#------------------------------------------------------------------------------
#$Date: 2009-05-03 21:56:13 +0300 (Sun, 03 May 2009) $
#$Revision: 691 $
#$URL: file:///home/coder/svn-repositories/cod/hkl/2/2218320.hkl $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided by IUCr Journals, http://journals.iucr.org/.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_2218320_Fobs
loop_
_publ_author_name
'Horchani-Naifer, Karima'
'F\'erid, Mokhtar'
_publ_section_title
;
 Lutetium ultraphosphate
;
_journal_coeditor_code           BR2072
_journal_issue                   6
_journal_name_full               'Acta Crystallographica Section E'
_journal_page_first              i33
_journal_volume                  64
_journal_year                    2008
_space_group_IT_number           15
_symmetry_space_group_name_Hall  '-C 2yc'
_symmetry_space_group_name_H-M   'C 1 2/c 1'
_cell_angle_alpha                90.000
_cell_angle_beta                 91.295
_cell_angle_gamma                90.000
_cell_length_a                   12.8128
_cell_length_b                   12.6821
_cell_length_c                   12.3330
_exptl_crystal_F_000             2064.00
_reflns_d_resolution_high        0.7110
_[local]_cod_data_source_file    br2072Isup2.hkl
_[local]_cod_data_source_block   I
#BEGIN Tags that were not found in dictionaries:
_shelx_title                     '    u14 in C 2/c'
_shelx_refln_list_code           4
_shelx_F_calc_maximum            696.31
_shelx_F_squared_multiplier      1.000
#END Tags that were not found in dictionaries
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, y, -z+1/2'
'x+1/2, y+1/2, z'
'-x+1/2, y+1/2, -z+1/2'
'-x, -y, -z'
'x, -y, z-1/2'
'-x+1/2, -y+1/2, -z'
'x+1/2, -y+1/2, z-1/2'
loop_
_refln_index_h
_refln_index_k
_refln_index_l
_refln_F_squared_calc
_refln_F_squared_meas
_refln_F_squared_sigma
_refln_observed_status
2 0 0 186269.81 224723.33 1576.54 o
4 0 0 81654.28 87061.59 751.41 o
6 0 0 235836.05 245272.28 1455.49 o
8 0 0 178415.88 189930.97 6188.54 o
10 0 0 68111.35 68367.91 643.87 o
12 0 0 166787.86 169731.03 2507.32 o
14 0 0 33803.59 35899.53 948.95 o
16 0 0 42389.71 42215.62 1552.61 o
18 0 0 9676.21 9716.27 797.69 o
1 1 0 243.36 624.79 46.34 o
3 1 0 34975.46 39560.08 804.08 o
5 1 0 25521.68 29409.58 879.72 o
7 1 0 223.42 243.91 35.63 o
9 1 0 1281.94 1268.29 71.42 o
11 1 0 677.99 672.11 82.87 o
13 1 0 3773.25 3762.62 195.89 o
15 1 0 1387.66 1330.02 139.95 o
17 1 0 1286.60 1282.14 296.32 o
0 2 0 128636.49 144042.63 4025.92 o
2 2 0 357531.56 387451.00 10287.15 o
4 2 0 139695.61 153340.30 3936.40 o
6 2 0 214280.03 228344.31 4521.03 o
8 2 0 141143.94 143851.52 1931.98 o
10 2 0 85924.22 88419.31 1468.53 o
12 2 0 36543.59 37650.99 892.67 o
14 2 0 107853.45 113977.23 2554.90 o
16 2 0 37700.57 41391.07 960.13 o
1 3 0 35307.98 39388.11 865.05 o
3 3 0 4711.28 5267.85 90.97 o
5 3 0 9790.55 9855.13 225.32 o
7 3 0 205.00 165.16 35.30 o
9 3 0 913.87 774.47 62.40 o
11 3 0 1379.53 1267.92 83.21 o
13 3 0 3082.30 2909.86 139.05 o
15 3 0 28.79 64.17 81.29 o
17 3 0 283.28 154.96 100.73 o
0 4 0 69554.72 73512.88 3018.23 o
2 4 0 54304.19 55348.75 1201.55 o
4 4 0 98584.23 105189.99 1337.60 o
6 4 0 78431.94 79486.52 926.57 o
8 4 0 96723.76 99528.41 1283.66 o
10 4 0 44604.51 44092.67 680.19 o
12 4 0 83315.08 82926.87 1300.76 o
14 4 0 46128.31 47021.68 774.09 o
16 4 0 25405.17 26946.09 656.21 o
1 5 0 18148.54 20955.73 408.32 o
3 5 0 1196.80 1520.45 54.59 o
5 5 0 8745.86 9397.57 207.68 o
7 5 0 19645.43 20606.85 555.06 o
9 5 0 381.62 331.29 47.74 o
11 5 0 283.41 281.12 81.60 o
13 5 0 1726.27 1675.54 128.34 o
15 5 0 1150.24 1091.36 142.46 o
17 5 0 531.75 397.38 126.66 o
0 6 0 35498.22 36550.20 1455.86 o
2 6 0 113881.23 118215.42 2292.29 o
4 6 0 8849.85 8130.10 228.48 o
6 6 0 109170.91 109885.37 1275.11 o
8 6 0 84391.31 86570.05 1305.88 o
10 6 0 25609.39 24169.72 397.33 o
12 6 0 5466.54 5175.17 196.91 o
14 6 0 30937.54 30987.76 818.96 o
16 6 0 2818.07 2706.44 223.27 o
1 7 0 1738.91 1748.56 61.67 o
3 7 0 7354.38 7760.28 148.53 o
5 7 0 1644.84 1649.53 65.56 o
7 7 0 8415.85 8833.99 241.21 o
9 7 0 7713.99 7059.61 500.12 o
11 7 0 85.97 110.91 69.42 o
13 7 0 15190.80 15054.04 351.24 o
15 7 0 1365.86 1146.80 172.66 o
0 8 0 49311.26 52499.43 809.26 o
2 8 0 2226.90 2325.80 74.10 o
4 8 0 33553.83 33843.13 607.80 o
6 8 0 13308.34 13441.70 303.57 o
8 8 0 2066.78 1973.17 113.62 o
10 8 0 12180.17 12168.57 661.79 o
12 8 0 13873.31 13797.71 340.25 o
14 8 0 2349.38 2392.18 242.77 o
16 8 0 10048.03 10442.39 580.67 o
1 9 0 3618.24 3712.03 95.55 o
3 9 0 31185.82 31536.88 462.92 o
5 9 0 16233.14 17398.29 250.06 o
7 9 0 5028.48 5270.60 175.48 o
9 9 0 12284.67 11927.44 554.23 o
11 9 0 11902.99 11746.23 316.62 o
13 9 0 1056.38 970.73 113.15 o
15 9 0 1718.46 1638.23 191.49 o
0 10 0 57972.12 55986.46 732.61 o
2 10 0 1190.19 1305.52 150.85 o
4 10 0 10976.11 10450.70 196.12 o
6 10 0 17713.37 17626.43 426.83 o
8 10 0 101.79 142.10 57.44 o
10 10 0 226.03 252.76 77.73 o
12 10 0 710.88 701.26 105.13 o
14 10 0 1056.54 1270.27 190.85 o
1 11 0 10143.46 9818.72 189.51 o
3 11 0 3519.47 3988.28 126.96 o
5 11 0 49337.73 48180.13 526.37 o
7 11 0 16001.68 15884.56 302.98 o
9 11 0 3242.45 3443.99 151.91 o
11 11 0 9812.24 9370.05 399.36 o
13 11 0 2161.67 2410.70 215.73 o
0 12 0 1408.88 1516.58 219.78 o
2 12 0 7613.78 7372.38 199.62 o
4 12 0 2552.12 2236.18 118.74 o
6 12 0 1755.79 1756.44 116.51 o
8 12 0 9240.50 8942.09 235.04 o
10 12 0 6178.75 5801.83 204.84 o
12 12 0 2235.12 2262.14 161.55 o
1 13 0 5343.21 5477.92 177.69 o
3 13 0 6721.09 6311.36 229.54 o
5 13 0 5857.47 5671.47 184.99 o
7 13 0 1471.85 1443.89 111.06 o
9 13 0 4652.09 4672.48 175.43 o
11 13 0 14261.72 13847.37 349.09 o
0 14 0 33111.25 34057.12 1273.54 o
2 14 0 7566.44 7250.43 245.38 o
4 14 0 4058.79 3964.74 191.16 o
6 14 0 22037.60 21324.39 424.04 o
8 14 0 20121.38 19815.13 352.17 o
10 14 0 1012.89 955.13 99.10 o
1 15 0 1342.94 1373.04 129.32 o
3 15 0 40027.96 39482.13 1433.26 o
5 15 0 5079.35 5082.47 215.83 o
7 15 0 171.57 131.27 71.25 o
9 15 0 8583.92 8385.11 268.20 o
0 16 0 39498.75 37123.88 979.71 o
2 16 0 31910.55 31805.29 1280.97 o
4 16 0 22037.80 20976.11 428.63 o
6 16 0 23130.93 22816.77 446.73 o
1 17 0 10704.73 10958.05 381.47 o
3 17 0 5437.88 5262.95 224.00 o
5 17 0 3366.86 3018.34 224.97 o
-17 1 1 5517.96 5461.96 441.97 o
-15 1 1 9189.22 9446.88 272.04 o
-13 1 1 52.71 131.60 56.20 o
-11 1 1 11390.27 10982.84 313.54 o
-9 1 1 17647.38 17861.42 670.18 o
-7 1 1 31748.74 34198.34 929.58 o
-5 1 1 14157.91 14661.80 185.79 o
-3 1 1 23293.98 26564.07 595.51 o
-1 1 1 4064.49 5075.04 101.15 o
1 1 1 2293.02 3137.47 106.97 o
3 1 1 2549.09 3378.98 263.40 o
5 1 1 1235.15 1257.35 53.43 o
7 1 1 1313.52 1760.71 172.03 o
9 1 1 323.35 388.39 47.32 o
11 1 1 1647.37 1556.96 84.57 o
13 1 1 241.83 287.41 52.42 o
15 1 1 911.49 939.39 128.27 o
17 1 1 6449.07 6346.71 672.59 o
-16 2 1 89.76 1.24 101.55 o
-14 2 1 6376.10 6399.71 229.72 o
-12 2 1 137.19 192.85 52.29 o
-10 2 1 13477.33 13209.62 437.31 o
-8 2 1 27108.71 27788.03 480.06 o
-6 2 1 7852.54 8278.50 148.65 o
-4 2 1 41621.29 46577.95 883.83 o
-2 2 1 1029.25 1430.50 50.60 o
0 2 1 31.39 370.69 21.94 o
2 2 1 16946.13 18095.73 517.44 o
4 2 1 56710.01 64386.58 1031.00 o
6 2 1 1434.91 1683.35 62.38 o
8 2 1 1130.54 1160.54 63.82 o
10 2 1 9676.49 9274.76 199.43 o
12 2 1 20.20 51.80 41.51 o
14 2 1 617.22 543.22 75.28 o
16 2 1 2247.80 2147.64 174.71 o
-17 3 1 2192.32 1978.91 216.77 o
-15 3 1 16169.91 17303.04 413.13 o
-13 3 1 18717.07 19803.74 552.90 o
-11 3 1 23738.00 22991.08 368.12 o
-9 3 1 56527.21 57286.00 1234.62 o
-7 3 1 65765.56 69388.72 757.79 o
-5 3 1 45862.13 48705.17 655.29 o
-3 3 1 134956.31 137189.14 1285.13 o
-1 3 1 567.17 865.79 49.10 o
1 3 1 76883.03 85064.72 2649.58 o
3 3 1 127397.49 135542.78 2112.15 o
5 3 1 5552.98 6012.39 162.42 o
7 3 1 7350.04 6686.60 268.63 o
9 3 1 69380.88 70043.05 827.69 o
11 3 1 548.16 494.84 59.84 o
13 3 1 21659.13 21267.81 452.69 o
15 3 1 14324.67 13877.20 342.64 o
17 3 1 4473.52 3988.27 355.11 o
-16 4 1 3092.14 3153.62 211.21 o
-14 4 1 72.69 102.66 74.64 o
-12 4 1 3631.91 3617.79 125.69 o
-10 4 1 5942.14 5910.05 148.36 o
-8 4 1 2928.28 2784.22 95.83 o
-6 4 1 7823.53 8677.36 150.82 o
-4 4 1 24265.06 28879.56 628.80 o
-2 4 1 77357.42 80649.81 717.34 o
0 4 1 395.94 450.90 32.02 o
2 4 1 25150.41 28636.15 316.86 o
4 4 1 3566.02 2839.92 93.92 o
6 4 1 13876.56 14604.02 252.32 o
8 4 1 2247.11 2232.28 85.53 o
10 4 1 20315.21 20762.81 360.72 o
12 4 1 8439.25 8094.27 286.48 o
14 4 1 3052.30 2872.41 168.38 o
16 4 1 251.51 285.04 113.15 o
-17 5 1 20729.81 21119.31 680.36 o
-15 5 1 1084.83 777.10 127.62 o
-13 5 1 44460.43 46109.09 754.85 o
-11 5 1 87943.09 86834.39 978.78 o
-9 5 1 3524.63 3686.90 114.03 o
-7 5 1 50109.43 51320.08 517.87 o
-5 5 1 214491.28 218413.55 2255.07 o
-3 5 1 17396.08 19345.53 292.37 o
-1 5 1 87537.88 85973.59 1561.93 o
1 5 1 160957.95 165098.78 3904.29 o
3 5 1 173918.88 177794.33 2726.39 o
5 5 1 122561.06 126582.02 2303.53 o
7 5 1 63544.62 65049.09 1101.90 o
9 5 1 78613.65 80245.35 485.31 o
11 5 1 83581.33 84944.73 845.25 o
13 5 1 24905.64 24570.59 563.13 o
15 5 1 52543.18 49979.13 1228.04 o
17 5 1 14523.24 14233.90 464.14 o
-16 6 1 2778.78 2608.68 164.24 o
-14 6 1 1967.09 2025.91 180.83 o
-12 6 1 344.09 315.78 73.47 o
-10 6 1 283.64 309.91 51.03 o
-8 6 1 587.58 540.09 48.41 o
-6 6 1 56.69 104.45 29.98 o
-4 6 1 953.89 964.36 51.52 o
-2 6 1 12943.50 13922.16 403.87 o
0 6 1 814.97 744.97 43.87 o
2 6 1 1629.00 1684.85 51.91 o
4 6 1 29485.98 30897.43 1030.44 o
6 6 1 22736.89 23558.17 391.66 o
8 6 1 83.32 144.31 41.36 o
10 6 1 9048.32 8632.92 372.36 o
12 6 1 1539.92 1599.00 172.19 o
14 6 1 1210.51 1150.22 122.42 o
16 6 1 3088.63 2925.74 228.60 o
-15 7 1 33474.63 32354.37 719.63 o
-13 7 1 43544.57 44860.48 756.79 o
-11 7 1 45294.43 46124.95 575.98 o
-9 7 1 123559.57 119969.73 1873.64 o
-7 7 1 54581.63 56156.21 775.91 o
-5 7 1 76275.25 73862.84 1148.20 o
-3 7 1 97727.97 92241.46 884.09 o
-1 7 1 66744.90 67212.81 1460.32 o
1 7 1 142344.89 147329.23 2514.85 o
3 7 1 313539.38 304738.00 5930.34 o
5 7 1 61470.44 61030.95 1076.65 o
7 7 1 36954.14 38010.12 718.90 o
9 7 1 87684.12 86313.91 2152.33 o
11 7 1 47035.84 46726.32 941.09 o
13 7 1 30326.19 28448.21 487.30 o
15 7 1 53515.24 52668.43 897.13 o
-16 8 1 2265.01 1988.47 309.92 o
-14 8 1 5456.74 5365.19 402.38 o
-12 8 1 1830.79 1703.36 139.31 o
-10 8 1 2426.52 2399.08 124.57 o
-8 8 1 1940.59 1898.44 89.56 o
-6 8 1 123.17 150.05 36.58 o
-4 8 1 211.71 256.13 39.14 o
-2 8 1 3998.90 4114.73 100.01 o
0 8 1 3313.04 3420.79 89.98 o
2 8 1 52.34 123.26 29.54 o
4 8 1 1112.88 1166.03 69.66 o
6 8 1 32.32 75.64 33.81 o
8 8 1 1909.25 1854.54 111.50 o
10 8 1 5251.63 5142.95 211.32 o
12 8 1 9.37 62.14 67.34 o
14 8 1 548.56 513.93 100.51 o
16 8 1 138.64 104.30 158.08 o
-15 9 1 44676.69 45458.41 903.76 o
-13 9 1 63225.73 64188.02 1169.47 o
-11 9 1 62016.88 63128.77 957.58 o
-9 9 1 55952.84 57575.19 1085.24 o
-7 9 1 57967.52 57569.29 701.36 o
-5 9 1 189088.80 177773.02 4060.00 o
-3 9 1 105688.20 100590.60 536.21 o
-1 9 1 72602.81 71287.84 902.57 o
1 9 1 166929.63 160807.25 1574.83 o
3 9 1 63833.70 62815.00 1506.33 o
5 9 1 32234.71 33242.36 360.61 o
7 9 1 134854.05 132260.17 1612.82 o
9 9 1 54895.93 55686.11 724.25 o
11 9 1 43887.49 42586.00 601.31 o
13 9 1 21388.26 20437.59 659.25 o
15 9 1 23279.39 23835.51 949.83 o
-14 10 1 7.48 96.94 106.24 o
-12 10 1 3308.22 3425.31 214.79 o
-10 10 1 5136.87 5369.73 182.43 o
-8 10 1 5508.41 5250.93 178.72 o
-6 10 1 19315.85 19641.71 274.88 o
-4 10 1 3318.51 2947.15 111.80 o
-2 10 1 10528.02 10443.85 163.95 o
0 10 1 669.49 681.95 53.22 o
2 10 1 80.11 112.08 40.63 o
4 10 1 2329.98 2146.47 95.38 o
6 10 1 73.49 78.44 53.19 o
8 10 1 2836.94 2600.97 131.22 o
10 10 1 172.44 256.29 81.95 o
12 10 1 2062.99 1968.94 150.41 o
14 10 1 4.21 61.57 97.30 o
-13 11 1 31731.84 32345.23 1847.95 o
-11 11 1 26058.27 26006.59 479.76 o
-9 11 1 26284.28 25700.06 389.37 o
-7 11 1 66557.54 67245.14 1074.82 o
-5 11 1 99954.30 94950.16 1947.51 o
-3 11 1 91647.19 86819.58 607.73 o
-1 11 1 20176.31 19921.31 350.84 o
1 11 1 116330.00 111373.03 2167.01 o
3 11 1 123480.38 114027.55 2060.62 o
5 11 1 64933.54 62334.30 1377.36 o
7 11 1 75729.42 74424.35 1068.03 o
9 11 1 88818.87 88295.25 1201.85 o
11 11 1 22576.37 21701.35 617.16 o
13 11 1 54163.15 50968.42 804.59 o
-12 12 1 1203.29 1006.09 206.03 o
-10 12 1 2449.94 2575.23 135.34 o
-8 12 1 1999.93 1890.12 117.63 o
-6 12 1 335.06 354.61 70.16 o
-4 12 1 7829.16 7376.58 174.01 o
-2 12 1 170.05 197.57 59.46 o
0 12 1 98.71 126.43 55.40 o
2 12 1 7829.30 7375.05 170.63 o
4 12 1 909.35 757.34 81.02 o
6 12 1 438.27 404.93 71.29 o
8 12 1 1629.26 1505.00 113.56 o
10 12 1 96.57 164.90 65.96 o
12 12 1 26.34 71.53 73.49 o
-11 13 1 40710.77 41741.22 1005.56 o
-9 13 1 13254.65 13069.84 283.45 o
-7 13 1 47858.55 45769.31 854.34 o
-5 13 1 49379.45 48933.38 541.51 o
-3 13 1 35071.14 35182.68 441.13 o
-1 13 1 91318.46 91068.27 1133.72 o
1 13 1 28675.76 29398.76 460.86 o
3 13 1 17966.35 18058.82 713.26 o
5 13 1 77384.63 72941.41 847.68 o
7 13 1 19429.21 19104.99 341.59 o
9 13 1 32771.26 31779.85 813.49 o
11 13 1 58005.23 57519.42 1448.06 o
-10 14 1 4554.02 4372.97 171.75 o
-8 14 1 1676.72 1625.10 117.92 o
-6 14 1 186.40 201.42 77.01 o
-4 14 1 3207.21 3238.47 176.50 o
-2 14 1 8972.48 9451.76 236.33 o
0 14 1 2479.84 2626.48 131.85 o
2 14 1 7889.93 7719.21 254.61 o
4 14 1 12759.06 12136.24 323.67 o
6 14 1 3390.94 3201.26 149.55 o
8 14 1 6076.66 5971.43 200.88 o
10 14 1 6830.38 6605.75 209.53 o
-9 15 1 34716.79 34623.02 842.13 o
-7 15 1 26807.64 26739.94 477.42 o
-5 15 1 8624.88 8859.48 341.37 o
-3 15 1 25703.24 24860.44 488.04 o
-1 15 1 22260.70 22023.54 420.24 o
1 15 1 15952.10 15883.42 451.85 o
3 15 1 16019.53 16257.14 376.74 o
5 15 1 2659.19 2455.69 160.13 o
7 15 1 11977.07 11508.93 314.67 o
9 15 1 14508.69 14765.40 424.84 o
-6 16 1 11812.68 12020.23 325.19 o
-4 16 1 3033.28 2991.44 176.09 o
-2 16 1 9228.91 9835.63 358.17 o
0 16 1 15187.29 15921.16 454.98 o
2 16 1 5983.93 6026.09 232.19 o
4 16 1 11479.20 11825.21 324.60 o
6 16 1 8015.82 7926.43 266.81 o
-5 17 1 6484.45 6182.80 239.91 o
-3 17 1 542.82 613.77 121.98 o
-1 17 1 6725.38 6828.42 304.60 o
1 17 1 6929.28 7108.45 312.84 o
3 17 1 3710.81 3535.39 190.77 o
5 17 1 6719.61 6831.48 460.14 o
-16 0 2 43587.19 46447.61 1951.99 o
-14 0 2 29925.34 31083.21 668.27 o
-12 0 2 159305.23 163895.28 2434.60 o
-10 0 2 128214.25 129643.35 928.93 o
-8 0 2 112954.22 116651.96 1486.16 o
-6 0 2 175748.45 187366.19 6636.28 o
-4 0 2 57547.73 57972.44 424.64 o
-2 0 2 168002.50 182699.06 7596.29 o
0 0 2 111588.62 99853.14 1612.82 o
2 0 2 167122.66 182419.52 16587.76 o
4 0 2 254040.22 243568.70 17749.05 o
6 0 2 190137.91 194508.13 6124.26 o
8 0 2 146465.44 140500.22 1855.24 o
10 0 2 141345.80 133543.22 1127.10 o
12 0 2 37307.79 39216.24 515.25 o
14 0 2 49677.39 50222.43 1896.50 o
16 0 2 112668.90 111934.80 1742.33 o
-17 1 2 9.84 16.93 110.94 o
-15 1 2 5826.88 6082.86 219.70 o
-13 1 2 6766.36 6736.33 217.08 o
-11 1 2 12317.39 11532.05 269.70 o
-9 1 2 5980.25 5840.72 210.02 o
-7 1 2 16256.05 16091.54 348.50 o
-5 1 2 5389.99 5051.49 101.15 o
-3 1 2 62326.00 66266.98 982.05 o
-1 1 2 23999.65 25837.58 672.70 o
1 1 2 16811.04 17946.77 651.76 o
3 1 2 34470.12 38585.99 1244.81 o
5 1 2 1469.69 1627.46 114.97 o
7 1 2 175.26 173.90 33.99 o
9 1 2 741.93 625.21 56.05 o
11 1 2 22.54 56.87 38.44 o
13 1 2 520.77 449.22 65.10 o
15 1 2 698.40 558.26 85.27 o
17 1 2 1241.95 942.45 208.30 o
-16 2 2 29170.80 31251.00 627.25 o
-14 2 2 73003.05 73247.22 1443.47 o
-12 2 2 59335.43 59019.79 582.86 o
-10 2 2 170361.38 168960.03 1482.32 o
-8 2 2 173837.16 177702.09 954.66 o
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