#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/84/2218440.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2218440_Fobs loop_ _publ_author_name 'Hojjat Kashani, Leila' 'Yousefi, Mohammad' 'Amani, Vahid' 'Khavasi, Hamid Reza' _publ_section_title ; 1,4,10,13-Tetraoxa-7,16-diazoniacyclooctadecane bis[tetrachloridoaurate(III)] dihydrate ; _journal_coeditor_code HK2465 _journal_issue 6 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m840 _journal_page_last m841 _journal_volume 64 _journal_year 2008 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 73.063 _cell_angle_beta 75.965 _cell_angle_gamma 74.929 _cell_length_a 8.0168 _cell_length_b 8.3359 _cell_length_c 11.2989 _exptl_crystal_F_000 1888.00 _reflns_d_resolution_high 0.8885 _[local]_cod_data_source_file hk2465Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' KH153 YOUSEFI/SHAHRE-REY BRANCH/20.11.86' _shelx_refln_list_code 4 _shelx_F_calc_maximum 154.72 _shelx_F_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 154.71 201.36 12.92 o 4 0 0 4976.46 4932.82 219.05 o 5 0 0 6356.40 5966.79 19.13 o 6 0 0 2701.49 2587.36 21.66 o 7 0 0 7427.20 6955.34 19.63 o 8 0 0 1003.52 969.79 8.27 o -8 1 0 17.85 32.41 5.25 o -7 1 0 3710.57 3827.01 14.55 o -6 1 0 994.11 1028.90 8.53 o -5 1 0 3693.51 3624.38 14.29 o -4 1 0 3468.65 3387.46 14.41 o -3 1 0 5462.55 5364.13 19.20 o -2 1 0 12745.30 12334.72 32.55 o -1 1 0 11716.72 11783.02 37.90 o 0 1 0 12838.82 12863.63 106.63 o 1 1 0 1890.41 1962.90 12.86 o 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