#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/83/2218360.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2218360_Fobs loop_ _publ_author_name 'Fun, Hoong-Kun' 'Jebas, Samuel Robinson' 'Sujith, K. V.' 'Patil, P. S.' 'Kalluraya, B.' 'Dharmaprakash, S. M' _publ_section_title ; 4-(4-Bromobenzylideneamino)-1-(diphenylaminomethyl)-3-[1-(4-isobutylphenyl)ethyl]-1H-1,2,4-triazole-5(4H)-thione ; _journal_coeditor_code CI2592 _journal_issue 6 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o1001 _journal_page_last o1002 _journal_volume 64 _journal_year 2008 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 105.966 _cell_angle_gamma 90.000 _cell_length_a 10.9672 _cell_length_b 9.7833 _cell_length_c 28.6210 _exptl_crystal_F_000 1296.00 _reflns_d_resolution_high 0.6135 _[local]_cod_data_source_file ci2592Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' patil116_0m in P2(1)/c (100K)' _shelx_refln_list_code 4 _shelx_F_calc_maximum 393.37 _shelx_F_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 135.34 9.07 4.46 o 2 0 0 5019.14 5019.23 169.23 o 3 0 0 2380.91 2449.21 96.99 o 4 0 0 4240.96 4431.44 164.78 o 5 0 0 3.05 27.05 22.90 o 6 0 0 444.66 455.35 31.06 o 7 0 0 1066.12 1006.43 37.72 o 8 0 0 3327.06 3236.75 74.70 o 9 0 0 513.70 498.60 31.06 o 10 0 0 6218.98 6267.01 116.27 o 11 0 0 119.46 137.81 25.68 o 12 0 0 637.34 638.32 39.89 o 13 0 0 192.55 171.56 35.54 o 14 0 0 1119.05 1165.75 69.75 o 15 0 0 22.17 -36.43 58.95 o 16 0 0 28.52 2.31 69.17 o 17 0 0 228.20 233.02 101.91 o 1 1 0 1.09 -2.55 2.55 o 2 1 0 3257.40 3273.80 67.91 o 3 1 0 1893.57 1910.11 47.18 o 4 1 0 8.75 7.63 11.39 o 5 1 0 724.45 689.01 30.79 o 6 1 0 1354.60 1490.21 46.80 o 7 1 0 31.47 21.18 10.20 o 8 1 0 582.85 577.76 21.99 o 9 1 0 233.87 237.07 17.34 o 10 1 0 8.49 -10.94 13.69 o 11 1 0 25.80 14.47 15.41 o 12 1 0 249.47 283.41 23.94 o 13 1 0 3.13 25.79 21.51 o 14 1 0 40.43 13.73 32.57 o 15 1 0 19.20 40.56 36.88 o 16 1 0 2.23 -41.45 41.45 o 17 1 0 24.08 41.61 60.51 o 0 2 0 154736.45 148163.38 2166.39 o 1 2 0 13744.33 14370.84 182.56 o 2 2 0 15724.65 16295.63 237.15 o 3 2 0 41.52 67.87 8.25 o 4 2 0 2011.30 1915.39 43.88 o 5 2 0 571.48 587.35 24.98 o 6 2 0 352.57 310.65 16.02 o 7 2 0 221.96 221.33 16.24 o 8 2 0 598.67 617.70 22.18 o 9 2 0 3112.71 3031.08 53.71 o 10 2 0 1392.24 1344.90 46.89 o 11 2 0 2248.34 2345.58 55.66 o 12 2 0 1673.19 1604.56 53.45 o 13 2 0 208.45 213.53 33.37 o 14 2 0 494.02 480.91 48.48 o 15 2 0 108.57 18.15 41.78 o 16 2 0 75.64 157.81 50.56 o 17 2 0 68.93 4.47 61.12 o 1 3 0 178.67 145.51 6.01 o 2 3 0 516.75 509.10 18.72 o 3 3 0 225.29 242.69 11.55 o 4 3 0 5309.82 5620.98 91.60 o 5 3 0 1800.76 1907.99 49.97 o 6 3 0 50.00 59.45 11.48 o 7 3 0 85.05 69.82 13.10 o 8 3 0 35.29 19.23 15.14 o 9 3 0 193.32 156.59 20.97 o 10 3 0 351.03 381.81 32.13 o 11 3 0 46.89 40.12 28.64 o 12 3 0 158.41 188.16 28.87 o 13 3 0 18.07 -17.43 30.16 o 14 3 0 3.00 3.08 34.26 o 15 3 0 368.02 403.85 58.23 o 16 3 0 59.41 30.42 49.46 o 0 4 0 17479.65 17771.81 252.68 o 1 4 0 1821.70 1779.99 22.33 o 2 4 0 10572.36 10259.78 126.54 o 3 4 0 5636.52 5369.65 80.21 o 4 4 0 1861.89 1953.55 33.32 o 5 4 0 287.97 319.61 14.71 o 6 4 0 808.52 857.07 25.24 o 7 4 0 3229.77 3182.22 53.89 o 8 4 0 1944.41 1766.67 48.88 o 9 4 0 139.57 180.01 25.21 o 10 4 0 2146.35 2021.51 84.39 o 11 4 0 2252.09 2275.32 71.21 o 12 4 0 1146.27 1136.56 54.29 o 13 4 0 649.86 669.24 46.24 o 14 4 0 362.53 416.62 44.13 o 15 4 0 64.79 135.29 60.21 o 16 4 0 104.08 71.08 50.26 o 1 5 0 1212.17 1307.48 22.95 o 2 5 0 5330.71 5372.09 63.96 o 3 5 0 804.99 888.99 16.93 o 4 5 0 582.12 549.98 18.42 o 5 5 0 143.99 105.62 11.35 o 6 5 0 1.01 5.22 10.29 o 7 5 0 193.34 145.44 16.44 o 8 5 0 83.60 92.70 20.33 o 9 5 0 201.04 242.23 31.39 o 10 5 0 0.79 32.87 23.78 o 11 5 0 358.62 356.72 36.56 o 12 5 0 38.54 21.59 32.44 o 13 5 0 477.38 519.48 51.22 o 14 5 0 173.39 276.74 45.37 o 15 5 0 44.15 7.09 43.65 o 16 5 0 2.15 -26.75 47.51 o 0 6 0 5657.55 5611.74 90.85 o 1 6 0 6269.54 6240.35 66.97 o 2 6 0 7315.03 6950.91 78.57 o 3 6 0 3707.54 3759.47 49.09 o 4 6 0 13.47 7.09 7.86 o 5 6 0 64.11 57.22 12.20 o 6 6 0 301.55 311.18 21.45 o 7 6 0 654.44 650.36 27.20 o 8 6 0 1579.78 1548.87 85.49 o 9 6 0 720.79 838.12 43.88 o 10 6 0 67.96 69.39 27.66 o 11 6 0 1479.77 1478.53 61.39 o 12 6 0 623.37 649.63 53.57 o 13 6 0 10.76 61.64 39.89 o 14 6 0 432.45 404.82 58.04 o 15 6 0 109.96 62.50 63.79 o 1 7 0 1067.30 1137.37 21.62 o 2 7 0 96.11 127.40 9.61 o 3 7 0 915.45 935.16 24.37 o 4 7 0 2032.75 1890.38 37.49 o 5 7 0 811.28 778.01 30.98 o 6 7 0 658.79 599.26 23.80 o 7 7 0 75.27 54.03 18.62 o 8 7 0 2.29 -21.35 21.35 o 9 7 0 27.31 37.09 21.26 o 10 7 0 6.66 35.16 28.46 o 11 7 0 28.93 26.57 32.08 o 12 7 0 77.38 60.19 36.10 o 13 7 0 1165.44 1261.01 83.31 o 14 7 0 11.53 152.51 65.58 o 15 7 0 5.71 10.28 71.01 o 0 8 0 4670.76 4516.05 89.07 o 1 8 0 837.87 846.47 24.36 o 2 8 0 4556.77 4460.84 58.44 o 3 8 0 2170.91 2131.06 38.80 o 4 8 0 15.64 -5.50 12.75 o 5 8 0 43.23 50.01 14.92 o 6 8 0 81.92 53.91 15.81 o 7 8 0 227.00 220.56 46.02 o 8 8 0 325.06 349.14 29.22 o 9 8 0 671.75 738.70 38.81 o 10 8 0 282.47 282.51 32.23 o 11 8 0 313.68 287.69 36.26 o 12 8 0 456.68 403.90 58.59 o 13 8 0 13.22 6.71 70.22 o 14 8 0 196.27 328.85 76.63 o 1 9 0 86.08 120.03 16.59 o 2 9 0 2.35 -16.54 16.54 o 3 9 0 178.11 125.56 15.88 o 4 9 0 564.57 497.63 24.04 o 5 9 0 120.66 108.37 17.30 o 6 9 0 1.94 -16.68 20.24 o 7 9 0 16.29 -4.93 18.65 o 8 9 0 10.28 -11.45 23.18 o 9 9 0 56.50 94.10 26.85 o 10 9 0 11.01 51.66 28.11 o 11 9 0 1.03 16.89 32.17 o 12 9 0 47.12 32.08 37.65 o 13 9 0 3.98 -26.44 58.73 o 14 9 0 8.94 30.97 64.49 o 0 10 0 1202.69 1226.33 50.43 o 1 10 0 81.22 77.44 18.29 o 2 10 0 396.35 376.16 29.18 o 3 10 0 724.54 724.96 35.37 o 4 10 0 3.45 21.48 17.77 o 5 10 0 0.62 24.93 18.60 o 6 10 0 21.37 2.96 19.74 o 7 10 0 141.23 172.78 27.68 o 8 10 0 66.77 71.02 23.43 o 9 10 0 660.76 728.14 58.12 o 10 10 0 443.63 500.07 42.78 o 11 10 0 328.83 379.24 69.64 o 12 10 0 91.64 91.22 45.32 o 13 10 0 160.48 227.53 56.29 o 1 11 0 86.16 54.56 19.47 o 2 11 0 184.31 152.00 29.22 o 3 11 0 22.40 50.82 29.33 o 4 11 0 229.81 222.81 35.94 o 5 11 0 84.13 86.09 29.10 o 6 11 0 2.23 -22.13 22.13 o 7 11 0 94.00 78.50 25.93 o 8 11 0 116.33 147.64 28.59 o 9 11 0 142.95 205.02 41.53 o 10 11 0 12.37 -16.94 40.91 o 11 11 0 10.05 24.67 44.40 o 12 11 0 158.59 121.87 51.56 o 0 12 0 449.84 485.45 57.58 o 1 12 0 40.40 38.25 28.46 o 2 12 0 304.95 305.03 31.78 o 3 12 0 216.55 270.50 62.63 o 4 12 0 234.61 208.41 46.62 o 5 12 0 252.75 306.14 48.50 o 6 12 0 215.08 200.98 38.86 o 7 12 0 4.17 0.10 34.13 o 8 12 0 27.28 -28.10 32.07 o 9 12 0 54.64 24.90 33.88 o 10 12 0 262.51 239.91 42.37 o 11 12 0 144.67 100.27 50.62 o 1 13 0 192.25 162.52 41.68 o 2 13 0 53.50 43.65 55.80 o 3 13 0 25.50 -13.69 37.74 o 4 13 0 112.54 112.38 62.79 o 5 13 0 19.84 1.92 69.94 o 6 13 0 2.53 63.18 44.12 o 7 13 0 162.90 156.35 42.72 o 8 13 0 232.13 178.36 44.31 o 9 13 0 31.24 38.11 41.14 o 0 14 0 454.59 649.11 86.08 o 1 14 0 156.80 155.20 47.26 o 2 14 0 95.88 138.80 63.33 o 3 14 0 399.96 393.96 77.78 o 4 14 0 1.93 -37.77 37.77 o 5 14 0 0.34 -49.42 49.42 o 6 14 0 154.75 128.69 102.52 o 7 14 0 194.63 231.73 53.95 o 8 14 0 13.50 5.76 48.56 o 1 15 0 50.87 21.44 45.79 o 2 15 0 53.73 48.26 64.87 o 3 15 0 2.19 -9.84 60.56 o 4 15 0 4.88 10.30 60.72 o 5 15 0 79.79 -50.42 62.71 o -17 1 1 4.85 18.40 96.76 o -16 1 1 56.38 53.61 46.20 o -15 1 1 222.26 236.11 44.16 o -14 1 1 347.07 353.60 43.28 o -13 1 1 2.12 -15.05 20.23 o -12 1 1 731.96 675.79 29.36 o -11 1 1 1249.31 1226.96 34.55 o -10 1 1 3798.50 3715.10 59.45 o -9 1 1 555.72 556.55 22.00 o -8 1 1 4069.62 4117.70 63.01 o -7 1 1 15990.88 15679.90 184.27 o -6 1 1 4184.76 4098.47 67.83 o -5 1 1 2904.75 2698.42 68.79 o -4 1 1 34.55 49.46 11.79 o -3 1 1 1538.85 1408.24 37.69 o -2 1 1 4633.75 4722.12 82.34 o -1 1 1 1978.08 1872.22 36.50 o 0 1 1 27009.39 26047.11 912.02 o 1 1 1 2019.47 2032.35 27.92 o 2 1 1 25263.60 24984.93 404.70 o 3 1 1 25578.57 25520.41 416.89 o 4 1 1 7679.49 7680.16 187.99 o 5 1 1 17306.99 17993.60 333.35 o 6 1 1 1525.97 1458.36 34.25 o 7 1 1 417.29 379.72 17.21 o 8 1 1 295.38 279.67 17.26 o 9 1 1 465.07 427.83 20.30 o 10 1 1 58.44 48.17 15.30 o 11 1 1 741.00 776.60 30.96 o 12 1 1 1095.69 1213.15 38.13 o 13 1 1 603.77 611.07 41.70 o 14 1 1 140.02 169.95 38.87 o 15 1 1 618.86 593.67 54.23 o 16 1 1 46.46 -19.59 42.51 o 17 1 1 57.24 86.38 61.00 o -17 2 1 28.10 20.98 47.03 o -16 2 1 32.98 15.73 45.51 o -15 2 1 4.71 -9.88 35.96 o -14 2 1 4.55 32.82 29.64 o -13 2 1 628.22 577.29 36.23 o -12 2 1 13.04 17.05 22.53 o -11 2 1 0.46 -4.32 16.49 o -10 2 1 61.25 30.30 15.23 o -9 2 1 110.28 111.78 19.68 o -8 2 1 181.88 183.00 15.13 o -7 2 1 160.10 153.78 15.80 o -6 2 1 200.26 247.02 17.29 o -5 2 1 2705.75 2924.06 50.97 o -4 2 1 289.68 343.60 42.19 o -3 2 1 17536.39 18123.04 298.54 o -2 2 1 1692.11 1679.06 36.23 o -1 2 1 2957.83 3182.29 47.98 o 0 2 1 1333.38 1379.00 23.90 o 1 2 1 14738.31 15296.92 193.50 o 2 2 1 96.56 138.84 10.74 o 3 2 1 4985.80 5181.46 93.78 o 4 2 1 4318.28 4790.27 90.75 o 5 2 1 0.02 -0.21 7.59 o 6 2 1 109.09 144.46 13.08 o 7 2 1 1288.98 1422.51 33.04 o 8 2 1 193.06 200.05 17.55 o 9 2 1 26.09 33.36 18.12 o 10 2 1 1.74 -11.58 15.27 o 11 2 1 108.47 98.95 21.58 o 12 2 1 85.28 125.91 26.53 o 13 2 1 67.95 40.22 32.65 o 14 2 1 22.02 28.85 35.02 o 15 2 1 12.53 -7.94 42.95 o 16 2 1 68.35 33.43 46.76 o -16 3 1 21.61 -21.08 48.43 o -15 3 1 99.65 120.15 47.51 o -14 3 1 29.22 44.50 31.85 o -13 3 1 91.59 92.17 30.89 o -12 3 1 1034.93 1197.72 83.74 o -11 3 1 385.51 399.59 36.73 o -10 3 1 8161.12 7960.90 145.60 o -9 3 1 1905.66 1687.41 43.69 o -8 3 1 5159.80 5014.26 81.58 o -7 3 1 4931.76 4873.41 76.11 o -6 3 1 2054.03 1924.25 40.78 o -5 3 1 1138.36 1014.82 28.24 o -4 3 1 2585.59 2275.73 44.92 o -3 3 1 3602.49 4005.99 71.35 o -2 3 1 1858.81 2063.52 43.96 o -1 3 1 873.11 914.10 22.02 o 0 3 1 22927.68 23357.81 234.05 o 1 3 1 329.49 294.91 10.83 o 2 3 1 614.33 452.34 13.85 o 3 3 1 14048.92 14098.33 278.57 o 4 3 1 13632.93 14007.47 189.79 o 5 3 1 3119.66 3045.70 67.24 o 6 3 1 4288.17 4196.52 66.10 o 7 3 1 12.62 25.24 15.53 o 8 3 1 29.68 2.51 14.62 o 9 3 1 46.32 22.98 17.36 o 10 3 1 101.90 125.02 26.74 o 11 3 1 1754.93 1842.06 61.14 o 12 3 1 260.09 312.37 33.07 o 13 3 1 971.87 1081.43 57.63 o 14 3 1 501.09 612.00 53.81 o 15 3 1 201.92 296.85 54.41 o 16 3 1 11.16 22.05 54.33 o -16 4 1 0.19 22.93 47.66 o -15 4 1 149.93 135.59 47.65 o -14 4 1 86.89 107.40 33.87 o -13 4 1 45.80 30.94 28.85 o -12 4 1 233.08 150.57 31.80 o -11 4 1 25.58 36.75 26.99 o -10 4 1 2.12 -20.49 20.49 o -9 4 1 477.34 535.87 40.24 o -8 4 1 452.43 499.32 32.74 o -7 4 1 36.39 45.33 11.92 o -6 4 1 449.58 467.84 15.77 o -5 4 1 275.18 362.40 12.75 o -4 4 1 2830.90 3127.84 46.15 o -3 4 1 1399.23 1472.13 29.31 o -2 4 1 155.66 135.75 11.25 o -1 4 1 1146.11 1210.79 17.81 o 0 4 1 24.95 47.71 4.81 o 1 4 1 720.90 725.10 12.40 o 2 4 1 411.04 432.99 12.09 o 3 4 1 5202.26 5600.88 82.64 o 4 4 1 297.06 326.87 14.33 o 5 4 1 309.90 355.06 19.34 o 6 4 1 16.85 11.01 9.12 o 7 4 1 21.06 10.28 11.66 o 8 4 1 69.57 42.94 20.96 o 9 4 1 16.46 5.49 20.74 o 10 4 1 205.90 181.53 28.52 o 11 4 1 104.36 95.48 28.62 o 12 4 1 517.66 613.51 44.48 o 13 4 1 96.95 67.54 31.80 o 14 4 1 90.93 87.11 49.72 o 15 4 1 48.27 35.57 46.80 o 16 4 1 0.00 21.66 47.49 o -16 5 1 3.57 -6.49 58.92 o -15 5 1 21.71 36.72 46.03 o -14 5 1 0.02 -16.43 36.24 o -13 5 1 34.67 39.73 54.20 o -12 5 1 1128.87 1216.68 67.33 o -11 5 1 526.57 541.60 48.89 o -10 5 1 1333.63 1364.80 65.91 o -9 5 1 1700.34 1691.41 55.98 o -8 5 1 5323.22 5232.17 96.37 o -7 5 1 1209.87 1116.97 37.38 o -6 5 1 2787.04 2728.80 60.19 o -5 5 1 330.83 290.92 14.42 o -4 5 1 996.96 989.77 20.21 o -3 5 1 553.56 624.91 15.60 o -2 5 1 543.92 612.09 17.51 o -1 5 1 3096.41 3065.85 36.03 o 0 5 1 271.74 229.37 10.44 o 1 5 1 12589.47 12747.33 126.30 o 2 5 1 9286.07 8872.64 100.35 o 3 5 1 4091.32 3877.33 44.89 o 4 5 1 7934.47 7680.67 93.80 o 5 5 1 1869.09 1853.33 31.90 o 6 5 1 533.45 526.04 20.50 o 7 5 1 319.21 324.54 20.76 o 8 5 1 605.34 596.49 34.21 o 9 5 1 951.84 927.68 56.68 o 10 5 1 4.43 -0.83 23.11 o 11 5 1 943.52 1082.53 59.90 o 12 5 1 286.17 389.39 44.53 o 13 5 1 903.54 899.83 62.71 o 14 5 1 167.03 133.36 60.74 o 15 5 1 206.12 227.19 56.32 o 16 5 1 95.13 226.30 57.86 o -15 6 1 315.40 432.18 198.90 o -14 6 1 188.33 275.66 48.50 o -13 6 1 131.99 110.23 40.08 o -12 6 1 112.43 2.66 46.55 o -11 6 1 19.45 9.94 29.05 o -10 6 1 5.32 27.74 25.97 o -9 6 1 41.03 21.58 23.91 o -8 6 1 0.56 -3.63 16.83 o -7 6 1 590.45 565.56 25.95 o -6 6 1 1596.81 1518.47 37.95 o -5 6 1 22.14 4.95 10.68 o -4 6 1 210.71 238.03 14.66 o -3 6 1 1087.69 1136.27 24.17 o -2 6 1 488.74 462.15 16.65 o -1 6 1 558.07 562.77 13.45 o 0 6 1 155.26 163.60 9.10 o 1 6 1 449.07 452.31 12.52 o 2 6 1 394.81 358.55 10.37 o 3 6 1 1380.71 1376.26 23.06 o 4 6 1 2035.55 1993.04 33.70 o 5 6 1 289.14 300.74 16.50 o 6 6 1 341.04 316.13 20.38 o 7 6 1 66.36 81.16 17.15 o 8 6 1 5.94 -16.50 16.50 o 9 6 1 1301.02 1109.57 48.36 o 10 6 1 66.21 55.74 26.88 o 11 6 1 26.71 56.74 28.91 o 12 6 1 31.74 57.87 34.71 o 13 6 1 16.61 -1.98 41.06 o 14 6 1 84.57 81.74 63.03 o 15 6 1 144.54 90.13 58.52 o -15 7 1 2.40 -42.18 61.57 o -14 7 1 0.98 39.34 49.68 o -13 7 1 1.01 25.13 42.90 o -12 7 1 38.06 -31.22 31.22 o -11 7 1 36.48 64.14 34.34 o -10 7 1 736.84 697.28 45.28 o -9 7 1 194.13 187.41 24.88 o -8 7 1 912.47 921.06 37.66 o -7 7 1 2838.26 2792.82 61.87 o -6 7 1 282.22 262.49 21.19 o -5 7 1 101.02 111.67 14.39 o -4 7 1 7025.68 6949.14 92.55 o -3 7 1 3082.63 3114.50 45.84 o -2 7 1 475.43 482.59 15.06 o -1 7 1 38.23 24.89 7.92 o 0 7 1 3462.87 3409.65 44.37 o 1 7 1 7007.12 7052.75 76.21 o 2 7 1 2411.22 2465.38 32.15 o 3 7 1 13068.01 12460.49 140.17 o 4 7 1 4078.62 3938.17 63.63 o 5 7 1 175.92 151.83 18.26 o 6 7 1 1697.27 1753.90 40.06 o 7 7 1 5.70 8.01 17.76 o 8 7 1 137.41 137.51 22.78 o 9 7 1 15.93 -7.71 19.86 o 10 7 1 115.01 135.80 26.53 o 11 7 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