+1/2, z' '-x, -y, -z' 'x-1/2, y-1/2, -z' 'y-1/2, -x, -z' '-y, x-1/2, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 1 0 36346.79 30800.82 8.24 o 0 2 0 76.01 475.05 242.84 o 2 2 0 46705.39 48152.54 194.19 o -1 3 0 1658.74 2967.33 99.42 o 1 3 0 22412.84 21306.04 118.32 o 3 3 0 107609.25 123476.43 1073.24 o -2 4 0 45290.68 44540.11 293.00 o 0 4 0 22738.13 21572.09 1601.36 o 2 4 0 19971.82 22535.14 313.12 o 4 4 0 1038.85 1059.21 19.62 o -3 5 0 3824.09 4053.84 78.18 o -1 5 0 16572.85 12651.82 914.85 o 1 5 0 8690.46 9104.80 152.08 o 3 5 0 2881.27 3737.76 68.88 o 5 5 0 39710.47 41274.15 772.21 o -4 6 0 47085.19 51864.56 753.69 o -2 6 0 8828.75 9055.54 124.80 o 0 6 0 3166.28 2512.16 68.02 o 2 6 0 520.20 651.82 16.75 o 4 6 0 8467.12 9025.68 307.77 o 6 6 0 262.53 340.54 9.09 o -5 7 0 51284.15 52270.66 893.19 o -3 7 0 8475.18 9660.23 145.89 o -1 7 0 5445.81 5419.65 205.36 o 1 7 0 8206.64 8558.37 193.67 o 3 7 0 822.92 733.13 26.40 o 5 7 0 27467.71 29000.03 347.88 o 7 7 0 410.33 506.18 10.26 o -6 8 0 8542.66 9056.74 90.68 o -4 8 0 9378.21 8784.43 115.14 o -2 8 0 904.79 1045.78 219.61 o 0 8 0 7404.57 7681.72 214.98 o 2 8 0 6.17 5.68 6.73 o 4 8 0 13077.82 14415.83 361.20 o 6 8 0 589.47 914.10 12.08 o 8 8 0 202.14 183.88 19.95 o -7 9 0 25157.65 24404.70 450.61 o -5 9 0 230.88 338.86 12.54 o -3 9 0 354.35 594.93 20.86 o -1 9 0 77.21 56.61 18.07 o 1 9 0 622.56 635.07 36.35 o 3 9 0 2969.48 2479.58 50.02 o 5 9 0 167.04 220.43 16.03 o 7 9 0 8817.95 7802.57 188.53 o 9 9 0 204.09 250.66 11.79 o -8 10 0 2517.02 2456.98 44.64 o -6 10 0 8738.23 9572.52 190.96 o -4 10 0 531.74 403.93 10.27 o -2 10 0 1579.51 2062.45 154.09 o 0 10 0 2168.15 2950.38 242.57 o 2 10 0 15513.80 16082.88 544.24 o 4 10 0 4391.91 4669.18 58.23 o 6 10 0 1929.23 1934.87 59.32 o 8 10 0 1696.71 1890.41 46.09 o 10 10 0 1.63 6.32 23.42 o -9 11 0 5079.75 4629.23 159.07 o -7 11 0 3440.58 3053.35 78.55 o -5 11 0 200.33 120.37 19.09 o -3 11 0 8057.04 8460.73 415.56 o -1 11 0 92.37 314.03 27.88 o 1 11 0 3009.19 2372.54 194.67 o 3 11 0 10711.44 10100.20 248.57 o 5 11 0 191.29 224.19 21.08 o 7 11 0 3073.67 3145.36 106.10 o 9 11 0 1248.63 1418.54 60.01 o 11 11 0 4400.80 4293.90 110.25 o -10 12 0 221.02 191.33 19.98 o -8 12 0 4845.38 4690.26 128.72 o -6 12 0 259.97 424.99 21.61 o -4 12 0 85.50 66.99 7.05 o -2 12 0 705.85 792.65 55.09 o 0 12 0 2257.81 2108.37 243.21 o 2 12 0 174.97 205.77 12.07 o 4 12 0 194.26 137.94 13.62 o 6 12 0 215.37 204.63 16.52 o 8 12 0 65.53 79.86 11.84 o 10 12 0 3035.73 3057.25 65.58 o 12 12 0 8.51 13.44 14.46 o -11 13 0 78.26 116.05 17.99 o -9 13 0 1934.77 1823.35 57.35 o -7 13 0 21.16 15.62 12.92 o -5 13 0 1447.85 1453.48 16.39 o -3 13 0 53.62 122.54 24.19 o -1 13 0 5107.18 5489.43 277.68 o 1 13 0 6293.47 6875.38 207.53 o 3 13 0 942.26 1110.36 25.39 o 5 13 0 2445.77 2340.49 52.78 o 7 13 0 76.79 123.62 17.65 o 9 13 0 83.25 117.81 22.24 o 11 13 0 7.68 39.65 16.60 o 13 13 0 1781.34 1725.83 19.46 o -12 14 0 503.53 551.55 47.58 o -10 14 0 525.80 514.65 25.25 o -8 14 0 962.32 914.65 43.53 o -6 14 0 413.24 341.65 8.87 o -4 14 0 1074.79 915.25 73.39 o -2 14 0 94.97 78.63 27.77 o 0 14 0 14054.93 13590.84 791.21 o 2 14 0 697.55 803.39 40.86 o 4 14 0 431.36 312.96 11.64 o 6 14 0 128.74 128.09 13.95 o 8 14 0 560.76 540.95 18.90 o 10 14 0 329.51 273.04 19.90 o 12 14 0 837.26 728.40 17.30 o 14 14 0 4491.65 4095.02 85.72 o -13 15 0 108.77 94.62 17.50 o -11 15 0 4589.56 4411.54 164.20 o -9 15 0 193.17 249.10 16.29 o -7 15 0 1010.62 771.75 43.34 o -5 15 0 351.69 506.18 48.92 o -3 15 0 725.61 683.25 142.12 o -1 15 0 113.35 69.64 29.43 o 1 15 0 4.14 0.00 37.28 o 3 15 0 6394.83 6234.78 265.64 o 5 15 0 72.74 94.11 22.25 o 7 15 0 1086.96 1137.36 48.53 o 9 15 0 651.07 697.84 20.36 o 11 15 0 1.74 17.41 14.68 o 13 15 0 2901.12 2864.64 106.53 o 15 15 0 179.63 178.26 18.07 o -14 16 0 84.13 70.98 18.15 o -12 16 0 1821.52 1628.61 45.69 o -10 16 0 2471.55 2394.86 89.02 o -8 16 0 1398.59 1433.60 48.34 o -6 16 0 107.57 151.93 70.65 o -4 16 0 0.09 0.00 31.79 o -2 16 0 2089.05 1848.72 241.46 o 0 16 0 100.78 104.08 30.80 o 2 16 0 2878.76 2691.71 223.67 o 4 16 0 1029.84 928.07 25.54 o 6 16 0 641.87 634.81 19.71 o 8 16 0 76.35 85.33 16.77 o 10 16 0 80.98 130.84 27.10 o 12 16 0 326.70 335.28 17.60 o 14 16 0 90.41 127.66 21.90 o 16 16 0 1597.97 1461.55 81.07 o -15 17 0 186.83 186.05 28.71 o -13 17 0 104.49 106.77 39.45 o -11 17 0 833.65 624.41 20.23 o -9 17 0 410.34 391.21 57.14 o -7 17 0 1102.74 1135.25 63.05 o -5 17 0 8.24 40.79 69.72 o -3 17 0 1037.35 999.76 35.28 o -1 17 0 610.43 656.06 95.57 o 1 17 0 227.94 235.09 33.90 o 3 17 0 1218.53 1340.43 53.18 o 5 17 0 2021.13 1858.08 86.29 o 7 17 0 621.77 634.50 24.86 o 9 17 0 74.69 97.58 16.10 o 11 17 0 3165.80 2853.34 80.58 o 13 17 0 21.86 33.17 16.74 o 15 17 0 172.89 216.73 18.57 o 17 17 0 178.88 222.45 22.37 o -14 18 0 511.43 475.40 55.25 o -12 18 0 361.63 346.11 56.47 o -10 18 0 24.72 30.36 23.16 o -8 18 0 1165.59 1224.46 40.71 o -6 18 0 51.68 31.76 88.61 o -4 18 0 0.33 47.36 61.31 o -2 18 0 23.76 0.00 43.83 o 0 18 0 559.02 603.02 46.25 o 2 18 0 40.06 98.77 70.81 o 4 18 0 205.20 304.06 45.98 o 6 18 0 1644.27 1497.45 121.65 o 8 18 0 35.12 50.34 25.59 o 10 18 0 969.40 833.43 31.90 o 12 18 0 32.87 58.23 24.28 o 14 18 0 234.12 250.41 20.95 o -13 19 0 784.16 707.96 36.59 o -11 19 0 18.67 42.10 38.59 o -9 19 0 176.53 245.36 55.92 o -7 19 0 102.45 137.95 36.73 o -5 19 0 1571.91 1558.01 117.00 o -3 19 0 84.12 160.94 49.42 o -1 19 0 66.29 62.05 38.15 o 1 19 0 209.68 125.00 51.85 o 3 19 0 50.68 87.80 75.11 o 5 19 0 261.09 354.42 41.11 o 7 19 0 51.14 87.98 44.14 o 9 19 0 772.08 662.78 31.00 o 11 19 0 95.04 112.74 24.30 o 13 19 0 217.43 268.72 32.98 o -12 20 0 0.13 23.46 59.40 o -10 20 0 676.83 634.05 39.85 o -8 20 0 214.77 232.39 60.07 o -6 20 0 584.10 725.90 110.13 o -4 20 0 2645.04 2613.57 170.26 o -2 20 0 264.24 357.10 72.77 o 0 20 0 24.06 166.79 86.44 o 2 20 0 86.15 156.27 53.17 o 4 20 0 445.34 454.24 53.15 o 6 20 0 0.46 5.58 24.81 o 8 20 0 2133.54 1837.67 134.10 o 10 20 0 311.37 273.57 19.06 o 12 20 0 78.85 53.71 19.81 o -11 21 0 55.89 115.94 39.75 o -9 21 0 438.90 547.01 107.81 o -7 21 0 3.43 5.38 61.28 o -5 21 0 503.20 600.87 61.26 o -3 21 0 14.42 0.00 74.58 o -1 21 0 453.48 497.29 40.34 o 1 21 0 5.10 66.71 38.27 o 3 21 0 109.46 311.34 60.40 o 5 21 0 226.14 216.13 48.54 o 7 21 0 258.49 319.38 76.86 o 9 21 0 807.56 732.39 38.40 o 11 21 0 206.31 183.75 34.47 o -8 22 0 161.81 174.87 43.07 o -6 22 0 460.76 443.66 68.82 o -4 22 0 75.96 149.26 64.92 o -2 22 0 579.98 601.39 54.42 o 0 22 0 6.52 64.06 51.95 o 2 22 0 0.08 0.00 50.54 o 4 22 0 0.22 20.92 119.46 o 6 22 0 46.02 23.93 44.67 o 8 22 0 4.41 45.58 52.13 o -7 23 0 750.89 803.15 83.88 o -5 23 0 173.69 273.27 50.26 o -3 23 0 0.53 189.22 69.24 o -1 23 0 217.73 287.67 69.35 o 1 23 0 179.03 134.65 70.23 o 5 23 0 152.10 79.52 68.48 o 7 23 0 373.85 323.61 65.34 o 0 24 0 37.12 0.00 75.17 o 0 0 1 255319.31 219793.80 6.36 o 0 1 1 436.33 6.01 4.27 o 1 1 1 9998.66 6766.84 1029.10 o -1 2 1 6919.68 4926.31 62.49 o 0 2 1 1960.32 2619.34 32.51 o 1 2 1 10377.40 9050.74 170.96 o 2 2 1 9014.80 9590.54 47.38 o -2 3 1 3373.98 4746.57 51.86 o -1 3 1 30961.23 30810.14 295.90 o 0 3 1 1304.19 1937.34 93.02 o 1 3 1 7622.88 7404.05 78.26 o 2 3 1 565.66 1720.33 177.45 o 3 3 1 64046.45 67409.33 369.01 o -3 4 1 1678.52 1112.04 9.17 o -2 4 1 40424.42 48321.09 446.58 o -1 4 1 4227.45 5039.81 166.78 o 0 4 1 20553.80 20129.59 193.30 o 1 4 1 1656.44 1581.82 32.56 o 2 4 1 6698.53 7549.06 74.54 o 3 4 1 570.35 957.62 201.71 o 4 4 1 9767.14 9940.33 68.61 o -4 5 1 3280.44 2998.06 27.40 o -3 5 1 1080.65 1514.28 18.44 o -2 5 1 4463.38 4703.02 48.66 o -1 5 1 2844.49 2141.19 38.81 o 0 5 1 653.77 501.50 54.77 o 1 5 1 3322.22 3702.15 111.42 o 2 5 1 8177.21 8687.05 80.78 o 3 5 1 4654.55 4489.65 31.82 o 4 5 1 238.40 268.81 15.23 o 5 5 1 16600.33 16315.81 388.92 o -5 6 1 297.74 199.84 9.23 o -4 6 1 34980.43 38095.97 312.17 o -3 6 1 531.50 388.85 30.62 o -2 6 1 9051.16 9231.53 136.54 o -1 6 1 1591.08 2325.02 47.06 o 0 6 1 19712.75 17899.44 262.25 o 1 6 1 153.47 267.13 11.18 o 2 6 1 628.16 968.48 17.92 o 3 6 1 883.82 934.86 8.64 o 4 6 1 5782.04 6146.33 67.65 o 5 6 1 225.85 296.21 13.46 o 6 6 1 29.92 14.63 7.37 o -6 7 1 1093.37 1062.96 16.26 o -5 7 1 27229.50 29902.13 298.90 o -4 7 1 1990.66 1911.11 32.94 o -3 7 1 3149.38 3015.69 33.73 o -2 7 1 253.21 182.31 6.43 o -1 7 1 994.19 1142.81 27.91 o 0 7 1 3296.42 2762.29 48.65 o 1 7 1 1.95 27.03 9.64 o 2 7 1 1138.18 1311.26 23.58 o 3 7 1 1869.67 1793.19 25.93 o 4 7 1 120.25 143.72 8.42 o 5 7 1 16726.83 16075.70 204.96 o 6 7 1 6548.35 6111.44 78.44 o 7 7 1 1382.90 1287.92 11.01 o -7 8 1 29.50 56.85 11.32 o -6 8 1 8728.67 9231.40 82.90 o -5 8 1 1009.81 1073.67 14.97 o -4 8 1 6409.47 6666.54 66.98 o -3 8 1 10178.52 11465.20 175.35 o -2 8 1 90.47 107.14 8.90 o -1 8 1 38.35 68.01 5.27 o 0 8 1 1154.99 1407.28 43.42 o 1 8 1 187.97 261.99 11.20 o 2 8 1 60.27 49.42 10.71 o 3 8 1 462.39 449.04 6.67 o 4 8 1 3756.16 3714.49 60.39 o 5 8 1 359.04 417.78 16.28 o 6 8 1 38.60 41.68 7.80 o 7 8 1 1869.85 2054.96 45.21 o 8 8 1 112.61 95.67 10.69 o -8 9 1 173.02 227.61 11.94 o -7 9 1 21159.12 21717.54 203.35 o -6 9 1 0.83 5.38 10.81 o -5 9 1 1215.29 1577.84 14.17 o -4 9 1 5576.15 5058.63 44.43 o -3 9 1 32.43 65.51 5.93 o -2 9 1 386.07 270.42 13.96 o -1 9 1 3303.08 2155.60 251.12 o 0 9 1 476.06 483.99 18.70 o 1 9 1 290.12 235.63 8.89 o 2 9 1 314.21 386.13 12.31 o 3 9 1 16.53 41.13 8.78 o 4 9 1 3413.73 3043.35 37.38 o 5 9 1 818.32 921.08 20.03 o 6 9 1 1393.31 1385.59 15.94 o 7 9 1 13867.51 13400.63 152.84 o 8 9 1 16.18 6.50 7.99 o 9 9 1 570.66 593.77 8.88 o -9 10 1 281.49 234.42 9.63 o -8 10 1 3223.30 3041.12 35.71 o -7 10 1 14.67 13.44 9.67 o -6 10 1 10320.08 9399.02 149.29 o -5 10 1 630.02 539.50 11.65 o -4 10 1 2543.17 2676.93 39.13 o -3 10 1 494.00 489.13 9.07 o -2 10 1 105.35 154.77 11.69 o -1 10 1 2159.55 2326.46 47.14 o 0 10 1 118.19 177.71 29.79 o 1 10 1 891.60 1150.53 29.86 o 2 10 1 5528.15 5431.38 79.88 o 3 10 1 1590.63 1774.82 25.01 o 4 10 1 3084.32 3221.80 37.24 o 5 10 1 296.28 230.63 9.36 o 6 10 1 1819.55 1784.04 20.21 o 7 10 1 0.14 28.62 11.40 o 8 10 1 4560.62 4569.37 48.41 o 9 10 1 57.30 80.14 13.12 o 10 10 1 13.33 7.65 9.26 o -10 11 1 888.73 911.81 15.19 o -9 11 1 3061.35 2962.23 41.81 o -8 11 1 399.42 412.61 10.29 o -7 11 1 1754.41 1879.06 36.59 o -6 11 1 1406.42 1417.55 21.01 o -5 11 1 399.51 296.62 9.54 o -4 11 1 40.27 50.51 15.64 o -3 11 1 11969.60 11868.37 235.74 o -2 11 1 5176.22 5181.99 92.38 o -1 11 1 665.78 477.70 14.09 o 0 11 1 601.43 509.10 12.33 o 1 11 1 1224.11 1138.86 21.28 o 2 11 1 2072.90 1961.26 22.32 o 3 11 1 3934.40 3565.69 42.05 o 4 11 1 58.71 70.45 8.56 o 5 11 1 2110.39 2330.37 33.93 o 6 11 1 55.29 105.91 7.95 o 7 11 1 2801.70 2573.53 23.00 o 8 11 1 315.03 291.30 14.17 o 9 11 1 1447.83 1437.78 38.11 o 10 11 1 193.16 199.98 10.23 o 11 11 1 1912.92 1878.78 41.25 o -11 12 1 91.30 97.60 10.07 o -10 12 1 103.57 162.94 14.50 o -9 12 1 116.89 167.71 17.61 o -8 12 1 3860.39 3860.66 73.08 o -7 12 1 932.62 798.95 14.23 o -6 12 1 35.92 85.74 13.02 o -5 12 1 2.04 17.79 10.02 o -4 12 1 1462.62 1442.95 23.53 o -3 12 1 5.43 12.05 19.78 o -2 12 1 1223.03 1163.54 28.70 o -1 12 1 285.09 314.44 23.27 o 0 12 1 560.54 551.80 46.35 o 1 12 1 246.63 244.66 13.85 o 2 12 1 2095.65 1970.52 40.89 o 3 12 1 1183.95 1252.69 17.87 o 4 12 1 1925.93 1724.41 27.88 o 5 12 1 45.93 47.25 7.10 o 6 12 1 645.37 520.42 9.25 o 7 12 1 12.39 27.87 13.72 o 8 12 1 257.24 259.94 8.90 o 9 12 1 330.12 379.79 13.82 o 10 12 1 2465.31 2382.73 48.19 o 11 12 1 105.04 109.16 10.92 o 12 12 1 8.77 31.72 13.52 o -12 13 1 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13.59 13.60 24.96 o 2 17 2 0.19 7.79 8.55 o 3 17 2 615.62 558.33 64.58 o 4 17 2 452.42 408.49 20.84 o 5 17 2 818.81 798.72 32.12 o 6 17 2 71.86 68.16 12.61 o 7 17 2 45.95 50.95 12.37 o 8 17 2 1077.28 1056.98 27.09 o 9 17 2 1.80 27.09 10.85 o 10 17 2 178.07 200.72 22.34 o 11 17 2 467.02 419.22 28.22 o 12 17 2 150.27 148.86 14.39 o 13 17 2 78.07 117.33 13.86 o 14 17 2 159.27 208.67 18.91 o 15 17 2 0.07 0.40 15.91 o 16 17 2 1.14 31.21 17.92 o -15 18 2 102.66 109.17 15.96 o -14 18 2 136.28 160.08 15.97 o -13 18 2 14.82 21.20 13.21 o -12 18 2 265.59 249.06 12.32 o -11 18 2 371.43 350.48 22.43 o -10 18 2 83.05 53.81 13.31 o -9 18 2 388.85 329.79 16.94 o -8 18 2 432.31 413.37 36.86 o -7 18 2 46.03 61.65 23.67 o -6 18 2 29.01 56.15 41.02 o -5 18 2 236.00 272.19 33.88 o -4 18 2 99.68 108.01 35.81 o -3 18 2 0.33 0.00 28.75 o -2 18 2 71.96 123.94 30.80 o -1 18 2 81.37 54.72 26.64 o 0 18 2 693.97 558.74 30.52 o 1 18 2 674.51 753.11 26.73 o 2 18 2 97.25 166.05 26.13 o 3 18 2 919.60 685.05 60.50 o 4 18 2 149.13 104.00 17.68 o 5 18 2 249.81 236.12 32.79 o 6 18 2 1233.94 1167.18 47.73 o 7 18 2 13.09 24.17 10.67 o 8 18 2 55.65 82.34 14.83 o 9 18 2 126.87 162.02 20.15 o 10 18 2 160.07 143.01 27.80 o 11 18 2 16.06 25.92 12.93 o 12 18 2 29.98 70.92 12.48 o 13 18 2 76.38 96.83 14.87 o 14 18 2 82.22 117.83 13.50 o 15 18 2 0.46 73.06 14.99 o -14 19 2 34.90 86.34 37.11 o -13 19 2 414.84 359.77 27.16 o -12 19 2 6.66 40.19 19.24 o -11 19 2 2.64 21.28 13.14 o -10 19 2 271.10 224.17 14.80 o -9 19 2 8.09 25.18 20.29 o -8 19 2 0.03 40.31 51.43 o -7 19 2 105.48 235.40 35.87 o -6 19 2 1.71 31.42 31.45 o -5 19 2 661.36 635.51 33.70 o -4 19 2 33.28 27.30 26.89 o -3 19 2 196.62 102.73 31.70 o -2 19 2 929.98 883.14 31.06 o -1 19 2 247.75 297.47 27.02 o 0 19 2 0.09 60.54 26.21 o 1 19 2 313.76 355.49 49.81 o 2 19 2 51.24 6.66 35.73 o 3 19 2 1.61 92.85 30.53 o 4 19 2 1282.42 825.57 208.26 o 5 19 2 216.68 202.86 30.48 o 6 19 2 87.16 72.78 12.13 o 7 19 2 116.52 132.54 19.17 o 8 19 2 46.70 65.03 12.97 o 9 19 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21 2 8.17 2.56 33.84 o -6 21 2 71.20 69.38 33.97 o -5 21 2 286.68 387.80 34.12 o -4 21 2 261.59 232.99 49.71 o -3 21 2 7.27 41.01 38.71 o -2 21 2 21.51 0.00 39.22 o -1 21 2 306.55 365.94 40.40 o 0 21 2 108.21 112.71 28.83 o 1 21 2 11.75 0.00 28.79 o 2 21 2 189.19 164.30 68.00 o 3 21 2 115.62 141.93 34.72 o 4 21 2 3.72 109.92 68.75 o 5 21 2 396.88 455.18 147.79 o 6 21 2 149.96 65.11 50.66 o 7 21 2 30.44 27.58 48.24 o 8 21 2 69.34 108.61 49.38 o 9 21 2 336.31 318.65 36.55 o 10 21 2 125.98 144.38 19.64 o 11 21 2 6.61 41.60 20.13 o -9 22 2 1.91 0.00 49.47 o -8 22 2 73.00 131.87 40.16 o -7 22 2 36.20 89.18 48.72 o -6 22 2 156.43 186.23 44.84 o -5 22 2 191.11 260.22 50.69 o -4 22 2 22.83 0.00 54.13 o -3 22 2 214.03 218.92 34.97 o -2 22 2 368.75 370.72 42.78 o -1 22 2 80.34 27.07 47.39 o 0 22 2 2.67 27.69 60.07 o 1 22 2 459.26 495.52 37.25 o 2 22 2 2.24 48.48 59.88 o 3 22 2 19.72 63.63 39.03 o 4 22 2 79.50 180.88 64.93 o 5 22 2 3.84 0.00 34.01 o 6 22 2 75.99 125.23 41.86 o 7 22 2 110.47 149.65 34.82 o 8 22 2 68.43 139.93 34.74 o 9 22 2 253.20 338.38 83.81 o -6 23 2 19.89 76.40 51.10 o -5 23 2 4.08 0.00 127.27 o -4 23 2 203.86 324.43 44.76 o -3 23 2 3.67 22.90 37.79 o -2 23 2 49.45 108.47 38.35 o -1 23 2 77.64 288.63 54.19 o 0 23 2 8.49 0.00 37.79 o 1 23 2 243.92 328.31 37.92 o 2 23 2 8.21 96.75 74.79 o 3 23 2 11.70 76.04 84.54 o 4 23 2 124.14 136.81 37.83 o 5 23 2 139.46 152.18 39.19 o 6 23 2 0.40 0.00 38.93 o 0 0 3 2654.53 2938.63 33.65 o 0 1 3 1053.86 1347.52 21.29 o 1 1 3 521.87 726.57 15.90 o -1 2 3 1359.37 1260.33 28.59 o 0 2 3 904.00 1008.76 19.31 o 1 2 3 5501.69 6066.80 120.68 o 2 2 3 1654.05 1379.32 18.25 o -2 3 3 3861.88 4795.69 65.43 o -1 3 3 6.62 28.74 13.86 o 0 3 3 4340.06 4136.76 74.65 o 1 3 3 5561.66 5369.19 85.03 o 2 3 3 6216.13 6802.79 150.48 o 3 3 3 13239.00 13204.35 191.07 o -3 4 3 3720.43 3144.04 44.21 o -2 4 3 1.96 143.17 28.95 o -1 4 3 465.81 517.69 24.39 o 0 4 3 3354.92 3555.09 61.59 o 1 4 3 2686.73 2643.45 46.08 o 2 4 3 231.54 359.89 13.52 o 3 4 3 1998.47 2160.24 27.32 o 4 4 3 1582.30 1374.72 40.72 o -4 5 3 284.80 405.86 19.88 o -3 5 3 4446.31 3624.62 36.28 o -2 5 3 11347.49 11197.37 117.54 o -1 5 3 3157.82 3160.21 23.12 o 0 5 3 5698.35 5967.92 101.81 o 1 5 3 943.53 873.25 19.83 o 2 5 3 2213.32 2045.75 19.46 o 3 5 3 287.88 402.99 14.82 o 4 5 3 11492.60 12934.83 107.58 o 5 5 3 195.40 347.87 13.99 o -5 6 3 2517.79 2713.84 35.31 o -4 6 3 47.93 58.03 8.95 o -3 6 3 3252.13 2513.71 28.86 o -2 6 3 1239.83 1442.60 21.98 o -1 6 3 5965.91 5039.20 66.74 o 0 6 3 2219.06 1952.39 24.06 o 1 6 3 255.76 292.58 16.67 o 2 6 3 2208.97 2533.38 27.58 o 3 6 3 8729.80 8681.00 85.60 o 4 6 3 15774.63 15905.66 129.17 o 5 6 3 1059.06 1014.49 15.81 o 6 6 3 3679.24 4188.75 55.46 o -6 7 3 4083.05 4098.66 52.55 o -5 7 3 3753.19 3193.53 41.97 o -4 7 3 1004.75 1030.35 21.71 o -3 7 3 3910.65 4278.78 54.27 o -2 7 3 1758.51 1560.24 16.21 o -1 7 3 1112.22 1234.81 14.95 o 0 7 3 306.91 224.50 13.52 o 1 7 3 3967.08 4243.96 56.40 o 2 7 3 7362.49 7367.80 61.10 o 3 7 3 5275.76 5201.13 58.99 o 4 7 3 1559.86 1654.05 28.47 o 5 7 3 3567.13 3478.94 39.86 o 6 7 3 5523.87 5653.61 37.66 o 7 7 3 267.35 141.55 10.74 o -7 8 3 3547.26 3229.83 22.92 o -6 8 3 8238.48 6826.46 23.94 o -5 8 3 3813.09 3882.46 30.56 o -4 8 3 3471.50 3808.77 39.53 o -3 8 3 8465.66 8700.02 72.04 o -2 8 3 843.35 1010.13 24.25 o -1 8 3 272.15 329.97 9.24 o 0 8 3 447.46 402.67 11.79 o 1 8 3 13736.05 13017.72 112.00 o 2 8 3 338.36 249.41 11.23 o 3 8 3 91.85 62.40 11.42 o 4 8 3 202.06 131.38 8.25 o 5 8 3 1942.69 1812.29 28.84 o 6 8 3 12.14 5.20 10.40 o 7 8 3 2709.31 2828.53 21.41 o 8 8 3 10.94 77.31 8.83 o -8 9 3 1361.05 1366.28 20.95 o -7 9 3 2207.49 2463.04 41.13 o -6 9 3 1791.37 1523.13 22.83 o -5 9 3 498.11 650.15 21.32 o -4 9 3 2495.16 2153.73 28.22 o -3 9 3 16.06 65.07 11.91 o -2 9 3 556.33 672.75 7.33 o -1 9 3 4651.19 4229.08 45.71 o 0 9 3 29.64 65.56 6.83 o 1 9 3 1205.22 1335.85 14.03 o 2 9 3 3365.57 3483.10 41.66 o 3 9 3 369.21 310.26 13.23 o 4 9 3 3971.53 3672.89 34.46 o 5 9 3 295.05 240.70 11.55 o 6 9 3 16.82 39.58 12.32 o 7 9 3 2785.87 2444.80 23.03 o 8 9 3 29.91 42.03 9.90 o 9 9 3 1316.53 1366.29 17.84 o -9 10 3 5958.03 5777.46 121.71 o -8 10 3 366.11 317.78 14.41 o -7 10 3 2849.68 2936.90 52.43 o -6 10 3 34.97 7.42 13.10 o -5 10 3 552.69 511.62 8.94 o -4 10 3 1875.22 1642.15 29.48 o -3 10 3 1036.87 1038.89 16.96 o -2 10 3 125.89 84.58 14.04 o -1 10 3 12734.47 13969.70 264.42 o 0 10 3 814.73 774.72 13.05 o 1 10 3 79.03 50.54 9.90 o 2 10 3 4709.67 4412.25 78.10 o 3 10 3 8880.35 9343.26 105.58 o 4 10 3 1606.52 1899.90 34.45 o 5 10 3 6404.00 6683.54 61.92 o 6 10 3 2418.42 2462.97 27.66 o 7 10 3 713.63 726.18 16.84 o 8 10 3 73.34 93.58 9.53 o 9 10 3 1370.81 1502.05 25.04 o 10 10 3 1918.05 1875.59 34.53 o -10 11 3 276.22 301.27 21.29 o -9 11 3 2.73 0.00 14.06 o -8 11 3 1783.65 1707.91 24.84 o -7 11 3 48.50 95.18 15.76 o -6 11 3 4396.93 4359.95 60.18 o -5 11 3 578.32 543.80 21.28 o -4 11 3 5.77 31.25 6.92 o -3 11 3 9175.39 9519.14 80.56 o -2 11 3 1327.55 1179.85 24.86 o -1 11 3 471.52 589.99 25.64 o 0 11 3 4060.67 3666.01 53.72 o 1 11 3 1368.50 1480.98 18.73 o 2 11 3 204.40 273.92 17.55 o 3 11 3 3819.48 3844.64 177.87 o 4 11 3 3134.82 2984.23 61.43 o 5 11 3 474.35 462.62 11.54 o 6 11 3 64.21 112.98 15.88 o 7 11 3 376.17 328.09 11.50 o 8 11 3 1704.94 1764.59 31.59 o 9 11 3 784.41 657.53 10.53 o 10 11 3 456.24 480.59 13.39 o 11 11 3 180.32 180.33 9.97 o -11 12 3 153.78 145.19 15.71 o -10 12 3 279.56 327.20 11.96 o -9 12 3 383.50 387.45 16.05 o -8 12 3 622.08 606.90 9.97 o -7 12 3 2333.80 2331.96 19.29 o -6 12 3 79.64 41.16 16.63 o -5 12 3 4815.55 4940.91 45.86 o -4 12 3 2281.33 2085.75 27.56 o -3 12 3 6.80 43.90 16.26 o -2 12 3 2.43 21.80 11.04 o -1 12 3 4927.67 4701.36 80.00 o 0 12 3 1555.05 1638.05 35.09 o 1 12 3 3348.16 3354.63 44.49 o 2 12 3 3956.46 3819.72 54.85 o 3 12 3 2909.54 2979.88 35.20 o 4 12 3 15.74 15.61 10.47 o 5 12 3 183.32 178.62 12.17 o 6 12 3 51.27 78.31 14.77 o 7 12 3 3882.73 3876.60 55.13 o 8 12 3 19.18 15.58 11.52 o 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3 790.16 777.08 35.18 o -8 14 3 2.93 16.17 13.60 o -7 14 3 840.12 745.93 26.14 o -6 14 3 2687.32 2512.76 37.36 o -5 14 3 5.62 26.45 16.60 o -4 14 3 10.36 37.45 18.41 o -3 14 3 4945.89 4966.71 93.61 o -2 14 3 930.33 859.09 23.35 o -1 14 3 194.34 257.19 10.30 o 0 14 3 5516.56 5214.81 58.95 o 1 14 3 744.31 779.96 17.32 o 2 14 3 57.95 42.65 12.52 o 3 14 3 584.15 617.72 23.63 o 4 14 3 614.59 537.50 18.85 o 5 14 3 1798.31 1714.58 28.24 o 6 14 3 497.11 540.51 17.14 o 7 14 3 3.21 31.23 18.16 o 8 14 3 218.17 249.56 17.19 o 9 14 3 3.13 19.90 12.88 o 10 14 3 17.50 39.02 11.91 o 11 14 3 502.60 526.52 14.84 o 12 14 3 446.98 461.89 17.83 o 13 14 3 18.53 17.88 19.30 o 14 14 3 467.34 451.08 17.25 o -14 15 3 82.74 94.41 15.12 o -13 15 3 451.80 437.73 19.46 o -12 15 3 352.16 366.34 19.13 o -11 15 3 77.81 84.20 15.70 o -10 15 3 20.39 35.01 10.34 o -9 15 3 75.12 102.38 12.95 o -8 15 3 1626.38 1602.43 32.80 o -7 15 3 256.49 239.54 16.73 o -6 15 3 170.51 169.57 10.46 o -5 15 3 158.97 166.81 14.99 o -4 15 3 1416.27 1428.63 25.58 o -3 15 3 0.00 4.48 15.03 o -2 15 3 1638.90 1415.83 38.08 o -1 15 3 260.90 259.86 11.12 o 0 15 3 1325.21 1341.13 52.98 o 1 15 3 44.28 30.85 10.23 o 2 15 3 60.43 92.57 10.93 o 3 15 3 638.46 685.97 20.61 o 4 15 3 1066.36 961.16 19.40 o 5 15 3 60.19 36.71 13.68 o 6 15 3 2903.27 2832.26 51.08 o 7 15 3 47.10 67.80 9.99 o 8 15 3 101.58 112.15 11.12 o 9 15 3 4.41 36.61 14.80 o 10 15 3 285.08 329.01 13.47 o 11 15 3 139.34 187.47 15.31 o 12 15 3 94.43 111.65 18.89 o 13 15 3 13.91 53.68 15.34 o 14 15 3 443.80 439.29 16.35 o 15 15 3 0.17 4.01 15.04 o -15 16 3 6.45 29.27 17.57 o -14 16 3 0.06 24.43 21.32 o -13 16 3 632.27 555.64 21.77 o -12 16 3 55.97 58.09 12.86 o -11 16 3 54.94 78.67 22.84 o -10 16 3 8.15 32.48 12.21 o -9 16 3 30.39 45.72 10.61 o -8 16 3 227.93 206.50 17.36 o -7 16 3 68.78 102.95 13.59 o -6 16 3 45.34 50.15 7.58 o -5 16 3 376.52 383.94 17.12 o -4 16 3 945.64 824.68 32.00 o -3 16 3 887.21 717.13 24.98 o -2 16 3 384.02 301.47 18.87 o -1 16 3 2491.01 2014.51 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