#------------------------------------------------------------------------------ #$Date: 2009-05-05 17:46:52 +0300 (Tue, 05 May 2009) $ #$Revision: 697 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2218080.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2218080_Fobs loop_ _publ_author_name 'Wong, Richard Chee Seng' 'Ooi, Mei Lee' 'Ng, Seik Weng' _publ_section_title ; (\m-4-Methylbenzenethiolato-\k^2^S:S)bis[carbonyl(\h^5^-cyclopentadienyl)molybdenum(II)] ; _journal_coeditor_code CI2579 _journal_issue 5 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m695 _journal_volume 64 _journal_year 2008 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 104.901 _cell_angle_gamma 90.000 _cell_length_a 13.2452 _cell_length_b 10.1347 _cell_length_c 18.0418 _exptl_crystal_F_000 1248.00 _reflns_d_resolution_high 0.7696 _[local]_cod_data_source_file ci2579Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' P21/n' _shelx_refln_list_code 4 _shelx_F_calc_maximum 402.91 _shelx_F_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 91076.16 92575.19 1348.77 o 4 0 0 76206.38 75903.74 884.74 o 6 0 0 16068.73 16129.39 285.88 o 8 0 0 18825.52 18638.08 919.14 o 10 0 0 2.57 -38.38 61.38 o 12 0 0 16.10 -19.64 113.87 o 14 0 0 269.76 505.78 201.04 o 16 0 0 68.83 558.49 228.43 o 1 1 0 108135.41 116911.48 815.44 o 2 1 0 13374.75 13333.67 119.77 o 3 1 0 31649.02 31194.46 264.85 o 4 1 0 6889.16 6675.13 112.29 o 5 1 0 30656.66 30220.35 299.95 o 6 1 0 6579.64 6118.50 119.30 o 7 1 0 11488.94 11451.77 169.92 o 8 1 0 11642.26 11651.74 182.70 o 9 1 0 776.04 831.85 62.81 o 10 1 0 2112.34 2286.93 124.21 o 11 1 0 88.74 13.32 62.12 o 12 1 0 633.68 562.89 120.97 o 13 1 0 30.59 150.28 106.55 o 14 1 0 4.01 0.68 117.06 o 15 1 0 291.48 389.65 136.77 o 16 1 0 177.68 62.67 124.94 o 0 2 0 7538.88 8231.82 214.47 o 1 2 0 22165.60 22895.22 297.73 o 2 2 0 1999.97 2350.51 53.81 o 3 2 0 12186.73 11505.86 143.07 o 4 2 0 6945.07 6932.20 114.18 o 5 2 0 14182.32 13179.08 216.33 o 6 2 0 418.29 354.11 53.65 o 7 2 0 11978.02 10968.50 217.92 o 8 2 0 3499.11 3435.22 135.51 o 9 2 0 6956.83 6914.49 192.67 o 10 2 0 251.16 79.91 77.80 o 11 2 0 3181.36 3714.41 167.61 o 12 2 0 181.05 187.49 80.28 o 13 2 0 84.95 107.26 100.40 o 14 2 0 266.34 203.88 120.27 o 15 2 0 106.17 -36.26 108.48 o 16 2 0 69.45 150.09 131.90 o 1 3 0 144.14 267.07 39.93 o 2 3 0 331.83 214.10 44.78 o 3 3 0 17782.86 17432.77 196.62 o 4 3 0 18488.70 18596.64 215.79 o 5 3 0 3199.04 3236.40 86.71 o 6 3 0 9533.51 8704.62 190.13 o 7 3 0 913.88 769.06 87.43 o 8 3 0 8690.67 8828.71 213.37 o 9 3 0 184.24 288.98 69.17 o 10 3 0 880.50 1090.64 146.74 o 11 3 0 79.86 -9.13 63.10 o 12 3 0 1962.28 2243.19 148.46 o 13 3 0 773.82 859.52 320.94 o 14 3 0 9.12 50.95 105.69 o 15 3 0 0.24 -23.71 119.12 o 16 3 0 811.11 340.65 150.33 o 0 4 0 27524.30 26687.40 586.92 o 1 4 0 93.02 37.88 31.17 o 2 4 0 74019.16 75097.20 885.58 o 3 4 0 3656.27 3966.71 127.72 o 4 4 0 29763.15 29751.16 374.74 o 5 4 0 377.93 381.03 50.05 o 6 4 0 12748.86 12125.12 212.27 o 7 4 0 384.20 522.02 124.06 o 8 4 0 1201.91 1207.58 99.12 o 9 4 0 359.36 332.21 77.58 o 10 4 0 2742.90 2260.06 158.17 o 11 4 0 167.28 94.90 75.63 o 12 4 0 781.04 774.63 157.72 o 13 4 0 119.40 62.21 90.52 o 14 4 0 343.09 418.09 138.20 o 15 4 0 806.45 717.84 327.31 o 1 5 0 72362.49 73460.21 746.28 o 2 5 0 63.22 -29.98 98.71 o 3 5 0 58277.71 58637.57 535.37 o 4 5 0 2931.87 2685.36 88.48 o 5 5 0 9149.27 8721.22 166.86 o 6 5 0 3500.92 3323.78 98.75 o 7 5 0 3826.17 3938.29 155.59 o 8 5 0 1312.20 1350.15 110.48 o 9 5 0 253.49 170.98 74.69 o 10 5 0 1636.25 1551.61 151.33 o 11 5 0 0.67 48.94 78.32 o 12 5 0 4243.63 4322.98 207.95 o 13 5 0 1128.21 1240.27 244.06 o 14 5 0 221.43 363.59 142.31 o 15 5 0 250.22 307.35 152.96 o 0 6 0 8373.18 8102.62 335.75 o 1 6 0 892.99 820.59 68.16 o 2 6 0 17611.41 17312.80 262.96 o 3 6 0 2710.99 2644.64 93.86 o 4 6 0 4174.37 3745.73 97.51 o 5 6 0 8876.85 8048.41 211.48 o 6 6 0 1864.76 2066.49 130.37 o 7 6 0 6632.20 6828.90 260.28 o 8 6 0 72.87 168.91 83.22 o 9 6 0 5702.41 5625.90 205.60 o 10 6 0 113.76 57.94 78.77 o 11 6 0 5022.26 4934.33 212.78 o 12 6 0 820.07 753.92 122.23 o 13 6 0 440.74 601.35 124.51 o 14 6 0 102.63 102.79 113.91 o 1 7 0 187.30 139.39 52.51 o 2 7 0 4801.50 4464.17 136.95 o 3 7 0 5.27 -55.02 36.68 o 4 7 0 7716.88 7432.28 202.46 o 5 7 0 93.63 13.38 60.95 o 6 7 0 9836.46 10048.76 319.18 o 7 7 0 4.09 125.22 92.16 o 8 7 0 6475.80 6712.50 280.83 o 9 7 0 3.44 -102.92 85.55 o 10 7 0 5058.22 4889.14 483.38 o 11 7 0 20.30 52.62 89.97 o 12 7 0 542.09 583.68 121.78 o 13 7 0 72.50 142.45 111.13 o 14 7 0 16.64 94.41 115.82 o 0 8 0 11488.54 11787.77 297.42 o 1 8 0 495.94 558.40 111.11 o 2 8 0 5105.23 5019.59 225.77 o 3 8 0 4880.46 4678.52 177.97 o 4 8 0 6527.06 6809.64 209.11 o 5 8 0 4842.58 4556.06 282.99 o 6 8 0 2578.90 2374.71 186.59 o 7 8 0 3513.20 3816.23 229.27 o 8 8 0 159.77 318.45 125.03 o 9 8 0 1981.79 1970.99 195.31 o 10 8 0 505.54 540.07 148.00 o 11 8 0 745.13 696.32 161.21 o 12 8 0 111.75 -1.56 125.93 o 13 8 0 2.64 -162.70 127.25 o 1 9 0 19983.52 20185.42 365.24 o 2 9 0 26.25 9.19 95.48 o 3 9 0 7139.32 7906.72 241.60 o 4 9 0 12.97 -76.23 78.83 o 5 9 0 4237.17 4426.98 247.41 o 6 9 0 53.73 -8.93 92.17 o 7 9 0 895.77 706.24 145.84 o 8 9 0 217.62 302.00 124.81 o 9 9 0 16.47 79.90 116.74 o 10 9 0 0.62 -98.76 118.76 o 11 9 0 710.11 828.64 185.32 o 12 9 0 331.52 473.73 165.80 o 0 10 0 3781.46 4284.99 344.36 o 1 10 0 228.80 60.14 106.47 o 2 10 0 7518.18 8078.24 366.71 o 3 10 0 1026.77 976.98 120.60 o 4 10 0 1370.50 1271.64 255.82 o 5 10 0 2335.40 2402.62 208.09 o 6 10 0 418.02 364.61 240.40 o 7 10 0 2852.56 2742.42 731.36 o 8 10 0 232.00 -53.31 289.41 o 9 10 0 2872.78 2995.83 255.26 o 10 10 0 853.98 623.57 516.63 o 1 11 0 16.87 68.44 112.88 o 2 11 0 599.89 363.16 110.05 o 3 11 0 49.82 75.56 111.69 o 4 11 0 2507.42 2485.46 224.58 o 5 11 0 0.17 -66.06 109.23 o 6 11 0 3263.50 3308.82 271.49 o 7 11 0 585.02 398.99 155.43 o 8 11 0 2834.35 2694.83 253.61 o 9 11 0 656.74 417.75 227.39 o 0 12 0 1990.14 2276.69 316.80 o 1 12 0 178.47 142.10 133.61 o 2 12 0 2481.51 2570.38 194.85 o 3 12 0 1358.75 1123.52 189.35 o 4 12 0 1991.64 2447.53 237.32 o 5 12 0 3991.31 3935.10 289.21 o 6 12 0 936.69 866.98 188.21 o 1 13 0 5687.30 5863.37 282.52 o 2 13 0 205.25 101.44 203.36 o -15 0 1 4498.80 4262.77 389.67 o -13 0 1 6911.36 6386.66 407.93 o -11 0 1 8481.40 7864.56 339.11 o -9 0 1 12865.58 12967.45 295.46 o -7 0 1 527.12 441.89 73.90 o -5 0 1 398.53 473.52 65.98 o -3 0 1 291.14 194.55 50.73 o -1 0 1 32.82 -62.79 41.86 o 1 0 1 785.16 726.09 48.41 o 3 0 1 10558.30 10457.17 144.33 o 5 0 1 1875.51 1597.16 80.33 o 7 0 1 7422.15 7462.31 188.41 o 9 0 1 5081.85 4560.22 172.10 o 11 0 1 17724.60 17265.72 615.51 o 13 0 1 1520.53 986.06 214.13 o 15 0 1 805.93 504.57 217.23 o -16 1 1 1076.20 778.48 175.97 o -15 1 1 1027.84 1524.50 197.16 o -14 1 1 3525.27 2332.50 206.60 o -13 1 1 928.08 1250.14 162.82 o -12 1 1 2021.19 2084.99 177.17 o -11 1 1 218.31 245.52 74.25 o -10 1 1 6681.91 6835.23 197.95 o -9 1 1 1101.13 1152.73 71.87 o -8 1 1 4986.27 5153.13 128.48 o -7 1 1 15.52 286.59 72.45 o -6 1 1 2297.60 2504.23 93.08 o -4 1 1 431.92 465.54 38.96 o -3 1 1 4950.97 5714.87 88.72 o -2 1 1 490.41 501.85 25.10 o -1 1 1 734.04 884.46 37.37 o 0 1 1 267.19 275.91 18.86 o 1 1 1 1593.15 1748.37 28.29 o 2 1 1 193.15 223.52 22.11 o 3 1 1 5269.28 5461.34 91.54 o 4 1 1 2974.44 2862.18 74.02 o 5 1 1 284.75 284.33 36.50 o 6 1 1 6458.24 6210.89 146.38 o 7 1 1 405.42 471.17 53.19 o 8 1 1 6151.88 6035.23 126.01 o 9 1 1 227.91 142.28 42.89 o 10 1 1 5859.81 5887.54 235.00 o 11 1 1 1605.06 1514.08 258.66 o 12 1 1 3103.04 2730.44 201.63 o 13 1 1 3387.02 3746.53 241.48 o 14 1 1 525.85 68.86 111.84 o 15 1 1 1225.45 1353.03 190.51 o 16 1 1 377.10 142.36 132.79 o -16 2 1 2554.60 3379.82 270.97 o -15 2 1 375.37 338.50 136.33 o -14 2 1 1117.29 1341.84 178.64 o -13 2 1 442.14 511.52 134.24 o -12 2 1 166.42 292.04 85.57 o -11 2 1 270.78 324.85 82.71 o -10 2 1 127.57 188.93 67.37 o -9 2 1 1447.60 1553.79 137.85 o -8 2 1 2661.92 2901.54 94.60 o -7 2 1 3815.76 4379.21 106.72 o -6 2 1 4656.55 5193.69 107.45 o -5 2 1 317.34 577.52 104.13 o -4 2 1 5594.50 5804.10 127.78 o -3 2 1 947.92 1078.60 58.41 o -2 2 1 584.43 903.33 60.24 o -1 2 1 1567.61 1681.33 108.53 o 0 2 1 5.53 -45.60 33.59 o 1 2 1 572.17 625.52 39.61 o 2 2 1 595.46 845.88 33.58 o 3 2 1 3.74 28.34 22.85 o 4 2 1 4039.27 4337.89 115.62 o 5 2 1 183.75 261.82 36.36 o 6 2 1 734.37 881.01 63.75 o 7 2 1 893.28 950.80 78.34 o 8 2 1 510.87 395.51 81.50 o 9 2 1 525.14 569.77 169.38 o 10 2 1 336.80 333.62 73.38 o 11 2 1 988.77 827.05 98.47 o 12 2 1 2758.77 3291.23 224.12 o 13 2 1 52.56 -93.37 100.17 o 14 2 1 3726.05 3869.60 262.26 o 15 2 1 38.59 -71.14 111.60 o 16 2 1 3968.55 4179.17 472.53 o -16 3 1 48.28 -133.91 131.01 o -15 3 1 1210.78 1539.86 347.29 o -14 3 1 78.24 -127.96 99.64 o -13 3 1 629.61 787.85 169.09 o -12 3 1 813.18 838.48 144.85 o -11 3 1 455.90 311.69 80.81 o -10 3 1 403.26 508.01 86.28 o -9 3 1 546.66 604.40 82.58 o -8 3 1 297.45 328.30 69.22 o -7 3 1 4123.56 4163.74 141.65 o -6 3 1 2309.44 2573.56 110.45 o -5 3 1 3643.80 3975.53 308.36 o -4 3 1 1312.38 1637.83 79.89 o -3 3 1 1526.92 1782.30 98.22 o -2 3 1 3363.30 3675.51 123.43 o -1 3 1 2747.44 2877.39 160.04 o 0 3 1 31.18 8.19 33.03 o 1 3 1 4169.37 3927.94 182.60 o 2 3 1 0.39 -27.60 25.31 o 3 3 1 5962.81 6521.61 106.70 o 4 3 1 1586.02 1787.20 88.44 o 5 3 1 2201.06 2182.76 108.81 o 6 3 1 6470.20 6827.51 137.46 o 7 3 1 1876.28 1979.99 129.17 o 8 3 1 3028.56 3216.56 136.93 o 9 3 1 661.20 608.74 105.64 o 10 3 1 877.79 653.66 179.89 o 11 3 1 72.08 43.80 72.39 o 12 3 1 209.25 67.42 84.96 o 13 3 1 1415.40 1455.32 180.16 o 14 3 1 483.00 119.18 164.77 o 15 3 1 2787.31 2911.90 250.75 o -16 4 1 25.81 -46.15 130.60 o -15 4 1 718.90 196.86 133.06 o -14 4 1 357.79 123.80 113.25 o -13 4 1 2490.72 2621.88 303.12 o -12 4 1 211.47 183.32 87.16 o -11 4 1 4748.54 4359.83 185.87 o -10 4 1 80.87 28.89 64.47 o -9 4 1 1286.24 1341.81 108.61 o -8 4 1 43.41 -44.25 51.51 o -7 4 1 3005.37 2913.96 128.49 o -6 4 1 329.09 328.22 80.71 o -5 4 1 374.04 417.11 83.57 o -4 4 1 2033.36 2547.95 309.05 o -3 4 1 0.73 83.35 116.63 o -1 4 1 31.81 -62.71 63.57 o 0 4 1 172.59 163.60 152.20 o 1 4 1 130.96 137.40 67.99 o 2 4 1 2898.62 3559.54 401.89 o 3 4 1 2155.50 2401.46 73.40 o 4 4 1 1239.40 1186.54 71.11 o 5 4 1 7493.87 7259.04 138.50 o 6 4 1 3473.33 3048.96 147.42 o 7 4 1 8753.28 8663.56 169.19 o 8 4 1 1976.87 1921.64 199.41 o 9 4 1 5589.31 5521.48 189.16 o 10 4 1 324.40 328.40 83.12 o 11 4 1 2640.09 2142.16 192.91 o 12 4 1 45.01 24.62 102.60 o 13 4 1 4528.88 3832.78 254.81 o 14 4 1 327.10 261.45 132.60 o 15 4 1 733.87 358.63 177.78 o -15 5 1 933.47 1377.94 205.80 o -14 5 1 1626.68 1186.65 147.63 o -13 5 1 31.42 23.16 90.29 o -12 5 1 6407.63 6257.08 234.20 o -11 5 1 26.35 117.58 76.64 o -10 5 1 1935.57 1533.62 127.14 o -9 5 1 106.70 177.35 69.71 o -8 5 1 150.02 125.84 68.88 o -7 5 1 126.03 118.78 69.25 o -6 5 1 77.14 137.06 55.76 o -5 5 1 34.76 126.73 142.81 o -4 5 1 527.63 630.87 86.26 o -3 5 1 960.35 1469.06 117.60 o -2 5 1 825.07 757.55 62.51 o 0 5 1 522.92 407.13 55.40 o 1 5 1 12.51 -111.97 75.63 o 2 5 1 1075.67 1229.14 67.39 o 3 5 1 7467.81 7549.81 170.80 o 4 5 1 127.94 116.66 35.88 o 5 5 1 12.06 -42.91 44.09 o 6 5 1 1794.88 1924.07 84.92 o 7 5 1 4026.24 3964.15 138.15 o 8 5 1 2764.97 2859.17 144.26 o 9 5 1 225.95 285.71 81.64 o 10 5 1 3383.27 3236.01 167.80 o 11 5 1 2785.41 2834.29 169.53 o 12 5 1 2801.68 3045.44 348.16 o 13 5 1 691.75 759.04 129.00 o 14 5 1 2461.64 1945.29 218.98 o 15 5 1 1101.81 1325.52 208.63 o -14 6 1 861.95 1228.36 154.75 o -13 6 1 953.36 1092.23 142.89 o -12 6 1 668.78 842.69 126.76 o -11 6 1 732.78 720.88 117.49 o -10 6 1 15.23 27.36 73.63 o -9 6 1 5.44 179.70 75.09 o -8 6 1 54.56 220.50 86.79 o -7 6 1 105.18 79.36 84.75 o -6 6 1 270.91 347.18 90.30 o -5 6 1 412.51 452.15 96.21 o -4 6 1 956.75 1155.07 221.97 o -3 6 1 3954.41 3881.78 105.78 o -2 6 1 4503.72 4797.99 297.18 o -1 6 1 6502.79 6164.56 197.59 o 0 6 1 1251.40 1303.06 104.03 o 1 6 1 2965.26 3119.98 114.48 o 2 6 1 575.65 715.38 103.73 o 3 6 1 322.55 288.66 44.69 o 4 6 1 39.86 23.59 39.11 o 5 6 1 21.97 -11.71 35.82 o 6 6 1 739.74 515.44 104.07 o 7 6 1 653.63 692.21 205.46 o 8 6 1 1467.06 1444.24 142.51 o 9 6 1 1221.33 1203.22 183.26 o 10 6 1 2896.78 2842.50 168.45 o 11 6 1 629.25 557.01 108.42 o 12 6 1 3028.73 3283.38 208.11 o 13 6 1 507.50 416.65 117.98 o 14 6 1 3840.59 3816.38 282.22 o -14 7 1 42.73 -27.24 111.30 o -13 7 1 94.05 136.85 110.98 o -12 7 1 15.02 12.90 103.79 o -11 7 1 2.82 -87.01 101.06 o -10 7 1 0.28 -71.77 103.71 o -9 7 1 1533.73 1680.30 173.33 o -8 7 1 208.42 200.89 99.55 o -7 7 1 2218.54 2469.13 190.61 o -6 7 1 340.20 319.88 82.06 o -5 7 1 4803.89 5434.12 177.79 o -4 7 1 5609.95 6496.31 190.12 o -3 7 1 2095.91 2183.86 139.67 o -2 7 1 1346.24 1390.66 109.70 o -1 7 1 3505.06 3511.77 108.29 o 0 7 1 2088.45 2136.14 108.72 o 1 7 1 868.97 766.47 75.29 o 2 7 1 2939.57 3042.77 119.20 o 3 7 1 75.57 -28.44 38.16 o 4 7 1 945.36 1108.95 210.14 o 5 7 1 749.61 865.30 88.30 o 6 7 1 19.87 39.99 105.00 o 7 7 1 730.02 413.93 111.99 o 8 7 1 64.58 203.80 98.88 o 9 7 1 171.79 167.51 102.56 o 10 7 1 2.69 51.32 83.23 o 11 7 1 4015.32 4237.19 213.76 o 12 7 1 1.99 75.58 99.17 o 13 7 1 2846.46 2833.42 204.70 o -13 8 1 166.16 228.77 147.34 o -12 8 1 347.20 276.86 144.12 o -11 8 1 811.06 924.46 171.60 o -10 8 1 1562.02 1673.87 189.74 o -9 8 1 2102.08 1563.40 181.96 o -8 8 1 3728.27 4034.19 240.49 o -7 8 1 4.03 58.59 94.49 o -6 8 1 5452.14 5129.55 248.14 o -5 8 1 951.00 1011.19 108.77 o -4 8 1 2344.16 2585.54 142.53 o -3 8 1 600.77 976.55 165.84 o -2 8 1 1539.82 1538.42 145.25 o -1 8 1 516.28 516.29 62.47 o 0 8 1 133.08 257.57 54.47 o 1 8 1 500.10 590.04 78.18 o 2 8 1 502.36 521.08 74.16 o 3 8 1 2730.09 3117.59 152.80 o 4 8 1 1038.61 1265.66 109.48 o 5 8 1 2428.88 2897.85 277.44 o 6 8 1 665.26 405.92 124.12 o 7 8 1 3565.68 3550.16 290.62 o 8 8 1 366.38 150.32 109.35 o 9 8 1 1934.72 2013.73 227.82 o 10 8 1 304.18 390.49 134.21 o 11 8 1 570.46 342.76 258.57 o 12 8 1 1019.76 1312.81 242.81 o 13 8 1 353.89 150.13 145.98 o -12 9 1 1170.84 1095.43 195.47 o -11 9 1 417.91 477.61 159.42 o -10 9 1 1169.86 1005.92 178.72 o -9 9 1 471.16 492.99 288.72 o -8 9 1 439.49 630.06 177.87 o -7 9 1 765.98 566.26 131.30 o -6 9 1 1212.13 1028.61 154.55 o -5 9 1 1388.05 1377.04 122.99 o -4 9 1 299.57 265.41 84.63 o -3 9 1 169.49 245.40 87.53 o -2 9 1 871.05 827.53 132.97 o -1 9 1 210.98 242.25 85.36 o 0 9 1 4390.46 4362.71 172.95 o 1 9 1 289.48 456.74 122.28 o 2 9 1 546.99 377.83 113.18 o 3 9 1 194.92 196.35 82.44 o 4 9 1 231.90 231.49 81.62 o 5 9 1 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