#------------------------------------------------------------------------------ #$Date: 2009-05-03 21:56:13 +0300 (Sun, 03 May 2009) $ #$Revision: 691 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2217981.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2217981_Fobs loop_ _publ_author_name 'Schachner, J\"org A.' 'Quail, J. Wilson' 'M\"uller, Jens' _publ_section_title ; The galla[1]ferrocenophane {[dimethyl(2-pyridyl)silyl]bis(trimethylsilyl)methyl-\k^2^C,N}(ferrocene-1,1'-diyl)gallium(III) ; _journal_coeditor_code OM2215 _journal_issue 4 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m517 _journal_volume 64 _journal_year 2008 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 92.521 _cell_angle_gamma 90.000 _cell_length_a 9.6463 _cell_length_b 35.2258 _cell_length_c 15.4862 _exptl_crystal_F_000 2288.00 _reflns_d_resolution_high 0.8069 _[local]_cod_data_source_file om2215Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' Compound 331 NOABS' _shelx_refln_list_code 4 _shelx_F_calc_maximum 439.26 _shelx_F_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 31.90 1.83 10.83 o 2 0 0 11881.10 12590.17 537.20 o 3 0 0 8308.35 9287.76 201.34 o 4 0 0 71373.89 72308.66 2332.91 o 5 0 0 78.86 137.30 50.30 o 6 0 0 7069.96 7795.42 245.95 o 7 0 0 148.71 98.89 135.02 o 8 0 0 2282.35 2001.67 203.75 o 9 0 0 1346.22 1319.77 157.82 o 10 0 0 3358.75 3249.49 218.50 o 11 0 0 5584.30 6014.97 614.36 o 2 1 0 45840.07 47612.05 624.53 o 3 1 0 361.22 527.93 33.09 o 4 1 0 27954.77 30538.22 428.45 o 5 1 0 1584.41 2042.59 220.89 o 6 1 0 1580.31 1674.34 56.14 o 7 1 0 2957.11 2600.49 73.42 o 8 1 0 1921.22 1774.84 89.92 o 9 1 0 38.46 38.98 69.61 o 10 1 0 624.08 606.53 162.91 o 11 1 0 286.98 293.27 127.80 o 2 2 0 24097.00 25550.54 516.73 o 3 2 0 22359.82 23757.45 361.72 o 4 2 0 671.99 841.89 58.08 o 5 2 0 7.94 26.96 28.07 o 6 2 0 3609.22 3456.14 129.06 o 7 2 0 3204.56 3413.66 137.19 o 8 2 0 71.67 -0.53 64.48 o 9 2 0 1114.71 647.59 132.40 o 10 2 0 1223.43 1142.90 157.77 o 11 2 0 2.49 130.37 99.68 o 1 3 0 310.82 374.66 38.01 o 2 3 0 17096.57 16445.64 183.54 o 3 3 0 4027.26 4609.73 93.43 o 4 3 0 10191.51 11309.19 159.45 o 5 3 0 1.35 28.25 47.89 o 6 3 0 27740.44 27229.77 495.21 o 7 3 0 2678.04 2710.42 78.41 o 8 3 0 4978.21 5081.33 166.52 o 9 3 0 3570.19 4234.39 195.68 o 10 3 0 508.84 870.27 135.94 o 11 3 0 173.12 106.70 94.97 o 1 4 0 537.70 674.25 15.27 o 2 4 0 10147.92 10410.42 116.48 o 3 4 0 121.00 146.53 31.62 o 4 4 0 41267.41 41110.09 547.53 o 5 4 0 19.35 51.34 43.64 o 6 4 0 6969.47 6795.89 156.30 o 7 4 0 6840.35 6798.46 124.77 o 8 4 0 2782.85 2357.17 142.30 o 9 4 0 232.72 340.39 96.17 o 10 4 0 6305.96 6863.88 581.76 o 11 4 0 0.35 10.54 85.61 o 1 5 0 789.04 963.87 21.02 o 2 5 0 425.37 582.00 26.37 o 3 5 0 1402.94 1597.36 39.38 o 4 5 0 913.61 1356.83 99.88 o 5 5 0 490.63 523.39 46.34 o 6 5 0 22756.85 22694.92 322.51 o 7 5 0 203.93 205.65 27.14 o 8 5 0 2554.69 2309.81 119.68 o 9 5 0 5012.96 4866.97 217.54 o 10 5 0 262.70 180.78 119.16 o 11 5 0 1285.47 1249.59 193.75 o 0 6 0 2061.06 1785.08 73.63 o 1 6 0 3926.55 3819.77 46.75 o 2 6 0 23.85 46.95 14.29 o 3 6 0 18348.31 19218.06 204.38 o 4 6 0 19683.52 20292.42 333.97 o 5 6 0 11219.58 11596.31 220.20 o 6 6 0 7542.38 7244.95 141.59 o 7 6 0 2116.51 2074.72 105.79 o 8 6 0 881.61 1190.21 101.82 o 9 6 0 812.89 552.59 147.56 o 10 6 0 34.85 -110.89 110.89 o 11 6 0 2055.08 2024.04 262.30 o 1 7 0 19966.08 20522.82 205.93 o 2 7 0 1816.93 1692.92 35.94 o 3 7 0 193.65 243.20 24.06 o 4 7 0 9112.89 9045.67 157.57 o 5 7 0 1202.36 1134.40 48.61 o 6 7 0 998.10 1132.02 83.12 o 7 7 0 1103.16 1072.84 138.36 o 8 7 0 38.51 133.36 56.04 o 9 7 0 6.82 94.12 169.87 o 10 7 0 3817.62 3665.86 219.45 o 11 7 0 511.83 658.97 209.91 o 0 8 0 45851.26 49922.57 2106.27 o 1 8 0 3967.50 4132.70 64.00 o 2 8 0 1054.52 1130.22 40.77 o 3 8 0 13285.13 13006.86 162.35 o 4 8 0 716.00 699.16 51.39 o 5 8 0 2276.90 3695.70 1378.58 o 6 8 0 1499.76 1551.79 55.02 o 7 8 0 662.54 629.79 78.05 o 8 8 0 1766.50 1793.92 95.55 o 9 8 0 1600.13 1562.11 144.11 o 10 8 0 2561.22 3173.29 260.18 o 11 8 0 241.05 435.31 184.03 o 1 9 0 3095.28 3152.40 43.52 o 2 9 0 14820.64 14843.00 152.84 o 3 9 0 314.40 294.17 23.91 o 4 9 0 3323.78 3468.23 65.10 o 5 9 0 38530.84 38339.40 509.73 o 6 9 0 3569.78 3607.17 92.78 o 7 9 0 174.65 174.61 47.40 o 8 9 0 386.07 267.86 109.97 o 9 9 0 2475.49 2165.50 162.20 o 10 9 0 2518.65 2093.73 172.64 o 11 9 0 60.27 68.88 123.85 o 0 10 0 1002.45 1081.52 37.83 o 1 10 0 209.73 213.10 19.23 o 2 10 0 7656.90 8734.43 98.25 o 3 10 0 1447.48 1750.02 44.49 o 4 10 0 29860.41 29658.50 336.12 o 5 10 0 3847.13 4029.78 109.39 o 6 10 0 1702.13 1561.15 69.89 o 7 10 0 2933.59 3081.66 112.32 o 8 10 0 5905.82 5968.64 261.53 o 9 10 0 1315.02 1229.52 132.83 o 10 10 0 3116.69 3680.71 206.25 o 11 10 0 838.74 1338.49 264.11 o 1 11 0 8822.18 8674.85 93.01 o 2 11 0 1570.30 1292.70 34.96 o 3 11 0 36573.89 35924.49 559.17 o 4 11 0 3563.60 4049.64 467.17 o 5 11 0 37151.10 37814.29 547.32 o 6 11 0 8011.08 8211.31 152.51 o 7 11 0 289.42 250.55 46.67 o 8 11 0 516.24 612.58 80.29 o 9 11 0 9753.99 10151.51 309.75 o 10 11 0 112.44 143.55 209.37 o 11 11 0 2664.01 2051.22 221.05 o 0 12 0 2542.18 2280.99 58.53 o 1 12 0 14034.34 13346.59 144.35 o 2 12 0 11148.35 11097.01 140.11 o 3 12 0 13418.11 13474.69 155.69 o 4 12 0 12240.60 12975.46 195.04 o 5 12 0 8661.29 8972.49 157.58 o 6 12 0 1685.64 1633.86 62.10 o 7 12 0 5121.27 5176.98 267.56 o 8 12 0 556.13 483.72 90.22 o 9 12 0 3488.42 3777.98 176.01 o 10 12 0 8.56 175.15 142.02 o 11 12 0 5346.76 5430.87 530.09 o 1 13 0 23696.59 23593.70 226.29 o 2 13 0 16310.37 16534.82 189.18 o 3 13 0 546.83 634.65 32.28 o 4 13 0 308.98 795.81 415.14 o 5 13 0 15520.68 15946.30 292.82 o 6 13 0 491.88 500.67 92.04 o 7 13 0 248.71 258.92 58.76 o 8 13 0 257.37 142.82 64.56 o 9 13 0 122.16 -58.46 103.72 o 10 13 0 246.32 431.99 149.15 o 11 13 0 388.21 199.39 149.03 o 0 14 0 17625.88 18853.68 452.63 o 1 14 0 6890.61 7303.20 105.08 o 2 14 0 3255.70 3117.61 55.84 o 3 14 0 88.03 36.60 18.57 o 4 14 0 34.76 93.29 32.93 o 5 14 0 2192.69 2365.33 83.16 o 6 14 0 4559.91 4763.58 131.65 o 7 14 0 367.61 379.82 59.52 o 8 14 0 55.32 39.09 81.26 o 9 14 0 259.34 143.65 86.39 o 10 14 0 431.76 221.36 153.90 o 11 14 0 3600.73 3632.70 304.81 o 1 15 0 42783.73 42123.75 406.85 o 2 15 0 25.03 43.80 15.73 o 3 15 0 14449.27 13947.91 211.54 o 4 15 0 1395.28 1359.43 89.02 o 5 15 0 20906.65 21418.54 308.21 o 6 15 0 6207.09 6336.35 163.31 o 7 15 0 1357.64 1241.57 83.84 o 8 15 0 407.24 182.43 66.14 o 9 15 0 8666.05 9492.70 536.48 o 10 15 0 11.33 -88.06 118.91 o 11 15 0 711.78 582.46 146.81 o 0 16 0 167.75 136.79 33.18 o 1 16 0 6523.48 6641.23 118.41 o 2 16 0 80.27 128.98 20.15 o 3 16 0 419.54 429.62 31.50 o 4 16 0 3124.63 3295.51 193.14 o 5 16 0 12843.95 12947.22 239.65 o 6 16 0 4676.98 4967.45 195.59 o 7 16 0 2163.02 2112.77 100.69 o 8 16 0 884.24 1008.37 101.21 o 9 16 0 3232.13 3893.85 456.27 o 10 16 0 6.17 -79.24 217.98 o 11 16 0 346.24 434.43 127.98 o 1 17 0 2030.73 2183.67 53.09 o 2 17 0 4087.43 4097.79 65.39 o 3 17 0 16383.97 16610.18 207.38 o 4 17 0 44.07 155.12 34.33 o 5 17 0 547.12 659.74 60.89 o 6 17 0 125.47 201.25 62.12 o 7 17 0 157.11 65.32 66.58 o 8 17 0 309.90 329.93 95.09 o 9 17 0 223.82 77.40 90.22 o 10 17 0 471.37 441.88 122.82 o 11 17 0 249.78 -134.17 199.42 o 0 18 0 4.27 -3.85 24.57 o 1 18 0 1475.02 1424.05 80.02 o 2 18 0 533.99 631.94 34.20 o 3 18 0 586.35 571.40 27.54 o 4 18 0 2231.25 2355.06 82.06 o 5 18 0 4468.59 4326.09 190.18 o 6 18 0 839.47 966.99 69.69 o 7 18 0 12966.94 12439.27 327.79 o 8 18 0 1482.40 1337.04 188.60 o 9 18 0 1098.70 1034.91 126.38 o 10 18 0 2342.53 1908.16 207.57 o 1 19 0 29963.51 31090.95 790.60 o 2 19 0 835.06 778.30 28.29 o 3 19 0 80.32 54.92 24.06 o 4 19 0 278.72 336.76 36.08 o 5 19 0 6980.91 6884.13 191.65 o 6 19 0 23.63 70.13 72.45 o 7 19 0 119.44 -3.81 64.97 o 8 19 0 1825.78 1534.51 270.58 o 9 19 0 1758.61 1801.31 124.82 o 10 19 0 775.64 717.00 144.11 o 0 20 0 1072.64 1055.26 47.42 o 1 20 0 982.63 1117.58 56.21 o 2 20 0 1604.02 1598.44 57.48 o 3 20 0 2561.51 2656.79 53.87 o 4 20 0 493.78 510.46 56.20 o 5 20 0 4584.31 4514.61 120.14 o 6 20 0 8.86 99.97 49.54 o 7 20 0 3605.44 3376.42 172.50 o 8 20 0 2943.50 2784.89 176.01 o 9 20 0 147.32 -52.89 130.73 o 10 20 0 113.96 -2.49 96.69 o 1 21 0 43765.84 47258.49 1615.73 o 2 21 0 1776.40 1626.35 54.73 o 3 21 0 614.90 642.67 35.71 o 4 21 0 939.77 1710.95 409.67 o 5 21 0 3987.39 3886.35 103.15 o 6 21 0 862.99 839.14 112.12 o 7 21 0 112.79 183.50 93.38 o 8 21 0 749.14 968.11 138.67 o 9 21 0 25.52 42.23 114.07 o 10 21 0 81.37 79.19 146.12 o 0 22 0 2180.17 2160.29 104.34 o 1 22 0 14319.04 15089.57 545.28 o 2 22 0 672.62 530.99 69.34 o 3 22 0 20898.90 20710.00 258.00 o 4 22 0 1307.56 1346.01 58.30 o 5 22 0 262.24 322.58 52.82 o 6 22 0 699.20 790.87 78.35 o 7 22 0 6246.16 5987.01 344.86 o 8 22 0 1180.90 1285.95 230.06 o 9 22 0 960.72 1175.28 216.90 o 10 22 0 698.86 492.82 163.85 o 1 23 0 889.77 793.29 75.51 o 2 23 0 2936.02 2889.94 106.04 o 3 23 0 8722.97 8238.38 141.43 o 4 23 0 405.07 711.23 98.48 o 5 23 0 4808.29 4723.58 110.00 o 6 23 0 469.11 616.76 108.67 o 7 23 0 414.54 285.22 169.03 o 8 23 0 31.44 -7.99 79.41 o 9 23 0 2252.28 2197.68 178.61 o 10 23 0 276.07 275.77 138.64 o 0 24 0 8180.18 8195.40 178.30 o 1 24 0 768.96 787.47 65.80 o 2 24 0 2351.82 2045.27 95.96 o 3 24 0 297.13 383.43 57.41 o 4 24 0 11668.35 11597.57 186.20 o 5 24 0 1868.32 1976.88 82.88 o 6 24 0 740.62 765.66 71.07 o 7 24 0 1155.02 1045.01 96.81 o 8 24 0 2648.45 3094.21 231.87 o 9 24 0 0.09 -14.86 190.67 o 1 25 0 2.19 57.49 36.94 o 2 25 0 97.08 36.38 27.30 o 3 25 0 16695.07 14452.32 1079.37 o 4 25 0 770.74 919.76 95.28 o 5 25 0 6120.69 6435.12 158.63 o 6 25 0 2069.15 2425.19 134.26 o 7 25 0 1225.71 1092.11 101.54 o 8 25 0 511.55 387.43 90.26 o 9 25 0 1522.94 1490.84 161.75 o 0 26 0 12277.29 12163.56 911.36 o 1 26 0 11036.33 12049.50 329.61 o 2 26 0 909.95 866.19 88.88 o 3 26 0 8339.56 8525.55 225.44 o 4 26 0 4940.11 5232.95 176.73 o 5 26 0 58.89 198.80 94.53 o 6 26 0 245.55 104.31 95.60 o 7 26 0 980.30 1146.65 101.71 o 8 26 0 1294.27 1402.46 169.93 o 9 26 0 203.91 245.56 112.18 o 1 27 0 1140.08 1205.08 69.17 o 2 27 0 4369.41 3635.97 281.93 o 3 27 0 1192.24 982.53 71.05 o 4 27 0 755.02 943.92 129.84 o 5 27 0 513.95 404.11 100.12 o 6 27 0 16.92 -27.99 60.15 o 7 27 0 133.37 270.87 181.11 o 8 27 0 219.24 27.63 83.46 o 9 27 0 6.62 56.96 97.70 o 0 28 0 2366.64 2296.25 147.28 o 1 28 0 58.50 103.31 41.62 o 2 28 0 1463.51 1470.50 142.59 o 3 28 0 3130.89 3083.39 91.22 o 4 28 0 4623.85 4673.81 157.22 o 5 28 0 4291.39 4579.58 134.41 o 6 28 0 6706.92 7124.24 207.27 o 7 28 0 291.87 134.63 76.92 o 8 28 0 22.73 -77.99 127.53 o 9 28 0 73.68 68.19 119.72 o 1 29 0 153.74 99.25 47.38 o 2 29 0 4052.19 3910.65 172.28 o 3 29 0 20.64 9.35 62.86 o 4 29 0 275.46 431.66 77.89 o 5 29 0 237.81 298.51 94.13 o 6 29 0 1599.95 1657.40 122.36 o 7 29 0 512.56 449.59 109.86 o 8 29 0 13.75 203.87 304.17 o 0 30 0 7494.76 7639.51 265.37 o 1 30 0 802.50 934.55 100.56 o 2 30 0 1084.94 1292.12 88.00 o 3 30 0 1018.71 1032.33 106.44 o 4 30 0 4163.18 4420.29 191.88 o 5 30 0 3234.85 2909.97 132.65 o 6 30 0 3229.86 3224.73 284.92 o 7 30 0 547.86 595.67 96.55 o 8 30 0 47.28 -29.19 114.22 o 1 31 0 956.29 956.49 161.94 o 2 31 0 82.14 67.10 38.91 o 3 31 0 47.38 62.32 68.03 o 4 31 0 1045.84 1148.99 103.62 o 5 31 0 210.28 260.45 132.16 o 6 31 0 988.35 1198.11 201.90 o 7 31 0 262.79 414.19 80.13 o 8 31 0 995.93 968.48 152.52 o 0 32 0 2791.15 2782.87 278.51 o 1 32 0 343.41 410.78 79.61 o 2 32 0 1399.23 1401.97 180.24 o 3 32 0 78.01 43.79 48.29 o 4 32 0 525.27 407.96 137.39 o 5 32 0 6.19 132.58 96.81 o 6 32 0 38.42 -138.60 191.89 o 7 32 0 644.67 719.91 119.03 o 8 32 0 0.96 -40.94 107.55 o 1 33 0 2017.86 2063.09 98.86 o 2 33 0 2176.59 2032.04 123.44 o 3 33 0 402.86 555.50 163.28 o 4 33 0 0.91 111.97 99.01 o 5 33 0 302.80 230.88 80.40 o 6 33 0 5799.12 6143.98 262.13 o 7 33 0 138.10 311.28 131.95 o 0 34 0 14612.34 16655.87 1481.07 o 1 34 0 14.27 32.79 98.26 o 2 34 0 4795.86 5475.06 303.64 o 3 34 0 39.26 -77.42 77.42 o 4 34 0 1192.12 1127.15 108.02 o 5 34 0 369.50 388.80 105.25 o 6 34 0 1857.21 2021.45 173.06 o 7 34 0 61.64 -36.62 141.47 o 1 35 0 620.51 1080.85 155.78 o 2 35 0 2138.73 2329.29 196.19 o 3 35 0 46.31 162.69 90.51 o 4 35 0 103.83 46.47 86.32 o 5 35 0 1472.80 1751.75 132.06 o 6 35 0 1347.42 1158.37 144.85 o 7 35 0 0.00 16.61 108.96 o 0 36 0 5789.92 6230.84 275.22 o 1 36 0 737.89 749.48 139.97 o 2 36 0 326.92 712.76 148.94 o 3 36 0 310.44 329.45 102.44 o 4 36 0 7.01 87.06 87.83 o 5 36 0 105.26 -17.24 119.41 o 6 36 0 59.07 160.05 151.97 o 1 37 0 2.48 -93.83 93.83 o 2 37 0 11463.22 12955.20 389.70 o 3 37 0 464.94 141.79 102.23 o 4 37 0 17.68 55.76 85.30 o 5 37 0 268.56 354.05 97.24 o 6 37 0 5298.83 5130.79 430.26 o 0 38 0 1012.24 982.99 213.36 o 1 38 0 6.06 -97.49 97.49 o 2 38 0 332.66 384.25 102.64 o 3 38 0 310.54 408.72 129.43 o 4 38 0 2684.01 2594.35 202.65 o 5 38 0 42.20 35.51 92.56 o 1 39 0 1299.80 1419.28 167.58 o 2 39 0 244.61 369.31 97.60 o 3 39 0 52.84 -58.08 112.51 o 4 39 0 345.85 326.28 172.22 o 5 39 0 2105.07 2018.24 171.74 o 0 40 0 21.81 93.09 153.59 o 1 40 0 193.23 23.35 111.00 o 2 40 0 63.65 99.48 98.50 o 3 40 0 134.81 232.30 108.84 o 4 40 0 204.84 190.89 100.36 o 1 41 0 560.98 549.47 142.80 o 2 41 0 3892.42 4217.62 412.15 o 3 41 0 98.57 201.40 174.48 o 0 42 0 370.99 331.06 179.79 o 1 42 0 678.17 784.24 176.61 o 2 42 0 717.49 579.64 206.80 o 3 42 0 113.54 96.23 142.05 o 1 43 0 1212.32 1177.57 244.92 o -11 1 1 4611.68 5199.82 220.34 o -10 1 1 105.29 156.41 83.58 o -9 1 1 5427.82 5389.70 202.12 o -8 1 1 94.22 83.29 54.49 o -7 1 1 25746.13 25300.03 470.58 o -6 1 1 2116.99 2101.25 57.94 o -5 1 1 36589.64 37083.21 485.33 o -4 1 1 38.99 140.78 30.37 o -3 1 1 128568.83 131510.63 1485.65 o -2 1 1 13020.94 13700.90 169.99 o -1 1 1 1352.43 1191.48 227.17 o 0 1 1 8.56 11.94 6.59 o 1 1 1 122582.73 104404.95 21035.29 o 2 1 1 1624.62 1908.66 51.47 o 3 1 1 8835.72 7883.02 136.38 o 4 1 1 1940.46 1946.39 77.47 o 5 1 1 11558.41 10743.39 284.86 o 6 1 1 14753.92 14355.57 541.39 o 7 1 1 9939.85 10211.23 233.07 o 8 1 1 863.05 819.02 82.60 o 9 1 1 1.26 -80.67 80.67 o 10 1 1 1090.40 951.77 124.63 o 11 1 1 4485.63 4618.83 336.49 o -11 2 1 62.99 59.16 187.10 o -10 2 1 145.61 196.61 215.86 o -9 2 1 70.75 404.74 94.81 o -8 2 1 29.46 58.24 65.28 o -7 2 1 1560.08 1182.56 116.87 o -6 2 1 1526.69 1551.32 64.78 o -5 2 1 14965.17 14858.60 228.65 o -4 2 1 296.49 367.22 36.02 o -3 2 1 82419.80 90509.60 1087.80 o -2 2 1 2563.89 2493.86 45.83 o 0 2 1 14.81 9.08 6.49 o 1 2 1 28039.99 25157.56 2679.94 o 2 2 1 32005.40 33876.64 432.28 o 3 2 1 22678.90 23467.70 363.81 o 4 2 1 1181.95 1154.42 46.98 o 5 2 1 2620.47 2648.49 96.83 o 6 2 1 65.30 76.41 88.99 o 7 2 1 145.22 173.73 46.64 o 8 2 1 1304.63 1387.28 99.34 o 9 2 1 3250.69 3194.72 148.96 o 10 2 1 1.80 10.37 86.49 o 11 2 1 58.33 101.12 91.42 o -11 3 1 2252.16 2246.31 162.38 o -10 3 1 1477.90 1870.33 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