#------------------------------------------------------------------------------ #$Date: 2016-04-03 01:48:51 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181100 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/80/2218045.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2218045_Fobs loop_ _publ_author_name 'Xu, Mao-Liang' 'Zhou, Rui' 'Wang, Ge-Yang' 'Ng, Seik Weng' _publ_section_title ; Poly[di-\m~5~-adipato-\k^4^O:O':O'':O''',O'''-\m~4~-adipato-\k^4^O:O':O'':O'''-bis[2-phenyl-1H-1,3,7,8-tetraazacyclopenta[l]phenanthrene-\k^2^N^7^,N^8^]tricobalt(II)] ; _journal_coeditor_code BH2161 _journal_issue 5 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m710 _journal_page_last m711 _journal_volume 64 _journal_year 2008 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 69.482 _cell_angle_beta 83.233 _cell_angle_gamma 87.340 _cell_length_a 8.1496 _cell_length_b 15.8962 _cell_length_c 20.4736 _exptl_crystal_F_000 1234.00 _reflns_d_resolution_high 0.7700 _cod_data_source_file bh2161Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 520.91 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 17762.71 16971.29 213.01 o 3 0 0 177.79 173.23 28.90 o 4 0 0 10.32 9.12 44.61 o 5 0 0 146.00 155.66 48.31 o 6 0 0 28.82 105.31 50.05 o 7 0 0 198.83 235.48 67.39 o 8 0 0 8.12 33.83 52.95 o 9 0 0 2.48 146.23 81.37 o 10 0 0 0.99 -48.93 157.85 o -10 1 0 181.68 364.62 185.97 o -9 1 0 563.30 637.94 116.10 o -8 1 0 151.45 105.83 126.12 o -7 1 0 59.91 43.37 55.04 o -6 1 0 2.38 -26.48 96.52 o -5 1 0 213.54 220.10 40.02 o -4 1 0 57.97 37.74 30.49 o -3 1 0 6647.36 6986.05 93.56 o -2 1 0 11.37 10.69 23.53 o 2 1 0 1286.68 1366.26 61.27 o 3 1 0 4687.31 4478.50 126.47 o 4 1 0 183.48 274.97 57.21 o 5 1 0 333.97 331.33 42.66 o 6 1 0 189.02 154.08 45.46 o 7 1 0 2462.83 2514.74 95.17 o 8 1 0 172.06 124.54 53.48 o 9 1 0 479.14 405.80 85.22 o 10 1 0 2.92 -11.43 94.14 o -10 2 0 547.44 570.51 220.91 o -9 2 0 508.55 421.04 71.75 o -8 2 0 2090.79 1945.13 197.02 o -7 2 0 113.18 32.54 86.89 o -6 2 0 792.45 847.20 96.76 o -5 2 0 208.42 501.35 101.01 o -4 2 0 151.48 142.67 25.35 o -3 2 0 0.09 -5.52 38.42 o -2 2 0 5383.34 4877.94 139.29 o -1 2 0 3.00 36.60 27.59 o 1 2 0 1127.67 1032.75 57.09 o 2 2 0 28642.74 28023.45 564.20 o 3 2 0 1310.72 1365.11 47.73 o 4 2 0 199.44 213.23 38.21 o 5 2 0 340.30 346.53 51.35 o 6 2 0 135.98 103.93 58.81 o 7 2 0 9.44 -41.86 41.86 o 8 2 0 768.46 788.51 64.52 o 9 2 0 70.41 137.18 84.34 o 10 2 0 21.79 -12.59 171.20 o -10 3 0 254.81 88.93 78.19 o -9 3 0 1337.27 1277.13 347.16 o -8 3 0 152.57 87.85 106.99 o -7 3 0 1937.98 1934.72 91.38 o -6 3 0 520.95 487.42 113.54 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70.38 o 9 4 0 73.64 112.75 121.18 o -10 5 0 27.22 186.00 86.37 o -9 5 0 246.39 281.35 92.53 o -8 5 0 64.74 25.90 41.63 o -7 5 0 1661.64 2112.99 76.44 o -6 5 0 78.52 84.08 37.17 o -5 5 0 9576.97 10505.54 403.63 o -4 5 0 11.83 16.10 33.82 o -3 5 0 1082.43 1011.49 49.32 o -2 5 0 2.51 32.73 40.96 o -1 5 0 97.83 107.00 46.17 o 0 5 0 693.36 708.05 72.02 o 1 5 0 619.78 728.73 58.66 o 2 5 0 105.82 85.78 50.92 o 3 5 0 456.68 493.66 61.19 o 4 5 0 761.38 758.54 83.40 o 5 5 0 4304.96 4501.90 169.51 o 6 5 0 436.95 700.29 144.90 o 7 5 0 1597.95 2075.67 98.95 o 8 5 0 1130.31 1400.73 96.08 o 9 5 0 28.19 53.51 75.58 o 10 5 0 248.78 187.74 78.94 o -9 6 0 21.33 -113.34 202.80 o -8 6 0 123.61 102.25 83.20 o -7 6 0 62.43 -7.64 60.49 o -6 6 0 1471.21 1733.60 306.06 o -5 6 0 198.34 238.47 29.82 o -4 6 0 2342.72 2405.31 176.92 o -3 6 0 97.99 66.33 43.99 o -2 6 0 5009.84 4576.26 124.38 o -1 6 0 130.26 97.89 56.65 o 0 6 0 7401.76 8504.56 214.53 o 1 6 0 660.34 719.78 57.84 o 2 6 0 300.38 191.30 80.02 o 3 6 0 602.33 559.80 54.85 o 4 6 0 109.43 102.80 85.11 o 5 6 0 2001.19 1992.88 101.59 o 6 6 0 123.85 136.37 56.71 o 7 6 0 2099.80 2210.68 107.19 o 8 6 0 327.55 447.30 73.28 o 9 6 0 683.93 610.17 76.98 o 10 6 0 0.45 -47.52 132.67 o -9 7 0 0.57 148.18 195.22 o -8 7 0 3.62 50.73 87.81 o -7 7 0 1194.25 1442.01 317.75 o -6 7 0 0.08 100.76 82.26 o -5 7 0 4925.27 5209.62 397.57 o -4 7 0 8.84 4.08 29.07 o -3 7 0 3195.28 3358.84 74.24 o -2 7 0 464.78 520.59 61.46 o -1 7 0 1881.72 1720.23 113.41 o 0 7 0 26.57 54.88 63.13 o 1 7 0 3761.91 4144.31 185.70 o 2 7 0 94.57 114.22 56.99 o 3 7 0 1846.72 1821.06 98.77 o 4 7 0 0.25 37.72 40.78 o 5 7 0 356.25 374.82 72.73 o 6 7 0 551.87 558.39 88.82 o 7 7 0 663.76 644.66 74.03 o 8 7 0 1112.55 1214.29 106.00 o 9 7 0 44.28 58.71 196.59 o -9 8 0 0.10 9.34 94.09 o -8 8 0 122.50 215.20 146.93 o -7 8 0 22.27 25.21 83.23 o -6 8 0 11.84 43.58 75.01 o -5 8 0 8.30 -48.03 48.03 o -4 8 0 843.37 1111.21 185.27 o -3 8 0 90.38 73.80 39.37 o -2 8 0 5492.45 5608.13 234.22 o -1 8 0 2686.62 2207.14 96.07 o 0 8 0 239.05 217.76 78.22 o 1 8 0 61.65 99.96 60.27 o 2 8 0 4332.34 4399.28 130.78 o 3 8 0 461.98 377.89 60.03 o 4 8 0 5.20 35.31 44.33 o 5 8 0 236.73 230.11 55.74 o 6 8 0 1413.24 1492.32 116.58 o 7 8 0 1315.22 1411.68 207.14 o 8 8 0 57.25 138.36 72.69 o 9 8 0 499.27 636.00 97.87 o -9 9 0 165.77 117.30 106.24 o -8 9 0 0.09 -177.70 218.02 o -7 9 0 20.46 4.42 77.15 o -6 9 0 11.40 84.88 64.77 o -5 9 0 148.19 243.02 71.99 o -4 9 0 13.10 8.90 36.99 o -3 9 0 1278.01 1042.63 163.68 o -2 9 0 1037.10 1103.37 85.36 o -1 9 0 1807.91 1656.42 91.79 o 0 9 0 1328.32 1320.91 140.98 o 1 9 0 830.71 892.14 126.74 o 2 9 0 43.42 -26.34 61.63 o 3 9 0 25.00 20.11 64.60 o 4 9 0 632.43 583.06 87.44 o 5 9 0 2433.33 2517.03 146.61 o 6 9 0 147.24 60.16 65.52 o 7 9 0 78.48 81.68 176.92 o 8 9 0 383.35 327.65 70.96 o 9 9 0 37.58 -80.92 80.92 o -8 10 0 48.52 27.59 75.03 o -7 10 0 8.38 112.00 115.27 o -6 10 0 57.40 39.17 168.89 o -5 10 0 16.90 47.87 42.25 o -4 10 0 393.25 444.76 68.46 o -3 10 0 346.11 398.02 156.82 o -2 10 0 1802.98 1989.56 151.17 o -1 10 0 2608.69 2324.53 140.56 o 0 10 0 6955.43 6878.80 398.47 o 1 10 0 1220.97 1081.43 104.30 o 2 10 0 2029.48 2004.33 180.81 o 3 10 0 167.19 131.80 164.37 o 4 10 0 492.42 515.58 76.59 o 5 10 0 144.16 60.36 60.52 o 6 10 0 549.19 571.86 95.20 o 7 10 0 47.06 68.59 112.89 o 8 10 0 1.08 130.53 95.45 o 9 10 0 23.53 46.73 78.59 o -8 11 0 0.00 232.68 203.82 o -7 11 0 42.02 33.89 90.68 o -6 11 0 7.11 -113.41 113.41 o -5 11 0 25.12 -50.60 102.88 o -4 11 0 96.98 93.34 26.01 o -3 11 0 232.06 311.22 81.46 o -2 11 0 1382.49 1562.23 196.18 o -1 11 0 3725.05 3430.25 243.93 o 0 11 0 836.47 945.87 91.88 o 1 11 0 2947.20 3110.43 168.40 o 2 11 0 2814.59 3012.94 271.38 o 3 11 0 2317.59 2309.22 136.76 o 4 11 0 306.73 334.76 63.59 o 5 11 0 180.83 190.76 69.94 o 6 11 0 250.72 251.38 73.90 o 7 11 0 23.20 -25.29 83.68 o 8 11 0 5.98 -31.56 76.81 o -8 12 0 121.17 264.42 177.05 o -7 12 0 15.74 -46.70 96.81 o -6 12 0 176.70 -4.88 111.87 o -5 12 0 93.79 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1 101.43 71.55 53.52 o 1 -14 1 155.65 101.30 49.57 o 2 -14 1 30.46 1.68 57.79 o 3 -14 1 24.36 36.46 59.52 o 4 -14 1 1.58 5.65 115.21 o 5 -14 1 35.59 104.55 226.81 o 6 -14 1 4.20 17.72 133.70 o 7 -14 1 83.55 -38.08 108.71 o -7 -13 1 68.68 30.19 67.64 o -6 -13 1 307.00 470.51 149.38 o -5 -13 1 17.25 -69.37 72.23 o -4 -13 1 492.84 422.62 83.27 o -3 -13 1 579.76 546.15 73.12 o -2 -13 1 393.05 360.22 70.13 o -1 -13 1 830.61 1056.64 90.27 o 0 -13 1 125.96 51.33 87.30 o 1 -13 1 291.87 91.61 115.72 o 2 -13 1 181.28 57.52 67.51 o 3 -13 1 2.38 -14.10 32.82 o 4 -13 1 1.42 131.52 210.25 o 5 -13 1 0.79 -32.37 117.13 o 6 -13 1 25.81 57.02 222.19 o 7 -13 1 0.85 26.67 110.84 o -8 -12 1 8.01 -37.58 93.86 o -7 -12 1 66.20 257.52 95.87 o -6 -12 1 281.49 297.07 72.38 o -5 -12 1 270.62 201.57 84.72 o -4 -12 1 226.44 202.04 69.54 o -3 -12 1 167.36 89.64 63.09 o -2 -12 1 1330.08 1488.33 132.86 o -1 -12 1 1876.41 1602.17 434.87 o 0 -12 1 1056.21 1089.40 192.20 o 1 -12 1 166.50 121.09 75.85 o 2 -12 1 42.74 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