#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/83/2218313.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2218313_Fobs loop_ _publ_author_name 'Teo, Yin Yin' 'Lo, Kong Mun' 'Ng, Seik Weng' _publ_section_title ; Bis[1,2-bis(diphenylphosphino)ethane-\k^2^P:P']silver(I) bis(chlorodifluoroacetato-\kO)(4-chlorophenyl)diphenylstannate(IV) ; _journal_coeditor_code BQ2076 _journal_issue 6 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m819 _journal_volume 64 _journal_year 2008 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 69.674 _cell_angle_beta 84.646 _cell_angle_gamma 74.030 _cell_length_a 13.4774 _cell_length_b 15.4957 _cell_length_c 18.1475 _exptl_crystal_F_000 1564.00 _reflns_d_resolution_high 0.7599 _[local]_cod_data_source_file bq2076Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' P-1' _shelx_refln_list_code 4 _shelx_F_calc_maximum 348.70 _shelx_F_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 2144.67 -11.29 7.53 o 2 0 0 25586.01 24475.16 708.90 o 3 0 0 10203.94 9924.31 320.72 o 4 0 0 2095.83 2274.15 174.40 o 5 0 0 4611.43 5089.82 417.66 o 6 0 0 300.89 176.29 62.27 o 7 0 0 1010.72 959.63 108.54 o 8 0 0 604.59 497.94 95.97 o 9 0 0 10.47 104.37 75.97 o 10 0 0 214.73 229.61 95.93 o 11 0 0 2238.45 2239.49 206.83 o 12 0 0 4312.26 4719.38 546.41 o 13 0 0 3176.23 3235.85 264.65 o 14 0 0 7.25 -47.75 105.05 o 15 0 0 550.48 498.98 156.90 o 16 0 0 171.50 171.91 149.56 o 17 0 0 254.27 251.86 226.09 o -16 1 0 3708.58 4179.73 699.13 o -15 1 0 151.89 76.57 203.04 o -14 1 0 1814.10 2190.53 245.53 o -13 1 0 153.80 59.00 163.85 o -12 1 0 90.18 77.47 95.99 o -11 1 0 38.21 64.10 91.88 o -10 1 0 5542.46 5604.94 293.40 o -9 1 0 216.05 234.07 87.63 o -8 1 0 5826.61 6829.86 303.75 o -7 1 0 4246.07 4253.55 223.74 o -6 1 0 404.25 428.07 108.78 o -5 1 0 59.36 -14.20 43.70 o -4 1 0 5148.44 5200.18 251.93 o -3 1 0 2576.73 2074.99 111.00 o -2 1 0 23196.86 22684.52 666.53 o -1 1 0 2045.75 2183.12 106.16 o 0 1 0 1978.95 -5.76 9.55 o 1 1 0 10208.18 5553.97 956.90 o 2 1 0 7620.33 7386.41 231.86 o 3 1 0 121592.32 122157.77 3429.63 o 4 1 0 2320.58 1979.33 180.99 o 5 1 0 2917.73 3304.93 155.78 o 6 1 0 12573.80 13054.65 443.91 o 7 1 0 805.48 775.98 100.17 o 8 1 0 187.61 116.26 68.85 o 9 1 0 5975.13 5981.34 283.14 o 10 1 0 1442.51 1439.66 162.46 o 11 1 0 14596.36 14449.99 557.94 o 12 1 0 369.93 429.46 120.68 o 13 1 0 8.19 -5.62 103.47 o 14 1 0 27.49 18.61 162.88 o 15 1 0 1631.44 1738.45 226.94 o 16 1 0 1727.27 2021.92 253.84 o 17 1 0 235.35 352.79 198.91 o -16 2 0 218.65 170.43 198.13 o -15 2 0 19.64 150.41 181.27 o -14 2 0 474.62 539.75 157.59 o -13 2 0 516.55 568.52 153.55 o -12 2 0 3320.54 3671.28 280.23 o -11 2 0 915.26 512.37 127.95 o -10 2 0 1546.87 1707.67 210.26 o -9 2 0 24.38 -11.96 52.00 o -8 2 0 179.56 136.95 52.03 o -7 2 0 11859.78 11645.14 353.72 o -6 2 0 323.06 371.98 52.15 o -5 2 0 29097.56 28892.88 748.53 o -4 2 0 319.51 220.62 34.09 o -3 2 0 387.55 638.43 55.76 o -2 2 0 51251.88 54054.47 1911.60 o -1 2 0 35804.41 39954.83 1113.92 o 0 2 0 6989.73 6910.12 384.84 o 1 2 0 39955.70 39660.99 1363.20 o 2 2 0 2959.09 3258.46 150.21 o 3 2 0 13752.33 13872.77 428.00 o 4 2 0 15324.49 15179.50 474.83 o 5 2 0 12557.02 12379.18 407.50 o 6 2 0 809.27 684.35 96.68 o 7 2 0 1395.92 1300.38 117.21 o 8 2 0 3371.82 2963.98 183.32 o 9 2 0 4969.34 5317.94 260.28 o 10 2 0 272.36 184.86 96.25 o 11 2 0 2575.77 2553.36 208.92 o 12 2 0 74.96 59.55 93.85 o 13 2 0 1750.46 1734.19 201.47 o 14 2 0 4173.44 3940.82 294.91 o 15 2 0 77.63 -15.24 116.15 o 16 2 0 116.61 -16.06 155.61 o 17 2 0 566.51 780.09 230.68 o -16 3 0 303.71 368.45 218.87 o -15 3 0 860.58 771.97 242.72 o -14 3 0 23.93 -52.16 145.78 o -13 3 0 349.27 449.74 181.72 o -12 3 0 225.57 361.27 265.67 o -11 3 0 1468.07 1672.61 274.58 o -10 3 0 53.55 -57.06 95.09 o -9 3 0 755.90 932.85 141.24 o -8 3 0 6334.40 6327.96 247.38 o -7 3 0 830.25 1051.43 77.12 o -6 3 0 7637.49 7345.21 288.36 o -5 3 0 6631.30 6816.43 241.96 o -4 3 0 2105.67 2174.64 169.78 o -3 3 0 3729.98 4104.59 223.93 o -2 3 0 6266.99 5558.89 382.02 o -1 3 0 12543.13 12080.61 683.45 o 0 3 0 34782.87 36958.11 1894.44 o 2 3 0 2071.30 1487.03 173.93 o 3 3 0 5004.88 5548.71 253.54 o 4 3 0 41588.25 40158.46 1169.11 o 5 3 0 2430.61 2496.65 133.13 o 6 3 0 15639.11 16012.48 523.23 o 7 3 0 409.29 440.15 83.14 o 8 3 0 3192.42 3272.79 219.65 o 9 3 0 2886.74 2867.89 193.80 o 10 3 0 6644.44 6488.60 305.54 o 11 3 0 1758.69 1780.02 220.79 o 12 3 0 1587.94 1517.08 178.87 o 13 3 0 18.31 43.84 102.61 o 14 3 0 16.73 32.59 112.93 o 15 3 0 354.38 251.81 132.51 o 16 3 0 476.50 598.97 383.86 o 17 3 0 800.00 1046.48 414.11 o -15 4 0 210.35 299.59 264.38 o -14 4 0 517.19 530.39 213.86 o -13 4 0 204.77 520.56 400.58 o -12 4 0 2695.24 3119.96 347.46 o -11 4 0 3129.82 2696.45 370.08 o -10 4 0 1528.20 1387.66 223.06 o -9 4 0 54.77 -28.40 99.55 o -8 4 0 936.48 1072.89 182.43 o -7 4 0 524.03 523.04 138.83 o -6 4 0 14659.37 14285.20 637.03 o -5 4 0 69.05 111.44 150.59 o -4 4 0 15510.25 15705.24 653.59 o -3 4 0 1081.76 1080.85 124.03 o -2 4 0 864.93 1319.78 198.61 o -1 4 0 20238.58 19857.17 1088.02 o 0 4 0 2908.20 2976.33 235.53 o 1 4 0 2315.80 1781.27 166.21 o 2 4 0 18915.07 19007.02 992.48 o 3 4 0 1053.53 1034.66 104.84 o 4 4 0 257.97 282.70 73.69 o 5 4 0 1143.56 1243.68 94.33 o 6 4 0 30793.46 30338.41 920.33 o 7 4 0 24338.95 22511.64 717.05 o 8 4 0 4854.73 4242.56 215.29 o 9 4 0 10163.95 10342.72 403.17 o 10 4 0 1469.80 1737.56 165.62 o 11 4 0 281.87 236.82 104.03 o 12 4 0 85.94 20.12 104.69 o 13 4 0 1730.95 1849.09 199.74 o 14 4 0 5.66 -74.85 93.67 o 15 4 0 2246.11 1752.57 269.03 o 16 4 0 161.05 78.95 160.09 o 17 4 0 76.07 118.69 169.59 o -15 5 0 167.15 -20.30 286.67 o -14 5 0 274.03 422.14 203.82 o -13 5 0 102.58 59.63 143.57 o -12 5 0 319.98 406.74 180.57 o -11 5 0 61.72 188.35 141.27 o -10 5 0 24.93 36.41 117.19 o -9 5 0 2986.15 3159.95 305.60 o -8 5 0 3977.77 4087.39 327.28 o -7 5 0 344.77 88.09 101.67 o -6 5 0 437.49 374.87 118.90 o -5 5 0 1594.38 1835.56 188.99 o -4 5 0 361.48 287.70 90.66 o -3 5 0 15133.98 15048.49 911.03 o -2 5 0 5597.58 5822.78 252.10 o -1 5 0 28886.13 28527.61 1538.14 o 0 5 0 1158.65 935.89 141.47 o 1 5 0 692.93 946.67 133.02 o 2 5 0 7607.92 7193.17 452.70 o 3 5 0 23295.65 23993.17 889.84 o 4 5 0 33.90 -47.98 55.50 o 5 5 0 43120.20 43313.56 1553.58 o 6 5 0 490.36 492.55 104.78 o 7 5 0 5162.47 5367.71 234.64 o 8 5 0 103.27 163.58 72.70 o 9 5 0 5195.31 5334.76 256.44 o 10 5 0 3899.25 4014.24 236.60 o 11 5 0 943.25 930.48 140.93 o 12 5 0 958.47 944.14 154.50 o 13 5 0 58.92 6.51 108.09 o 14 5 0 1646.35 1867.69 662.45 o 15 5 0 157.66 393.51 162.36 o 16 5 0 523.19 387.91 186.48 o 17 5 0 1368.82 1535.37 364.14 o -14 6 0 21.09 3.55 164.33 o -13 6 0 2419.46 2983.92 619.40 o -12 6 0 981.92 1062.17 240.84 o -11 6 0 4631.55 4506.85 409.95 o -10 6 0 313.24 252.84 146.44 o -9 6 0 103.16 176.95 201.42 o -8 6 0 1209.37 1483.68 229.50 o -7 6 0 1829.48 1923.38 235.90 o -6 6 0 487.77 311.09 120.32 o -5 6 0 3101.29 2671.35 235.47 o -4 6 0 2491.79 2095.51 217.53 o -3 6 0 12516.42 13561.38 521.28 o -2 6 0 1509.10 1545.14 250.84 o -1 6 0 4917.04 5016.90 385.70 o 0 6 0 5529.41 5023.76 366.59 o 1 6 0 11306.17 11443.94 674.76 o 2 6 0 4053.06 3521.47 196.24 o 3 6 0 1881.12 1353.80 188.26 o 4 6 0 28.48 70.62 65.99 o 5 6 0 540.05 577.03 111.88 o 6 6 0 3975.79 4137.40 259.98 o 7 6 0 4055.98 3527.85 249.22 o 8 6 0 11879.12 11770.02 456.33 o 9 6 0 2377.25 2171.42 165.96 o 10 6 0 4917.26 4649.50 355.14 o 11 6 0 128.50 167.66 116.94 o 12 6 0 552.30 814.91 169.60 o 13 6 0 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