#------------------------------------------------------------------------------ #$Date: 2009-05-03 21:56:13 +0300 (Sun, 03 May 2009) $ #$Revision: 691 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2217984.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2217984_Fobs loop_ _publ_author_name 'Gowda, B. Thimme' 'Foro, Sabine' 'Babitha, K. S.' 'Fuess, Hartmut' _publ_section_title ; 4-Bromophenyl benzoate ; _journal_coeditor_code OM2221 _journal_issue 4 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o771 _journal_volume 64 _journal_year 2008 _space_group_IT_number 29 _symmetry_space_group_name_Hall 'P 2c -2ac' _symmetry_space_group_name_H-M 'P c a 21' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 7.7480 _cell_length_b 5.5946 _cell_length_c 26.8140 _exptl_crystal_F_000 552.00 _reflns_d_resolution_high 0.8379 _[local]_cod_data_source_file om2221Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' E9 PCA21' _shelx_refln_list_code 4 _shelx_F_calc_maximum 145.88 _shelx_F_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, z+1/2' '-x+1/2, y, z+1/2' 'x+1/2, -y, z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 0 0 -8 16620.19 14169.96 66.06 o 2 0 -8 7397.48 7029.81 44.93 o 4 0 -8 506.66 507.35 13.48 o 6 0 -8 3.44 5.04 3.80 o 0 1 -8 1297.44 1091.54 25.19 o 1 1 -8 6465.34 5602.49 91.18 o 2 1 -8 106.33 107.73 2.33 o 3 1 -8 2360.89 2255.74 47.75 o 4 1 -8 298.65 348.99 11.85 o 5 1 -8 143.05 140.91 3.19 o 6 1 -8 17.12 15.75 2.07 o 0 2 -8 1209.67 1089.96 16.14 o 1 2 -8 162.66 171.64 7.20 o 2 2 -8 2189.77 2093.52 24.34 o 3 2 -8 2.66 1.88 3.76 o 4 2 -8 389.12 412.91 11.69 o 5 2 -8 19.08 20.13 2.89 o 6 2 -8 177.00 195.84 6.01 o 0 3 -8 413.18 490.20 13.52 o 1 3 -8 634.11 577.98 10.47 o 2 3 -8 75.56 75.87 3.30 o 3 3 -8 691.96 665.46 17.79 o 4 3 -8 44.85 41.99 2.80 o 5 3 -8 39.51 33.88 3.07 o 6 3 -8 23.37 21.78 3.03 o 0 4 -8 160.16 192.04 5.68 o 1 4 -8 112.15 117.01 3.35 o 2 4 -8 439.67 396.59 12.01 o 3 4 -8 101.09 97.65 4.68 o 4 4 -8 43.59 33.88 3.67 o 5 4 -8 42.46 31.36 2.93 o 6 4 -8 7.52 -2.75 4.31 o 0 5 -8 6.74 12.74 2.80 o 1 5 -8 14.69 11.22 2.09 o 2 5 -8 82.45 79.72 4.08 o 3 5 -8 96.63 90.27 4.08 o 4 5 -8 14.28 11.74 2.15 o 5 5 -8 10.50 9.17 2.02 o 0 6 -8 2.71 0.00 3.30 o 1 6 -8 1.85 0.57 2.39 o 2 6 -8 3.27 1.05 3.16 o 3 6 -8 6.08 -3.16 3.44 o 2 0 -7 1060.76 976.64 14.26 o 4 0 -7 2481.62 2631.90 31.45 o 6 0 -7 308.86 307.06 9.21 o 8 0 -7 62.63 55.65 3.44 o 1 1 -7 432.30 415.08 4.29 o 2 1 -7 725.12 792.60 8.85 o 3 1 -7 1424.15 1413.76 58.52 o 4 1 -7 14.98 19.59 1.70 o 5 1 -7 838.64 875.52 14.27 o 6 1 -7 48.54 61.26 3.90 o 7 1 -7 185.17 203.79 18.45 o 8 1 -7 8.73 2.62 3.07 o 1 2 -7 678.29 719.94 9.17 o 2 2 -7 751.08 836.54 14.94 o 3 2 -7 72.58 92.01 2.98 o 4 2 -7 608.44 587.07 15.59 o 5 2 -7 144.79 225.18 6.69 o 6 2 -7 485.78 543.97 15.77 o 7 2 -7 14.73 6.78 2.61 o 8 2 -7 84.56 73.26 3.44 o 1 3 -7 171.51 154.93 3.32 o 2 3 -7 578.59 635.02 15.77 o 3 3 -7 251.69 264.29 7.56 o 4 3 -7 27.23 31.26 2.75 o 5 3 -7 23.01 21.32 3.62 o 6 3 -7 55.03 77.93 4.13 o 7 3 -7 202.15 173.24 4.63 o 8 3 -7 21.85 10.41 2.06 o 1 4 -7 116.35 138.35 5.46 o 2 4 -7 87.28 97.92 4.40 o 3 4 -7 173.14 154.54 5.13 o 4 4 -7 205.87 222.38 6.78 o 5 4 -7 55.14 65.51 3.48 o 6 4 -7 28.42 20.63 2.84 o 7 4 -7 2.71 6.01 1.65 o 1 5 -7 6.14 -0.16 2.55 o 2 5 -7 16.06 13.20 3.07 o 3 5 -7 3.17 11.28 2.57 o 4 5 -7 1.06 1.33 4.45 o 5 5 -7 44.62 38.37 2.80 o 1 6 -7 9.47 12.83 1.90 o 2 6 -7 0.09 2.89 3.58 o 3 6 -7 0.37 1.19 1.79 o 0 0 -6 6601.61 5451.75 31.17 o 2 0 -6 4376.34 3948.60 28.33 o 4 0 -6 507.87 563.00 15.04 o 6 0 -6 33.60 34.98 4.22 o 8 0 -6 12.14 12.38 2.48 o 0 1 -6 669.31 645.20 12.06 o 1 1 -6 7178.97 6056.64 64.44 o 2 1 -6 665.97 580.17 11.83 o 3 1 -6 1790.38 1709.72 89.23 o 4 1 -6 69.03 84.01 4.10 o 5 1 -6 183.05 217.53 5.68 o 6 1 -6 6.63 3.30 2.45 o 7 1 -6 11.77 9.71 4.17 o 8 1 -6 10.42 17.63 1.68 o 0 2 -6 4492.67 3863.38 29.61 o 1 2 -6 144.55 151.68 3.18 o 2 2 -6 3978.85 3902.07 32.50 o 3 2 -6 124.82 155.45 4.63 o 4 2 -6 767.74 765.76 17.83 o 5 2 -6 58.93 60.01 3.35 o 6 2 -6 39.76 47.95 3.80 o 7 2 -6 37.08 50.15 3.25 o 8 2 -6 19.72 12.29 2.38 o 0 3 -6 1020.28 1022.53 18.02 o 1 3 -6 1754.76 1820.96 17.63 o 2 3 -6 94.52 -3.35 3.35 o 3 3 -6 124.56 119.88 3.85 o 4 3 -6 63.49 70.46 3.62 o 5 3 -6 513.52 534.39 15.68 o 6 3 -6 140.58 137.21 4.72 o 7 3 -6 11.27 7.93 2.66 o 8 3 -6 3.46 3.03 3.30 o 0 4 -6 419.46 461.23 12.84 o 1 4 -6 67.08 67.15 2.39 o 2 4 -6 51.08 -4.77 4.77 o 3 4 -6 101.17 122.26 4.58 o 4 4 -6 12.20 8.34 3.12 o 5 4 -6 13.73 9.49 2.98 o 6 4 -6 46.92 37.50 2.93 o 7 4 -6 25.62 24.02 2.02 o 0 5 -6 103.82 121.35 4.31 o 1 5 -6 73.26 102.46 3.04 o 2 5 -6 43.44 17.79 2.52 o 3 5 -6 4.03 4.08 4.63 o 4 5 -6 11.49 9.49 2.25 o 5 5 -6 1.52 -1.10 3.99 o 0 6 -6 14.77 16.69 2.15 o 1 6 -6 13.08 7.58 1.59 o 2 6 -6 5.40 3.67 2.20 o 3 6 -6 0.74 -0.32 1.83 o 2 0 -5 1250.24 1278.06 13.80 o 4 0 -5 1714.18 1926.92 27.69 o 6 0 -5 475.09 466.50 13.71 o 8 0 -5 27.51 28.33 2.98 o 1 1 -5 1418.70 1321.13 31.60 o 2 1 -5 80.22 74.04 3.97 o 3 1 -5 1003.21 1149.84 34.15 o 4 1 -5 1157.29 1430.41 32.43 o 5 1 -5 901.86 959.46 15.09 o 6 1 -5 6.93 5.80 2.52 o 7 1 -5 176.46 189.65 8.57 o 8 1 -5 10.92 15.01 1.71 o 9 1 -5 7.50 7.93 1.17 o 1 2 -5 243.05 219.77 4.28 o 2 2 -5 785.73 828.20 14.26 o 3 2 -5 554.65 711.62 14.62 o 4 2 -5 978.37 1208.29 22.05 o 5 2 -5 209.11 280.01 8.44 o 6 2 -5 250.90 239.39 7.11 o 7 2 -5 38.00 40.80 3.30 o 8 2 -5 88.48 96.27 3.67 o 1 3 -5 1005.50 1207.70 29.50 o 2 3 -5 5.33 3.25 3.58 o 3 3 -5 222.58 267.63 8.34 o 4 3 -5 262.81 344.33 10.41 o 5 3 -5 237.67 273.87 8.85 o 6 3 -5 17.36 22.33 2.66 o 7 3 -5 148.58 137.12 4.54 o 8 3 -5 30.67 22.51 2.29 o 1 4 -5 93.42 113.33 2.79 o 2 4 -5 27.81 40.89 3.12 o 3 4 -5 157.84 195.57 6.05 o 4 4 -5 163.51 189.79 5.73 o 5 4 -5 14.42 15.08 2.52 o 6 4 -5 7.86 0.41 4.72 o 7 4 -5 2.08 -3.62 3.62 o 1 5 -5 115.68 111.38 3.20 o 2 5 -5 19.38 16.73 2.52 o 3 5 -5 2.89 7.70 2.57 o 4 5 -5 25.79 22.10 2.75 o 5 5 -5 10.10 9.63 1.83 o 1 6 -5 27.18 32.97 2.75 o 2 6 -5 0.00 -1.88 4.45 o 3 6 -5 30.51 28.33 2.52 o 0 0 -4 1995.79 1652.14 12.88 o 2 0 -4 13747.22 13429.23 58.08 o 4 0 -4 615.72 732.57 16.69 o 6 0 -4 24.73 31.82 2.93 o 8 0 -4 2.35 3.48 2.48 o 0 1 -4 1553.66 1368.82 37.91 o 1 1 -4 10520.97 9426.29 214.26 o 2 1 -4 3872.30 4360.92 160.31 o 3 1 -4 1389.64 1428.34 118.92 o 4 1 -4 418.19 448.18 21.96 o 5 1 -4 310.16 349.56 7.47 o 6 1 -4 4.40 4.18 2.55 o 7 1 -4 4.59 7.44 6.53 o 8 1 -4 13.76 11.82 1.73 o 9 1 -4 9.04 4.69 1.10 o 0 2 -4 13374.65 12331.74 59.60 o 1 2 -4 228.44 266.25 8.73 o 2 2 -4 1625.96 1670.16 19.71 o 3 2 -4 964.86 1242.67 19.02 o 4 2 -4 542.09 540.26 14.90 o 5 2 -4 223.37 256.54 7.84 o 6 2 -4 112.82 144.13 5.00 o 7 2 -4 15.68 7.84 1.70 o 8 2 -4 18.18 13.80 2.52 o 0 3 -4 393.39 366.61 10.54 o 1 3 -4 2366.71 2430.24 82.72 o 2 3 -4 122.64 147.34 4.36 o 3 3 -4 259.18 237.10 7.11 o 4 3 -4 59.90 45.57 3.16 o 5 3 -4 81.02 103.28 4.68 o 6 3 -4 35.26 44.47 3.25 o 7 3 -4 90.78 0.96 2.34 o 8 3 -4 6.01 4.17 1.79 o 0 4 -4 259.63 338.51 9.99 o 1 4 -4 92.06 93.68 3.44 o 2 4 -4 262.65 279.69 8.71 o 3 4 -4 134.47 139.50 4.45 o 4 4 -4 147.24 145.69 4.63 o 5 4 -4 11.97 18.34 2.57 o 6 4 -4 27.91 22.46 2.66 o 7 4 -4 1.02 -3.44 3.44 o 0 5 -4 278.01 278.73 8.34 o 1 5 -4 9.28 19.62 1.86 o 2 5 -4 106.46 112.59 4.54 o 3 5 -4 74.45 69.31 3.39 o 4 5 -4 11.75 15.36 2.34 o 5 5 -4 0.67 -3.76 3.76 o 6 5 -4 7.98 -1.60 4.03 o 0 6 -4 45.08 35.53 2.61 o 1 6 -4 7.60 10.20 5.55 o 2 6 -4 44.46 46.16 2.61 o 3 6 -4 43.81 37.13 2.57 o 2 0 -3 398.99 472.96 8.85 o 4 0 -3 3052.28 3227.90 35.02 o 6 0 -3 250.45 242.65 6.97 o 8 0 -3 73.02 56.07 3.48 o 1 1 -3 816.66 891.80 27.90 o 2 1 -3 3548.78 3911.76 143.99 o 3 1 -3 2884.13 3449.12 183.83 o 4 1 -3 1012.97 1299.71 17.51 o 5 1 -3 831.52 1016.16 51.16 o 6 1 -3 56.22 77.69 2.94 o 7 1 -3 166.48 158.93 13.25 o 8 1 -3 15.49 11.73 1.75 o 9 1 -3 5.64 6.35 1.12 o 1 2 -3 280.83 308.64 17.03 o 2 2 -3 1417.31 1750.15 19.99 o 3 2 -3 526.98 675.13 14.17 o 4 2 -3 2457.04 3144.84 35.62 o 5 2 -3 64.23 84.63 3.67 o 6 2 -3 440.65 514.59 15.68 o 7 2 -3 28.04 30.53 3.39 o 8 2 -3 4.45 8.62 2.15 o 1 3 -3 329.85 344.56 6.43 o 2 3 -3 61.10 70.83 2.75 o 3 3 -3 567.01 734.68 17.51 o 4 3 -3 59.69 59.00 3.16 o 5 3 -3 672.20 742.20 20.90 o 6 3 -3 90.91 123.13 4.95 o 7 3 -3 0.52 1.93 4.81 o 8 3 -3 8.50 2.15 3.99 o 1 4 -3 341.61 343.71 13.84 o 2 4 -3 52.32 77.75 3.44 o 3 4 -3 49.74 38.28 3.44 o 4 4 -3 42.59 46.44 3.62 o 5 4 -3 24.35 38.14 3.07 o 6 4 -3 51.62 59.55 3.16 o 7 4 -3 3.01 0.96 4.17 o 1 5 -3 153.22 179.15 4.05 o 2 5 -3 51.59 56.94 3.53 o 3 5 -3 14.12 11.64 2.93 o 4 5 -3 8.72 11.69 2.34 o 5 5 -3 0.15 1.93 1.93 o 6 5 -3 10.21 9.08 1.93 o 1 6 -3 44.76 51.50 3.16 o 2 6 -3 18.70 19.71 2.29 o 3 6 -3 4.24 5.55 1.60 o 0 0 -2 935.70 612.23 5.59 o 2 0 -2 19258.75 21218.47 87.93 o 4 0 -2 766.42 729.96 16.23 o 6 0 -2 273.72 251.08 7.47 o 8 0 -2 4.95 3.44 2.48 o 0 1 -2 176.00 186.90 12.88 o 1 1 -2 10675.87 10077.33 242.02 o 2 1 -2 1623.11 1715.12 65.03 o 3 1 -2 6175.33 7177.57 304.51 o 4 1 -2 48.01 49.17 1.84 o 5 1 -2 125.91 184.25 7.36 o 6 1 -2 15.60 14.62 2.13 o 7 1 -2 11.64 15.63 2.12 o 8 1 -2 7.30 10.62 1.56 o 9 1 -2 5.38 2.12 1.40 o 0 2 -2 6736.59 6693.73 38.28 o 1 2 -2 571.45 581.68 29.68 o 2 2 -2 6549.04 7016.38 43.64 o 3 2 -2 330.10 403.65 11.09 o 4 2 -2 251.82 283.59 8.53 o 5 2 -2 74.31 98.47 3.71 o 6 2 -2 79.49 91.14 4.54 o 7 2 -2 35.72 41.40 3.39 o 8 2 -2 6.33 10.59 2.20 o 0 3 -2 471.34 468.10 11.60 o 1 3 -2 1369.46 1390.19 71.45 o 2 3 -2 217.65 174.07 5.68 o 3 3 -2 1030.90 1148.69 21.45 o 4 3 -2 34.01 32.59 2.66 o 5 3 -2 11.32 19.99 3.16 o 6 3 -2 28.33 30.35 3.39 o 7 3 -2 13.48 16.09 2.43 o 8 3 -2 6.78 10.54 1.93 o 0 4 -2 459.40 491.30 13.11 o 1 4 -2 93.92 90.53 2.61 o 2 4 -2 223.92 228.67 6.88 o 3 4 -2 18.00 23.33 2.93 o 4 4 -2 33.10 41.99 3.62 o 5 4 -2 51.46 59.14 3.67 o 6 4 -2 8.03 9.21 2.29 o 7 4 -2 13.18 9.12 1.97 o 0 5 -2 144.30 143.44 4.63 o 1 5 -2 178.69 185.24 5.64 o 2 5 -2 41.49 53.22 3.53 o 3 5 -2 6.15 11.23 2.43 o 4 5 -2 0.70 4.22 2.34 o 5 5 -2 0.54 3.53 1.97 o 6 5 -2 0.93 2.20 1.65 o 0 6 -2 41.17 46.26 3.03 o 1 6 -2 45.50 49.03 2.09 o 2 6 -2 4.74 4.17 1.93 o 3 6 -2 15.77 19.16 2.29 o 4 6 -2 1.37 -0.50 3.12 o 2 0 -1 19179.58 22921.54 93.29 o 4 0 -1 2364.16 2962.79 33.42 o 6 0 -1 1133.68 1110.73 26.59 o 8 0 -1 41.57 37.55 2.93 o 1 1 -1 13149.42 13000.61 279.20 o 2 1 -1 3254.46 3654.30 114.70 o 3 1 -1 5313.75 6803.36 116.12 o 4 1 -1 869.09 1182.53 29.02 o 5 1 -1 1345.83 1642.10 74.84 o 6 1 -1 22.01 22.88 4.84 o 7 1 -1 111.64 112.41 11.62 o 8 1 -1 4.15 -1.97 3.48 o 9 1 -1 15.91 14.40 1.13 o 1 2 -1 185.37 173.79 13.13 o 2 2 -1 1341.66 1641.09 18.80 o 3 2 -1 101.05 129.87 3.99 o 4 2 -1 979.43 1205.67 21.45 o 5 2 -1 6.42 14.90 2.80 o 6 2 -1 191.34 222.57 6.28 o 7 2 -1 2.44 -1.15 5.09 o 8 2 -1 16.43 16.60 2.25 o 1 3 -1 262.09 275.62 10.34 o 2 3 -1 129.73 141.11 4.17 o 3 3 -1 548.19 636.12 16.09 o 4 3 -1 196.83 235.45 6.65 o 5 3 -1 52.87 57.35 3.71 o 6 3 -1 9.67 11.92 2.84 o 7 3 -1 41.88 37.73 2.93 o 8 3 -1 4.59 6.88 1.97 o 1 4 -1 40.97 38.62 1.99 o 2 4 -1 216.43 258.37 7.24 o 3 4 -1 322.23 350.84 10.13 o 4 4 -1 177.92 187.22 5.18 o 5 4 -1 36.31 56.20 3.12 o 6 4 -1 25.23 24.25 2.80 o 7 4 -1 2.81 1.65 3.94 o 1 5 -1 49.25 48.40 3.19 o 2 5 -1 21.12 29.52 2.98 o 3 5 -1 58.44 79.17 3.90 o 4 5 -1 59.10 66.43 3.30 o 5 5 -1 41.90 36.40 2.75 o 6 5 -1 2.91 3.07 1.70 o 1 6 -1 15.21 18.53 1.86 o 2 6 -1 15.74 19.85 2.29 o 3 6 -1 4.05 6.97 1.65 o 4 6 -1 0.17 1.60 2.89 o 2 0 0 212.26 309.72 7.66 o 4 0 0 1258.39 1412.61 22.88 o 6 0 0 21.30 29.06 3.35 o 8 0 0 213.20 131.39 4.36 o 0 1 0 1096.40 1207.46 12.74 o 1 1 0 21281.87 19369.44 551.40 o 2 1 0 1015.69 1134.28 17.01 o 3 1 0 526.36 552.95 17.44 o 4 1 0 41.63 75.36 3.46 o 5 1 0 415.75 530.80 30.78 o 6 1 0 2.33 0.67 3.63 o 7 1 0 98.74 82.28 6.74 o 8 1 0 0.36 0.56 4.13 o 9 1 0 0.55 -0.28 1.24 o 0 2 0 2140.48 2424.18 20.63 o 1 2 0 531.65 534.00 18.59 o 2 2 0 1115.06 954.41 14.26 o 3 2 0 740.61 905.58 16.14 o 4 2 0 421.46 561.58 14.90 o 5 2 0 302.07 380.68 11.32 o 6 2 0 3.29 15.45 3.44 o 7 2 0 7.69 -1.70 6.23 o 8 2 0 1.25 3.16 4.49 o 0 3 0 5.85 5.82 1.51 o 1 3 0 1659.07 1605.08 54.78 o 2 3 0 376.26 388.57 11.32 o 3 3 0 230.26 228.44 6.92 o 4 3 0 27.30 30.85 2.70 o 5 3 0 4.51 15.59 2.70 o 6 3 0 12.69 16.69 2.89 o 7 3 0 3.63 8.85 2.48 o 8 3 0 0.88 4.31 1.65 o 0 4 0 1005.96 1011.21 20.58 o 1 4 0 77.54 71.59 4.33 o 2 4 0 556.19 533.75 15.82 o 3 4 0 265.87 295.32 8.44 o 4 4 0 7.84 9.95 2.61 o 5 4 0 186.26 188.83 5.78 o 6 4 0 3.60 2.38 2.38 o 7 4 0 0.08 -3.94 3.94 o 0 5 0 25.23 18.15 3.03 o 1 5 0 208.61 193.89 7.29 o 2 5 0 125.85 124.65 4.49 o 3 5 0 40.55 41.26 3.44 o 4 5 0 6.86 11.00 2.29 o 5 5 0 6.13 6.01 2.02 o 6 5 0 0.05 -3.71 3.71 o 0 6 0 89.87 97.19 3.85 o 1 6 0 2.75 4.04 4.38 o 2 6 0 4.24 6.10 1.93 o 3 6 0 1.89 3.03 1.70 o 4 6 0 6.76 2.66 2.93 o 2 0 1 19845.13 21518.10 209.23 o 4 0 1 2282.19 2671.51 31.54 o 6 0 1 1208.71 1118.20 26.50 o 8 0 1 34.06 26.68 2.38 o 1 1 1 13647.14 13726.88 174.59 o 2 1 1 3317.47 3729.04 17.83 o 3 1 1 5045.66 6192.47 238.80 o 4 1 1 834.21 1126.87 61.13 o 5 1 1 1341.66 1573.74 149.93 o 6 1 1 24.32 25.93 3.74 o 7 1 1 131.07 127.12 10.75 o 8 1 1 4.27 4.62 2.27 o 9 1 1 13.74 9.53 1.12 o 1 2 1 186.00 179.75 5.87 o 2 2 1 1330.35 1641.92 19.07 o 3 2 1 81.65 99.66 2.84 o 4 2 1 851.00 999.10 19.67 o 5 2 1 5.16 12.88 2.89 o 6 2 1 187.56 208.04 6.28 o 7 2 1 2.22 6.88 2.84 o 8 2 1 16.20 17.47 2.25 o 1 3 1 242.05 257.52 5.51 o 2 3 1 126.04 148.62 4.81 o 3 3 1 567.61 675.36 16.50 o 4 3 1 200.52 241.96 6.78 o 5 3 1 48.24 70.28 3.80 o 6 3 1 7.72 15.08 2.89 o 7 3 1 36.63 31.31 2.93 o 8 3 1 4.50 6.28 1.97 o 1 4 1 36.50 35.05 1.98 o 2 4 1 227.56 275.01 8.57 o 3 4 1 339.37 363.31 10.86 o 4 4 1 186.61 200.01 5.78 o 5 4 1 35.46 54.05 3.71 o 6 4 1 27.56 25.31 2.89 o 7 4 1 2.60 6.60 1.97 o 1 5 1 52.20 54.98 2.50 o 2 5 1 17.98 18.02 3.03 o 3 5 1 58.63 81.33 3.94 o 4 5 1 62.72 64.23 3.25 o 5 5 1 43.28 42.54 2.84 o 6 5 1 2.41 2.57 2.84 o 1 6 1 14.44 17.26 1.77 o 2 6 1 15.52 17.97 2.29 o 3 6 1 3.32 -2.02 4.03 o 4 6 1 0.28 0.28 2.93 o 0 0 2 1330.19 841.72 6.60 o 2 0 2 19911.73 19637.66 82.52 o 4 0 2 819.71 675.18 16.09 o 6 0 2 272.06 226.92 7.11 o 8 0 2 3.14 4.22 1.88 o 0 1 2 159.75 158.06 13.25 o 1 1 2 11252.92 10771.08 131.20 o 2 1 2 1592.22 1685.52 15.01 o 3 1 2 5933.74 6652.23 298.46 o 4 1 2 48.30 54.62 1.88 o 5 1 2 140.92 177.40 23.79 o 6 1 2 14.51 22.37 6.65 o 7 1 2 14.02 12.44 4.70 o 8 1 2 6.68 9.41 4.93 o 9 1 2 6.02 3.51 1.37 o 0 2 2 6751.42 6876.00 39.15 o 1 2 2 519.95 554.24 7.10 o 2 2 2 6405.93 6761.76 42.73 o 3 2 2 341.63 390.40 10.77 o 4 2 2 200.15 218.90 7.24 o 5 2 2 77.61 103.10 3.85 o 6 2 2 80.78 96.00 4.58 o 7 2 2 34.55 34.66 3.48 o 8 2 2 6.10 6.19 2.20 o 0 3 2 480.97 456.23 11.23 o 1 3 2 1340.01 1344.27 34.57 o 2 3 2 232.64 192.50 5.46 o 3 3 2 1017.67 1083.91 20.68 o 4 3 2 34.01 34.70 2.75 o 5 3 2 8.53 43.32 3.80 o 6 3 2 28.93 36.58 3.48 o 7 3 2 12.94 10.73 2.43 o 8 3 2 7.20 5.18 1.93 o 0 4 2 484.76 499.74 12.88 o 1 4 2 104.36 105.25 4.79 o 2 4 2 245.67 250.44 8.21 o 3 4 2 20.18 20.90 2.38 o 4 4 2 26.96 32.64 3.16 o 5 4 2 52.80 51.67 3.76 o 6 4 2 7.59 13.80 2.38 o 7 4 2 11.87 10.27 1.97 o 0 5 2 130.80 125.79 4.49 o 1 5 2 194.03 200.82 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10 82.99 84.18 5.55 o 5 1 10 118.91 109.72 3.12 o 6 1 10 22.20 18.12 1.98 o 7 1 10 33.34 31.91 2.17 o 8 1 10 4.02 2.63 2.87 o 0 2 10 6815.05 5893.27 43.00 o 1 2 10 118.18 76.16 2.13 o 2 2 10 1216.13 1021.11 19.02 o 3 2 10 14.02 16.87 2.02 o 4 2 10 374.88 402.46 12.01 o 5 2 10 1.01 -3.48 5.23 o 6 2 10 7.27 5.50 6.74 o 7 2 10 73.63 72.62 4.03 o 8 2 10 8.84 4.54 1.83 o 0 3 10 246.46 210.42 6.69 o 1 3 10 789.11 726.00 20.72 o 2 3 10 206.08 160.68 4.58 o 3 3 10 390.01 354.83 10.31 o 4 3 10 20.15 10.31 3.44 o 5 3 10 43.53 38.78 3.71 o 6 3 10 8.53 9.90 2.75 o 7 3 10 15.24 12.65 2.29 o 0 4 10 225.36 237.65 6.56 o 1 4 10 69.22 52.94 4.86 o 2 4 10 120.02 107.23 4.17 o 3 4 10 15.80 14.67 2.25 o 4 4 10 90.00 66.43 4.08 o 5 4 10 14.00 9.67 2.70 o 6 4 10 0.76 -1.60 3.99 o 0 5 10 19.95 18.52 2.52 o 1 5 10 60.28 55.87 2.46 o 2 5 10 1.24 4.08 4.63 o 3 5 10 15.04 13.29 2.48 o 4 5 10 1.17 2.61 2.20 o 5 5 10 5.45 0.64 1.93 o 0 6 10 28.51 26.41 2.43 o 1 6 10 1.93 1.62 2.18 o 2 6 10 1.90 2.20 3.80 o 2 0 11 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19 0.63 0.57 2.66 o 2 5 19 4.17 0.60 3.67 o 0 0 20 3695.33 3601.57 44.47 o 2 0 20 1172.90 1111.51 23.70 o 4 0 20 230.78 248.19 7.52 o 6 0 20 15.48 13.94 2.25 o 0 1 20 704.13 732.01 14.39 o 1 1 20 1711.19 1648.22 33.89 o 2 1 20 205.61 212.37 4.41 o 3 1 20 562.03 527.14 10.64 o 4 1 20 4.14 1.43 1.82 o 5 1 20 22.37 25.64 1.94 o 6 1 20 8.86 10.57 1.72 o 7 1 20 0.53 0.80 1.94 o 0 2 20 1378.25 1219.79 28.06 o 1 2 20 56.29 51.79 4.63 o 2 2 20 372.12 385.08 11.69 o 3 2 20 41.10 42.59 3.44 o 4 2 20 138.14 130.93 4.81 o 5 2 20 33.21 32.69 3.07 o 6 2 20 8.14 9.76 1.88 o 0 3 20 267.58 252.87 7.24 o 1 3 20 241.05 223.49 18.09 o 2 3 20 4.76 3.58 5.36 o 3 3 20 265.40 276.94 8.80 o 4 3 20 1.72 1.42 5.13 o 5 3 20 60.11 53.82 2.80 o 0 4 20 108.72 116.21 4.72 o 1 4 20 97.45 83.30 4.88 o 2 4 20 76.38 73.44 3.85 o 3 4 20 6.93 7.79 2.06 o 4 4 20 20.17 17.97 2.15 o 0 5 20 10.17 9.31 1.93 o 1 5 20 23.73 28.36 1.63 o 2 5 20 7.93 9.58 1.83 o 2 0 21 882.63 829.35 21.04 o 4 0 21 470.23 479.61 14.30 o 6 0 21 215.08 233.75 7.20 o 1 1 21 27.16 36.11 4.72 o 2 1 21 27.88 33.68 2.17 o 3 1 21 489.85 544.04 11.03 o 4 1 21 11.86 12.12 1.75 o 5 1 21 272.68 276.25 5.97 o 6 1 21 5.85 8.54 1.27 o 1 2 21 267.26 253.49 11.60 o 2 2 21 13.03 14.03 2.93 o 3 2 21 31.11 28.51 3.35 o 4 2 21 225.12 233.62 7.01 o 5 2 21 11.22 14.03 2.43 o 6 2 21 13.06 19.21 1.93 o 1 3 21 73.11 67.19 9.33 o 2 3 21 38.94 44.83 3.39 o 3 3 21 140.32 158.34 5.13 o 4 3 21 38.29 34.15 2.93 o 5 3 21 11.31 13.29 1.79 o 1 4 21 0.71 -1.78 3.60 o 2 4 21 8.15 16.14 2.61 o 3 4 21 51.93 50.29 3.25 o 4 4 21 52.35 47.36 2.34 o 0 0 22 1765.47 1742.45 31.82 o 2 0 22 1349.57 1393.26 27.55 o 4 0 22 285.68 284.14 8.11 o 6 0 22 8.48 4.31 1.83 o 0 1 22 87.85 92.21 2.97 o 1 1 22 854.32 851.93 16.53 o 2 1 22 45.43 43.35 2.18 o 3 1 22 793.30 773.43 14.84 o 4 1 22 6.64 9.49 1.68 o 5 1 22 8.04 12.07 1.70 o 6 1 22 16.99 16.53 1.95 o 0 2 22 604.16 659.13 18.20 o 1 2 22 27.52 24.30 2.11 o 2 2 22 459.55 468.79 13.75 o 3 2 22 2.72 -0.55 5.36 o 4 2 22 83.97 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107.00 122.42 4.65 o 1 1 24 1042.46 1094.31 15.79 o 2 1 24 122.29 119.30 3.00 o 3 1 24 89.38 87.55 2.66 o 4 1 24 9.31 9.81 1.51 o 5 1 24 166.01 173.95 5.48 o 0 2 24 773.25 764.02 21.91 o 1 2 24 39.52 43.38 6.35 o 2 2 24 316.02 328.97 9.86 o 3 2 24 11.25 12.84 2.29 o 4 2 24 58.44 69.45 2.98 o 5 2 24 6.83 7.56 1.60 o 0 3 24 11.23 9.67 2.57 o 1 3 24 206.35 218.17 8.78 o 2 3 24 14.74 15.40 2.66 o 3 3 24 87.09 106.40 3.67 o 4 3 24 0.02 0.83 3.30 o 0 4 24 47.89 54.64 2.75 o 1 4 24 0.80 -0.44 1.76 o 2 4 24 9.02 10.77 1.65 o 2 0 25 26.33 36.22 2.89 o 4 0 25 594.04 631.44 16.69 o 1 1 25 16.64 18.77 2.36 o 2 1 25 34.35 36.87 2.02 o 3 1 25 282.30 310.93 6.67 o 4 1 25 33.08 33.52 1.86 o 5 1 25 60.99 62.55 1.89 o 1 2 25 17.92 18.42 1.92 o 2 2 25 107.45 118.41 4.26 o 3 2 25 32.87 33.33 2.89 o 4 2 25 103.91 114.97 3.62 o 5 2 25 13.98 13.94 1.79 o 1 3 25 31.46 33.57 3.46 o 2 3 25 2.85 3.48 3.48 o 3 3 25 51.19 67.16 3.12 o 4 3 25 2.65 2.48 1.56 o 1 4 25 19.74 20.15 1.44 o 0 0 26 524.90 554.84 15.45 o 2 0 26 653.79 647.40 18.25 o 4 0 26 62.21 71.74 3.12 o 0 1 26 55.87 56.79 2.40 o 1 1 26 605.96 616.09 16.18 o 2 1 26 18.92 22.71 1.72 o 3 1 26 218.82 230.28 6.67 o 4 1 26 0.31 1.79 2.66 o 5 1 26 6.73 9.98 2.15 o 0 2 26 340.40 333.65 9.95 o 1 2 26 11.43 16.75 1.74 o 2 2 26 303.14 361.15 11.51 o 3 2 26 10.48 14.81 2.15 o 4 2 26 36.10 30.62 2.25 o 0 3 26 18.76 20.72 2.38 o 1 3 26 150.24 166.44 7.86 o 2 3 26 4.63 3.58 1.65 o 3 3 26 49.23 47.31 2.57 o 2 0 27 115.26 127.86 4.22 o 4 0 27 198.84 196.76 5.73 o 1 1 27 83.77 94.00 2.01 o 2 1 27 2.51 1.55 2.75 o 3 1 27 176.95 176.32 3.55 o 4 1 27 6.95 5.77 4.58 o 1 2 27 2.12 4.04 3.80 o 2 2 27 86.84 106.22 3.71 o 3 2 27 16.31 14.21 2.15 o 4 2 27 104.67 102.14 3.44 o 1 3 27 28.76 36.39 1.83 o 2 3 27 15.59 17.97 1.88 o 0 0 28 847.49 903.89 21.36 o 2 0 28 273.60 258.46 7.56 o 4 0 28 37.46 45.71 2.29 o 0 1 28 27.95 25.91 1.83 o 1 1 28 509.93 529.52 7.64 o 2 1 28 4.49 3.85 3.23 o 3 1 28 137.36 150.65 4.63 o 4 1 28 2.44 4.39 1.08 o 0 2 28 381.87 425.15 12.10 o 1 2 28 9.92 13.43 1.60 o 2 2 28 184.22 185.80 5.68 o 3 2 28 0.59 -2.57 3.58 o 0 3 28 24.66 20.63 2.15 o 1 3 28 114.48 117.78 2.66 o 2 0 29 244.18 239.21 7.56 o 1 1 29 36.53 37.07 1.26 o 2 1 29 5.89 6.30 1.34 o 3 1 29 141.90 146.47 2.97 o 1 2 29 3.27 4.33 2.61 o 2 2 29 54.02 58.63 2.61 o 0 0 30 641.24 636.81 15.13 o 2 0 30 268.08 286.47 8.66 o 0 1 30 7.20 11.15 1.30 o 1 1 30 329.42 346.33 4.90 o 2 1 30 1.18 2.63 1.40 o 0 2 30 274.40 270.34 8.16 o 1 2 30 5.31 5.51 3.00 o 2 0 31 70.39 75.32 2.52 o 1 1 31 10.49 9.95 0.85 o 0 0 32 304.31 349.87 9.86 o