#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/83/2218386.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2218386_Fobs loop_ _publ_author_name 'Wen, Xiao-Chun' _publ_section_title ; Diaqua[5-(2-pyridyl)tetrazolato-\k^2^N^1^,N^5^]manganese(II) ; _journal_coeditor_code DN2338 _journal_issue 6 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m768 _journal_volume 64 _journal_year 2008 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 106.597 _cell_angle_gamma 90.000 _cell_length_a 6.1850 _cell_length_b 12.1097 _cell_length_c 10.6148 _exptl_crystal_F_000 390.00 _reflns_d_resolution_high 0.7596 _[local]_cod_data_source_file dn2338Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 111 in P2(1)/n' _shelx_refln_list_code 4 _shelx_F_calc_maximum 89.54 _shelx_F_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 625.48 623.83 9.25 o 6 0 0 131.94 138.38 6.73 o 1 1 0 602.73 609.50 2.01 o 2 1 0 340.16 323.36 2.30 o 3 1 0 894.59 845.27 7.31 o 4 1 0 72.28 61.78 2.07 o 5 1 0 32.23 28.80 1.71 o 6 1 0 20.90 18.67 1.63 o 7 1 0 103.63 109.40 3.74 o 0 2 0 216.57 203.55 1.46 o 1 2 0 1160.77 1096.38 3.27 o 2 2 0 839.98 805.07 7.74 o 3 2 0 766.89 873.21 5.62 o 4 2 0 756.35 753.92 5.71 o 5 2 0 4.33 2.84 0.42 o 6 2 0 265.00 263.91 5.34 o 7 2 0 3.21 1.76 0.91 o 1 3 0 3644.33 3468.71 22.93 o 2 3 0 5.56 6.45 0.65 o 3 3 0 997.10 980.36 5.83 o 4 3 0 904.98 937.16 11.31 o 5 3 0 596.57 614.01 9.32 o 6 3 0 20.39 17.82 1.50 o 7 3 0 6.86 6.62 0.97 o 0 4 0 646.08 644.29 5.18 o 1 4 0 1305.50 1308.88 5.95 o 2 4 0 2113.38 2155.19 12.46 o 3 4 0 214.33 241.44 1.74 o 4 4 0 654.90 651.58 5.70 o 5 4 0 102.34 86.92 1.89 o 6 4 0 50.79 66.38 3.46 o 7 4 0 3.28 3.24 0.99 o 1 5 0 3060.62 3007.20 19.99 o 2 5 0 11.33 22.62 0.87 o 3 5 0 416.32 375.70 2.84 o 4 5 0 27.08 18.60 1.06 o 5 5 0 300.45 305.30 3.91 o 6 5 0 12.53 13.20 1.27 o 7 5 0 106.50 99.61 6.61 o 0 6 0 407.52 413.85 4.40 o 1 6 0 14.34 15.09 0.82 o 2 6 0 535.61 505.12 3.69 o 3 6 0 118.65 124.34 1.94 o 4 6 0 2.99 4.22 0.56 o 5 6 0 82.68 67.10 2.13 o 6 6 0 28.57 22.25 1.66 o 7 6 0 33.63 30.66 2.56 o 1 7 0 1015.48 949.80 5.96 o 2 7 0 262.78 272.53 2.93 o 3 7 0 125.92 132.72 1.73 o 4 7 0 0.22 0.77 0.50 o 5 7 0 721.44 748.61 16.23 o 6 7 0 0.50 0.74 0.80 o 7 7 0 36.51 31.43 3.67 o 0 8 0 47.02 48.74 5.25 o 1 8 0 143.99 147.50 2.20 o 2 8 0 1064.32 1065.56 8.03 o 3 8 0 0.71 1.26 0.54 o 4 8 0 607.64 629.06 8.23 o 5 8 0 11.07 5.78 1.07 o 6 8 0 146.38 138.95 4.12 o 1 9 0 208.33 205.92 2.46 o 2 9 0 98.29 98.92 2.10 o 3 9 0 1180.31 1243.56 6.52 o 4 9 0 40.01 41.16 2.08 o 5 9 0 199.43 203.75 3.62 o 6 9 0 12.54 14.94 1.72 o 0 10 0 52.99 68.79 4.22 o 1 10 0 14.58 9.74 0.86 o 2 10 0 131.18 120.51 2.31 o 3 10 0 176.42 169.16 2.40 o 4 10 0 238.49 249.77 4.75 o 5 10 0 40.18 34.15 1.78 o 6 10 0 96.34 95.39 5.51 o 1 11 0 392.97 405.24 5.36 o 2 11 0 28.88 24.75 1.99 o 3 11 0 350.41 363.83 7.61 o 4 11 0 11.55 10.96 1.31 o 5 11 0 34.32 32.50 2.25 o 0 12 0 998.69 1035.55 20.23 o 1 12 0 65.76 57.43 2.38 o 2 12 0 383.29 392.82 8.39 o 3 12 0 97.02 98.98 3.39 o 4 12 0 42.79 42.29 2.45 o 5 12 0 0.49 0.98 0.72 o 1 13 0 5.89 6.50 1.34 o 2 13 0 73.35 68.12 4.16 o 3 13 0 75.18 70.13 3.28 o 4 13 0 12.04 11.41 1.92 o 0 14 0 32.84 40.39 3.45 o 1 14 0 1.76 0.87 0.99 o 2 14 0 167.41 160.60 3.70 o 3 14 0 1.73 1.41 1.00 o 1 15 0 43.46 31.44 2.94 o 2 15 0 0.13 0.73 0.57 o -7 0 1 299.38 298.11 8.33 o -5 0 1 164.64 169.61 5.81 o -3 0 1 606.14 574.86 5.40 o -1 0 1 7182.34 6146.85 35.81 o 1 0 1 3095.87 2944.91 17.30 o 3 0 1 4898.46 4816.06 20.76 o 5 0 1 7.78 10.40 1.49 o 7 0 1 4.87 3.85 1.48 o -7 1 1 3.66 3.52 1.12 o -6 1 1 70.94 70.70 2.85 o -5 1 1 157.87 156.91 2.40 o -4 1 1 531.83 548.83 5.69 o -3 1 1 58.38 70.09 0.96 o -2 1 1 666.18 613.31 4.38 o -1 1 1 20.39 24.38 0.32 o 0 1 1 4153.44 3434.62 12.44 o 1 1 1 3075.77 2842.79 14.28 o 2 1 1 2440.34 2462.22 9.97 o 3 1 1 21.48 21.24 1.03 o 4 1 1 251.91 217.58 3.13 o 5 1 1 351.50 340.32 3.99 o 6 1 1 154.39 159.74 3.47 o 7 1 1 61.78 73.19 3.37 o -7 2 1 12.13 9.21 1.01 o -6 2 1 52.95 54.30 3.55 o -5 2 1 4.87 7.15 0.66 o -4 2 1 0.38 0.90 0.57 o -3 2 1 25.03 57.70 1.07 o -2 2 1 103.32 90.98 0.88 o -1 2 1 69.24 67.76 0.67 o 0 2 1 1211.98 1213.42 9.91 o 1 2 1 3882.46 3629.25 22.00 o 2 2 1 517.56 592.28 7.06 o 3 2 1 887.89 869.43 7.66 o 4 2 1 1.76 4.32 0.56 o 5 2 1 1126.26 1168.12 13.13 o 6 2 1 28.50 20.69 2.29 o 7 2 1 151.78 155.50 4.38 o -7 3 1 0.32 0.75 0.98 o -6 3 1 585.62 608.53 13.02 o -5 3 1 70.46 69.07 2.63 o -4 3 1 375.56 398.64 5.22 o -3 3 1 6.77 15.15 0.65 o -2 3 1 1274.51 1259.31 4.30 o -1 3 1 1196.19 1189.44 6.58 o 0 3 1 1741.77 1680.77 6.01 o 1 3 1 245.00 236.42 1.68 o 2 3 1 4459.18 4454.04 33.17 o 3 3 1 10.33 9.65 0.75 o 4 3 1 1030.79 1067.91 8.79 o 5 3 1 175.79 189.72 6.46 o 6 3 1 78.12 79.41 2.55 o 7 3 1 2.00 1.87 0.86 o -7 4 1 89.54 86.79 3.62 o -6 4 1 454.53 460.95 24.98 o -5 4 1 379.18 405.04 4.00 o -4 4 1 21.38 25.37 0.98 o -3 4 1 2227.88 2293.18 10.25 o -2 4 1 284.75 306.08 1.93 o -1 4 1 1885.21 1873.27 9.18 o 0 4 1 595.96 601.62 2.40 o 1 4 1 710.18 680.50 4.50 o 2 4 1 701.28 764.52 7.47 o 3 4 1 277.90 271.73 2.01 o 4 4 1 452.67 443.67 3.90 o 5 4 1 16.57 21.14 1.37 o 6 4 1 29.52 31.36 3.10 o 7 4 1 38.78 39.65 2.49 o -7 5 1 7.26 6.81 1.21 o -6 5 1 29.37 27.35 1.82 o -5 5 1 33.76 31.56 1.36 o -4 5 1 362.38 369.97 4.24 o -3 5 1 1067.96 1152.73 5.56 o -2 5 1 621.25 607.87 3.94 o -1 5 1 2559.30 2704.08 17.64 o 0 5 1 3717.55 3537.72 18.59 o 1 5 1 196.12 214.36 1.53 o 2 5 1 325.28 290.72 2.04 o 3 5 1 6.21 8.89 0.72 o 4 5 1 621.70 627.11 6.51 o 5 5 1 30.22 28.52 1.94 o 6 5 1 188.70 196.78 4.18 o 7 5 1 8.45 8.21 1.65 o -7 6 1 67.09 75.00 4.13 o -6 6 1 0.28 0.04 0.56 o -5 6 1 267.37 275.01 3.10 o -4 6 1 146.65 147.33 1.80 o -3 6 1 164.69 158.12 2.09 o -2 6 1 2.36 4.55 0.37 o -1 6 1 566.95 511.33 4.23 o 0 6 1 23.30 31.91 1.15 o 1 6 1 2133.56 2186.33 16.43 o 2 6 1 41.18 33.79 1.00 o 3 6 1 1088.01 1121.08 7.43 o 4 6 1 161.84 141.85 2.58 o 5 6 1 289.35 273.48 5.55 o 6 6 1 17.18 15.31 1.80 o 7 6 1 115.54 131.53 6.19 o -7 7 1 3.72 2.94 1.14 o -6 7 1 18.54 15.11 1.18 o -5 7 1 0.21 0.93 0.53 o -4 7 1 48.62 52.06 2.36 o -3 7 1 378.21 384.84 3.28 o -2 7 1 1565.93 1664.71 10.72 o -1 7 1 2.50 3.00 0.69 o 0 7 1 15.85 32.72 0.64 o 1 7 1 146.39 150.13 1.67 o 2 7 1 111.04 104.03 1.61 o 3 7 1 238.68 216.63 2.19 o 4 7 1 190.72 175.58 2.98 o 5 7 1 42.64 37.11 1.97 o 6 7 1 39.09 39.75 3.83 o -6 8 1 3.97 5.39 1.00 o -5 8 1 775.74 821.51 13.58 o -4 8 1 155.29 156.58 2.30 o -3 8 1 1911.00 1977.42 9.66 o -2 8 1 18.51 16.62 0.94 o -1 8 1 1097.33 1114.95 8.81 o 0 8 1 169.63 170.46 1.88 o 1 8 1 982.22 1027.05 8.19 o 2 8 1 294.91 282.57 3.19 o 3 8 1 10.44 10.84 0.89 o 4 8 1 47.24 39.43 3.47 o 5 8 1 228.43 213.92 4.21 o 6 8 1 0.27 3.72 2.00 o -6 9 1 198.74 210.34 4.29 o -5 9 1 72.53 67.48 3.95 o -4 9 1 235.18 240.56 4.05 o -3 9 1 163.41 144.70 2.34 o -2 9 1 300.35 302.15 3.58 o -1 9 1 0.99 2.89 0.55 o 0 9 1 367.40 389.24 5.03 o 1 9 1 3.22 3.38 0.51 o 2 9 1 543.23 548.99 6.35 o 3 9 1 169.86 171.57 2.83 o 4 9 1 228.59 238.98 4.95 o 5 9 1 106.33 112.22 2.83 o 6 9 1 187.91 191.94 4.43 o -6 10 1 0.02 0.67 0.75 o -5 10 1 61.58 53.79 3.92 o -4 10 1 11.23 9.51 0.98 o -3 10 1 138.56 134.15 2.35 o -2 10 1 153.62 153.22 2.75 o -1 10 1 407.92 441.87 12.81 o 0 10 1 227.56 223.46 4.31 o 1 10 1 1.64 2.72 0.42 o 2 10 1 240.32 246.91 3.07 o 3 10 1 171.19 172.88 2.39 o 4 10 1 47.73 46.61 1.82 o 5 10 1 108.74 117.78 3.15 o -5 11 1 4.27 4.70 0.87 o -4 11 1 494.69 520.90 6.35 o -3 11 1 1.00 1.64 0.49 o -2 11 1 416.87 407.24 5.31 o -1 11 1 128.05 135.11 3.47 o 0 11 1 383.96 393.05 5.15 o 1 11 1 24.50 21.41 1.35 o 2 11 1 144.19 142.06 2.50 o 3 11 1 0.00 0.94 0.47 o 4 11 1 56.02 52.30 2.21 o 5 11 1 22.59 21.54 1.60 o -5 12 1 114.95 124.64 8.26 o -4 12 1 4.17 4.97 0.91 o -3 12 1 259.28 265.73 4.28 o -2 12 1 0.20 -0.95 1.07 o -1 12 1 404.61 394.10 7.35 o 0 12 1 0.04 1.55 0.69 o 1 12 1 205.45 207.13 4.19 o 2 12 1 162.61 161.24 3.70 o 3 12 1 99.79 91.95 3.29 o 4 12 1 7.22 8.13 1.49 o -4 13 1 177.22 193.56 4.25 o -3 13 1 26.00 25.87 2.38 o -2 13 1 194.34 208.49 5.03 o -1 13 1 12.59 12.99 1.57 o 0 13 1 239.03 252.21 4.31 o 1 13 1 6.59 5.91 0.96 o 2 13 1 66.33 65.77 4.51 o 3 13 1 4.44 3.60 0.92 o 4 13 1 37.31 34.70 2.10 o -3 14 1 147.11 163.43 5.83 o -2 14 1 40.24 43.85 2.81 o -1 14 1 67.16 67.46 3.71 o 0 14 1 48.30 52.03 3.17 o 1 14 1 68.94 71.53 3.57 o 2 14 1 0.70 0.16 0.61 o 3 14 1 266.97 299.83 5.45 o -2 15 1 18.78 12.80 1.43 o -1 15 1 2.04 2.77 0.89 o 0 15 1 124.76 121.14 4.23 o 1 15 1 4.45 4.74 0.80 o 2 15 1 28.90 27.89 3.23 o -8 0 2 247.94 274.44 8.12 o -6 0 2 453.64 450.54 7.39 o -4 0 2 1195.65 1255.34 8.54 o -2 0 2 2359.97 2411.41 16.64 o 0 0 2 2460.97 2198.23 16.60 o 2 0 2 1152.62 1186.59 11.14 o 4 0 2 7.97 11.14 1.53 o 6 0 2 397.92 415.06 9.49 o -8 1 2 33.45 30.71 1.84 o -7 1 2 291.65 286.66 4.35 o -6 1 2 129.06 121.05 2.91 o -5 1 2 112.60 111.23 2.89 o -4 1 2 492.29 543.04 3.45 o -3 1 2 43.57 30.24 0.92 o -2 1 2 162.78 168.02 1.32 o -1 1 2 5393.27 4993.60 321.71 o 0 1 2 2946.62 2870.40 15.77 o 1 1 2 1739.82 1534.55 6.92 o 2 1 2 2.77 4.29 0.44 o 3 1 2 2819.56 2935.49 20.81 o 4 1 2 257.80 252.30 4.82 o 5 1 2 197.21 188.86 3.74 o 6 1 2 66.06 58.35 2.81 o 7 1 2 119.02 132.16 3.84 o -7 2 2 0.39 1.94 0.89 o -6 2 2 54.00 50.20 2.06 o -5 2 2 131.03 139.68 2.67 o -4 2 2 567.84 580.79 6.97 o -3 2 2 5.57 15.08 1.26 o -2 2 2 588.23 537.61 2.44 o -1 2 2 3490.71 3310.44 60.11 o 0 2 2 100.30 85.96 0.80 o 1 2 2 1061.67 1024.06 7.85 o 2 2 2 1059.60 1039.56 4.13 o 3 2 2 0.02 1.03 0.54 o 4 2 2 966.39 1002.95 10.41 o 5 2 2 138.33 136.74 2.85 o 6 2 2 78.14 83.21 3.88 o 7 2 2 0.74 0.80 1.01 o -7 3 2 80.62 87.36 3.12 o -6 3 2 613.56 611.53 10.01 o -5 3 2 900.65 928.07 12.09 o -4 3 2 217.13 220.57 2.43 o -3 3 2 2470.06 2522.69 13.41 o -2 3 2 333.51 338.01 2.11 o -1 3 2 339.21 370.65 1.88 o 0 3 2 75.84 82.00 2.05 o 1 3 2 467.78 446.11 2.55 o 2 3 2 2255.10 2497.19 14.37 o 3 3 2 1087.04 1177.18 8.35 o 4 3 2 13.96 13.07 1.02 o 5 3 2 1530.72 1584.72 12.22 o 6 3 2 0.09 1.38 1.03 o 7 3 2 53.16 56.20 2.96 o -7 4 2 10.43 11.38 1.20 o -6 4 2 251.75 263.27 10.53 o -5 4 2 16.56 15.15 1.27 o -4 4 2 193.14 194.13 2.12 o -3 4 2 333.87 355.96 3.00 o -2 4 2 1052.41 1041.88 6.67 o -1 4 2 1161.48 1175.03 4.38 o 0 4 2 407.23 322.45 2.91 o 1 4 2 224.60 226.66 1.53 o 2 4 2 451.64 402.06 2.26 o 3 4 2 13.11 21.08 3.41 o 4 4 2 377.70 375.69 4.46 o 5 4 2 0.26 0.70 0.61 o 6 4 2 99.51 110.98 3.90 o 7 4 2 47.62 43.78 3.35 o -7 5 2 47.51 46.88 2.37 o -6 5 2 2.84 5.05 0.69 o -5 5 2 253.36 243.89 3.89 o -4 5 2 4.93 6.73 0.54 o -3 5 2 265.73 237.67 2.57 o -2 5 2 107.46 134.18 1.37 o -1 5 2 2036.00 2047.18 15.15 o 0 5 2 6.52 13.98 1.50 o 1 5 2 2111.48 2070.13 12.30 o 2 5 2 268.89 282.91 2.61 o 3 5 2 223.31 225.15 2.80 o 4 5 2 37.00 36.73 1.49 o 5 5 2 1.50 3.73 0.85 o 6 5 2 2.62 2.81 0.83 o -7 6 2 8.74 8.67 1.50 o -6 6 2 206.25 201.68 2.84 o -5 6 2 52.28 50.46 1.65 o -4 6 2 32.96 36.85 1.23 o -3 6 2 9.35 6.60 0.60 o -2 6 2 2165.57 2232.79 9.22 o -1 6 2 352.09 355.58 2.58 o 0 6 2 2345.76 2357.00 12.65 o 1 6 2 480.20 521.14 3.83 o 2 6 2 1667.11 1719.15 10.80 o 3 6 2 11.59 12.28 0.86 o 4 6 2 612.05 614.59 4.87 o 5 6 2 21.16 16.82 1.53 o 6 6 2 91.37 93.14 3.45 o -7 7 2 16.60 11.91 1.98 o -6 7 2 0.09 0.90 0.81 o -5 7 2 76.75 77.17 2.63 o -4 7 2 460.76 462.25 4.01 o -3 7 2 176.72 184.47 3.08 o -2 7 2 72.09 61.39 1.78 o -1 7 2 154.89 137.28 1.82 o 0 7 2 514.98 514.68 6.38 o 1 7 2 1460.01 1453.12 7.73 o 2 7 2 567.31 588.51 5.26 o 3 7 2 44.32 39.85 1.39 o 4 7 2 132.38 113.56 2.42 o 5 7 2 47.91 42.27 2.92 o 6 7 2 0.58 1.30 0.94 o -6 8 2 162.80 167.60 3.17 o -5 8 2 46.62 42.70 2.16 o -4 8 2 737.11 764.93 7.69 o -3 8 2 89.11 85.57 1.79 o -2 8 2 1258.21 1299.69 10.97 o -1 8 2 73.42 80.53 1.78 o 0 8 2 766.89 789.88 5.14 o 1 8 2 16.90 10.30 1.01 o 2 8 2 127.96 128.52 3.58 o 3 8 2 51.00 48.40 1.66 o 4 8 2 559.05 571.34 10.21 o 5 8 2 3.45 3.36 1.40 o 6 8 2 75.73 61.87 4.11 o -6 9 2 5.17 6.18 1.07 o -5 9 2 160.34 152.87 3.01 o -4 9 2 28.86 28.68 1.47 o -3 9 2 1358.67 1435.78 7.17 o -2 9 2 158.20 150.69 3.55 o -1 9 2 520.89 536.30 4.10 o 0 9 2 59.71 54.04 1.58 o 1 9 2 1.37 1.24 0.78 o 2 9 2 365.56 345.15 4.70 o 3 9 2 496.52 517.99 4.46 o 4 9 2 5.86 3.82 1.03 o 5 9 2 99.47 108.87 2.93 o 6 9 2 24.59 29.72 3.23 o -6 10 2 0.78 0.50 0.84 o -5 10 2 38.30 37.86 2.22 o -4 10 2 260.80 270.82 8.10 o -3 10 2 0.83 0.55 0.69 o -2 10 2 296.26 298.36 3.41 o -1 10 2 64.26 61.60 1.89 o 0 10 2 1178.11 1209.83 12.14 o 1 10 2 1.48 1.63 0.43 o 2 10 2 411.14 409.79 5.12 o 3 10 2 93.12 88.40 2.48 o 4 10 2 16.58 16.19 1.58 o 5 10 2 12.68 11.75 1.39 o -5 11 2 51.08 43.53 5.05 o -4 11 2 7.85 6.52 0.76 o -3 11 2 23.37 25.50 1.50 o -2 11 2 187.07 175.32 2.49 o -1 11 2 1047.40 1069.42 10.80 o 0 11 2 52.82 47.31 2.53 o 1 11 2 243.40 245.85 5.12 o 2 11 2 68.76 71.38 1.91 o 3 11 2 173.18 177.65 4.33 o 4 11 2 19.45 21.45 2.29 o 5 11 2 7.87 3.59 0.74 o -5 12 2 0.46 1.51 1.09 o -4 12 2 172.33 170.73 4.09 o -3 12 2 101.14 93.19 3.24 o -2 12 2 195.92 198.51 3.67 o -1 12 2 2.72 4.55 0.82 o 0 12 2 289.20 291.25 6.28 o 1 12 2 45.18 37.56 2.37 o 2 12 2 187.25 199.60 3.52 o 3 12 2 21.04 20.21 3.04 o 4 12 2 1.02 0.80 1.17 o -4 13 2 60.74 67.60 3.80 o -3 13 2 346.51 376.26 4.74 o -2 13 2 0.50 1.14 0.89 o -1 13 2 424.45 468.85 10.85 o 0 13 2 57.73 47.79 4.70 o 1 13 2 390.64 412.66 6.05 o 2 13 2 33.79 35.00 1.96 o 3 13 2 74.27 66.35 3.83 o 4 13 2 8.06 10.22 1.49 o -3 14 2 2.87 4.48 0.84 o -2 14 2 154.30 147.54 4.39 o -1 14 2 2.51 2.81 1.08 o 0 14 2 56.84 56.98 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