#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/83/2218317.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2218317_Fobs loop_ _publ_author_name 'Dornhaus, Franz' 'Lerner, Hans-Wolfram' 'Bolte, Michael' _publ_section_title ; \m-Bis(diphenylphosphanyl)borato-\k^2^P:P'-bis[dicarbonyl(\h^5^-cyclopentadienyl)iron(II)] tetrachloridoferrate(III) chloroform solvate ; _journal_coeditor_code BQ2081 _journal_issue 6 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m835 _journal_volume 64 _journal_year 2008 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 113.296 _cell_angle_gamma 90.000 _cell_length_a 16.0627 _cell_length_b 17.8223 _cell_length_c 17.2050 _exptl_crystal_F_000 2124.00 _reflns_d_resolution_high 0.8170 _[local]_cod_data_source_file bq2081Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' wa619 in P2(1)/n' _shelx_refln_list_code 4 _shelx_F_calc_maximum 382.72 _shelx_F_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 15375.21 14856.06 1683.09 o 6 0 0 10323.71 8346.54 1155.66 o 8 0 0 14869.41 13952.05 1211.92 o 10 0 0 24518.72 26262.93 1215.82 o 12 0 0 513.14 821.42 947.54 o 14 0 0 2446.28 2646.96 913.66 o 16 0 0 6146.72 6413.61 927.17 o 3 1 0 798.01 938.61 1340.99 o 4 1 0 27656.01 27342.86 1296.78 o 5 1 0 198.88 884.29 1105.01 o 6 1 0 1508.10 1348.69 918.38 o 7 1 0 6117.24 5897.74 754.06 o 8 1 0 1159.30 784.11 691.02 o 9 1 0 156.85 411.97 682.54 o 10 1 0 467.18 1976.63 716.89 o 11 1 0 365.73 1551.26 768.19 o 12 1 0 7587.41 8172.46 776.66 o 13 1 0 261.52 438.54 649.55 o 14 1 0 3243.48 3051.51 604.62 o 15 1 0 1910.60 1613.03 641.32 o 16 1 0 760.94 -6.44 608.39 o 17 1 0 0.31 -100.49 606.18 o 2 2 0 1957.69 1729.64 1658.16 o 3 2 0 5345.27 5349.33 1411.26 o 4 2 0 110.57 992.46 1435.68 o 5 2 0 9882.58 9266.74 1083.42 o 6 2 0 3059.81 2168.64 955.60 o 7 2 0 18.74 740.72 835.18 o 8 2 0 7546.08 7554.42 740.65 o 9 2 0 924.39 1436.67 639.50 o 10 2 0 3.54 408.34 692.76 o 11 2 0 3290.57 4281.88 772.73 o 12 2 0 1151.98 1342.74 659.33 o 13 2 0 27.64 616.85 712.45 o 14 2 0 767.70 741.15 667.58 o 15 2 0 144.40 -219.64 667.49 o 16 2 0 42.29 92.90 625.75 o 17 2 0 253.82 587.24 625.52 o 1 3 0 6608.57 5068.34 1110.45 o 2 3 0 8717.34 8838.10 1163.53 o 3 3 0 37934.84 37271.66 1445.05 o 4 3 0 5397.93 4748.45 1309.02 o 5 3 0 44594.91 44835.12 1292.69 o 6 3 0 4721.91 3580.60 1007.29 o 7 3 0 1210.89 2197.91 828.08 o 8 3 0 92.36 13.27 725.04 o 9 3 0 51.99 602.48 697.34 o 10 3 0 88.18 573.32 714.68 o 11 3 0 330.79 1317.31 711.53 o 12 3 0 1207.83 1490.41 657.76 o 13 3 0 365.85 1264.43 666.49 o 14 3 0 5.98 612.38 653.48 o 15 3 0 0.29 83.32 654.35 o 16 3 0 485.79 267.11 603.25 o 17 3 0 174.63 670.33 671.36 o 0 4 0 85.75 58.63 1227.81 o 1 4 0 10769.21 11241.60 1004.61 o 2 4 0 84.27 751.09 1204.52 o 3 4 0 839.24 1533.80 1314.47 o 4 4 0 1435.94 1160.19 1222.66 o 5 4 0 5751.26 4835.91 1105.69 o 6 4 0 2393.04 2808.27 823.22 o 7 4 0 6072.99 5141.09 854.01 o 8 4 0 6122.15 5302.37 800.72 o 9 4 0 4994.15 4559.02 855.97 o 10 4 0 1913.48 1986.80 783.33 o 11 4 0 256.52 404.32 797.01 o 12 4 0 803.04 979.89 698.68 o 13 4 0 1858.35 1377.13 620.27 o 14 4 0 70.75 817.82 614.42 o 15 4 0 2765.51 2639.37 707.48 o 16 4 0 187.49 -323.42 642.46 o 17 4 0 386.82 310.06 611.16 o 1 5 0 766.38 978.35 1094.78 o 2 5 0 321.82 684.90 1067.96 o 3 5 0 2769.49 1728.40 1050.82 o 4 5 0 11351.39 10898.51 1114.96 o 5 5 0 4940.24 6414.61 1005.28 o 6 5 0 1330.34 2255.13 1026.08 o 7 5 0 35333.54 34783.12 1095.12 o 8 5 0 3441.04 4175.46 876.72 o 9 5 0 20586.79 21069.66 840.41 o 10 5 0 931.36 860.15 780.58 o 11 5 0 339.79 1206.05 825.39 o 12 5 0 413.96 1100.82 716.68 o 13 5 0 4747.45 5077.31 678.83 o 14 5 0 164.70 -292.94 590.60 o 15 5 0 140.08 246.07 571.94 o 16 5 0 55.44 369.45 729.41 o 17 5 0 11.83 153.48 735.59 o 0 6 0 7611.19 7241.82 1523.15 o 1 6 0 5626.19 3378.87 971.15 o 2 6 0 5088.94 3671.79 1035.68 o 3 6 0 1444.84 1462.52 846.95 o 4 6 0 1639.69 2129.06 987.06 o 5 6 0 927.60 1306.16 762.09 o 6 6 0 3494.18 2868.43 890.69 o 7 6 0 846.37 1453.14 880.44 o 8 6 0 4099.22 4218.40 808.60 o 9 6 0 7732.04 7930.87 1025.45 o 10 6 0 523.47 2060.45 854.62 o 11 6 0 1929.81 1682.70 569.68 o 12 6 0 839.72 1632.93 692.80 o 13 6 0 2374.51 1541.23 649.97 o 14 6 0 359.66 542.24 724.57 o 15 6 0 4829.06 4462.42 663.38 o 16 6 0 259.04 308.18 539.18 o 17 6 0 46.30 398.30 558.92 o 1 7 0 2800.55 2589.60 830.78 o 2 7 0 4.25 -19.59 755.27 o 3 7 0 2041.42 2059.63 744.11 o 4 7 0 16940.36 16314.53 801.72 o 5 7 0 2019.91 1907.96 772.99 o 6 7 0 12943.83 12094.65 793.10 o 7 7 0 639.87 1691.68 779.25 o 8 7 0 2641.34 3520.31 812.61 o 9 7 0 678.20 1519.81 902.37 o 10 7 0 4314.85 5135.85 1209.19 o 11 7 0 2.43 526.84 707.96 o 12 7 0 25.40 1013.26 802.98 o 13 7 0 1634.84 1926.93 553.55 o 14 7 0 2084.63 2366.38 705.76 o 15 7 0 1780.39 1688.93 737.52 o 16 7 0 60.07 -437.39 666.01 o 0 8 0 13159.08 15413.48 1190.32 o 1 8 0 8775.83 8893.60 683.34 o 2 8 0 3001.47 2931.53 699.46 o 3 8 0 12521.22 13614.88 834.10 o 4 8 0 13743.61 13063.35 766.93 o 5 8 0 51.50 1328.52 733.50 o 6 8 0 715.06 312.16 785.55 o 7 8 0 5815.35 5894.33 801.76 o 8 8 0 4124.60 4681.05 764.03 o 9 8 0 321.98 1012.36 728.67 o 10 8 0 3876.34 4385.92 934.26 o 11 8 0 3963.76 4560.37 588.67 o 12 8 0 2536.27 2609.78 615.62 o 13 8 0 1.68 156.79 552.80 o 14 8 0 1.20 887.12 628.57 o 15 8 0 453.88 126.53 628.93 o 16 8 0 307.24 -241.15 561.62 o 1 9 0 29.26 400.90 644.15 o 2 9 0 957.69 1354.07 637.79 o 3 9 0 367.80 1022.09 785.38 o 4 9 0 6876.14 6653.12 730.01 o 5 9 0 3987.42 4252.02 623.65 o 6 9 0 1886.29 2359.55 707.72 o 7 9 0 951.43 1743.93 686.80 o 8 9 0 1175.98 2013.64 720.81 o 9 9 0 610.42 923.41 698.13 o 10 9 0 37.42 221.66 565.19 o 11 9 0 253.61 954.05 569.63 o 12 9 0 281.14 446.50 680.93 o 13 9 0 0.11 694.32 684.11 o 14 9 0 1858.21 1043.93 670.40 o 15 9 0 65.90 1003.93 511.89 o 16 9 0 352.16 328.93 555.19 o 0 10 0 70436.33 72745.77 945.44 o 1 10 0 36.16 110.26 551.94 o 2 10 0 15414.65 15876.91 651.20 o 3 10 0 1164.56 2061.03 661.67 o 4 10 0 3614.43 3080.49 662.49 o 5 10 0 369.56 366.36 728.59 o 6 10 0 104.71 536.52 710.99 o 7 10 0 82.03 86.89 776.24 o 8 10 0 1987.73 2027.77 674.34 o 9 10 0 7.53 1852.54 914.32 o 10 10 0 4283.45 4545.01 659.12 o 11 10 0 11.74 -101.21 568.18 o 12 10 0 335.58 700.65 537.40 o 13 10 0 1460.63 1663.88 600.68 o 14 10 0 2447.02 1757.28 561.53 o 15 10 0 193.24 -556.25 556.25 o 1 11 0 399.99 496.30 642.53 o 2 11 0 969.10 1049.99 545.28 o 3 11 0 444.09 483.44 600.64 o 4 11 0 8581.55 8701.97 645.03 o 5 11 0 197.18 289.60 585.15 o 6 11 0 1704.71 2112.95 612.46 o 7 11 0 4120.77 4048.46 677.93 o 8 11 0 3903.13 4155.51 642.25 o 9 11 0 302.58 617.00 617.75 o 10 11 0 699.47 301.03 704.49 o 11 11 0 174.47 -571.47 578.85 o 12 11 0 5772.62 5594.60 569.96 o 13 11 0 96.10 400.93 582.80 o 14 11 0 1229.47 1575.07 540.46 o 15 11 0 80.49 121.89 495.98 o 0 12 0 27467.09 28741.96 1723.80 o 1 12 0 1.10 107.56 687.22 o 2 12 0 12582.16 12577.81 637.14 o 3 12 0 4122.23 3879.55 516.35 o 4 12 0 3175.36 3867.88 593.89 o 5 12 0 806.81 1990.57 630.18 o 6 12 0 3435.89 3177.63 670.94 o 7 12 0 1039.66 1579.54 618.75 o 8 12 0 794.14 1868.63 652.95 o 9 12 0 65.12 -364.35 592.96 o 10 12 0 633.97 1304.86 662.55 o 11 12 0 2706.53 2864.85 606.83 o 12 12 0 54.37 241.35 600.37 o 13 12 0 484.75 440.09 537.53 o 14 12 0 3311.63 2570.69 559.46 o 1 13 0 425.88 600.72 557.10 o 2 13 0 3196.44 3173.94 568.84 o 3 13 0 1869.07 2223.75 597.06 o 4 13 0 996.35 1277.14 576.73 o 5 13 0 7272.15 8079.73 625.05 o 6 13 0 68.13 871.43 570.51 o 7 13 0 737.83 861.90 624.95 o 8 13 0 787.61 1245.46 517.47 o 9 13 0 238.34 227.76 553.77 o 10 13 0 125.82 862.54 744.63 o 11 13 0 607.20 972.61 642.52 o 12 13 0 1167.96 766.31 598.35 o 13 13 0 74.43 411.30 506.02 o 14 13 0 21.54 241.91 482.45 o 0 14 0 10988.98 12300.61 1481.03 o 1 14 0 28031.21 27010.89 778.06 o 2 14 0 577.52 710.77 523.88 o 3 14 0 850.25 1052.64 618.54 o 4 14 0 245.39 1250.34 538.77 o 5 14 0 2875.47 2770.86 559.70 o 6 14 0 40.72 326.91 614.23 o 7 14 0 175.01 555.23 535.94 o 8 14 0 364.07 714.96 550.67 o 9 14 0 3377.30 2787.54 653.31 o 10 14 0 508.93 1432.39 552.77 o 11 14 0 0.97 576.28 618.84 o 12 14 0 253.90 1212.58 552.62 o 13 14 0 29.51 1268.99 530.70 o 1 15 0 86.11 226.06 508.17 o 2 15 0 1685.85 2424.93 526.76 o 3 15 0 1260.84 1790.85 553.02 o 4 15 0 528.72 883.06 537.25 o 5 15 0 433.26 512.64 549.99 o 6 15 0 1573.62 1623.56 529.78 o 7 15 0 1313.13 2174.50 570.03 o 8 15 0 2014.13 1430.08 539.41 o 9 15 0 177.56 -555.63 555.63 o 10 15 0 319.27 101.40 550.71 o 11 15 0 300.16 94.42 567.10 o 12 15 0 382.59 189.44 556.70 o 0 16 0 6057.49 6638.69 661.54 o 1 16 0 3532.58 2711.73 570.42 o 2 16 0 266.74 1435.59 572.37 o 3 16 0 425.60 603.07 511.26 o 4 16 0 243.67 174.42 523.73 o 5 16 0 919.83 1097.86 491.98 o 6 16 0 1028.21 593.03 552.71 o 7 16 0 1925.08 3039.98 640.44 o 8 16 0 199.14 629.54 482.61 o 9 16 0 755.46 1009.71 605.15 o 10 16 0 1.46 -43.68 481.82 o 11 16 0 171.88 -130.73 493.65 o 12 16 0 482.46 325.06 583.22 o 1 17 0 3297.95 3815.11 536.98 o 2 17 0 1285.66 1374.03 468.94 o 3 17 0 396.61 722.49 552.42 o 4 17 0 3218.78 2737.27 487.10 o 5 17 0 216.93 228.72 515.56 o 6 17 0 284.30 1504.83 499.72 o 7 17 0 907.43 738.21 505.08 o 8 17 0 96.36 956.51 537.93 o 9 17 0 1453.77 1447.27 487.31 o 10 17 0 100.01 755.12 499.14 o 11 17 0 409.72 796.84 698.34 o 0 18 0 4034.63 3612.74 753.55 o 1 18 0 3158.78 3678.12 511.19 o 2 18 0 179.67 561.61 501.77 o 3 18 0 1073.58 729.58 534.32 o 4 18 0 465.60 174.70 507.22 o 5 18 0 62.03 855.28 482.94 o 6 18 0 230.74 144.85 690.01 o 7 18 0 534.75 293.81 449.55 o 8 18 0 388.91 1107.11 509.17 o 9 18 0 60.04 -205.41 426.05 o 1 19 0 560.67 1263.67 407.46 o 2 19 0 0.59 153.52 506.04 o 3 19 0 1231.93 1377.63 454.67 o 4 19 0 1425.76 1113.85 473.39 o 5 19 0 1107.26 1161.99 499.41 o 6 19 0 64.30 449.15 409.85 o 7 19 0 169.31 1180.33 525.04 o 8 19 0 876.94 1151.49 534.17 o 0 20 0 923.45 411.26 814.56 o 1 20 0 67.90 271.75 456.65 o 2 20 0 266.81 591.61 446.81 o 3 20 0 335.84 776.28 421.36 o 4 20 0 2.29 500.05 510.50 o 5 20 0 586.28 818.70 456.29 o 6 20 0 61.04 193.12 549.67 o 1 21 0 52.37 381.66 414.45 o 2 21 0 119.40 761.63 454.89 o 3 21 0 255.73 1286.10 460.30 o 4 21 0 241.76 188.59 443.00 o -17 0 1 128.66 694.98 808.34 o -15 0 1 2970.27 3212.82 1073.04 o -13 0 1 205.47 284.17 1045.34 o -11 0 1 5676.93 6129.60 1118.51 o -9 0 1 7499.99 7271.65 894.43 o -7 0 1 6416.97 6154.31 1177.80 o -5 0 1 11112.33 11464.53 1588.74 o -3 0 1 135043.23 134725.83 3523.06 o 3 0 1 38313.33 40670.06 2069.98 o 5 0 1 696.89 655.60 1630.52 o 7 0 1 43966.06 44177.98 1456.98 o 9 0 1 6453.81 5515.66 1133.17 o 11 0 1 1406.31 1954.34 1236.68 o 13 0 1 1878.43 2295.81 1007.90 o 15 0 1 787.90 955.47 865.11 o 17 0 1 527.51 323.98 875.31 o -18 1 1 762.74 600.76 624.97 o -17 1 1 7.49 337.38 556.66 o -16 1 1 515.24 143.72 612.22 o -15 1 1 167.16 903.47 647.66 o -14 1 1 247.50 202.42 679.60 o -13 1 1 1051.72 1560.58 783.77 o -12 1 1 3581.02 3984.75 786.15 o -11 1 1 562.33 702.97 716.54 o -10 1 1 3146.42 3996.00 734.16 o -9 1 1 2.68 112.12 746.04 o -8 1 1 1780.67 1600.39 772.92 o -7 1 1 36162.24 35819.05 970.17 o -6 1 1 685.75 668.64 982.24 o -5 1 1 106.21 887.40 1160.52 o -4 1 1 3655.83 3900.50 1169.02 o -3 1 1 12762.77 11004.08 1459.19 o 2 1 1 1308.46 1034.32 2024.96 o 3 1 1 11830.13 11978.59 1373.23 o 4 1 1 2451.38 1903.60 981.29 o 5 1 1 9042.32 8244.24 1055.51 o 6 1 1 898.15 1605.63 826.51 o 7 1 1 269.75 1046.08 714.60 o 8 1 1 263.86 980.14 677.19 o 9 1 1 209.94 915.24 779.77 o 10 1 1 620.61 1050.95 718.40 o 11 1 1 172.40 -4.05 807.74 o 12 1 1 78.79 1129.89 747.65 o 13 1 1 33.16 803.60 678.38 o 14 1 1 265.86 -307.60 634.64 o 15 1 1 1360.30 1454.98 642.70 o 16 1 1 13.09 566.27 589.56 o 17 1 1 1.69 156.16 581.58 o -18 2 1 238.56 96.00 671.06 o -17 2 1 17.28 250.95 643.50 o -16 2 1 11.51 -152.79 639.13 o -15 2 1 1901.83 1818.95 611.26 o -14 2 1 6.59 254.26 667.65 o -13 2 1 235.84 227.28 593.39 o -12 2 1 1082.09 1041.51 706.25 o -11 2 1 299.38 1262.28 771.86 o -10 2 1 1114.63 1454.10 659.72 o -9 2 1 243.60 280.62 694.81 o -8 2 1 7472.77 7316.78 785.02 o -7 2 1 3552.00 3086.79 805.60 o -6 2 1 448.17 747.02 944.72 o -5 2 1 7188.75 6407.42 1183.21 o -4 2 1 2073.59 2175.24 1289.26 o -3 2 1 8403.98 8476.11 1387.19 o 2 2 1 9387.10 7620.65 1213.54 o 3 2 1 1173.29 1114.35 1447.70 o 4 2 1 109.69 960.43 1201.67 o 5 2 1 29450.69 26867.75 1101.28 o 6 2 1 8.80 559.94 765.09 o 7 2 1 1263.51 2145.07 833.58 o 8 2 1 10347.50 10580.41 707.70 o 9 2 1 3662.70 2548.31 631.58 o 10 2 1 5300.28 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