#------------------------------------------------------------------------------ #$Date: 2009-05-03 21:56:13 +0300 (Sun, 03 May 2009) $ #$Revision: 691 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2218433.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2218433_Fobs loop_ _publ_author_name 'He, Wei' 'Sun, Hong-Shun' 'Ji, Chun-Xiang' 'Yang, Dong-Ling' 'Guo, Cheng' _publ_section_title ; Methyl 4-(4-fluorophenyl)-6-isopropyl-2-(methylsulfonyl)pyrimidine-5-carboxylate ; _journal_issue 6 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o1127 _journal_volume 64 _journal_year 2008 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 98.090 _cell_angle_gamma 90.000 _cell_length_a 28.8750 _cell_length_b 9.8870 _cell_length_c 18.4000 _exptl_crystal_F_000 2208.00 _reflns_d_resolution_high 0.8102 _[local]_cod_data_source_file hk2457Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' H in P2(1)/c' _shelx_refln_list_code 4 _shelx_F_calc_maximum 324.00 _shelx_F_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 2256.79 3949.66 3949.66 o 3 0 0 82873.73 70976.95 1573.46 o 4 0 0 7448.02 4498.70 4498.70 o 5 0 0 89718.45 75334.31 2784.41 o 6 0 0 22685.48 23492.90 277.16 o 7 0 0 10026.96 9060.03 414.69 o 8 0 0 1965.74 1232.30 1232.30 o 9 0 0 20633.83 19623.32 183.60 o 10 0 0 3800.58 4017.30 146.70 o 11 0 0 266.59 123.23 123.23 o 12 0 0 26.78 1030.99 1030.99 o 13 0 0 13165.00 15490.79 183.97 o 14 0 0 15038.14 17244.37 361.43 o 15 0 0 15.13 1404.02 1404.02 o 16 0 0 656.67 401.39 401.39 o 17 0 0 7104.29 8344.10 179.65 o 18 0 0 4425.68 3781.57 239.92 o 19 0 0 3104.73 3435.84 292.40 o 20 0 0 211.59 128.20 128.20 o 21 0 0 701.03 677.98 102.21 o 22 0 0 141.16 172.20 172.20 o 23 0 0 2250.12 2165.23 118.19 o 24 0 0 42.79 267.71 267.71 o 25 0 0 1479.32 1706.64 117.73 o 26 0 0 81.60 286.81 286.81 o 27 0 0 846.19 884.56 123.90 o 28 0 0 193.94 113.05 113.05 o 29 0 0 365.03 301.65 90.90 o 30 0 0 266.52 116.59 116.59 o 31 0 0 277.72 332.13 69.52 o 32 0 0 54.96 66.98 66.98 o 33 0 0 41.70 17.13 131.38 o 34 0 0 11.19 8.61 65.36 o 1 1 0 1385.22 1672.10 88.44 o 2 1 0 19581.64 22790.18 753.66 o 3 1 0 2823.85 2886.72 94.13 o 4 1 0 407.61 417.79 23.16 o 5 1 0 17107.73 18040.61 124.93 o 6 1 0 2723.72 3121.15 58.04 o 7 1 0 758.93 982.63 180.48 o 8 1 0 5767.71 4854.04 635.17 o 9 1 0 622.49 2262.97 7346.97 o 10 1 0 9746.53 9218.61 439.34 o 11 1 0 10893.33 11141.93 2665.54 o 12 1 0 2278.75 3101.63 84.05 o 13 1 0 93.14 2938.04 3151.33 o 14 1 0 2271.91 2222.49 80.00 o 15 1 0 62.62 1868.03 1868.03 o 16 1 0 1107.80 950.18 404.32 o 17 1 0 963.03 515.42 1180.17 o 18 1 0 1360.39 1099.56 387.99 o 19 1 0 32.50 563.10 563.10 o 20 1 0 123.12 96.41 72.35 o 21 1 0 22.88 86.54 128.05 o 22 1 0 33.79 119.47 119.47 o 23 1 0 164.44 270.55 270.55 o 24 1 0 1722.83 1640.74 152.29 o 25 1 0 967.91 758.43 758.43 o 26 1 0 898.34 280.79 280.79 o 27 1 0 1414.82 1266.21 142.56 o 28 1 0 610.73 314.88 384.64 o 29 1 0 29.52 107.22 107.22 o 30 1 0 10.89 82.63 82.63 o 31 1 0 463.75 310.37 225.56 o 32 1 0 215.69 70.75 70.75 o 33 1 0 47.17 2.61 51.16 o 34 1 0 8.17 48.95 48.95 o 0 2 0 36.98 77.07 22.12 o 1 2 0 380.70 403.12 35.57 o 2 2 0 31548.40 33002.68 1581.64 o 3 2 0 29172.49 31259.06 798.87 o 4 2 0 3.57 31.02 33.69 o 5 2 0 12613.17 13206.25 554.67 o 6 2 0 5017.52 4983.60 79.09 o 7 2 0 15327.03 16379.90 195.35 o 8 2 0 546.05 577.77 36.51 o 9 2 0 1761.90 2329.85 128.32 o 10 2 0 6309.04 6293.19 109.75 o 11 2 0 19.39 337.74 714.57 o 12 2 0 197.44 215.52 37.11 o 13 2 0 106.96 332.95 949.28 o 14 2 0 1001.06 1096.17 67.73 o 15 2 0 8.38 811.64 1064.63 o 16 2 0 358.68 216.00 102.35 o 17 2 0 690.48 513.65 272.54 o 18 2 0 40.38 859.01 859.01 o 19 2 0 899.89 625.93 1193.67 o 20 2 0 2455.51 2001.39 183.15 o 21 2 0 200.91 1328.84 1333.16 o 22 2 0 349.47 1166.72 1166.72 o 23 2 0 2184.50 984.35 570.73 o 24 2 0 1378.32 219.49 1072.77 o 25 2 0 279.88 358.10 775.22 o 26 2 0 15.52 155.62 228.58 o 27 2 0 1.35 69.34 69.34 o 28 2 0 91.25 28.74 70.27 o 29 2 0 148.04 77.50 77.50 o 30 2 0 209.87 44.24 195.12 o 31 2 0 87.15 33.52 73.97 o 32 2 0 11.10 65.94 65.94 o 33 2 0 122.58 115.83 78.57 o 34 2 0 0.72 52.84 52.84 o 1 3 0 8802.88 8919.85 163.81 o 2 3 0 757.37 618.21 74.88 o 3 3 0 76044.04 78190.04 1928.64 o 4 3 0 2365.07 2634.98 61.77 o 5 3 0 16.76 46.88 33.88 o 6 3 0 5964.64 6376.22 101.49 o 7 3 0 1015.33 1033.59 44.91 o 8 3 0 2777.10 2891.35 71.39 o 9 3 0 350.99 394.54 86.08 o 10 3 0 2393.88 2825.71 82.72 o 11 3 0 21235.22 22512.48 213.96 o 12 3 0 690.38 391.07 159.63 o 13 3 0 1132.04 1017.60 136.90 o 14 3 0 23.61 139.16 164.06 o 15 3 0 547.21 110.26 610.61 o 16 3 0 1695.51 1484.61 84.17 o 17 3 0 243.02 298.49 516.83 o 18 3 0 327.89 172.94 48.89 o 19 3 0 23.91 95.10 95.10 o 20 3 0 0.49 648.94 650.56 o 21 3 0 1027.78 1076.45 81.78 o 22 3 0 1.91 287.16 287.16 o 23 3 0 170.31 5.73 83.82 o 24 3 0 193.77 847.74 847.74 o 25 3 0 1816.84 1653.21 107.51 o 26 3 0 29.32 602.20 602.20 o 27 3 0 315.47 230.44 96.58 o 28 3 0 7.18 98.91 109.16 o 29 3 0 68.43 84.20 50.13 o 30 3 0 25.29 77.43 117.20 o 31 3 0 187.12 57.14 76.13 o 32 3 0 195.94 161.93 62.81 o 33 3 0 33.92 53.07 53.07 o 34 3 0 92.03 3.67 55.10 o 0 4 0 210.44 248.93 38.05 o 1 4 0 13703.76 14154.91 544.77 o 2 4 0 896.88 883.68 41.89 o 3 4 0 1791.03 1792.34 69.57 o 4 4 0 1562.89 1361.19 52.24 o 5 4 0 4197.39 4372.35 114.63 o 6 4 0 76.87 95.24 26.90 o 7 4 0 13.22 9.70 22.30 o 8 4 0 210.13 233.75 31.90 o 9 4 0 444.56 554.44 42.62 o 10 4 0 1523.35 1637.76 66.86 o 11 4 0 1511.00 1415.48 139.36 o 12 4 0 152.96 115.42 37.93 o 13 4 0 145.94 114.98 56.38 o 14 4 0 192.15 75.20 204.78 o 15 4 0 2484.34 2334.58 101.94 o 16 4 0 1823.48 1310.16 402.25 o 17 4 0 1735.81 1795.21 280.34 o 18 4 0 119.34 163.48 464.02 o 19 4 0 1094.30 1103.58 393.46 o 20 4 0 1070.69 966.63 245.76 o 21 4 0 396.19 177.51 332.38 o 22 4 0 245.42 261.04 103.43 o 23 4 0 29.55 138.55 138.55 o 24 4 0 418.61 265.86 132.33 o 25 4 0 252.89 668.30 668.30 o 26 4 0 1241.19 1267.48 245.74 o 27 4 0 107.60 191.71 384.51 o 28 4 0 44.80 56.95 56.95 o 29 4 0 0.71 214.61 263.11 o 30 4 0 431.93 290.54 99.76 o 31 4 0 184.74 73.71 152.63 o 32 4 0 0.30 49.30 49.30 o 33 4 0 1.91 51.28 74.03 o 1 5 0 199.46 270.64 37.95 o 2 5 0 746.60 822.25 94.61 o 3 5 0 4804.73 4508.61 151.70 o 4 5 0 1157.14 1335.53 54.82 o 5 5 0 1350.95 1168.40 53.50 o 6 5 0 7.65 25.70 42.23 o 7 5 0 165.99 165.06 27.81 o 8 5 0 49.28 111.69 36.80 o 9 5 0 682.02 672.53 49.25 o 10 5 0 3501.58 3251.60 208.67 o 11 5 0 194.74 149.94 37.58 o 12 5 0 211.29 191.57 37.99 o 13 5 0 17.97 31.19 28.38 o 14 5 0 40.29 52.46 30.70 o 15 5 0 257.78 443.62 145.44 o 16 5 0 2081.31 1983.61 87.51 o 17 5 0 4.36 40.73 40.73 o 18 5 0 12.53 172.85 229.68 o 19 5 0 795.68 670.26 70.52 o 20 5 0 285.38 140.57 122.72 o 21 5 0 587.38 198.93 400.64 o 22 5 0 1152.40 836.35 182.47 o 23 5 0 223.54 214.92 74.93 o 24 5 0 1.41 52.85 52.85 o 25 5 0 132.86 40.12 50.88 o 26 5 0 5.65 89.97 89.97 o 27 5 0 172.75 193.35 56.61 o 28 5 0 0.34 54.65 54.65 o 29 5 0 17.15 168.67 311.21 o 30 5 0 577.42 332.93 245.11 o 31 5 0 1.37 62.95 183.66 o 32 5 0 7.67 5.24 63.41 o 0 6 0 116.49 96.01 37.90 o 1 6 0 548.77 359.39 108.18 o 2 6 0 599.42 684.04 57.82 o 3 6 0 469.64 442.98 73.59 o 4 6 0 271.64 191.69 34.71 o 5 6 0 220.17 244.63 36.53 o 6 6 0 160.73 206.91 37.93 o 7 6 0 116.01 103.20 37.02 o 8 6 0 2113.76 2025.36 78.68 o 9 6 0 324.41 251.12 42.65 o 10 6 0 269.66 217.45 61.76 o 11 6 0 11.42 9.46 46.41 o 12 6 0 111.92 84.27 38.13 o 13 6 0 329.43 458.42 59.83 o 14 6 0 165.13 238.74 77.11 o 15 6 0 16.85 79.51 56.53 o 16 6 0 224.22 234.13 39.43 o 17 6 0 31.67 41.44 80.04 o 18 6 0 820.18 1006.30 74.31 o 19 6 0 504.73 403.60 153.31 o 20 6 0 12.76 15.32 40.35 o 21 6 0 44.99 75.88 75.88 o 22 6 0 795.63 717.43 158.05 o 23 6 0 138.27 236.48 55.92 o 24 6 0 124.48 128.55 123.92 o 25 6 0 26.12 30.66 62.49 o 26 6 0 90.97 144.91 197.45 o 27 6 0 7.35 71.35 122.35 o 28 6 0 532.29 622.95 72.62 o 29 6 0 115.13 61.38 61.38 o 30 6 0 18.80 2.17 50.59 o 1 7 0 547.18 492.96 51.30 o 2 7 0 1140.69 1155.96 67.46 o 3 7 0 43.59 81.20 50.50 o 4 7 0 543.07 371.15 72.38 o 5 7 0 2172.00 2095.65 216.75 o 6 7 0 47.47 40.38 30.91 o 7 7 0 54.92 102.17 34.72 o 8 7 0 4.89 14.14 29.88 o 9 7 0 788.04 844.71 60.85 o 10 7 0 70.65 78.58 47.14 o 11 7 0 309.82 334.03 44.66 o 12 7 0 2.06 20.30 34.95 o 13 7 0 863.19 952.67 67.20 o 14 7 0 210.23 168.17 59.58 o 15 7 0 11.64 14.74 61.08 o 16 7 0 465.15 490.93 87.34 o 17 7 0 607.28 741.14 79.72 o 18 7 0 3.51 14.82 43.34 o 19 7 0 12.43 27.43 118.47 o 20 7 0 760.89 960.32 76.14 o 21 7 0 16.59 59.92 59.92 o 22 7 0 468.24 717.31 74.82 o 23 7 0 113.96 133.46 97.56 o 24 7 0 0.23 48.64 48.64 o 25 7 0 126.52 105.62 55.72 o 26 7 0 26.83 36.80 52.98 o 27 7 0 135.06 146.37 67.65 o 28 7 0 134.31 110.00 59.64 o 0 8 0 2136.18 1977.19 119.74 o 1 8 0 949.26 749.52 324.56 o 2 8 0 229.41 126.11 88.56 o 3 8 0 455.64 330.12 279.21 o 4 8 0 354.87 222.08 196.85 o 5 8 0 40.99 5.76 36.35 o 6 8 0 37.03 9.26 38.92 o 7 8 0 728.06 436.61 345.60 o 8 8 0 45.77 32.57 46.62 o 9 8 0 53.91 98.60 47.49 o 10 8 0 1084.24 892.76 672.25 o 11 8 0 262.72 98.08 171.41 o 12 8 0 0.13 65.78 38.50 o 13 8 0 2.96 22.72 111.48 o 14 8 0 2.25 31.95 77.25 o 15 8 0 260.23 203.82 99.40 o 16 8 0 9.73 11.92 38.71 o 17 8 0 5.24 16.62 39.34 o 18 8 0 10.50 37.58 40.48 o 19 8 0 33.26 25.89 67.79 o 20 8 0 188.26 60.15 126.27 o 21 8 0 42.33 45.00 46.47 o 22 8 0 260.10 132.23 164.88 o 23 8 0 10.92 22.75 47.58 o 24 8 0 88.95 92.30 42.77 o 25 8 0 4.25 14.38 51.87 o 26 8 0 7.74 80.44 37.01 o 1 9 0 303.57 254.59 55.10 o 2 9 0 0.65 7.25 36.97 o 3 9 0 315.14 234.34 84.58 o 4 9 0 4.51 46.32 40.45 o 5 9 0 2.40 33.89 40.08 o 6 9 0 0.59 13.20 38.70 o 7 9 0 9.55 27.64 34.38 o 8 9 0 2.32 22.78 57.99 o 9 9 0 18.21 66.19 65.59 o 10 9 0 0.23 7.01 96.74 o 11 9 0 6.05 82.36 71.25 o 12 9 0 254.59 222.05 55.44 o 13 9 0 427.27 341.71 62.18 o 14 9 0 9.02 63.59 115.57 o 15 9 0 791.86 893.05 76.05 o 16 9 0 83.05 194.55 63.20 o 17 9 0 158.03 186.67 68.11 o 18 9 0 159.08 207.30 54.76 o 19 9 0 18.02 4.00 55.37 o 20 9 0 14.77 6.74 44.77 o 21 9 0 0.30 52.95 49.05 o 22 9 0 6.71 28.96 48.05 o 23 9 0 58.31 70.58 105.16 o 0 10 0 258.05 313.31 57.65 o 1 10 0 65.33 80.88 43.52 o 2 10 0 144.14 198.24 59.81 o 3 10 0 421.59 516.08 65.65 o 4 10 0 42.53 97.34 44.06 o 5 10 0 107.35 183.54 51.11 o 6 10 0 11.29 96.03 40.82 o 7 10 0 10.00 12.29 41.12 o 8 10 0 541.87 737.21 118.36 o 9 10 0 578.27 642.48 74.01 o 10 10 0 26.05 71.38 49.50 o 11 10 0 267.08 277.87 106.97 o 12 10 0 966.13 1049.87 83.11 o 13 10 0 446.63 611.92 69.80 o 14 10 0 94.45 67.24 51.69 o 15 10 0 145.55 169.99 55.00 o 16 10 0 3.91 40.61 71.17 o 17 10 0 32.12 37.96 51.81 o 18 10 0 25.53 35.34 41.22 o 19 10 0 6.58 25.21 43.65 o 20 10 0 0.07 88.02 126.86 o 1 11 0 6.56 34.20 60.46 o 2 11 0 15.07 80.49 36.03 o 3 11 0 58.57 68.69 47.75 o 4 11 0 66.32 38.31 47.48 o 5 11 0 22.84 32.99 51.56 o 6 11 0 50.55 37.84 46.85 o 7 11 0 0.81 25.97 43.35 o 8 11 0 27.99 35.87 60.65 o 9 11 0 4.20 92.24 92.24 o 10 11 0 4.06 36.43 104.64 o 11 11 0 0.72 51.27 48.62 o 12 11 0 0.00 51.18 51.18 o 13 11 0 0.00 3.68 88.14 o 14 11 0 24.31 8.36 48.78 o 15 11 0 56.42 14.43 53.20 o -34 1 1 2.17 125.99 49.82 o -33 1 1 1.91 65.20 57.63 o -32 1 1 0.02 66.83 69.92 o -31 1 1 123.60 339.66 64.63 o -30 1 1 53.34 25.67 92.65 o -29 1 1 182.18 188.53 77.57 o -28 1 1 523.46 459.99 108.45 o -27 1 1 0.85 104.73 104.73 o -26 1 1 625.39 479.00 110.17 o -25 1 1 94.00 32.18 98.00 o -24 1 1 202.93 172.03 78.22 o -23 1 1 194.52 105.46 81.16 o -22 1 1 17.22 61.42 61.42 o -21 1 1 143.90 13.67 73.66 o -20 1 1 1722.99 1457.26 129.41 o -19 1 1 1455.55 1459.53 118.61 o -18 1 1 1249.32 1319.03 109.12 o -17 1 1 195.60 59.00 52.28 o -16 1 1 70.82 70.01 44.68 o -15 1 1 2679.63 2610.51 122.75 o -14 1 1 3319.14 3248.48 126.93 o -13 1 1 562.24 552.07 59.75 o -12 1 1 0.14 39.79 27.76 o -11 1 1 447.92 414.95 52.93 o -10 1 1 2801.91 3054.14 102.49 o -9 1 1 371.36 325.46 36.73 o -8 1 1 25.50 19.27 24.79 o -7 1 1 8307.01 8270.49 137.45 o -6 1 1 11749.20 12787.36 157.47 o -5 1 1 730.87 819.63 42.49 o -4 1 1 24.90 21.50 21.50 o -3 1 1 18499.13 20981.27 160.37 o -2 1 1 31391.79 32457.75 777.95 o -1 1 1 1166.87 1310.91 37.54 o 0 1 1 1475.60 1710.60 43.13 o 1 1 1 3807.03 4161.09 66.48 o 2 1 1 21.65 26.04 16.84 o 3 1 1 14596.53 16125.85 149.76 o 4 1 1 4784.63 5377.69 96.24 o 5 1 1 39935.86 41537.37 276.64 o 6 1 1 7859.66 7807.95 129.72 o 7 1 1 3650.34 3661.89 95.58 o 8 1 1 132.35 150.99 32.88 o 9 1 1 12.41 11.58 31.16 o 10 1 1 19.88 36.93 36.93 o 11 1 1 3616.52 3935.56 126.84 o 12 1 1 19516.83 22254.81 303.12 o 13 1 1 896.91 778.04 82.26 o 14 1 1 5442.43 6188.24 182.94 o 15 1 1 1810.80 1951.42 111.58 o 16 1 1 844.98 875.53 96.34 o 17 1 1 1.43 89.61 89.61 o 18 1 1 23.36 17.80 58.99 o 19 1 1 15.43 93.48 93.48 o 20 1 1 237.68 252.44 78.59 o 21 1 1 6.17 208.01 208.01 o 22 1 1 1767.91 1605.63 217.56 o 23 1 1 1168.87 1140.26 254.60 o 24 1 1 286.89 231.29 231.29 o 25 1 1 269.02 167.25 167.25 o 26 1 1 550.91 233.42 127.01 o 27 1 1 203.82 137.19 137.19 o 28 1 1 1.06 97.29 97.29 o 29 1 1 0.31 43.25 84.26 o 30 1 1 74.65 115.51 115.51 o 31 1 1 220.59 205.33 81.12 o 32 1 1 0.64 101.22 101.22 o 33 1 1 100.59 89.33 89.33 o 34 1 1 131.91 15.76 70.65 o -34 2 1 8.27 31.40 71.01 o -33 2 1 98.51 90.66 90.66 o -32 2 1 472.58 414.66 89.31 o -31 2 1 6.32 102.28 102.28 o -30 2 1 1.09 85.79 85.79 o -29 2 1 336.55 421.65 86.03 o -28 2 1 175.47 33.42 100.91 o -27 2 1 1333.28 1380.62 154.60 o -26 2 1 232.91 120.52 126.77 o -25 2 1 171.54 46.88 108.28 o -24 2 1 742.65 838.51 119.20 o -23 2 1 58.85 92.19 92.19 o -22 2 1 346.35 389.79 85.84 o -21 2 1 132.27 159.25 67.06 o -20 2 1 49.58 63.04 52.72 o -19 2 1 713.03 804.60 91.73 o -18 2 1 186.91 95.48 58.12 o -17 2 1 583.36 485.32 68.78 o -16 2 1 556.93 523.47 73.23 o -15 2 1 325.57 387.15 55.32 o -14 2 1 25.26 30.07 33.55 o -13 2 1 90.45 59.65 46.22 o -12 2 1 13406.38 13675.57 233.86 o -11 2 1 6650.72 6908.69 162.65 o -10 2 1 10870.70 11652.03 197.25 o -9 2 1 4.99 20.13 25.53 o -8 2 1 9865.01 10279.67 169.99 o -7 2 1 4461.58 4220.78 108.25 o -6 2 1 27543.04 27668.96 251.74 o -5 2 1 503.91 506.56 39.59 o -4 2 1 4981.49 5177.44 102.03 o -3 2 1 6001.63 7104.15 114.49 o -2 2 1 19958.42 21268.45 189.40 o -1 2 1 62358.71 58388.80 1283.94 o 0 2 1 447.98 483.09 35.27 o 1 2 1 54933.06 56561.05 304.74 o 2 2 1 21786.31 21720.73 198.61 o 3 2 1 29032.19 31404.41 246.63 o 4 2 1 462.74 509.91 39.74 o 5 2 1 2088.64 1917.78 71.66 o 6 2 1 16931.11 18334.29 214.41 o 7 2 1 14850.59 15618.32 207.21 o 8 2 1 53.62 39.61 30.47 o 9 2 1 6773.03 6951.53 152.50 o 10 2 1 2.07 6.68 31.26 o 11 2 1 1289.79 1399.19 82.85 o 12 2 1 0.86 46.84 41.65 o 13 2 1 734.33 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111.90 111.90 o 5 1 21 377.74 426.94 131.34 o 6 1 21 55.40 139.70 106.36 o 7 1 21 2.16 0.00 91.64 o 8 1 21 97.07 42.95 133.44 o -16 2 21 408.28 512.35 118.23 o -15 2 21 8.08 169.44 79.36 o -14 2 21 14.39 38.83 111.99 o -13 2 21 373.50 358.61 102.43 o -12 2 21 660.32 811.57 137.80 o -11 2 21 433.24 501.38 121.55 o -10 2 21 71.40 136.11 99.85 o -9 2 21 2.37 73.25 103.54 o -8 2 21 338.58 360.90 117.84 o -7 2 21 361.99 213.55 123.25 o -6 2 21 138.10 117.16 113.61 o -5 2 21 95.00 23.22 97.19 o -4 2 21 268.44 254.45 108.48 o -3 2 21 40.34 34.72 77.68 o -2 2 21 85.27 93.33 96.19 o -1 2 21 752.84 838.63 125.54 o 0 2 21 220.08 96.14 118.93 o 1 2 21 136.22 196.07 97.98 o 2 2 21 65.76 112.69 116.72 o 3 2 21 226.81 76.73 112.93 o 4 2 21 676.32 835.61 138.22 o 5 2 21 129.28 13.33 116.87 o 6 2 21 96.50 27.17 101.36 o 7 2 21 47.35 206.67 98.42 o -14 3 21 44.42 100.20 103.25 o -13 3 21 0.79 24.77 106.76 o -12 3 21 294.85 441.88 104.12 o -11 3 21 0.00 48.55 80.38 o -10 3 21 40.89 23.96 91.16 o -9 3 21 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300.77 124.65 176.18 o -5 0 22 101.34 138.75 138.75 o -4 0 22 499.47 412.83 169.54 o -3 0 22 330.31 638.25 123.53 o -2 0 22 195.48 408.94 131.22 o -1 0 22 55.62 136.12 120.06 o 0 0 22 106.12 45.46 136.25 o 1 0 22 14.32 45.13 113.48 o 2 0 22 1.12 60.41 112.97 o 3 0 22 335.84 608.21 137.66 o -12 1 22 1.25 100.67 94.26 o -11 1 22 50.72 28.47 111.96 o -10 1 22 75.06 154.56 96.44 o -9 1 22 64.45 0.00 112.71 o -8 1 22 13.49 13.75 120.19 o -7 1 22 50.85 40.60 112.35 o -6 1 22 72.72 123.97 123.97 o -5 1 22 7.59 26.55 110.97 o -4 1 22 28.77 79.17 102.27 o -3 1 22 0.55 158.55 102.41 o -2 1 22 212.35 265.77 99.49 o -1 1 22 188.10 161.08 131.55 o 0 1 22 218.27 176.99 116.33 o 1 1 22 122.44 235.17 116.60 o 2 1 22 93.77 14.06 128.23 o 3 1 22 177.04 372.40 112.76 o -10 2 22 102.97 26.42 100.51 o -9 2 22 7.57 120.78 120.78 o -8 2 22 47.74 122.58 122.58 o -7 2 22 112.04 253.59 94.86 o -6 2 22 0.65 37.59 78.29 o -5 2 22 0.09 24.84 103.98 o -4 2 22 201.06 235.37 125.65 o -3 2 22 152.44 198.58 99.28 o -2 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