#------------------------------------------------------------------------------ #$Date: 2016-04-03 01:49:48 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181103 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/83/2218377.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2218377_Fobs loop_ _publ_author_name 'Rizal, Mohd. Razali' 'Ng, Seik Weng' _publ_section_title ; Low-temperature redetermination of trans-cyclohexane-1,2-dicarboxylic acid ; _journal_coeditor_code CV2404 _journal_issue 6 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o992 _journal_volume 64 _journal_year 2008 _space_group_IT_number 15 _symmetry_space_group_name_Hall '-C 2yc' _symmetry_space_group_name_H-M 'C 1 2/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 96.114 _cell_angle_gamma 90.000 _cell_length_a 5.5853 _cell_length_b 13.8404 _cell_length_c 10.0353 _exptl_crystal_F_000 368.00 _reflns_d_resolution_high 0.7697 _cod_data_source_file cv2404Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' CYHCAC10 in C2/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 127.35 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 13.51 21.32 2.11 o 4 0 0 280.83 308.96 9.76 o 6 0 0 32.93 45.09 10.41 o 1 1 0 3205.41 3009.25 37.05 o 3 1 0 2162.70 2402.13 31.62 o 5 1 0 443.29 494.01 14.63 o 7 1 0 77.74 75.28 9.92 o 0 2 0 13.25 17.72 1.51 o 2 2 0 4202.82 4188.37 67.70 o 4 2 0 172.59 163.82 6.03 o 6 2 0 0.02 -3.90 3.94 o 1 3 0 112.30 129.05 3.29 o 3 3 0 98.25 110.03 5.22 o 5 3 0 546.27 563.36 14.10 o 7 3 0 285.41 315.93 17.18 o 0 4 0 3402.38 3204.71 85.14 o 2 4 0 12.59 8.84 3.86 o 4 4 0 706.33 695.65 17.94 o 6 4 0 0.61 -0.21 4.29 o 1 5 0 77.69 83.36 3.06 o 3 5 0 1139.38 1179.75 34.69 o 5 5 0 577.42 563.36 16.97 o 0 6 0 4133.70 3896.04 78.34 o 2 6 0 211.52 204.24 5.78 o 4 6 0 59.75 60.95 5.62 o 6 6 0 33.50 45.95 6.30 o 1 7 0 1509.24 1571.48 23.02 o 3 7 0 580.44 519.36 15.55 o 5 7 0 235.06 217.85 12.35 o 0 8 0 801.21 771.70 20.02 o 2 8 0 768.75 763.71 14.61 o 4 8 0 72.52 91.25 13.92 o 6 8 0 0.09 -2.53 5.02 o 1 9 0 288.00 286.34 7.02 o 3 9 0 100.65 94.75 7.91 o 5 9 0 176.24 169.77 14.49 o 0 10 0 528.58 511.58 21.86 o 2 10 0 592.89 581.72 14.09 o 4 10 0 387.66 373.31 16.33 o 1 11 0 13.04 48.64 10.04 o 3 11 0 691.09 673.78 22.37 o 5 11 0 6.06 4.50 5.77 o 0 12 0 324.39 373.57 17.00 o 2 12 0 18.28 26.56 7.21 o 4 12 0 29.29 37.62 10.30 o 1 13 0 725.31 730.07 16.06 o 3 13 0 59.20 62.99 8.25 o 0 14 0 25.26 23.45 5.56 o 2 14 0 5.21 9.08 5.81 o 4 14 0 52.53 57.46 9.30 o 1 15 0 669.16 665.17 24.09 o 3 15 0 4.84 4.80 5.54 o 0 16 0 0.18 4.69 5.05 o 2 16 0 89.79 102.97 10.62 o 1 17 0 4.23 2.03 6.39 o -7 1 1 124.27 117.81 11.38 o -5 1 1 891.60 921.90 22.21 o -3 1 1 2415.59 2605.93 43.58 o -1 1 1 1940.39 1926.98 43.70 o 1 1 1 1638.92 1500.35 24.77 o 3 1 1 522.18 559.04 9.82 o 5 1 1 8.62 2.02 5.67 o 7 1 1 10.14 23.81 8.06 o -6 2 1 43.99 34.63 5.67 o -4 2 1 184.44 196.19 6.60 o -2 2 1 75.79 97.41 6.86 o 0 2 1 1825.15 1770.45 23.60 o 2 2 1 1227.22 1252.37 25.90 o 4 2 1 220.71 211.07 7.27 o 6 2 1 57.00 53.98 8.38 o -7 3 1 0.96 5.86 5.55 o -5 3 1 186.09 203.63 7.53 o -3 3 1 133.37 142.66 7.57 o -1 3 1 359.72 359.83 6.59 o 1 3 1 15.44 19.80 1.38 o 3 3 1 41.67 35.08 3.65 o 5 3 1 2.81 8.33 3.46 o 7 3 1 58.80 56.31 10.12 o -6 4 1 178.34 179.70 10.88 o -4 4 1 39.61 43.56 4.48 o -2 4 1 98.46 108.15 3.47 o 0 4 1 1920.73 1855.27 28.12 o 2 4 1 431.31 422.32 10.67 o 4 4 1 791.33 729.66 18.52 o 6 4 1 316.09 324.13 18.33 o -5 5 1 1199.94 1164.76 23.68 o -3 5 1 269.35 256.25 6.47 o -1 5 1 181.91 147.26 3.88 o 1 5 1 6422.22 6499.08 95.62 o 3 5 1 36.27 39.23 4.00 o 5 5 1 451.19 391.46 15.51 o -6 6 1 12.72 20.19 5.25 o -4 6 1 86.37 79.40 7.48 o -2 6 1 833.54 886.45 17.95 o 0 6 1 643.19 635.80 11.41 o 2 6 1 395.80 421.57 9.51 o 4 6 1 1487.52 1361.05 30.19 o 6 6 1 65.29 78.63 9.71 o -5 7 1 2.57 -2.05 4.06 o -3 7 1 602.98 638.48 29.74 o -1 7 1 241.33 230.40 5.64 o 1 7 1 173.54 198.18 5.36 o 3 7 1 656.63 613.95 15.98 o 5 7 1 104.55 91.16 8.78 o -6 8 1 32.81 31.19 7.25 o -4 8 1 911.82 901.89 26.57 o -2 8 1 166.20 171.81 5.73 o 0 8 1 25.48 23.71 2.58 o 2 8 1 496.32 494.88 11.62 o 4 8 1 3.96 5.22 4.28 o 6 8 1 17.84 20.75 10.69 o -5 9 1 64.07 69.80 12.07 o -3 9 1 5.01 9.08 3.46 o -1 9 1 703.30 704.09 12.81 o 1 9 1 488.71 488.52 12.94 o 3 9 1 1.93 1.11 3.62 o 5 9 1 79.32 82.14 9.00 o -6 10 1 9.52 9.03 6.56 o -4 10 1 433.31 489.89 39.59 o -2 10 1 62.33 66.37 5.89 o 0 10 1 2052.91 2027.96 32.46 o 2 10 1 20.21 12.00 4.17 o 4 10 1 30.52 37.47 6.80 o -5 11 1 0.92 1.34 5.17 o -3 11 1 807.14 804.63 35.19 o -1 11 1 523.69 529.82 12.58 o 1 11 1 274.84 288.73 8.51 o 3 11 1 1234.31 1110.76 31.45 o 5 11 1 72.54 58.96 15.19 o -4 12 1 1087.02 994.48 31.26 o -2 12 1 249.66 274.96 13.13 o 0 12 1 976.28 930.68 18.46 o 2 12 1 363.08 354.65 30.80 o 4 12 1 21.75 12.54 5.75 o -5 13 1 6.75 8.80 6.69 o -3 13 1 175.45 169.46 11.92 o -1 13 1 377.43 403.35 14.36 o 1 13 1 30.01 30.55 5.59 o 3 13 1 13.04 13.29 5.36 o -4 14 1 480.16 456.46 20.79 o -2 14 1 187.23 177.06 16.44 o 0 14 1 6.05 7.05 3.28 o 2 14 1 65.62 60.88 11.34 o 4 14 1 8.48 10.99 6.46 o -3 15 1 55.50 50.58 8.66 o -1 15 1 92.55 87.59 6.31 o 1 15 1 38.92 34.35 7.03 o 3 15 1 198.29 152.05 24.66 o -2 16 1 51.98 54.24 8.88 o 0 16 1 160.50 150.61 8.03 o 2 16 1 101.81 93.93 10.27 o -1 17 1 50.52 62.19 14.66 o 1 17 1 100.96 109.87 11.34 o -6 0 2 719.28 856.86 30.93 o -4 0 2 3414.39 3729.37 68.80 o -2 0 2 638.22 631.18 15.16 o 0 0 2 1842.84 1715.53 67.86 o 2 0 2 5244.67 5593.44 152.92 o 4 0 2 85.86 109.31 6.46 o 6 0 2 105.21 69.84 12.81 o -7 1 2 98.54 128.62 9.59 o -5 1 2 62.41 69.55 6.37 o -3 1 2 380.37 419.52 9.53 o -1 1 2 16218.92 15338.60 450.84 o 1 1 2 1575.53 1508.18 31.57 o 3 1 2 1981.16 2083.26 35.89 o 5 1 2 114.20 93.23 9.02 o 7 1 2 4.53 2.81 6.52 o -6 2 2 2.99 4.01 4.05 o -4 2 2 131.64 146.00 5.68 o -2 2 2 623.84 648.36 13.33 o 0 2 2 4425.00 4291.72 59.04 o 2 2 2 11.03 20.09 2.61 o 4 2 2 39.71 43.89 4.43 o 6 2 2 20.05 23.83 6.71 o -7 3 2 39.20 43.37 9.67 o -5 3 2 22.28 20.28 3.59 o -3 3 2 697.89 696.54 16.80 o -1 3 2 1421.11 1250.19 24.76 o 1 3 2 359.40 350.87 11.36 o 3 3 2 2786.69 2700.76 45.44 o 5 3 2 407.37 399.21 12.82 o -6 4 2 2.50 6.10 4.51 o -4 4 2 646.91 638.07 21.74 o -2 4 2 133.98 130.84 5.12 o 0 4 2 613.76 633.35 10.00 o 2 4 2 18.63 19.01 5.56 o 4 4 2 60.35 74.48 6.73 o 6 4 2 158.96 167.92 12.89 o -5 5 2 301.51 318.19 9.88 o -3 5 2 191.33 196.42 9.07 o -1 5 2 28.31 44.88 2.53 o 1 5 2 2815.85 3027.30 50.08 o 3 5 2 29.47 33.48 6.54 o 5 5 2 249.98 284.85 14.69 o -6 6 2 195.81 190.71 10.21 o -4 6 2 140.84 119.53 7.88 o -2 6 2 437.41 470.04 9.58 o 0 6 2 1662.23 1696.75 26.01 o 2 6 2 0.52 -0.09 2.62 o 4 6 2 1089.91 1077.06 29.24 o 6 6 2 142.84 164.42 26.01 o -5 7 2 6.65 7.19 4.25 o -3 7 2 51.87 52.46 3.53 o -1 7 2 1468.20 1437.88 21.61 o 1 7 2 150.71 172.90 8.07 o 3 7 2 98.74 99.55 7.71 o 5 7 2 35.86 35.69 6.64 o -6 8 2 1.74 6.90 5.88 o -4 8 2 18.42 22.42 4.11 o -2 8 2 98.40 101.46 4.77 o 0 8 2 184.55 172.36 5.62 o 2 8 2 119.13 113.92 4.99 o 4 8 2 205.79 207.71 16.29 o 6 8 2 28.25 28.09 7.36 o -5 9 2 13.57 10.75 8.77 o -3 9 2 102.32 113.40 7.44 o -1 9 2 890.71 869.52 15.16 o 1 9 2 153.06 169.52 6.52 o 3 9 2 130.98 115.57 12.06 o 5 9 2 17.44 13.95 5.88 o -6 10 2 28.50 31.44 7.98 o -4 10 2 645.41 610.54 21.65 o -2 10 2 0.01 3.65 2.49 o 0 10 2 103.14 98.07 5.58 o 2 10 2 38.17 36.26 5.79 o 4 10 2 1042.95 981.33 29.69 o -5 11 2 44.40 57.13 8.77 o -3 11 2 165.07 147.10 14.60 o -1 11 2 780.42 783.09 14.95 o 1 11 2 10.44 10.25 3.02 o 3 11 2 10.66 12.48 4.86 o 5 11 2 42.67 38.87 7.87 o -4 12 2 15.85 65.19 42.06 o -2 12 2 161.86 159.62 10.61 o 0 12 2 180.21 171.95 10.53 o 2 12 2 513.76 432.33 31.47 o 4 12 2 316.20 321.92 18.94 o -3 13 2 265.06 275.87 14.69 o -1 13 2 83.85 89.65 5.69 o 1 13 2 20.32 14.34 3.80 o 3 13 2 11.97 8.62 7.75 o -4 14 2 23.50 37.36 7.89 o -2 14 2 25.79 33.38 6.82 o 0 14 2 0.09 3.30 2.80 o 2 14 2 7.83 3.95 4.48 o 4 14 2 2.41 -2.12 5.31 o -3 15 2 46.94 50.92 8.66 o -1 15 2 33.75 41.57 6.23 o 1 15 2 38.52 57.48 11.13 o 3 15 2 228.98 238.31 15.20 o -2 16 2 19.63 16.85 6.61 o 0 16 2 255.19 267.76 10.30 o 2 16 2 44.69 26.45 12.42 o -1 17 2 9.91 8.20 5.97 o 1 17 2 561.10 614.72 34.78 o -7 1 3 50.05 51.11 13.49 o -5 1 3 679.81 748.14 18.42 o -3 1 3 88.92 96.88 6.05 o -1 1 3 117.22 143.22 6.24 o 1 1 3 756.14 776.56 18.38 o 3 1 3 131.24 121.79 4.97 o 5 1 3 507.44 460.13 20.26 o -6 2 3 3.22 3.00 3.95 o -4 2 3 2.04 4.88 2.48 o -2 2 3 566.70 597.28 11.31 o 0 2 3 9338.96 9133.87 174.18 o 2 2 3 1207.58 1235.68 22.57 o 4 2 3 102.02 105.87 7.35 o 6 2 3 0.41 4.30 5.82 o -7 3 3 0.92 7.66 6.73 o -5 3 3 12.83 11.70 4.01 o -3 3 3 357.38 382.12 9.23 o -1 3 3 601.96 712.67 15.46 o 1 3 3 814.18 845.44 17.49 o 3 3 3 20.96 22.95 2.50 o 5 3 3 55.82 65.92 9.68 o -6 4 3 139.87 145.25 8.96 o -4 4 3 64.16 70.70 4.85 o -2 4 3 1065.62 1121.05 21.57 o 0 4 3 13853.80 13795.24 176.63 o 2 4 3 727.12 634.90 18.67 o 4 4 3 180.61 168.93 9.58 o 6 4 3 198.54 179.76 15.77 o -5 5 3 74.99 80.18 5.60 o -3 5 3 133.16 121.40 6.22 o -1 5 3 484.67 444.93 11.36 o 1 5 3 776.37 806.68 20.16 o 3 5 3 1877.37 1759.21 41.17 o 5 5 3 461.45 445.38 17.31 o -6 6 3 246.91 246.55 11.89 o -4 6 3 226.73 247.83 10.47 o -2 6 3 1169.61 1154.92 19.42 o 0 6 3 966.78 1019.73 15.87 o 2 6 3 1190.99 1065.34 26.83 o 4 6 3 1974.32 1806.74 44.02 o 6 6 3 226.74 214.26 15.35 o -5 7 3 497.03 524.75 30.30 o -3 7 3 125.79 114.72 5.10 o -1 7 3 0.40 0.38 1.48 o 1 7 3 385.18 410.43 10.27 o 3 7 3 1647.29 1563.84 38.41 o 5 7 3 79.85 58.92 12.74 o -6 8 3 6.18 2.45 5.87 o -4 8 3 111.90 102.93 11.09 o -2 8 3 0.01 -1.00 1.98 o 0 8 3 124.28 134.32 5.08 o 2 8 3 0.41 1.94 3.28 o 4 8 3 170.19 165.65 10.84 o 6 8 3 177.26 198.83 21.39 o -5 9 3 6.06 7.92 5.35 o -3 9 3 715.61 706.04 19.43 o -1 9 3 169.70 177.13 5.75 o 1 9 3 568.30 524.72 14.16 o 3 9 3 607.59 555.65 19.17 o 5 9 3 62.67 67.85 10.47 o -4 10 3 439.60 465.29 18.54 o -2 10 3 0.29 0.06 2.43 o 0 10 3 4.04 0.85 2.30 o 2 10 3 263.79 225.96 11.22 o 4 10 3 34.63 32.18 6.73 o -5 11 3 412.83 409.65 19.18 o -3 11 3 6.29 8.69 4.60 o -1 11 3 3634.68 3528.66 50.33 o 1 11 3 305.43 342.60 10.77 o 3 11 3 8.47 9.19 4.87 o 5 11 3 85.61 98.39 10.84 o -4 12 3 195.67 188.16 20.57 o -2 12 3 749.50 732.60 16.83 o 0 12 3 49.74 44.15 4.09 o 2 12 3 10.95 0.38 4.01 o 4 12 3 130.63 99.46 11.50 o -3 13 3 41.97 38.46 7.27 o -1 13 3 7.58 7.80 3.06 o 1 13 3 389.92 314.07 16.66 o 3 13 3 4.22 9.39 5.44 o -4 14 3 86.32 88.39 10.89 o -2 14 3 18.39 16.30 6.51 o 0 14 3 6.63 2.97 3.53 o 2 14 3 46.53 42.96 7.19 o 4 14 3 151.22 140.06 20.36 o -3 15 3 14.85 22.68 7.05 o -1 15 3 246.03 234.37 14.19 o 1 15 3 17.15 9.52 8.32 o 3 15 3 14.15 12.59 6.31 o -2 16 3 10.05 5.59 6.08 o 0 16 3 37.56 33.00 5.14 o 2 16 3 108.28 101.42 13.33 o -1 17 3 159.44 198.34 50.73 o 1 17 3 245.37 258.29 15.94 o -6 0 4 82.29 66.80 18.66 o -4 0 4 998.93 1023.65 123.25 o -2 0 4 1570.91 1734.91 41.78 o 0 0 4 3429.36 3200.53 126.52 o 2 0 4 1797.43 1935.37 57.99 o 4 0 4 379.32 290.57 19.35 o 6 0 4 217.15 227.96 22.00 o -7 1 4 124.15 137.55 27.67 o -5 1 4 1614.83 1647.08 34.92 o -1 1 4 1018.32 1200.20 26.00 o 1 1 4 14.54 10.92 3.84 o 3 1 4 35.24 50.35 6.49 o 5 1 4 185.35 140.71 11.29 o -6 2 4 95.21 94.82 9.44 o -4 2 4 123.97 132.35 7.12 o -2 2 4 1020.12 1158.48 22.39 o 0 2 4 774.95 835.66 18.61 o 2 2 4 285.64 243.73 9.54 o 4 2 4 26.27 21.17 4.64 o 6 2 4 5.18 1.85 5.92 o -5 3 4 893.40 946.62 22.33 o -3 3 4 783.79 815.28 14.92 o -1 3 4 618.33 607.87 23.03 o 1 3 4 424.86 440.02 10.98 o 3 3 4 219.99 239.95 7.49 o 5 3 4 0.69 -2.92 4.56 o -6 4 4 15.06 10.99 4.81 o -4 4 4 132.93 125.51 6.09 o -2 4 4 347.64 367.93 12.27 o 0 4 4 41.38 54.27 4.44 o 2 4 4 524.01 540.92 16.13 o 4 4 4 125.32 108.41 14.34 o 6 4 4 38.25 33.35 9.71 o -5 5 4 83.31 85.31 8.63 o -3 5 4 440.02 496.66 13.06 o -1 5 4 1203.25 1217.18 18.54 o 1 5 4 318.90 311.59 12.36 o 3 5 4 689.75 667.35 28.88 o 5 5 4 18.18 23.22 6.18 o -6 6 4 4.64 1.96 4.53 o -4 6 4 178.03 180.62 9.35 o -2 6 4 83.60 70.91 4.05 o 0 6 4 3524.69 3671.99 47.45 o 2 6 4 27.71 25.63 4.55 o 4 6 4 14.99 11.70 4.94 o 6 6 4 20.33 22.54 7.99 o -5 7 4 20.88 20.02 4.62 o -3 7 4 171.53 168.09 7.34 o -1 7 4 48.40 47.58 2.98 o 1 7 4 294.94 288.92 10.95 o 3 7 4 985.36 897.43 26.69 o 5 7 4 221.70 229.84 13.18 o -6 8 4 43.09 42.87 8.20 o -4 8 4 84.95 75.45 10.00 o -2 8 4 220.44 230.97 7.22 o 0 8 4 85.62 89.00 4.27 o 2 8 4 212.35 193.33 15.41 o 4 8 4 3.36 0.72 4.10 o -5 9 4 201.08 187.50 12.74 o -3 9 4 1.16 1.62 2.55 o -1 9 4 62.71 58.56 3.87 o 1 9 4 142.48 150.35 6.69 o 3 9 4 282.93 294.87 13.67 o 5 9 4 42.08 44.43 7.97 o -4 10 4 204.75 163.47 10.30 o -2 10 4 1151.84 1124.69 22.46 o 0 10 4 141.98 141.44 5.78 o 2 10 4 9.46 -0.37 3.66 o 4 10 4 29.05 29.93 7.04 o -5 11 4 80.63 86.40 13.87 o -3 11 4 95.97 94.61 7.85 o -1 11 4 138.36 126.31 5.82 o 1 11 4 17.72 7.17 3.54 o 3 11 4 23.71 28.25 6.27 o 5 11 4 85.51 81.94 15.01 o -4 12 4 775.29 793.98 30.55 o -2 12 4 1.10 3.19 3.08 o 0 12 4 35.49 39.22 4.02 o 2 12 4 31.36 37.67 6.52 o 4 12 4 10.32 15.07 6.33 o -3 13 4 120.15 126.81 11.40 o -1 13 4 1.19 -1.61 2.76 o 1 13 4 220.83 222.24 12.16 o 3 13 4 169.23 151.76 11.91 o -4 14 4 19.00 9.05 6.74 o -2 14 4 2.78 8.29 5.44 o 0 14 4 0.07 2.93 3.10 o 2 14 4 11.30 11.21 5.70 o -3 15 4 25.58 19.15 6.90 o -1 15 4 2.08 5.03 4.02 o 1 15 4 41.80 35.07 10.14 o 3 15 4 467.52 531.32 23.57 o -2 16 4 107.53 144.53 17.61 o 0 16 4 799.14 919.61 41.16 o 2 16 4 111.52 108.52 11.24 o -1 17 4 377.66 382.33 25.10 o -5 1 5 34.02 36.67 10.45 o -3 1 5 76.38 70.11 4.03 o -1 1 5 1226.68 1227.25 39.62 o 1 1 5 580.24 599.15 18.38 o 3 1 5 1600.73 1607.72 30.39 o 5 1 5 209.94 217.17 14.22 o -6 2 5 258.78 302.56 23.15 o -4 2 5 478.34 502.02 18.71 o -2 2 5 409.75 410.77 37.14 o 0 2 5 47.98 43.66 3.42 o 2 2 5 50.24 50.00 5.16 o 4 2 5 41.33 35.39 5.63 o 6 2 5 0.60 6.82 6.66 o -5 3 5 13.30 10.99 4.84 o -3 3 5 10.50 12.10 6.51 o -1 3 5 35.15 42.48 4.94 o 1 3 5 96.51 104.31 5.19 o 3 3 5 113.63 114.67 5.66 o 5 3 5 0.39 2.68 5.47 o -6 4 5 50.67 49.87 12.97 o -4 4 5 158.20 153.97 8.40 o -2 4 5 346.99 366.24 13.91 o 0 4 5 95.73 119.93 4.72 o 2 4 5 1143.74 1095.88 32.95 o 4 4 5 4.09 0.81 4.26 o 6 4 5 0.07 2.28 6.62 o -5 5 5 1.18 2.58 3.69 o -3 5 5 7.13 7.44 3.12 o -1 5 5 3551.06 3630.11 66.01 o 1 5 5 155.32 150.15 6.17 o 3 5 5 2619.52 2476.77 56.21 o 5 5 5 135.54 162.85 11.54 o -6 6 5 14.07 14.30 5.56 o -4 6 5 441.04 446.02 13.72 o -2 6 5 16.31 17.28 3.31 o 0 6 5 2541.93 2558.98 48.64 o 2 6 5 404.86 363.08 13.61 o 4 6 5 225.46 251.05 13.00 o -5 7 5 29.03 29.66 5.12 o -3 7 5 373.10 391.27 10.27 o -1 7 5 109.23 111.52 4.29 o 1 7 5 276.36 279.22 11.07 o 3 7 5 0.30 -5.03 3.35 o 5 7 5 471.13 455.98 19.06 o -6 8 5 44.12 59.13 8.30 o -4 8 5 396.22 377.34 13.10 o -2 8 5 66.60 66.29 5.80 o 0 8 5 85.54 84.92 4.87 o 2 8 5 325.37 309.85 27.42 o 4 8 5 312.98 288.89 26.41 o -5 9 5 245.65 222.67 13.18 o -3 9 5 0.32 1.06 2.71 o -1 9 5 702.13 635.85 11.93 o 1 9 5 64.72 77.70 6.90 o 3 9 5 10.53 18.05 5.48 o 5 9 5 59.64 75.96 9.80 o -4 10 5 135.86 142.85 14.27 o -2 10 5 713.17 725.35 15.58 o 0 10 5 102.15 112.02 6.00 o 2 10 5 110.60 93.31 17.40 o 4 10 5 303.66 325.93 22.18 o -5 11 5 338.62 399.85 19.34 o -3 11 5 1.40 -1.50 3.94 o -1 11 5 17.07 18.84 3.88 o 1 11 5 0.08 -1.02 4.02 o 3 11 5 45.91 51.18 7.68 o -4 12 5 4.62 0.21 6.28 o -2 12 5 376.36 372.76 14.28 o 0 12 5 61.21 69.98 6.07 o 2 12 5 18.18 13.26 5.45 o 4 12 5 675.31 744.77 27.18 o -3 13 5 125.83 119.20 11.12 o -1 13 5 3.08 4.70 3.43 o 1 13 5 5.38 -1.55 3.72 o 3 13 5 1.62 1.64 5.13 o -2 14 5 25.88 29.27 7.46 o 0 14 5 4.20 10.87 4.46 o 2 14 5 184.99 177.99 20.05 o -3 15 5 1.32 5.75 6.18 o -1 15 5 93.85 100.20 11.13 o 1 15 5 1.92 8.00 9.87 o -2 16 5 0.00 4.34 7.51 o 0 16 5 0.00 10.55 7.83 o -6 0 6 615.34 630.81 49.34 o -4 0 6 0.95 2.86 6.73 o -2 0 6 3467.68 3708.56 153.22 o 0 0 6 3434.73 3330.64 135.28 o 2 0 6 945.47 944.98 34.31 o 4 0 6 877.48 785.92 37.05 o 6 0 6 508.00 521.17 33.50 o -5 1 6 239.23 191.15 68.19 o -3 1 6 400.19 497.67 16.46 o -1 1 6 15.90 11.58 4.98 o 1 1 6 162.63 157.50 7.61 o 3 1 6 192.08 180.20 7.58 o 5 1 6 62.04 58.22 9.45 o -6 2 6 35.26 27.71 11.85 o -4 2 6 179.62 73.93 11.40 o -2 2 6 12.70 4.29 3.03 o 0 2 6 1216.01 1223.11 27.41 o 2 2 6 489.04 467.98 13.52 o 4 2 6 245.55 220.99 9.90 o 6 2 6 108.49 103.93 13.45 o -3 3 6 11.74 9.16 5.14 o -1 3 6 11.80 23.17 5.88 o 1 3 6 113.26 110.49 5.43 o 3 3 6 179.25 162.33 13.67 o 5 3 6 275.64 285.90 16.16 o -6 4 6 98.58 117.33 17.08 o -4 4 6 25.54 17.35 5.07 o -2 4 6 1.48 1.06 2.88 o 0 4 6 663.74 662.37 14.33 o 2 4 6 58.21 52.05 4.87 o 4 4 6 276.34 288.07 13.86 o -5 5 6 171.15 206.98 27.28 o -3 5 6 320.39 335.99 22.16 o -1 5 6 19.39 13.14 4.15 o 1 5 6 454.19 462.31 12.60 o 3 5 6 961.24 882.86 25.75 o 5 5 6 35.10 23.30 10.58 o -6 6 6 54.98 49.67 13.21 o -4 6 6 217.30 231.02 9.99 o -2 6 6 65.76 72.47 8.91 o 0 6 6 291.51 293.30 12.22 o 2 6 6 1071.99 1027.55 27.75 o 4 6 6 157.91 154.42 10.95 o -5 7 6 59.72 55.64 10.13 o -3 7 6 44.25 44.52 4.47 o -1 7 6 2111.38 2173.05 40.18 o 1 7 6 67.54 61.99 8.21 o 3 7 6 37.24 38.21 6.30 o 5 7 6 49.13 40.58 7.84 o -4 8 6 22.19 23.48 5.15 o -2 8 6 503.57 498.89 12.19 o 0 8 6 275.69 291.18 10.31 o 2 8 6 34.88 35.11 7.04 o 4 8 6 161.16 142.05 13.30 o -5 9 6 19.32 20.19 5.53 o -3 9 6 5.89 4.23 3.07 o -1 9 6 468.95 460.31 12.76 o 1 9 6 89.33 73.39 19.97 o 3 9 6 0.21 0.32 4.19 o -4 10 6 5.76 4.00 4.34 o -2 10 6 25.43 33.65 7.54 o 0 10 6 23.74 14.27 5.77 o 2 10 6 4.82 7.86 4.76 o 4 10 6 745.53 802.72 39.67 o -3 11 6 14.26 18.23 5.42 o -1 11 6 91.06 89.16 6.52 o 1 11 6 0.48 2.65 4.02 o 3 11 6 235.17 262.18 14.80 o -4 12 6 3.29 -2.91 5.81 o -2 12 6 57.09 53.84 5.78 o 0 12 6 0.57 0.89 3.59 o 2 12 6 25.24 20.95 8.91 o -3 13 6 102.69 113.68 10.09 o -1 13 6 635.82 634.54 17.14 o 1 13 6 208.73 215.88 15.72 o 3 13 6 25.33 17.05 10.30 o -2 14 6 34.50 29.49 6.96 o 0 14 6 49.95 49.66 6.86 o 2 14 6 1.17 -3.93 6.68 o -1 15 6 846.61 995.50 27.65 o 1 15 6 79.10 69.52 18.38 o -3 1 7 415.07 386.12 68.88 o -1 1 7 26.67 20.97 6.27 o 1 1 7 4.52 4.26 3.27 o 3 1 7 117.99 123.40 7.00 o 5 1 7 7.22 3.80 6.23 o -6 2 7 1.78 -0.03 9.84 o -4 2 7 25.20 13.12 7.22 o -2 2 7 64.07 84.28 10.59 o 0 2 7 833.73 868.05 31.00 o 2 2 7 364.56 372.04 12.40 o 4 2 7 0.33 -0.88 3.45 o -5 3 7 2.01 7.58 6.77 o -3 3 7 75.85 67.81 15.56 o -1 3 7 8.98 14.95 6.11 o 1 3 7 196.26 184.35 9.07 o 3 3 7 30.50 36.67 7.75 o 5 3 7 16.54 14.30 7.09 o -6 4 7 15.67 13.78 10.40 o -4 4 7 242.89 261.56 25.17 o -2 4 7 56.17 40.34 11.38 o 0 4 7 613.62 566.37 23.72 o 2 4 7 1103.55 1134.66 29.99 o 4 4 7 71.96 65.25 9.19 o -3 5 7 136.51 126.02 17.24 o -1 5 7 1545.78 1014.42 51.74 o 1 5 7 118.15 113.96 6.96 o 3 5 7 89.45 84.41 9.67 o 5 5 7 4.64 7.04 9.72 o -6 6 7 65.51 43.94 12.33 o -4 6 7 66.45 62.01 12.12 o -2 6 7 1557.27 1599.36 44.42 o 0 6 7 218.51 209.40 10.26 o 2 6 7 558.22 533.83 18.23 o 4 6 7 50.49 68.31 8.44 o -5 7 7 79.93 64.52 20.13 o -3 7 7 11.18 10.65 5.37 o -1 7 7 855.67 876.43 29.34 o 1 7 7 259.50 240.95 10.10 o 3 7 7 138.53 135.25 10.17 o -4 8 7 272.99 271.67 14.16 o -2 8 7 260.22 258.53 10.78 o 0 8 7 285.42 276.59 24.80 o 2 8 7 14.78 13.64 4.91 o 4 8 7 6.78 1.24 5.15 o -5 9 7 120.20 94.44 15.67 o -3 9 7 331.29 330.38 10.58 o -1 9 7 190.22 204.79 10.43 o 1 9 7 71.42 114.39 17.76 o 3 9 7 0.04 -1.76 4.56 o -4 10 7 76.73 86.96 8.30 o -2 10 7 191.12 172.12 9.62 o 0 10 7 177.90 222.61 15.10 o 2 10 7 16.07 5.48 4.80 o 4 10 7 110.40 101.46 10.77 o -3 11 7 15.40 11.28 5.38 o -1 11 7 42.82 43.29 6.61 o 1 11 7 76.11 44.48 8.55 o 3 11 7 1025.94 1165.57 34.95 o -4 12 7 44.77 38.27 9.39 o -2 12 7 82.88 82.66 7.04 o 0 12 7 57.45 100.39 11.29 o 2 12 7 5.89 4.89 7.40 o -3 13 7 49.09 31.54 7.25 o -1 13 7 6.71 7.86 6.29 o 1 13 7 172.60 204.15 15.98 o -2 14 7 128.56 142.47 9.84 o 0 14 7 38.91 33.77 19.32 o -1 15 7 0.40 -2.00 4.81 o -6 0 8 30.08 22.80 17.83 o -4 0 8 21.34 15.45 10.06 o -2 0 8 145.90 139.39 19.33 o 0 0 8 221.58 234.31 21.46 o 2 0 8 595.30 579.92 19.01 o 4 0 8 93.04 88.87 14.26 o -5 1 8 17.67 14.80 7.79 o -3 1 8 166.48 189.02 19.43 o -1 1 8 170.92 178.70 30.92 o 1 1 8 0.01 2.73 3.48 o 3 1 8 1623.77 1612.71 27.21 o 5 1 8 162.41 186.83 15.37 o -6 2 8 272.55 234.04 23.65 o -4 2 8 33.42 14.41 7.60 o -2 2 8 70.25 95.10 11.96 o 0 2 8 80.90 68.71 8.97 o 2 2 8 10.79 13.74 4.21 o 4 2 8 0.20 -4.28 5.21 o -5 3 8 110.35 167.14 27.93 o -3 3 8 0.38 -3.59 5.07 o -1 3 8 532.23 537.96 24.78 o 1 3 8 219.27 223.10 8.51 o 3 3 8 687.88 720.47 38.24 o 5 3 8 164.71 183.17 15.58 o -4 4 8 346.21 285.22 60.60 o -2 4 8 9.14 10.00 6.53 o 0 4 8 95.80 109.02 10.91 o 2 4 8 31.51 30.39 5.25 o 4 4 8 57.35 61.90 8.27 o -5 5 8 195.51 136.90 76.16 o -3 5 8 47.00 38.23 18.09 o -1 5 8 345.82 329.24 19.21 o 1 5 8 0.20 4.82 5.13 o 3 5 8 54.00 46.12 7.24 o -4 6 8 0.01 5.50 8.39 o -2 6 8 976.92 1057.87 33.11 o 0 6 8 10.99 4.69 5.19 o 2 6 8 102.87 99.49 7.75 o 4 6 8 7.36 3.66 5.46 o -5 7 8 66.03 55.86 23.18 o -3 7 8 32.05 24.35 12.08 o -1 7 8 54.14 56.45 8.67 o 1 7 8 196.66 171.82 13.23 o 3 7 8 133.26 112.24 9.77 o -4 8 8 6.26 8.02 9.78 o -2 8 8 23.14 23.35 4.84 o 0 8 8 152.25 127.51 11.66 o 2 8 8 15.96 22.09 7.28 o 4 8 8 10.23 12.26 7.36 o -3 9 8 76.72 84.71 7.25 o -1 9 8 25.60 23.22 6.81 o 1 9 8 18.12 15.55 6.53 o 3 9 8 201.85 168.99 17.96 o -4 10 8 24.46 28.63 11.14 o -2 10 8 192.37 188.41 10.91 o 0 10 8 145.07 140.86 17.48 o 2 10 8 10.44 4.01 6.19 o -3 11 8 4.54 1.10 6.75 o -1 11 8 54.75 79.04 11.73 o 1 11 8 123.52 108.03 25.78 o 3 11 8 130.24 113.96 16.40 o -2 12 8 85.76 92.24 9.11 o 0 12 8 25.04 27.70 8.49 o 2 12 8 222.57 244.84 18.19 o -1 13 8 125.76 123.93 13.11 o 1 13 8 0.00 4.13 6.75 o 0 14 8 10.88 8.12 7.38 o -5 1 9 21.03 17.48 8.04 o -3 1 9 123.45 138.67 15.90 o -1 1 9 16.40 8.11 6.78 o 1 1 9 124.48 124.08 12.37 o 3 1 9 235.39 258.79 10.61 o -4 2 9 50.39 39.87 25.02 o -2 2 9 195.64 236.67 17.31 o 0 2 9 417.97 410.02 21.40 o 2 2 9 314.94 311.50 12.72 o 4 2 9 84.78 116.47 11.97 o -5 3 9 4.02 5.30 7.28 o -3 3 9 50.06 27.93 21.35 o -1 3 9 201.11 209.59 15.70 o 1 3 9 0.56 0.99 4.15 o 3 3 9 78.16 85.64 8.15 o -4 4 9 4.97 6.79 8.16 o -2 4 9 1332.53 916.66 54.16 o 0 4 9 92.36 114.26 9.04 o 2 4 9 173.80 183.56 14.16 o 4 4 9 0.84 -4.73 4.84 o -5 5 9 136.73 148.65 27.31 o -3 5 9 218.26 258.34 28.30 o -1 5 9 25.90 20.61 8.10 o 1 5 9 381.24 391.42 19.60 o 3 5 9 64.55 55.68 8.07 o -4 6 9 241.43 259.40 22.62 o 0 6 9 361.86 343.52 18.12 o 2 6 9 170.89 170.95 39.75 o 4 6 9 160.96 184.33 13.41 o -3 7 9 0.12 -2.50 7.61 o -1 7 9 230.96 229.73 19.31 o 1 7 9 324.54 294.19 23.90 o 3 7 9 113.20 127.32 16.07 o -4 8 9 89.23 85.09 15.03 o -2 8 9 32.91 31.25 11.09 o 0 8 9 34.40 35.57 8.02 o 2 8 9 7.72 5.14 6.30 o -3 9 9 1.51 -2.02 6.06 o -1 9 9 279.38 281.74 18.71 o 1 9 9 145.30 147.74 13.94 o 3 9 9 276.09 341.87 24.91 o -2 10 9 1.62 3.51 7.66 o 0 10 9 1.94 0.48 5.78 o 2 10 9 273.87 310.41 19.41 o -3 11 9 41.50 30.17 8.93 o -1 11 9 1049.50 1132.54 39.70 o 1 11 9 57.93 71.75 11.54 o -2 12 9 46.36 51.39 10.17 o 0 12 9 226.46 268.86 23.00 o -4 0 10 106.11 61.59 17.70 o -2 0 10 37.93 26.59 13.35 o 0 0 10 37.07 50.41 14.02 o 2 0 10 2404.58 2481.16 67.32 o 4 0 10 233.33 258.75 24.21 o -5 1 10 102.39 33.41 9.46 o -3 1 10 70.99 47.49 12.23 o -1 1 10 461.61 493.18 25.57 o 1 1 10 134.10 128.00 13.40 o 3 1 10 96.82 113.93 8.21 o -4 2 10 63.60 83.72 21.70 o -2 2 10 37.64 36.03 10.30 o 0 2 10 365.59 345.71 20.78 o 2 2 10 25.34 44.53 11.03 o -5 3 10 503.07 514.26 47.17 o -3 3 10 163.90 228.09 28.88 o -1 3 10 30.07 37.23 9.36 o 1 3 10 5.78 15.47 6.71 o 3 3 10 49.20 62.46 15.38 o -4 4 10 30.70 22.20 9.98 o -2 4 10 495.33 432.26 57.32 o 0 4 10 40.11 58.66 9.66 o 2 4 10 210.14 177.41 14.54 o -3 5 10 267.61 234.72 28.83 o -1 5 10 210.13 213.63 27.77 o 1 5 10 24.08 13.61 8.39 o 3 5 10 4.18 11.18 7.42 o -4 6 10 0.02 -0.29 10.12 o -2 6 10 83.19 80.78 18.68 o 0 6 10 30.40 30.09 8.12 o 2 6 10 123.80 128.52 13.52 o -3 7 10 64.71 67.07 9.63 o -1 7 10 322.81 310.55 18.38 o 1 7 10 83.22 86.32 11.76 o 3 7 10 55.55 53.71 10.67 o -2 8 10 75.48 71.58 11.24 o 0 8 10 185.00 176.72 15.11 o 2 8 10 0.45 0.86 7.32 o -3 9 10 0.63 -3.76 6.70 o -1 9 10 68.50 91.73 17.89 o 1 9 10 12.92 9.87 7.35 o -2 10 10 229.39 259.14 18.40 o 0 10 10 15.06 8.49 7.57 o -1 11 10 188.69 167.57 15.60 o -3 1 11 22.15 20.62 10.91 o -1 1 11 15.98 13.76 8.57 o 1 1 11 1.86 -0.40 6.76 o -4 2 11 4.94 17.74 9.04 o -2 2 11 262.77 271.56 25.89 o 0 2 11 88.36 90.19 14.67 o 2 2 11 0.32 -2.22 5.93 o -3 3 11 93.49 122.94 23.70 o -1 3 11 34.16 44.86 10.88 o 1 3 11 55.12 57.49 10.33 o 3 3 11 4.19 3.49 8.81 o -4 4 11 11.81 19.58 11.22 o -2 4 11 0.27 3.43 8.43 o 0 4 11 60.84 61.05 10.44 o 2 4 11 0.28 5.10 7.15 o -3 5 11 355.67 371.57 36.46 o -1 5 11 0.14 -1.78 6.13 o 1 5 11 6.78 0.85 6.24 o -2 6 11 33.00 37.99 16.07 o 0 6 11 8.55 7.16 6.74 o 2 6 11 6.21 -6.75 6.49 o -3 7 11 45.28 54.39 14.43 o -1 7 11 0.80 -6.68 5.97 o 1 7 11 6.62 16.54 8.29 o -2 8 11 355.21 442.69 29.64 o 0 8 11 83.72 70.19 11.64 o -1 9 11 122.75 121.03 14.19 o -2 0 12 1395.23 1430.85 80.44 o 0 0 12 18.57 25.71 14.17 o 2 0 12 27.44 59.90 13.49 o -3 1 12 39.84 45.77 14.74 o -1 1 12 152.69 153.93 16.94 o 1 1 12 479.20 541.48 45.34 o -2 2 12 1.98 10.54 24.12 o 0 2 12 96.67 122.43 22.32 o -3 3 12 125.24 93.52 26.65 o -1 3 12 54.43 35.29 17.04 o 1 3 12 25.59 37.96 10.06 o -2 4 12 163.13 163.69 18.73 o 0 4 12 15.72 25.04 9.05 o -1 5 12 14.45 13.04 7.73 o 1 5 12 146.22 153.00 15.85 o -2 6 12 74.88 89.41 23.44 o 0 6 12 48.44 57.27 11.80 o -1 1 13 42.13 42.40 17.64 o