#------------------------------------------------------------------------------ #$Date: 2009-05-03 21:56:13 +0300 (Sun, 03 May 2009) $ #$Revision: 691 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2218106.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2218106_Fobs loop_ _publ_author_name 'Koch, Christian' 'G\"orls, Helmar' 'Westerhausen, Matthias' _publ_section_title ; Bis[(2-pyridylmethyl)(triisopropylsilyl)amido]zinc(II)--toluene--tetrahydrofuran (4/2/1) ; _journal_coeditor_code FJ2104 _journal_issue 5 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m664 _journal_volume 64 _journal_year 2008 _space_group_IT_number 4 _symmetry_space_group_name_Hall 'P 2yb' _symmetry_space_group_name_H-M 'P 1 21 1' _cell_angle_alpha 90.000 _cell_angle_beta 91.018 _cell_angle_gamma 90.000 _cell_length_a 13.2410 _cell_length_b 17.6223 _cell_length_c 16.7978 _exptl_crystal_F_000 1420.00 _reflns_d_resolution_high 0.7700 _[local]_cod_data_source_file fj2104Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' p21 in P2(1)' _shelx_refln_list_code 4 _shelx_F_calc_maximum 220.62 _shelx_F_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 3 -22 0 160.33 238.67 84.69 o 4 -22 0 70.31 -46.19 80.84 o 1 -21 0 81.67 169.38 65.44 o 2 -21 0 693.59 854.58 123.18 o 3 -21 0 100.33 111.63 96.24 o 4 -21 0 343.20 511.98 134.73 o 5 -21 0 65.59 -80.84 80.84 o 6 -21 0 0.18 -55.15 65.65 o 0 -20 0 219.83 300.26 80.84 o 1 -20 0 105.27 132.81 38.11 o 2 -20 0 233.81 352.41 65.44 o 3 -20 0 389.56 192.47 76.99 o 4 -20 0 56.37 3.85 61.59 o 5 -20 0 5.66 69.29 73.14 o 6 -20 0 473.46 424.67 85.45 o 7 -20 0 31.71 125.22 71.79 o 8 -20 0 13.29 -13.33 175.15 o 1 -19 0 338.54 274.24 48.09 o 2 -19 0 642.03 675.20 56.39 o 3 -19 0 523.62 498.19 43.08 o 4 -19 0 177.30 196.32 73.14 o 5 -19 0 245.51 334.90 92.39 o 6 -19 0 50.38 88.54 84.69 o 7 -19 0 54.30 75.34 65.44 o 8 -19 0 161.73 120.58 113.56 o 9 -19 0 128.42 121.72 85.71 o 0 -18 0 381.69 319.50 65.44 o 1 -18 0 256.40 244.18 36.67 o 2 -18 0 54.92 21.81 34.65 o 3 -18 0 1608.38 1573.89 105.86 o 4 -18 0 27.17 -57.74 57.74 o 5 -18 0 134.65 -92.39 92.39 o 6 -18 0 189.60 123.18 80.84 o 7 -18 0 427.82 518.73 82.19 o 8 -18 0 10.95 -92.07 92.07 o 9 -18 0 407.72 521.95 96.60 o 10 -18 0 8.32 -103.59 165.53 o 1 -17 0 926.08 981.24 96.24 o 2 -17 0 591.89 579.65 51.50 o 3 -17 0 116.96 128.89 24.10 o 4 -17 0 375.44 334.90 73.14 o 5 -17 0 427.58 354.15 100.09 o 6 -17 0 142.40 265.61 111.63 o 7 -17 0 24.21 31.16 56.39 o 8 -17 0 268.94 374.66 93.17 o 9 -17 0 184.38 119.33 68.05 o 10 -17 0 172.10 100.23 71.17 o 11 -17 0 175.80 131.59 204.02 o 0 -16 0 1580.45 1355.01 100.09 o 1 -16 0 37.09 46.34 36.57 o 2 -16 0 448.36 547.23 55.82 o 3 -16 0 243.52 254.34 30.62 o 4 -16 0 813.81 896.92 115.48 o 5 -16 0 163.06 69.29 57.74 o 6 -16 0 1312.60 1412.75 146.28 o 7 -16 0 194.98 118.78 56.97 o 8 -16 0 90.89 68.07 59.70 o 9 -16 0 96.01 93.70 63.92 o 10 -16 0 390.63 458.77 89.33 o 11 -16 0 44.13 -21.17 73.49 o 12 -16 0 195.84 246.01 88.18 o 1 -15 0 205.85 252.12 36.95 o 2 -15 0 1678.05 1638.37 182.85 o 3 -15 0 718.61 827.31 98.16 o 4 -15 0 958.43 777.59 92.39 o 5 -15 0 26.99 84.69 61.59 o 6 -15 0 149.07 88.54 65.44 o 7 -15 0 381.26 416.67 80.84 o 8 -15 0 741.08 667.07 79.44 o 9 -15 0 763.87 693.70 309.88 o 10 -15 0 321.70 206.12 74.52 o 11 -15 0 10.37 -48.33 73.34 o 12 -15 0 509.62 618.70 144.35 o 0 -14 0 136.86 134.73 34.65 o 1 -14 0 684.63 645.04 94.31 o 2 -14 0 1915.51 1972.50 81.12 o 3 -14 0 2498.92 2371.01 91.86 o 4 -14 0 677.78 658.26 84.69 o 5 -14 0 457.64 461.93 84.69 o 6 -14 0 1159.28 1177.93 123.18 o 7 -14 0 157.49 110.42 51.50 o 8 -14 0 42.36 47.70 61.02 o 9 -14 0 831.83 841.55 138.58 o 10 -14 0 340.84 360.63 83.96 o 11 -14 0 87.34 16.53 78.91 o 12 -14 0 52.78 101.58 121.26 o 13 -14 0 286.56 331.00 96.37 o 1 -13 0 3416.63 3345.92 113.93 o 2 -13 0 90.44 80.84 25.62 o 3 -13 0 699.06 637.27 38.20 o 4 -13 0 418.84 485.03 69.29 o 5 -13 0 3015.20 3160.40 200.17 o 6 -13 0 22.40 46.19 57.74 o 7 -13 0 803.35 893.29 80.26 o 8 -13 0 105.30 148.59 67.40 o 9 -13 0 547.88 622.60 78.38 o 10 -13 0 195.07 219.14 80.84 o 11 -13 0 653.94 795.97 97.98 o 12 -13 0 383.91 512.63 105.74 o 13 -13 0 278.56 239.40 78.38 o 14 -13 0 3.14 -83.20 83.20 o 0 -12 0 1432.31 1189.48 76.99 o 1 -12 0 2515.69 2542.57 88.43 o 2 -12 0 129.72 79.42 32.72 o 3 -12 0 5284.46 5237.99 145.78 o 4 -12 0 1390.34 1401.20 115.48 o 5 -12 0 714.13 577.42 73.14 o 6 -12 0 173.20 220.42 86.61 o 7 -12 0 896.48 1202.64 84.38 o 8 -12 0 98.93 99.32 61.59 o 9 -12 0 809.53 703.46 180.92 o 10 -12 0 83.16 -3.22 94.31 o 11 -12 0 260.62 280.20 100.09 o 12 -12 0 647.99 509.03 88.18 o 13 -12 0 346.69 441.70 65.84 o 14 -12 0 121.59 77.16 93.17 o 1 -11 0 1252.68 1393.51 54.57 o 2 -11 0 7351.52 7574.30 202.12 o 3 -11 0 771.70 876.39 39.06 o 4 -11 0 5474.35 5662.54 261.76 o 5 -11 0 1045.83 1054.75 92.39 o 6 -11 0 738.57 726.83 121.26 o 7 -11 0 76.19 52.65 42.12 o 8 -11 0 1831.14 2132.22 136.66 o 9 -11 0 98.98 91.84 55.43 o 10 -11 0 1385.17 1562.77 110.01 o 11 -11 0 124.91 74.49 53.63 o 12 -11 0 47.67 -20.02 103.94 o 13 -11 0 9.47 -42.26 49.12 o 14 -11 0 364.55 483.37 94.80 o 15 -11 0 33.80 30.10 88.72 o 0 -10 0 12572.41 11898.64 419.59 o 1 -10 0 36.35 17.32 19.05 o 2 -10 0 1686.70 1971.43 113.56 o 3 -10 0 369.69 381.48 53.89 o 4 -10 0 3258.76 2960.23 157.83 o 5 -10 0 286.93 400.34 76.99 o 6 -10 0 2182.70 2081.14 188.62 o 7 -10 0 42.34 75.13 39.40 o 8 -10 0 281.83 339.10 165.53 o 9 -10 0 41.25 21.17 46.27 o 10 -10 0 1232.94 1344.73 96.60 o 11 -10 0 276.41 342.60 69.37 o 12 -10 0 446.78 344.19 55.42 o 13 -10 0 433.99 423.02 58.29 o 14 -10 0 15.85 -84.69 84.69 o 15 -10 0 69.05 17.93 88.74 o 1 -9 0 4184.23 3737.82 110.01 o 2 -9 0 2862.40 2615.41 78.94 o 3 -9 0 1361.60 1367.99 86.61 o 4 -9 0 1969.29 2163.39 115.48 o 5 -9 0 2817.16 2505.99 138.58 o 6 -9 0 169.90 98.16 38.11 o 7 -9 0 5946.00 6103.42 204.09 o 8 -9 0 1517.41 1418.95 142.43 o 9 -9 0 106.86 148.05 50.30 o 10 -9 0 1013.21 1121.33 115.48 o 11 -9 0 824.25 855.07 97.88 o 12 -9 0 553.98 488.15 52.63 o 13 -9 0 103.30 145.51 61.59 o 14 -9 0 209.16 113.01 82.76 o 15 -9 0 75.60 108.67 105.22 o 0 -8 0 3959.12 4130.46 165.53 o 1 -8 0 8262.10 8130.18 209.80 o 2 -8 0 1873.24 1852.69 58.23 o 3 -8 0 4463.58 3761.01 102.47 o 4 -8 0 135.87 150.13 42.34 o 5 -8 0 308.43 327.20 57.74 o 6 -8 0 1346.33 1485.59 125.11 o 7 -8 0 4873.46 4916.49 277.16 o 8 -8 0 771.41 837.20 98.16 o 9 -8 0 2470.97 2810.68 248.29 o 10 -8 0 822.47 1000.07 82.99 o 11 -8 0 133.12 139.80 41.94 o 12 -8 0 138.90 126.07 47.45 o 13 -8 0 1887.94 1983.20 113.75 o 14 -8 0 58.73 87.95 48.96 o 15 -8 0 378.61 255.88 159.75 o 16 -8 0 70.27 22.03 84.69 o 1 -7 0 10448.33 9608.54 244.57 o 2 -7 0 4183.82 4612.64 124.80 o 3 -7 0 7650.43 8628.18 213.35 o 4 -7 0 96.66 7.70 38.49 o 5 -7 0 6662.64 6785.17 190.30 o 6 -7 0 398.29 442.93 48.12 o 7 -7 0 2625.21 2651.74 179.00 o 8 -7 0 831.78 675.34 58.47 o 9 -7 0 25.23 -23.83 61.59 o 10 -7 0 211.36 182.20 30.62 o 11 -7 0 1933.99 2048.38 74.52 o 12 -7 0 73.72 129.70 34.15 o 13 -7 0 934.62 1010.12 62.43 o 14 -7 0 349.59 385.60 49.86 o 15 -7 0 6.40 -115.77 165.53 o 16 -7 0 71.76 7.70 123.18 o 0 -6 0 18217.15 18115.50 615.91 o 1 -6 0 11143.22 11685.03 291.21 o 2 -6 0 2741.16 3107.51 85.96 o 3 -6 0 1885.28 1820.79 100.09 o 4 -6 0 8084.35 7225.41 288.71 o 5 -6 0 1002.49 1044.74 55.75 o 6 -6 0 2172.66 2122.75 128.96 o 7 -6 0 4185.77 4360.05 112.43 o 8 -6 0 2177.29 2148.10 102.05 o 9 -6 0 707.78 701.95 48.20 o 10 -6 0 803.78 809.76 43.30 o 11 -6 0 279.93 256.70 65.44 o 12 -6 0 2161.30 2384.11 100.09 o 13 -6 0 85.70 24.17 33.94 o 14 -6 0 263.76 308.08 46.27 o 15 -6 0 144.88 106.09 67.37 o 16 -6 0 700.48 1100.94 173.23 o 1 -5 0 7618.17 7593.01 193.03 o 2 -5 0 11095.61 10740.42 261.81 o 3 -5 0 576.38 754.49 57.74 o 4 -5 0 9997.79 9763.46 243.60 o 5 -5 0 69.57 45.62 25.02 o 6 -5 0 3541.93 3173.44 81.02 o 7 -5 0 1751.14 1698.58 190.55 o 8 -5 0 4552.46 4344.56 161.68 o 9 -5 0 3280.15 3451.48 96.37 o 10 -5 0 508.86 517.34 46.19 o 11 -5 0 90.50 141.94 30.51 o 12 -5 0 285.94 345.56 61.59 o 13 -5 0 54.20 24.94 33.30 o 14 -5 0 1041.23 1201.22 107.78 o 15 -5 0 95.29 119.54 47.71 o 16 -5 0 102.66 38.49 165.53 o 0 -4 0 26557.68 26872.99 893.07 o 1 -4 0 5495.76 5780.20 146.31 o 2 -4 0 4021.05 4303.21 109.01 o 3 -4 0 4072.68 3772.46 161.68 o 4 -4 0 8704.27 8584.08 178.70 o 5 -4 0 4787.13 5345.61 118.83 o 6 -4 0 6732.11 6563.76 147.98 o 7 -4 0 2776.55 2903.08 83.28 o 8 -4 0 124.93 144.61 23.02 o 9 -4 0 2407.36 2326.30 67.89 o 10 -4 0 1078.10 1045.19 49.86 o 11 -4 0 832.97 785.33 67.37 o 12 -4 0 2103.29 2098.20 81.66 o 13 -4 0 564.81 602.09 53.40 o 14 -4 0 55.59 133.65 43.30 o 15 -4 0 31.78 68.62 65.44 o 16 -4 0 224.15 154.67 50.56 o 1 -3 0 6500.18 7152.59 174.79 o 2 -3 0 24516.95 24732.70 827.63 o 3 -3 0 4471.56 4176.20 92.55 o 4 -3 0 171.09 130.90 20.97 o 5 -3 0 14945.62 14856.81 296.95 o 6 -3 0 512.09 571.90 30.62 o 7 -3 0 6369.42 6199.48 348.37 o 8 -3 0 1139.97 1207.93 42.12 o 9 -3 0 4057.25 4097.76 108.88 o 10 -3 0 482.25 409.77 40.42 o 11 -3 0 2615.65 2548.32 125.11 o 12 -3 0 471.94 526.32 54.11 o 13 -3 0 177.88 172.53 94.31 o 14 -3 0 31.00 36.21 73.14 o 15 -3 0 108.23 200.04 51.25 o 16 -3 0 28.82 2.67 48.96 o 17 -3 0 335.44 400.34 146.28 o 1 -2 0 13409.99 17159.60 395.98 o 2 -2 0 4437.39 4852.99 101.82 o 3 -2 0 2642.63 2333.10 57.74 o 4 -2 0 2666.64 3140.88 109.71 o 5 -2 0 21.59 63.81 14.79 o 6 -2 0 1037.54 687.49 30.80 o 7 -2 0 3943.95 4183.60 91.16 o 8 -2 0 528.94 622.69 32.66 o 9 -2 0 6656.46 6856.29 155.08 o 10 -2 0 669.67 678.90 40.83 o 11 -2 0 747.89 777.39 54.11 o 12 -2 0 1267.06 1217.18 73.05 o 13 -2 0 927.96 888.36 66.59 o 14 -2 0 69.56 20.66 39.75 o 15 -2 0 50.80 155.77 52.99 o 16 -2 0 216.68 265.61 76.99 o 17 -2 0 65.07 -84.69 115.48 o 2 -1 0 6671.48 9103.94 307.96 o 3 -1 0 3578.52 3043.08 69.06 o 4 -1 0 7109.14 6943.98 126.55 o 5 -1 0 3221.84 3106.26 66.65 o 6 -1 0 4493.70 4455.37 91.16 o 7 -1 0 3631.83 3599.95 144.35 o 8 -1 0 1475.52 1554.74 48.12 o 9 -1 0 203.06 291.99 31.32 o 10 -1 0 149.83 204.71 46.19 o 11 -1 0 899.07 897.02 54.77 o 12 -1 0 212.44 212.65 38.44 o 13 -1 0 214.67 179.67 57.74 o 14 -1 0 1193.67 1250.63 150.13 o 15 -1 0 34.23 19.86 55.73 o 16 -1 0 232.60 157.83 73.14 o 17 -1 0 98.77 146.28 157.83 o 2 0 0 10613.33 6155.27 153.98 o 3 0 0 2329.21 1807.41 39.40 o 4 0 0 46.61 86.26 13.61 o 5 0 0 609.51 957.41 28.48 o 6 0 0 10886.71 12783.62 261.11 o 7 0 0 65.62 113.55 23.10 o 8 0 0 842.90 841.71 41.96 o 9 0 0 95.57 92.96 23.73 o 10 0 0 412.18 384.65 90.46 o 11 0 0 14.63 14.47 40.42 o 12 0 0 1978.25 1922.93 184.77 o 13 0 0 654.37 743.42 96.24 o 14 0 0 17.45 -76.99 76.99 o 15 0 0 133.31 44.96 119.33 o 16 0 0 513.94 392.64 84.69 o 17 0 0 6.73 19.25 138.58 o 2 1 0 6360.65 9165.54 223.27 o 3 1 0 3633.05 3001.00 155.90 o 4 1 0 6876.36 6774.32 146.61 o 5 1 0 3511.74 3485.91 84.73 o 6 1 0 4462.66 4444.26 109.13 o 7 1 0 3472.81 3728.32 221.34 o 8 1 0 1681.17 1858.21 65.29 o 9 1 0 171.97 153.93 28.59 o 10 1 0 100.41 75.11 59.67 o 11 1 0 915.61 904.94 54.73 o 12 1 0 174.43 180.02 80.84 o 13 1 0 171.15 121.70 47.02 o 14 1 0 1141.70 1206.99 83.67 o 15 1 0 54.94 -42.34 111.63 o 16 1 0 238.52 296.41 127.03 o 17 1 0 114.62 61.59 138.58 o 2 2 0 4195.16 4608.02 117.82 o 3 2 0 3175.04 2591.60 63.38 o 4 2 0 2638.62 3158.99 75.48 o 5 2 0 62.10 131.50 21.17 o 6 2 0 852.43 615.11 32.03 o 7 2 0 3933.64 4279.34 107.53 o 8 2 0 513.96 568.63 61.59 o 9 2 0 6467.65 6680.97 207.87 o 10 2 0 565.28 632.38 44.76 o 11 2 0 757.24 688.19 50.56 o 12 2 0 1377.37 1257.70 74.61 o 13 2 0 792.70 719.28 63.38 o 14 2 0 70.52 50.98 53.40 o 15 2 0 106.98 196.32 111.63 o 16 2 0 260.16 358.00 134.73 o 1 3 0 6311.42 6609.50 254.06 o 2 3 0 24035.32 26024.19 601.56 o 3 3 0 4356.22 4142.40 130.88 o 4 3 0 220.53 201.63 50.04 o 5 3 0 14950.44 14777.22 368.76 o 6 3 0 513.11 519.19 38.49 o 7 3 0 5681.99 5420.27 138.58 o 8 3 0 1048.00 1142.65 49.51 o 9 3 0 4040.85 4099.45 190.55 o 10 3 0 432.26 471.73 41.96 o 11 3 0 2804.57 2734.12 130.31 o 12 3 0 493.81 398.96 57.34 o 13 3 0 177.75 130.88 51.25 o 14 3 0 43.80 61.08 60.84 o 15 3 0 124.66 138.58 103.94 o 16 3 0 22.96 7.70 76.99 o 17 3 0 385.13 315.65 119.33 o 0 4 0 26100.96 25822.09 846.88 o 1 4 0 5954.45 6082.13 227.12 o 2 4 0 4336.14 4727.12 192.47 o 3 4 0 3260.86 2734.28 94.31 o 4 4 0 8376.68 8518.86 219.00 o 5 4 0 5058.27 5695.72 151.05 o 6 4 0 7677.97 7687.34 361.85 o 7 4 0 2581.77 2735.07 99.72 o 8 4 0 130.94 192.94 42.34 o 9 4 0 2667.75 2725.41 107.26 o 10 4 0 1246.65 1210.98 113.56 o 11 4 0 862.08 827.24 73.14 o 12 4 0 1872.32 1938.86 113.45 o 13 4 0 537.30 410.82 73.33 o 14 4 0 56.61 53.89 92.39 o 15 4 0 60.67 84.69 69.29 o 16 4 0 180.50 227.12 100.09 o 1 5 0 7771.46 8097.09 209.89 o 2 5 0 10589.07 10097.10 358.00 o 3 5 0 580.42 877.98 46.19 o 4 5 0 9696.81 9671.92 195.11 o 5 5 0 49.51 47.55 17.77 o 6 5 0 3526.90 3388.16 211.72 o 7 5 0 1777.56 1907.55 71.10 o 8 5 0 4714.52 4508.87 150.62 o 9 5 0 3280.56 3439.72 128.24 o 10 5 0 365.90 337.97 45.47 o 11 5 0 106.71 91.10 50.04 o 12 5 0 366.60 358.81 52.99 o 13 5 0 59.57 8.00 71.21 o 14 5 0 1150.22 1143.29 123.18 o 15 5 0 92.66 188.62 73.14 o 16 5 0 74.77 107.78 88.54 o 0 6 0 18911.18 19224.14 642.86 o 1 6 0 10648.76 11098.53 274.56 o 2 6 0 3161.69 3453.07 109.71 o 3 6 0 1720.30 1895.38 63.52 o 4 6 0 8289.87 7529.80 152.72 o 5 6 0 946.27 944.63 32.44 o 6 6 0 2390.94 2404.30 63.85 o 7 6 0 4347.08 4302.89 136.83 o 8 6 0 2324.66 2385.81 90.38 o 9 6 0 552.33 575.51 48.99 o 10 6 0 929.06 888.42 60.52 o 11 6 0 271.41 186.61 56.46 o 12 6 0 2219.37 2510.39 236.74 o 13 6 0 55.28 83.67 52.83 o 14 6 0 261.99 273.31 73.14 o 15 6 0 158.78 188.62 100.09 o 16 6 0 617.76 577.42 111.63 o 1 7 0 10471.28 9598.76 242.07 o 2 7 0 3761.56 4045.03 111.20 o 3 7 0 7803.97 8975.08 223.00 o 4 7 0 34.55 10.59 17.32 o 5 7 0 6361.87 6615.85 139.65 o 6 7 0 366.17 406.61 44.27 o 7 7 0 2817.47 3193.53 196.32 o 8 7 0 684.11 573.34 65.44 o 9 7 0 33.31 19.25 32.64 o 10 7 0 277.80 349.59 44.27 o 11 7 0 2140.96 2275.39 121.71 o 12 7 0 69.27 69.74 40.55 o 13 7 0 1003.78 1331.91 111.63 o 14 7 0 375.94 307.96 65.44 o 15 7 0 8.15 23.10 57.74 o 16 7 0 67.49 61.59 100.09 o 0 8 0 3908.39 3941.83 161.68 o 1 8 0 7730.68 7582.76 195.98 o 2 8 0 1864.12 1928.90 62.65 o 3 8 0 4667.08 4033.48 110.71 o 4 8 0 130.44 101.08 11.14 o 5 8 0 368.58 505.25 28.87 o 6 8 0 1360.88 1386.25 138.58 o 7 8 0 4606.41 4922.71 157.83 o 8 8 0 760.17 819.25 36.57 o 9 8 0 2412.61 2634.62 83.59 o 10 8 0 853.03 883.37 67.37 o 11 8 0 146.71 172.19 38.20 o 12 8 0 135.75 153.72 63.52 o 13 8 0 1772.21 1986.31 115.48 o 14 8 0 60.89 38.49 53.89 o 15 8 0 405.95 442.69 88.54 o 1 9 0 4196.92 3681.58 107.49 o 2 9 0 2973.68 2801.58 86.94 o 3 9 0 1379.15 1389.16 78.91 o 4 9 0 2070.07 2174.05 194.40 o 5 9 0 2710.02 2717.18 103.94 o 6 9 0 156.36 149.51 14.81 o 7 9 0 5743.61 5761.77 137.15 o 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