#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/81/2218122.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2218122_Fobs loop_ _publ_author_name 'Xia, Jin Hong' 'Liu, Zheng' 'Wang, Yuan' 'Feng, Xiao Zhen' _publ_section_title ; {2-[(3,5-Dichloro-2-oxidobenzylidene)amino-\k^2^N,O]-3-methylpentanoato-\kO}(N,N'-dimethylformamide-\kO)copper(II) ; _journal_coeditor_code GW2039 _journal_issue 5 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m660 _journal_page_last m661 _journal_volume 64 _journal_year 2008 _space_group_IT_number 18 _symmetry_space_group_name_Hall 'P 2 2ab' _symmetry_space_group_name_H-M 'P 21 21 2' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 11.6710 _cell_length_b 27.4650 _cell_length_c 5.8890 _exptl_crystal_F_000 900.00 _reflns_d_resolution_high 0.8406 _[local]_cod_data_source_file gw2039Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 061224e in P21212' _shelx_refln_list_code 4 _shelx_F_calc_maximum 175.83 _shelx_F_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, z' 'x+1/2, -y+1/2, -z' '-x+1/2, y+1/2, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 5162.17 4897.81 189.28 o 4 0 0 1456.43 1864.26 195.69 o 6 0 0 2113.34 2178.96 120.46 o 8 0 0 10841.81 9226.76 387.36 o 10 0 0 1.70 213.24 71.44 o 12 0 0 56.99 117.55 100.80 o 1 1 0 15049.48 13652.80 446.79 o 2 1 0 7886.56 7481.79 251.82 o 3 1 0 15394.89 13337.34 350.11 o 4 1 0 2250.91 2282.23 90.54 o 6 1 0 10340.56 9451.00 268.83 o 7 1 0 5612.43 4337.58 144.55 o 8 1 0 2112.76 2081.31 90.96 o 9 1 0 1064.60 1116.56 70.49 o 10 1 0 914.66 958.83 76.68 o 11 1 0 141.22 339.38 61.23 o 12 1 0 23.20 48.61 65.98 o 13 1 0 0.89 45.47 93.06 o 0 2 0 4775.56 4053.74 142.72 o 1 2 0 22550.85 19975.31 578.67 o 2 2 0 1814.94 2366.07 170.44 o 3 2 0 5752.55 4304.28 124.20 o 4 2 0 3027.30 3339.09 273.66 o 5 2 0 1843.39 1531.33 62.66 o 6 2 0 38.46 110.41 45.62 o 7 2 0 2655.02 2475.19 96.70 o 8 2 0 325.94 514.81 88.94 o 9 2 0 2918.67 2603.57 109.18 o 10 2 0 252.64 353.90 60.60 o 11 2 0 298.16 318.70 69.23 o 12 2 0 23.77 89.78 60.09 o 13 2 0 135.20 125.51 97.64 o 1 3 0 2289.32 2112.99 53.36 o 2 3 0 182.23 391.82 77.50 o 3 3 0 728.00 671.93 33.93 o 4 3 0 1034.67 1520.55 177.73 o 5 3 0 589.32 671.97 42.31 o 6 3 0 3234.45 2568.40 94.49 o 7 3 0 1072.55 995.66 59.57 o 8 3 0 619.11 901.47 70.98 o 9 3 0 1403.29 1132.95 71.18 o 10 3 0 722.82 812.34 76.50 o 11 3 0 40.99 193.56 60.25 o 12 3 0 197.65 334.16 72.28 o 13 3 0 4.97 42.93 92.48 o 0 4 0 30916.66 26135.93 748.41 o 1 4 0 479.96 598.65 88.93 o 2 4 0 338.11 295.07 49.23 o 3 4 0 2868.19 2183.82 71.82 o 4 4 0 1502.59 1948.75 98.68 o 5 4 0 59.99 249.03 48.78 o 6 4 0 132.52 393.99 214.75 o 7 4 0 96.50 139.59 35.70 o 8 4 0 1102.71 1083.57 74.68 o 9 4 0 16.51 24.76 36.36 o 10 4 0 432.95 531.29 64.13 o 11 4 0 501.43 338.51 69.37 o 12 4 0 313.18 346.23 97.39 o 13 4 0 85.75 -41.04 91.39 o 1 5 0 1754.77 1640.79 44.71 o 2 5 0 4026.33 3567.93 100.01 o 3 5 0 9828.92 8549.80 232.39 o 4 5 0 4487.07 4299.72 129.65 o 5 5 0 1538.28 1392.36 73.07 o 6 5 0 4299.00 4290.26 138.88 o 7 5 0 1873.53 1600.03 73.20 o 9 5 0 57.52 71.54 40.00 o 10 5 0 458.56 695.50 83.71 o 11 5 0 1630.75 1340.80 169.07 o 12 5 0 4.34 67.25 78.53 o 13 5 0 22.41 52.36 81.79 o 0 6 0 5263.36 5749.79 175.53 o 1 6 0 12357.21 10323.17 232.32 o 2 6 0 932.01 1190.73 76.26 o 3 6 0 2693.65 2643.69 155.85 o 4 6 0 41.88 165.25 37.41 o 5 6 0 5983.29 5339.45 161.20 o 6 6 0 185.47 382.99 69.16 o 7 6 0 1411.26 1242.34 63.75 o 8 6 0 1213.12 1491.16 74.86 o 9 6 0 1262.42 1377.21 75.95 o 10 6 0 860.41 1017.04 95.23 o 11 6 0 146.65 205.19 80.27 o 12 6 0 36.62 54.62 78.68 o 13 6 0 448.35 361.85 105.55 o 1 7 0 4990.33 4037.97 98.80 o 2 7 0 17997.19 15021.24 446.28 o 3 7 0 12168.36 9746.85 264.33 o 4 7 0 3882.36 3950.42 135.03 o 5 7 0 3152.06 3151.96 106.16 o 6 7 0 3602.57 2752.62 99.45 o 7 7 0 2308.96 1830.48 80.36 o 8 7 0 231.70 427.21 50.53 o 9 7 0 76.88 283.53 66.99 o 10 7 0 1151.27 1293.86 89.51 o 11 7 0 416.19 535.20 103.60 o 12 7 0 135.66 270.14 94.40 o 13 7 0 261.58 194.17 92.94 o 0 8 0 51.27 143.58 34.22 o 1 8 0 15232.95 13529.98 282.85 o 2 8 0 4102.98 3793.68 96.61 o 3 8 0 1.15 311.18 149.81 o 4 8 0 10977.81 9011.74 278.10 o 5 8 0 481.55 809.48 73.95 o 6 8 0 56.92 192.23 40.79 o 7 8 0 18.80 123.37 34.74 o 9 8 0 552.93 588.74 72.20 o 10 8 0 462.97 577.61 102.41 o 11 8 0 66.76 238.39 86.09 o 12 8 0 1176.91 962.49 194.87 o 13 8 0 72.21 229.62 99.60 o 1 9 0 513.41 862.08 107.41 o 2 9 0 1228.06 1342.91 53.77 o 3 9 0 1848.65 1501.51 50.35 o 4 9 0 3557.86 3698.37 126.00 o 5 9 0 946.11 1064.66 143.36 o 6 9 0 1545.41 1505.52 69.19 o 7 9 0 2293.83 2171.62 103.29 o 8 9 0 44.98 160.22 45.16 o 9 9 0 439.46 542.63 94.71 o 10 9 0 97.83 158.56 74.82 o 11 9 0 1030.98 1340.12 183.15 o 12 9 0 16.11 71.68 78.89 o 13 9 0 2.87 -7.32 158.01 o 0 10 0 895.64 1115.87 56.49 o 2 10 0 1357.51 1572.75 51.06 o 3 10 0 3598.60 2912.90 81.95 o 4 10 0 297.10 786.44 132.49 o 5 10 0 2000.67 1951.21 78.51 o 6 10 0 1611.44 1253.26 63.78 o 7 10 0 492.16 644.87 112.59 o 8 10 0 2424.63 1866.59 87.73 o 9 10 0 938.16 1046.24 123.04 o 10 10 0 410.58 411.22 93.50 o 11 10 0 314.33 386.01 97.73 o 12 10 0 102.59 111.29 84.70 o 13 10 0 434.96 458.15 119.41 o 2 11 0 6275.62 5082.60 128.15 o 3 11 0 1358.32 1684.12 56.71 o 4 11 0 1117.29 1352.38 92.75 o 5 11 0 950.98 706.20 43.52 o 6 11 0 785.39 891.16 89.42 o 7 11 0 375.82 571.88 90.46 o 8 11 0 290.76 298.67 74.42 o 9 11 0 1007.31 1206.48 122.74 o 10 11 0 2228.05 1620.96 131.59 o 11 11 0 255.04 275.86 89.68 o 12 11 0 203.62 127.06 86.67 o 13 11 0 208.68 166.92 95.18 o 0 12 0 4341.50 3908.72 134.92 o 1 12 0 2947.42 2842.58 74.29 o 2 12 0 348.80 460.75 57.08 o 4 12 0 4473.36 4185.11 129.02 o 5 12 0 865.94 723.97 51.63 o 6 12 0 771.78 895.79 46.81 o 7 12 0 136.32 240.88 44.33 o 8 12 0 1995.84 1542.93 119.29 o 9 12 0 705.31 613.65 103.41 o 10 12 0 14.50 49.48 69.21 o 11 12 0 29.53 127.89 77.51 o 12 12 0 334.30 492.36 121.99 o 1 13 0 1404.31 1435.33 48.48 o 3 13 0 1026.14 1128.64 53.47 o 4 13 0 6.45 198.68 86.55 o 5 13 0 2269.83 2231.49 77.17 o 6 13 0 64.47 241.51 74.61 o 7 13 0 5824.56 4876.14 260.55 o 8 13 0 47.31 241.70 73.54 o 9 13 0 4.49 87.07 62.68 o 10 13 0 171.52 174.05 79.17 o 11 13 0 423.66 530.01 111.05 o 12 13 0 36.04 -3.09 82.77 o 0 14 0 4276.61 3806.69 136.00 o 1 14 0 1337.54 1433.13 65.89 o 2 14 0 236.96 442.03 41.43 o 3 14 0 589.91 679.47 66.70 o 4 14 0 6987.65 5610.79 166.48 o 5 14 0 2263.09 2334.11 79.82 o 6 14 0 52.64 217.33 39.86 o 7 14 0 819.20 1010.97 112.03 o 8 14 0 117.55 327.01 80.13 o 9 14 0 59.28 110.02 70.52 o 10 14 0 341.80 252.70 88.05 o 11 14 0 405.78 347.08 99.52 o 12 14 0 291.18 136.88 92.14 o 1 15 0 637.11 810.46 39.56 o 2 15 0 2010.90 1511.59 55.55 o 3 15 0 2859.45 2704.33 98.79 o 4 15 0 1742.73 1656.00 104.33 o 5 15 0 758.08 613.04 47.53 o 6 15 0 188.54 224.60 40.84 o 7 15 0 3136.49 2550.19 156.35 o 8 15 0 0.93 146.31 66.13 o 9 15 0 11.62 41.25 64.23 o 10 15 0 602.97 601.10 112.84 o 11 15 0 92.61 143.41 84.88 o 12 15 0 99.47 93.77 85.73 o 0 16 0 758.40 750.39 53.03 o 1 16 0 113.01 264.16 58.01 o 2 16 0 3231.19 3306.10 96.50 o 3 16 0 360.46 555.87 49.71 o 4 16 0 2565.67 2299.76 88.03 o 5 16 0 112.78 230.98 49.41 o 6 16 0 852.34 884.90 85.45 o 7 16 0 370.19 334.89 78.30 o 8 16 0 276.20 397.43 130.66 o 9 16 0 57.59 47.77 65.68 o 10 16 0 28.95 58.92 72.09 o 11 16 0 0.04 62.01 75.11 o 12 16 0 242.90 216.85 100.07 o 1 17 0 43.17 155.11 28.95 o 2 17 0 88.46 261.80 49.46 o 3 17 0 1730.96 1348.75 55.67 o 5 17 0 2251.08 2023.51 95.31 o 6 17 0 36.25 316.29 104.61 o 7 17 0 305.00 749.56 103.88 o 8 17 0 17.39 37.69 59.85 o 9 17 0 257.90 130.53 74.95 o 10 17 0 54.18 -30.72 68.42 o 11 17 0 1014.06 720.50 131.29 o 0 18 0 471.24 529.00 54.83 o 1 18 0 1423.70 1435.74 53.04 o 2 18 0 111.35 281.86 33.75 o 3 18 0 631.53 778.31 45.79 o 4 18 0 3752.60 2968.55 107.18 o 5 18 0 736.86 936.02 75.64 o 6 18 0 489.99 526.26 89.35 o 7 18 0 153.41 196.35 75.09 o 8 18 0 333.04 385.09 88.71 o 9 18 0 2.29 35.22 82.59 o 10 18 0 257.60 309.55 98.18 o 11 18 0 69.87 66.05 83.98 o 2 19 0 4472.54 4013.37 139.33 o 3 19 0 493.94 613.42 47.67 o 4 19 0 740.92 1004.79 58.78 o 5 19 0 67.21 187.53 41.18 o 6 19 0 1373.04 1101.72 122.37 o 7 19 0 18.39 13.07 56.04 o 8 19 0 91.44 63.05 68.68 o 9 19 0 7.60 -9.65 65.52 o 10 19 0 412.05 596.36 123.87 o 11 19 0 4.81 95.99 85.01 o 0 20 0 17.59 357.78 104.50 o 1 20 0 777.13 878.09 43.48 o 3 20 0 1784.59 1360.42 60.20 o 4 20 0 2188.51 1712.50 79.00 o 5 20 0 520.73 541.36 89.43 o 6 20 0 3.91 61.50 66.18 o 7 20 0 389.14 249.54 77.84 o 8 20 0 4.19 144.14 73.89 o 9 20 0 310.86 290.00 95.96 o 10 20 0 78.51 204.70 93.57 o 1 21 0 1602.48 1127.78 50.09 o 2 21 0 0.23 54.89 28.22 o 3 21 0 489.20 704.23 54.08 o 4 21 0 367.15 399.14 51.67 o 5 21 0 272.22 345.35 79.09 o 6 21 0 249.17 282.32 77.65 o 7 21 0 1312.99 1266.52 141.62 o 8 21 0 199.95 285.65 87.47 o 9 21 0 42.15 69.42 79.15 o 10 21 0 7.57 -0.47 73.80 o 0 22 0 4360.04 3319.24 138.92 o 1 22 0 1442.04 1373.89 62.12 o 2 22 0 234.03 315.63 41.58 o 3 22 0 134.98 181.21 37.03 o 4 22 0 21.60 126.10 40.22 o 5 22 0 283.77 207.50 69.60 o 6 22 0 231.49 250.39 84.06 o 7 22 0 21.81 93.82 71.32 o 8 22 0 649.11 361.83 134.59 o 9 22 0 30.99 36.18 73.37 o 10 22 0 3.37 2.03 78.29 o 2 23 0 2129.61 1703.92 72.00 o 3 23 0 132.70 174.62 36.75 o 4 23 0 128.21 163.73 54.65 o 5 23 0 541.65 720.61 223.66 o 6 23 0 989.63 855.18 129.36 o 7 23 0 64.22 40.65 68.66 o 8 23 0 103.97 201.91 84.89 o 9 23 0 3.98 32.63 91.81 o 0 24 0 262.48 573.50 68.57 o 1 24 0 532.18 647.02 55.27 o 2 24 0 253.18 380.60 47.15 o 3 24 0 1030.47 1105.30 62.12 o 4 24 0 600.50 407.04 93.44 o 5 24 0 767.17 636.00 108.84 o 6 24 0 5.66 26.73 67.73 o 7 24 0 147.67 141.19 81.21 o 8 24 0 483.95 523.48 112.21 o 9 24 0 424.20 454.78 117.37 o 1 25 0 2581.52 1718.27 74.96 o 2 25 0 55.71 5.66 32.62 o 3 25 0 409.11 593.76 57.22 o 4 25 0 4.34 73.87 65.23 o 5 25 0 80.45 144.74 77.82 o 6 25 0 777.20 1024.56 136.26 o 7 25 0 1426.03 1567.05 168.25 o 8 25 0 262.90 268.70 103.48 o 0 26 0 4605.01 3473.39 178.22 o 1 26 0 442.41 521.30 53.57 o 2 26 0 90.14 106.95 37.57 o 3 26 0 146.95 167.83 47.17 o 4 26 0 421.16 447.76 119.44 o 5 26 0 42.91 49.44 74.51 o 6 26 0 62.13 143.00 80.46 o 7 26 0 3.28 33.30 93.58 o 8 26 0 365.11 304.39 102.04 o 1 27 0 9.31 178.08 44.35 o 2 27 0 1143.93 896.03 69.47 o 3 27 0 453.45 749.39 118.18 o 4 27 0 0.04 86.61 80.40 o 5 27 0 2.84 117.43 79.79 o 6 27 0 938.37 957.58 141.62 o 7 27 0 0.70 -22.13 69.67 o 0 28 0 612.89 561.51 92.86 o 1 28 0 141.06 153.04 46.65 o 2 28 0 45.64 93.78 44.76 o 3 28 0 185.90 228.74 90.60 o 4 28 0 168.95 199.30 88.54 o 5 28 0 210.18 97.69 85.06 o 6 28 0 26.38 13.89 76.18 o 7 28 0 277.31 245.85 99.07 o 1 29 0 249.94 204.82 51.50 o 2 29 0 1.69 128.38 52.14 o 3 29 0 1139.69 1110.70 148.02 o 4 29 0 82.96 107.27 85.75 o 5 29 0 129.51 147.09 91.09 o 6 29 0 32.51 140.07 90.00 o 0 30 0 329.82 304.07 77.11 o 1 30 0 59.96 64.89 53.63 o 2 30 0 248.53 213.76 148.02 o 3 30 0 71.43 5.35 107.70 o 4 30 0 595.12 633.00 125.54 o 5 30 0 52.04 121.09 91.84 o 1 31 0 46.62 45.72 50.65 o 2 31 0 223.75 245.52 137.12 o 3 31 0 358.17 270.81 136.52 o 4 31 0 8.04 174.74 93.68 o 0 32 0 53.08 50.48 64.28 o 1 32 0 14.92 -17.62 52.21 o 2 32 0 39.40 -64.24 111.81 o 0 0 1 95.39 81.90 31.74 o 1 0 1 1116.29 812.97 44.98 o 2 0 1 1515.51 2020.52 107.92 o 3 0 1 1772.25 2100.41 84.49 o 4 0 1 414.04 764.67 96.25 o 5 0 1 448.23 891.86 83.55 o 6 0 1 1860.40 1709.74 72.31 o 7 0 1 1894.67 1772.79 140.55 o 8 0 1 244.43 331.64 49.17 o 9 0 1 208.05 388.12 55.30 o 10 0 1 20.82 108.54 55.35 o 11 0 1 536.14 417.27 74.35 o 12 0 1 420.75 411.75 103.11 o 13 0 1 125.08 193.70 93.23 o -13 1 1 373.70 213.79 101.65 o -12 1 1 360.65 659.47 124.97 o -11 1 1 20.52 26.14 54.24 o -10 1 1 94.38 284.62 63.57 o -9 1 1 1081.97 1072.82 81.17 o -8 1 1 231.01 371.71 49.74 o -6 1 1 427.75 866.32 130.58 o -5 1 1 845.70 1062.55 96.29 o -4 1 1 2417.13 2603.73 106.27 o -3 1 1 4236.98 4275.64 124.00 o -2 1 1 2456.33 2653.25 69.20 o -1 1 1 5084.32 4517.99 140.13 o 0 1 1 5063.73 4285.46 161.34 o 1 1 1 4546.02 3854.79 108.30 o 2 1 1 2486.31 2600.70 71.19 o 3 1 1 4060.54 4221.61 108.78 o 4 1 1 2603.75 2680.74 89.14 o 5 1 1 786.56 1055.73 69.47 o 6 1 1 448.22 781.43 72.01 o 8 1 1 342.99 518.61 57.75 o 9 1 1 1018.08 1028.36 69.15 o 10 1 1 64.52 243.66 53.60 o 11 1 1 11.83 58.03 56.94 o 12 1 1 328.93 533.06 89.35 o 13 1 1 343.26 211.05 124.92 o -13 2 1 87.86 75.61 94.08 o -12 2 1 144.52 392.47 103.24 o -11 2 1 67.00 73.74 71.73 o -10 2 1 1358.35 1219.57 121.51 o -9 2 1 229.96 342.89 60.55 o -8 2 1 1555.99 1559.76 77.43 o -7 2 1 1270.30 1947.08 132.43 o -6 2 1 11927.27 9953.31 324.08 o -5 2 1 1049.04 1256.15 111.12 o -4 2 1 1575.88 1882.50 68.71 o -2 2 1 8716.69 7385.57 234.52 o -1 2 1 1802.12 1780.47 88.10 o 0 2 1 216.37 256.73 128.71 o 1 2 1 1943.97 1897.60 51.61 o 2 2 1 7577.06 6701.78 180.00 o 4 2 1 1634.52 1803.92 194.84 o 5 2 1 970.98 1173.47 56.96 o 6 2 1 12429.75 10508.14 297.65 o 7 2 1 1306.43 1834.79 81.85 o 8 2 1 1520.89 1552.07 78.53 o 9 2 1 263.12 368.67 55.35 o 10 2 1 1133.53 1175.44 87.67 o 11 2 1 70.75 55.50 55.57 o 12 2 1 163.92 266.33 76.96 o 13 2 1 79.12 103.29 111.40 o -13 3 1 94.38 175.68 101.60 o -12 3 1 413.09 654.40 121.00 o -11 3 1 275.45 275.85 91.24 o -10 3 1 206.21 399.73 72.85 o -9 3 1 1701.69 1625.16 97.67 o -8 3 1 343.04 583.84 53.43 o -6 3 1 411.70 708.58 61.72 o -5 3 1 6733.29 6494.67 188.31 o -4 3 1 1484.54 1426.26 65.64 o -3 3 1 24689.58 22370.77 577.71 o -2 3 1 17208.30 14684.71 459.07 o -1 3 1 4099.51 3722.46 155.57 o 0 3 1 14502.19 13515.32 399.51 o 1 3 1 4056.17 3616.58 90.43 o 2 3 1 17559.09 15262.58 383.45 o 3 3 1 24411.19 21557.72 493.82 o 4 3 1 1297.48 1176.78 44.98 o 5 3 1 7050.68 6699.85 197.65 o 6 3 1 391.98 663.72 51.61 o 8 3 1 305.35 492.68 55.88 o 9 3 1 1559.00 1447.50 79.75 o 10 3 1 226.78 372.56 61.36 o 11 3 1 265.35 248.63 69.48 o 12 3 1 399.11 584.53 94.22 o 13 3 1 91.52 131.98 83.09 o -13 4 1 29.66 127.25 89.32 o -12 4 1 17.66 8.64 73.33 o -11 4 1 538.81 626.40 116.53 o -10 4 1 692.91 755.11 113.60 o -9 4 1 964.58 975.72 121.75 o -8 4 1 452.55 740.18 62.54 o -7 4 1 3390.40 3134.44 112.99 o -6 4 1 502.03 779.94 51.45 o -5 4 1 516.63 891.52 89.41 o -4 4 1 1718.70 2108.11 86.53 o -3 4 1 10523.34 9456.53 307.99 o -2 4 1 10623.59 10768.26 419.63 o -1 4 1 22180.32 20189.30 740.75 o 0 4 1 2381.47 2012.13 92.50 o 1 4 1 21631.13 19569.48 437.08 o 2 4 1 10941.75 11003.30 282.58 o 3 4 1 11156.11 10125.46 239.59 o 4 4 1 1687.15 2040.93 66.24 o 6 4 1 462.23 675.14 79.74 o 7 4 1 3462.84 3340.18 123.60 o 8 4 1 482.61 714.96 66.63 o 9 4 1 985.55 1084.00 90.35 o 10 4 1 737.29 738.78 77.89 o 11 4 1 452.01 619.64 78.28 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