#------------------------------------------------------------------------------ #$Date: 2009-05-03 21:56:13 +0300 (Sun, 03 May 2009) $ #$Revision: 691 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2218370.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2218370_Fobs loop_ _publ_author_name 'Yuan, Ji-Hong' 'Wang, Cheng' 'Yu, Ming-Juan' 'Li, Jing' _publ_section_title ; Tris[3,3'-(p-phenylenedimethylene)diimidazol-1-ium] bis(phosphatododecamolybdate) ; _journal_coeditor_code CS2077 _journal_issue 6 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m831 _journal_volume 64 _journal_year 2008 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 73.382 _cell_angle_beta 87.297 _cell_angle_gamma 67.557 _cell_length_a 11.8790 _cell_length_b 12.5030 _cell_length_c 18.4180 _exptl_crystal_F_000 2062.00 _reflns_d_resolution_high 0.7489 _[local]_cod_data_source_file cs2077Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' mm in P-1' _shelx_refln_list_code 4 _shelx_F_calc_maximum 709.52 _shelx_F_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 29057.15 29687.62 471.15 o 2 0 0 7264.57 7851.99 161.55 o 3 0 0 204199.02 199609.44 3034.78 o 4 0 0 22905.49 23382.72 439.65 o 5 0 0 21315.26 21654.73 434.25 o 6 0 0 7901.17 8711.03 246.60 o 7 0 0 26073.71 26720.34 558.90 o 8 0 0 8805.54 9451.73 294.75 o 9 0 0 3764.54 3767.37 189.00 o 10 0 0 11549.37 11478.06 368.10 o 11 0 0 1267.96 1320.74 132.30 o 12 0 0 91.50 37.50 33.89 o 13 0 0 8207.35 8103.54 356.85 o 14 0 0 115.06 140.40 77.85 o -14 1 0 1189.47 1077.74 157.95 o -13 1 0 2222.93 1980.88 188.10 o -12 1 0 4171.74 3993.72 237.60 o -11 1 0 781.12 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159759.25 155971.83 1787.46 o 3 3 0 110431.26 109158.17 1210.57 o 4 3 0 2084.70 2053.75 189.67 o 5 3 0 1196.22 1250.08 39.71 o 6 3 0 23087.48 22285.53 254.93 o 7 3 0 19012.50 18978.30 239.35 o 8 3 0 0.81 52.40 28.38 o 9 3 0 4.57 15.85 16.39 o 10 3 0 27852.46 28304.34 360.18 o 11 3 0 3035.18 3201.80 117.50 o 12 3 0 1562.88 1634.76 97.69 o -12 4 0 660.20 530.10 126.00 o -11 4 0 7871.79 7294.89 350.10 o -10 4 0 4103.89 4034.22 245.70 o -9 4 0 7839.60 7984.74 339.30 o -8 4 0 6107.10 6086.65 279.90 o -7 4 0 1644.32 1669.04 140.85 o -6 4 0 18599.95 19079.40 497.70 o -5 4 0 5670.42 5772.55 232.65 o -4 4 0 451.55 460.35 69.75 o -3 4 0 60338.33 61366.47 1083.14 o -2 4 0 515.09 630.90 69.30 o -1 4 0 45460.14 43774.76 786.59 o 0 4 0 10210.66 10307.62 261.45 o 1 4 0 11.95 86.12 75.82 o 2 4 0 112022.32 109713.48 2191.94 o 3 4 0 30812.57 30855.13 403.47 o 4 4 0 6446.27 6389.08 132.40 o 5 4 0 226.99 292.77 98.10 o 6 4 0 4825.83 4735.38 102.13 o 7 4 0 262711.41 256286.09 2234.39 o 8 4 0 25989.54 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3827.22 265.05 o -9 6 0 10462.17 10205.02 423.90 o -8 6 0 605.33 556.20 114.75 o -7 6 0 2144.18 2214.43 177.75 o -6 6 0 1396.60 1533.14 148.05 o -5 6 0 2884.44 2896.63 184.05 o -4 6 0 1398.07 1332.44 127.35 o -3 6 0 53.17 85.95 46.35 o -2 6 0 419.80 495.90 77.85 o -1 6 0 575.17 517.95 74.70 o 0 6 0 9811.79 11033.46 322.20 o 1 6 0 1081.25 1162.79 93.60 o 2 6 0 6815.18 6479.20 155.23 o 3 6 0 83424.87 82327.77 986.09 o 4 6 0 21150.33 20747.91 326.97 o 5 6 0 142.77 239.20 48.15 o 6 6 0 25922.18 24922.16 380.59 o 7 6 0 8.08 7.06 25.87 o 8 6 0 588.39 627.80 62.32 o 9 6 0 730.28 867.08 65.36 o 10 6 0 454.18 473.13 54.58 o 11 6 0 958.48 647.87 292.72 o 12 6 0 363.99 231.75 74.25 o 13 6 0 1448.21 1496.24 156.15 o 14 6 0 637.11 627.75 121.50 o -9 7 0 358.76 368.10 112.05 o -8 7 0 336.16 433.80 112.95 o -7 7 0 3.67 -5.40 45.00 o -6 7 0 302.79 279.00 85.05 o -5 7 0 449.35 432.45 96.30 o -4 7 0 152.47 123.30 58.50 o -3 7 0 299.36 314.10 76.05 o -2 7 0 10476.68 10471.42 349.20 o -1 7 0 14243.20 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3560.28 3712.92 251.55 o 1 3 24 510.91 402.75 109.35 o 2 3 24 766.72 710.54 139.05 o -2 4 24 31.51 58.05 53.10 o -1 4 24 156.39 88.20 59.85 o 0 4 24 2089.49 2407.93 216.90 o 1 4 24 396.59 342.45 108.45 o 2 4 24 144.09 103.05 77.40 o 3 4 24 485.70 526.50 123.30 o -2 5 24 593.22 1033.64 159.30 o -1 5 24 362.28 322.65 98.55 o 0 5 24 4913.87 5491.31 315.45 o 1 5 24 652.31 634.95 131.40 o 2 5 24 176.70 197.10 79.65 o 3 5 24 627.21 443.25 118.35 o 4 5 24 1596.03 1600.19 188.10 o -1 6 24 47.48 44.55 55.35 o 0 6 24 1180.51 1250.54 171.00 o 1 6 24 378.63 353.25 94.05 o 2 6 24 1121.32 1040.39 165.15 o 3 6 24 7342.32 8647.13 410.40 o 4 6 24 4934.90 4775.81 303.30 o 0 7 24 4091.73 4468.02 291.15 o 1 7 24 280.68 186.30 81.90 o 2 7 24 734.86 769.49 142.20 o 3 7 24 1890.13 1683.89 193.95 o 2 8 24 1574.20 1401.74 184.50 o