#------------------------------------------------------------------------------ #$Date: 2009-05-05 17:46:52 +0300 (Tue, 05 May 2009) $ #$Revision: 697 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2218220.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2218220_Fobs loop_ _publ_author_name 'Ahmad, Matloob' 'Siddiqui, Hamid Latif' 'Zia-ur-Rehman, Muhammad' 'Ashiq, Muhammad Irfan' 'Tizzard, Graham John' _publ_section_title ; 1-(4-Hydroxy-2-methyl-1,1-dioxo-2H-1,2-benzothiazin-3-yl)ethanone ; _journal_coeditor_code PV2072 _journal_issue 5 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o788 _journal_volume 64 _journal_year 2008 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 72.132 _cell_angle_beta 77.962 _cell_angle_gamma 80.036 _cell_length_a 6.8523 _cell_length_b 8.3222 _cell_length_c 10.4880 _exptl_crystal_F_000 264.00 _reflns_d_resolution_high 0.7702 _[local]_cod_data_source_file pv2072Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 2007sot1195 in P-1' _shelx_refln_list_code 4 _shelx_F_calc_maximum 68.83 _shelx_F_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 710.19 654.57 26.26 o 3 0 0 1376.92 1292.41 24.90 o 4 0 0 1776.86 1984.90 23.72 o 5 0 0 0.91 1.49 0.45 o 6 0 0 241.27 256.49 5.59 o 7 0 0 0.52 0.71 0.70 o 8 0 0 181.98 168.74 9.67 o -8 1 0 68.12 69.26 3.89 o -7 1 0 94.17 91.51 3.32 o -6 1 0 650.23 680.07 14.95 o -5 1 0 4.77 5.41 0.68 o -4 1 0 387.63 413.09 6.47 o -3 1 0 15.20 36.54 1.04 o -2 1 0 1472.42 1530.10 18.65 o -1 1 0 1422.76 1283.62 12.49 o 1 1 0 3789.31 3422.28 128.55 o 3 1 0 913.23 977.13 11.00 o 4 1 0 2735.97 2721.39 38.32 o 5 1 0 293.59 291.75 6.02 o 6 1 0 206.91 221.66 5.62 o 7 1 0 3.40 2.83 1.05 o 8 1 0 11.43 7.75 1.89 o -8 2 0 43.65 45.01 3.78 o -7 2 0 12.94 10.69 0.86 o -6 2 0 205.67 209.86 5.47 o -5 2 0 558.02 573.01 8.92 o -4 2 0 129.03 121.30 2.06 o -3 2 0 14.03 12.42 0.55 o -2 2 0 316.24 269.15 3.41 o -1 2 0 342.10 291.69 4.40 o 0 2 0 106.68 125.85 2.31 o 1 2 0 690.38 612.36 11.20 o 2 2 0 176.31 212.14 3.89 o 3 2 0 91.65 103.84 2.06 o 4 2 0 149.38 180.00 3.47 o 5 2 0 76.23 79.67 2.39 o 6 2 0 886.55 914.00 21.64 o 7 2 0 62.30 60.28 3.43 o 8 2 0 256.29 227.08 9.14 o -7 3 0 4.36 2.39 1.26 o -6 3 0 38.31 38.06 1.39 o -5 3 0 484.36 509.32 7.49 o -4 3 0 207.26 199.96 3.15 o -3 3 0 0.22 0.44 0.32 o -2 3 0 297.23 280.18 3.55 o -1 3 0 51.13 50.49 1.08 o 0 3 0 487.33 453.80 7.89 o 1 3 0 37.78 34.30 1.05 o 2 3 0 91.59 96.01 1.87 o 3 3 0 36.31 34.20 0.89 o 4 3 0 1.39 0.68 0.34 o 5 3 0 55.75 52.89 1.45 o 6 3 0 17.57 18.90 1.33 o 7 3 0 117.73 122.88 5.91 o 8 3 0 129.66 112.82 5.78 o -7 4 0 205.19 207.34 9.20 o -6 4 0 97.17 103.99 3.49 o -5 4 0 267.52 277.43 4.71 o -4 4 0 125.86 127.67 2.28 o -3 4 0 1.32 2.01 0.43 o -2 4 0 15.58 19.05 0.73 o -1 4 0 2.29 0.48 0.77 o 0 4 0 1149.04 1129.88 16.96 o 1 4 0 507.55 512.65 7.23 o 2 4 0 6.48 7.30 0.70 o 3 4 0 129.42 121.74 2.86 o 4 4 0 10.92 8.82 0.74 o 5 4 0 227.74 241.24 4.97 o 6 4 0 8.14 7.65 0.89 o 7 4 0 29.66 27.45 2.85 o 8 4 0 46.98 48.53 4.05 o -7 5 0 29.34 23.60 3.24 o -6 5 0 57.72 53.45 3.21 o -5 5 0 298.80 318.05 7.03 o -4 5 0 30.93 33.07 1.31 o -3 5 0 236.67 251.82 3.99 o -2 5 0 67.18 65.60 1.50 o -1 5 0 8.55 7.06 0.64 o 0 5 0 127.53 116.46 2.48 o 1 5 0 141.63 151.57 2.82 o 2 5 0 132.16 139.53 2.91 o 3 5 0 0.31 1.08 0.52 o 4 5 0 77.88 77.70 2.39 o 5 5 0 280.73 300.07 7.83 o 6 5 0 141.86 138.94 4.55 o 7 5 0 0.00 -1.14 1.75 o 8 5 0 113.83 110.15 7.21 o -6 6 0 107.30 111.81 5.58 o -5 6 0 7.58 7.80 1.48 o -4 6 0 0.62 1.62 0.69 o -3 6 0 743.89 770.99 12.85 o -2 6 0 127.13 125.24 3.05 o -1 6 0 1569.77 1555.24 21.72 o 0 6 0 1432.80 1449.32 25.02 o 1 6 0 911.74 916.58 15.26 o 2 6 0 1355.39 1395.74 22.23 o 3 6 0 58.74 54.61 1.74 o 4 6 0 571.10 590.83 15.01 o 5 6 0 0.56 -0.05 0.91 o 6 6 0 2.25 3.04 0.74 o 7 6 0 56.09 50.31 4.21 o -5 7 0 481.14 491.86 22.80 o -4 7 0 175.34 198.39 7.71 o -3 7 0 130.87 134.27 4.31 o -2 7 0 74.15 82.46 2.43 o -1 7 0 407.22 403.07 9.83 o 0 7 0 148.11 150.34 3.43 o 1 7 0 1523.66 1611.57 24.43 o 2 7 0 60.73 60.20 2.82 o 3 7 0 1543.09 1643.21 35.77 o 4 7 0 182.67 192.10 10.14 o 5 7 0 279.35 310.63 12.11 o 6 7 0 232.32 233.24 12.35 o 7 7 0 30.16 25.47 5.18 o -4 8 0 46.11 40.77 3.04 o -3 8 0 345.50 364.56 15.13 o -2 8 0 3.17 1.51 1.12 o -1 8 0 208.50 230.69 7.28 o 0 8 0 280.76 286.17 7.59 o 1 8 0 3.64 2.23 1.02 o 2 8 0 0.47 1.52 1.14 o 3 8 0 26.98 25.06 2.20 o 4 8 0 0.68 0.96 1.50 o 5 8 0 331.15 371.01 16.73 o 6 8 0 53.85 52.55 5.15 o -3 9 0 71.83 71.22 4.35 o -2 9 0 37.48 32.08 2.91 o -1 9 0 0.06 0.98 2.19 o 0 9 0 11.61 9.14 1.97 o 1 9 0 75.97 76.16 4.00 o 2 9 0 57.19 54.54 4.11 o 3 9 0 20.07 13.81 2.28 o 4 9 0 40.36 44.89 3.46 o 5 9 0 0.70 -0.19 2.69 o -1 10 0 53.84 56.04 5.55 o 0 10 0 32.23 26.57 3.58 o 1 10 0 21.42 16.28 2.55 o 2 10 0 20.25 17.88 2.86 o 3 10 0 7.56 6.01 2.52 o -1 -10 1 10.39 6.99 2.21 o -4 -9 1 0.01 0.79 1.34 o -3 -9 1 49.85 53.82 3.99 o -2 -9 1 0.23 0.62 1.15 o -1 -9 1 12.89 12.09 2.47 o 0 -9 1 24.90 22.15 4.04 o 1 -9 1 3.79 4.53 1.84 o 2 -9 1 120.06 128.04 8.66 o -5 -8 1 36.62 34.66 2.82 o -4 -8 1 0.15 -1.40 0.93 o -3 -8 1 9.71 9.42 1.62 o -2 -8 1 1.90 0.87 0.78 o -1 -8 1 81.63 86.34 3.69 o 0 -8 1 2.71 4.70 0.96 o 1 -8 1 110.01 111.83 3.95 o 2 -8 1 163.91 157.04 5.92 o 3 -8 1 16.58 12.39 1.57 o 4 -8 1 58.33 54.03 5.83 o -6 -7 1 1.54 2.36 2.64 o -5 -7 1 115.94 119.27 5.09 o -4 -7 1 294.59 315.28 9.75 o -3 -7 1 17.47 12.98 2.44 o -2 -7 1 154.09 158.64 4.95 o -1 -7 1 63.70 66.07 2.14 o 0 -7 1 50.48 48.71 1.72 o 1 -7 1 99.26 101.01 2.89 o 2 -7 1 19.24 19.97 1.31 o 3 -7 1 421.19 446.26 10.20 o 4 -7 1 3.10 1.91 3.30 o 5 -7 1 315.24 337.25 13.68 o -7 -6 1 5.99 5.19 2.25 o -6 -6 1 76.31 66.90 4.37 o -5 -6 1 15.59 16.61 2.17 o -4 -6 1 97.21 102.70 2.80 o -3 -6 1 691.51 665.95 14.78 o -2 -6 1 4.13 3.32 0.61 o -1 -6 1 451.35 454.25 8.84 o 0 -6 1 758.00 768.06 11.56 o 1 -6 1 40.08 38.28 1.28 o 2 -6 1 3.20 2.92 0.74 o 3 -6 1 134.27 136.72 3.20 o 4 -6 1 47.78 45.38 2.66 o 5 -6 1 11.13 8.93 4.68 o 6 -6 1 39.62 39.66 2.52 o -7 -5 1 16.45 16.48 4.28 o -6 -5 1 4.03 5.03 0.95 o -5 -5 1 14.57 15.56 0.99 o -4 -5 1 118.40 118.38 2.92 o -3 -5 1 211.81 218.62 3.28 o -2 -5 1 180.19 163.09 2.91 o -1 -5 1 18.00 21.31 0.84 o 0 -5 1 441.53 469.15 6.42 o 1 -5 1 86.81 85.84 1.90 o 2 -5 1 300.98 283.17 4.72 o 3 -5 1 0.57 1.22 0.72 o 4 -5 1 375.45 394.23 8.31 o 5 -5 1 476.97 488.03 8.89 o 6 -5 1 15.51 18.17 1.83 o 7 -5 1 45.26 38.78 3.35 o -8 -4 1 79.69 73.38 6.38 o -7 -4 1 3.32 1.98 1.09 o -6 -4 1 262.54 263.01 6.86 o -5 -4 1 165.98 176.82 4.06 o -4 -4 1 56.11 48.81 1.53 o -3 -4 1 2.49 3.91 0.58 o -2 -4 1 136.43 116.40 2.99 o -1 -4 1 147.51 144.18 2.38 o 0 -4 1 163.06 164.25 3.00 o 1 -4 1 81.40 89.14 2.01 o 2 -4 1 2.23 3.00 0.42 o 3 -4 1 0.90 1.28 0.51 o 4 -4 1 32.10 27.82 0.85 o 5 -4 1 83.54 84.35 2.38 o 6 -4 1 424.61 408.09 9.60 o 7 -4 1 80.81 84.03 5.06 o -8 -3 1 279.43 288.19 14.19 o -7 -3 1 9.01 9.66 1.29 o -6 -3 1 127.63 117.71 3.41 o -5 -3 1 433.69 450.72 8.05 o -4 -3 1 164.91 166.69 2.97 o -3 -3 1 13.03 9.72 0.57 o -2 -3 1 437.64 465.12 7.02 o -1 -3 1 38.92 32.10 1.18 o 0 -3 1 0.06 0.47 0.25 o 1 -3 1 225.49 200.47 3.58 o 2 -3 1 434.89 468.32 6.30 o 3 -3 1 98.88 92.13 1.98 o 4 -3 1 196.07 190.94 3.49 o 5 -3 1 0.02 0.78 0.47 o 6 -3 1 155.73 160.61 4.23 o 7 -3 1 56.52 47.14 5.41 o -8 -2 1 3.70 2.14 1.09 o -7 -2 1 197.30 188.07 7.90 o -6 -2 1 222.40 245.22 5.88 o -5 -2 1 248.27 249.02 5.49 o -4 -2 1 241.49 238.61 6.71 o -3 -2 1 254.98 230.94 3.51 o -2 -2 1 102.09 124.72 2.41 o -1 -2 1 264.52 261.22 4.98 o 0 -2 1 2197.31 2054.03 35.36 o 1 -2 1 69.41 57.21 1.09 o 2 -2 1 62.59 59.96 1.24 o 3 -2 1 8.71 12.14 0.55 o 4 -2 1 11.32 10.52 0.60 o 5 -2 1 226.81 222.78 4.04 o 6 -2 1 9.71 7.56 0.99 o 7 -2 1 1.03 1.05 0.74 o 8 -2 1 64.87 60.70 4.05 o -8 -1 1 0.05 -0.31 1.61 o -7 -1 1 16.71 13.77 2.33 o -6 -1 1 36.65 35.40 1.80 o -5 -1 1 195.94 225.98 4.64 o -4 -1 1 220.69 265.07 5.43 o -3 -1 1 259.51 278.83 4.68 o -2 -1 1 102.69 94.74 1.64 o -1 -1 1 101.55 118.75 2.19 o 0 -1 1 399.92 360.24 7.16 o 1 -1 1 26.51 27.24 0.81 o 2 -1 1 2861.73 2676.58 31.71 o 3 -1 1 255.78 274.64 4.40 o 4 -1 1 1124.36 1178.92 19.38 o 5 -1 1 1500.02 1550.94 18.21 o 6 -1 1 14.47 17.38 1.39 o 7 -1 1 138.53 135.82 3.95 o 8 -1 1 4.72 0.52 1.27 o -8 0 1 3.04 3.48 1.54 o -7 0 1 3.94 2.45 0.96 o -6 0 1 4.47 2.90 1.28 o -5 0 1 50.01 38.02 1.56 o -4 0 1 589.25 650.42 10.65 o -3 0 1 1321.60 1542.30 28.74 o -2 0 1 368.41 335.00 5.93 o 1 0 1 1895.07 1632.61 63.87 o 2 0 1 6.06 4.35 0.29 o 3 0 1 45.00 48.66 1.12 o 4 0 1 87.20 84.45 1.51 o 5 0 1 156.72 177.54 3.29 o 6 0 1 855.96 876.80 13.91 o 7 0 1 44.27 40.42 1.46 o 8 0 1 199.28 194.94 10.01 o -8 1 1 167.56 170.30 7.49 o -7 1 1 4.52 2.12 0.86 o -6 1 1 85.33 81.07 2.64 o 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726.52 11.34 o 1 3 1 22.46 13.88 0.73 o 2 3 1 106.48 88.97 1.62 o 3 3 1 5.40 7.81 0.64 o 4 3 1 45.41 47.19 1.15 o 5 3 1 173.20 175.87 3.42 o 6 3 1 58.45 54.11 2.12 o 7 3 1 102.19 103.70 4.36 o 8 3 1 2.82 -1.29 1.33 o -7 4 1 157.31 146.33 10.53 o -6 4 1 29.69 32.46 1.79 o -5 4 1 622.60 623.82 9.45 o -4 4 1 346.84 357.92 4.82 o -3 4 1 4.26 3.54 0.45 o -2 4 1 277.49 256.79 3.80 o -1 4 1 357.82 359.57 5.18 o 0 4 1 5.25 6.44 0.47 o 1 4 1 330.04 345.33 5.22 o 2 4 1 22.17 24.34 0.82 o 3 4 1 116.42 115.26 2.45 o 4 4 1 9.38 8.65 0.44 o 5 4 1 16.70 12.26 0.60 o 6 4 1 228.49 224.68 5.95 o 7 4 1 113.89 113.17 5.31 o 8 4 1 0.66 -0.72 2.29 o -7 5 1 17.49 10.76 2.33 o -6 5 1 22.26 9.64 2.90 o -5 5 1 1.06 -1.03 0.68 o -4 5 1 114.78 112.09 2.98 o -3 5 1 379.11 383.21 5.55 o -2 5 1 1.53 0.49 0.42 o -1 5 1 102.01 98.70 1.89 o 0 5 1 590.24 574.16 10.46 o 1 5 1 279.18 278.38 3.70 o 2 5 1 139.90 143.36 3.06 o 3 5 1 186.56 183.34 3.88 o 4 5 1 215.58 223.73 5.11 o 5 5 1 31.78 30.08 1.08 o 6 5 1 217.14 233.30 7.87 o 7 5 1 48.10 45.49 3.23 o 8 5 1 0.63 -1.15 1.86 o -6 6 1 0.86 -2.40 2.52 o -5 6 1 38.00 35.04 2.35 o -4 6 1 44.78 37.79 2.71 o -3 6 1 0.66 0.59 0.74 o -2 6 1 195.46 194.81 3.46 o -1 6 1 162.26 161.34 3.58 o 0 6 1 663.58 671.07 10.91 o 1 6 1 541.41 556.94 7.60 o 2 6 1 28.44 25.38 1.42 o 3 6 1 9.38 11.63 1.65 o 4 6 1 0.25 0.56 0.84 o 5 6 1 399.30 396.84 8.37 o 6 6 1 213.00 215.34 6.83 o 7 6 1 64.28 56.08 4.61 o -5 7 1 24.07 22.22 2.34 o -4 7 1 0.01 0.27 1.43 o -3 7 1 9.32 7.74 0.75 o -2 7 1 19.55 19.22 1.26 o -1 7 1 132.64 123.23 3.70 o 0 7 1 189.47 196.17 4.95 o 1 7 1 96.26 103.81 2.53 o 2 7 1 676.53 694.36 14.79 o 3 7 1 43.04 45.53 2.09 o 4 7 1 183.34 187.46 5.23 o 5 7 1 175.26 190.54 6.43 o 6 7 1 44.19 42.49 2.82 o 7 7 1 14.53 12.51 2.57 o -4 8 1 101.85 106.49 5.62 o -3 8 1 12.27 7.89 3.16 o -2 8 1 19.26 19.16 1.42 o -1 8 1 96.87 96.51 3.71 o 0 8 1 143.91 154.12 4.13 o 1 8 1 19.98 20.16 1.14 o 2 8 1 30.64 33.87 2.78 o 3 8 1 0.68 0.01 0.65 o 4 8 1 0.01 -1.08 1.15 o 5 8 1 36.04 36.49 2.24 o 6 8 1 59.47 63.53 7.73 o -3 9 1 221.66 234.57 18.39 o -2 9 1 2.46 1.09 2.49 o -1 9 1 51.44 46.91 2.75 o 0 9 1 217.77 230.05 7.98 o 1 9 1 88.15 83.66 3.23 o 2 9 1 0.04 -1.57 1.04 o 3 9 1 173.98 160.33 8.43 o 4 9 1 0.49 -0.19 1.42 o 5 9 1 13.18 7.24 1.96 o -1 10 1 3.85 -2.45 7.89 o 0 10 1 155.89 150.82 7.67 o 1 10 1 105.36 99.13 5.87 o 2 10 1 6.14 4.13 1.45 o 3 10 1 10.65 8.53 1.71 o -3 -9 2 38.34 34.73 3.53 o -2 -9 2 64.36 65.08 4.39 o -1 -9 2 84.98 98.16 5.36 o 0 -9 2 2.33 -0.96 1.83 o 1 -9 2 0.14 -2.71 3.41 o 2 -9 2 9.17 7.62 2.02 o -5 -8 2 15.11 14.18 1.65 o -4 -8 2 55.52 61.18 3.38 o -3 -8 2 85.90 77.84 3.96 o -2 -8 2 1.04 1.85 1.67 o -1 -8 2 15.41 15.59 1.48 o 0 -8 2 134.72 140.10 5.66 o 1 -8 2 60.46 56.61 3.96 o 2 -8 2 17.59 15.73 1.73 o 3 -8 2 19.38 17.22 1.97 o 4 -8 2 10.42 8.80 1.86 o -6 -7 2 5.60 3.92 2.90 o -5 -7 2 4.95 3.20 1.51 o -4 -7 2 106.92 103.27 5.03 o -3 -7 2 14.87 12.96 1.24 o -2 -7 2 128.90 132.27 5.29 o -1 -7 2 122.34 121.46 3.21 o 0 -7 2 107.73 116.09 3.11 o 1 -7 2 279.72 281.62 6.08 o 2 -7 2 238.88 240.94 6.30 o 3 -7 2 28.89 23.64 1.39 o 4 -7 2 145.52 156.26 5.19 o 5 -7 2 84.73 83.12 4.12 o -6 -6 2 7.68 5.01 1.97 o -5 -6 2 93.45 90.41 4.05 o -4 -6 2 162.74 158.29 5.15 o -3 -6 2 5.09 2.92 0.76 o -2 -6 2 3.21 3.69 0.62 o -1 -6 2 139.76 144.00 3.58 o 0 -6 2 141.95 135.48 2.89 o 1 -6 2 0.05 -0.80 0.53 o 2 -6 2 400.26 415.99 7.80 o 3 -6 2 131.02 134.03 2.95 o 4 -6 2 55.25 54.87 3.70 o 5 -6 2 225.60 225.01 9.06 o 6 -6 2 45.78 46.43 3.17 o -7 -5 2 11.26 10.23 2.38 o -6 -5 2 6.29 3.87 0.99 o -5 -5 2 0.12 0.37 0.58 o -4 -5 2 106.54 103.80 2.56 o -3 -5 2 524.54 537.61 8.34 o -2 -5 2 3.64 4.23 0.57 o -1 -5 2 357.08 377.58 6.12 o 0 -5 2 434.53 405.53 8.07 o 1 -5 2 105.30 110.16 2.48 o 2 -5 2 0.25 0.40 0.81 o 3 -5 2 246.23 250.66 4.40 o 4 -5 2 75.61 75.14 1.79 o 5 -5 2 49.44 46.55 1.79 o 6 -5 2 123.94 125.81 6.44 o -7 -4 2 51.34 53.37 3.96 o -6 -4 2 203.01 209.10 8.62 o -5 -4 2 7.53 7.59 0.98 o -4 -4 2 212.03 224.94 4.42 o -3 -4 2 522.88 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42.21 3.49 o 2 0 12 40.82 47.97 4.51 o 3 0 12 248.77 289.40 19.36 o 4 0 12 107.30 129.12 7.43 o -2 1 12 5.84 5.41 2.60 o -1 1 12 131.31 147.40 13.00 o 0 1 12 244.33 260.54 12.41 o 1 1 12 8.13 4.81 1.32 o 2 1 12 67.21 65.48 3.18 o 3 1 12 101.11 91.01 6.64 o 4 1 12 18.55 17.38 2.50 o 5 1 12 0.89 3.18 1.85 o -2 2 12 15.47 18.82 2.45 o -1 2 12 4.70 -6.56 4.37 o 0 2 12 21.68 21.20 1.67 o 1 2 12 101.26 106.25 6.23 o 2 2 12 29.91 22.93 1.81 o 3 2 12 49.79 51.56 4.93 o 4 2 12 339.82 323.25 16.26 o 5 2 12 31.27 30.63 2.80 o -2 3 12 138.69 130.29 7.24 o -1 3 12 19.76 23.78 2.31 o 0 3 12 2.23 1.65 3.30 o 1 3 12 52.89 56.24 2.57 o 2 3 12 9.73 9.70 1.43 o 3 3 12 12.87 6.56 1.59 o 4 3 12 57.83 61.57 2.60 o 5 3 12 100.63 82.88 3.63 o -2 4 12 65.32 58.83 3.80 o -1 4 12 162.22 179.34 5.94 o 0 4 12 49.23 51.94 2.10 o 1 4 12 25.70 22.97 1.40 o 2 4 12 18.02 18.47 1.45 o 3 4 12 22.38 29.47 2.39 o 4 4 12 1.12 -2.77 2.01 o 5 4 12 0.17 0.16 1.18 o -1 5 12 1.31 -0.41 1.11 o 0 5 12 35.47 28.48 1.94 o 1 5 12 131.90 146.33 6.24 o 2 5 12 7.29 9.77 2.78 o 3 5 12 156.00 163.55 11.08 o 4 5 12 210.77 226.98 10.10 o 5 5 12 0.17 -0.61 1.20 o -1 6 12 162.80 162.06 8.20 o 0 6 12 10.10 12.17 1.83 o 1 6 12 41.03 46.87 2.94 o 2 6 12 1.21 0.45 1.25 o 3 6 12 164.59 167.91 12.44 o 4 6 12 57.02 58.89 3.30 o 5 6 12 403.99 407.29 17.64 o 0 7 12 3.48 4.35 2.54 o 1 7 12 151.99 172.86 7.87 o 2 7 12 5.13 6.95 1.94 o 3 7 12 3.02 3.28 2.07 o 4 7 12 3.44 5.92 1.56 o 0 1 13 1.39 2.26 1.82 o 1 1 13 4.78 5.87 1.52 o 2 1 13 11.61 9.60 1.28 o 3 1 13 27.67 24.64 3.40 o 0 2 13 45.68 47.98 7.68 o 1 2 13 0.03 0.71 1.22 o 2 2 13 0.24 -0.84 1.69 o 3 2 13 99.87 84.02 5.65 o 4 2 13 39.83 40.65 4.56 o 0 3 13 238.49 238.58 12.74 o 1 3 13 57.59 67.78 3.96 o 2 3 13 17.97 14.23 1.57 o 3 3 13 75.80 73.28 6.76 o 4 3 13 46.40 45.26 3.24 o 0 4 13 16.45 17.45 2.10 o 1 4 13 82.53 78.83 4.79 o 2 4 13 15.54 14.14 1.98 o 3 4 13 0.01 0.90 1.51 o 4 4 13 92.44 78.79 3.94 o 0 5 13 33.75 44.64 4.37 o 1 5 13 27.79 21.62 1.71 o 2 5 13 19.46 25.91 1.97 o 3 5 13 2.90 3.55 1.49 o 4 5 13 12.08 12.56 3.08 o 2 6 13 13.42 11.32 3.08 o 3 6 13 45.41 36.66 4.48 o