#------------------------------------------------------------------------------ #$Date: 2016-04-03 01:50:10 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181104 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/84/2218443.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2218443_Fobs loop_ _publ_author_name 'Wang, Zhi-Xiang' 'Li, Xiu-Bing' 'Sun, Bai-Wang' _publ_section_title ; Poly[diaquabis(\m^2^-azido-\k^2^N^1^:N^1^)bis(\m~3~-1-oxoisonicotinato-\k^3^O:O':O'')dicadmium(II)] ; _journal_coeditor_code HY2123 _journal_issue 6 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m792 _journal_page_last m793 _journal_volume 64 _journal_year 2008 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 99.668 _cell_angle_beta 97.164 _cell_angle_gamma 107.566 _cell_length_a 6.5409 _cell_length_b 7.8502 _cell_length_c 9.4096 _exptl_crystal_F_000 300.00 _reflns_d_resolution_high 0.8410 _cod_data_source_file hy2123Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' sun691m in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 131.62 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 8501.98 7039.62 111.34 o 2 0 0 274.28 251.16 5.77 o 3 0 0 4859.90 4803.15 73.26 o 4 0 0 2762.85 3051.93 47.20 o 5 0 0 1508.45 1462.29 27.90 o 6 0 0 1071.58 1103.55 29.92 o 7 0 0 764.68 771.01 26.62 o -7 1 0 0.67 1.14 1.54 o -6 1 0 52.18 49.53 2.90 o -5 1 0 18.37 15.91 1.62 o -4 1 0 818.20 875.14 14.21 o -3 1 0 66.17 64.00 2.21 o -2 1 0 5119.90 5602.80 103.34 o -1 1 0 27.53 30.34 0.94 o 0 1 0 1221.07 1173.01 30.16 o 1 1 0 333.16 282.40 5.75 o 2 1 0 574.29 578.44 21.86 o 3 1 0 0.94 0.00 0.72 o 4 1 0 1.25 5.36 1.30 o 5 1 0 39.31 56.13 5.63 o 6 1 0 319.32 285.04 13.87 o -7 2 0 1219.06 1177.65 23.47 o -6 2 0 1187.13 1159.05 22.72 o -5 2 0 1545.91 1609.39 30.33 o -4 2 0 7670.58 7823.89 139.80 o -3 2 0 8018.21 8255.33 147.06 o -2 2 0 879.25 904.35 16.79 o -1 2 0 2373.12 2262.51 40.65 o 0 2 0 7585.55 6721.09 169.72 o 1 2 0 3787.33 3640.44 92.78 o 2 2 0 5706.89 5823.87 104.15 o 3 2 0 3175.21 3350.64 66.35 o 4 2 0 870.47 853.40 18.61 o 5 2 0 1231.65 1270.12 24.95 o 6 2 0 936.99 895.65 37.74 o -7 3 0 1.49 7.57 2.64 o -6 3 0 134.86 145.26 4.60 o -5 3 0 0.27 0.00 0.98 o -4 3 0 65.34 74.51 2.74 o -3 3 0 4.68 10.38 1.10 o -2 3 0 390.00 428.44 8.45 o -1 3 0 338.31 373.92 7.44 o 0 3 0 973.75 990.19 26.41 o 1 3 0 41.23 28.58 2.50 o 2 3 0 146.95 195.25 7.07 o 3 3 0 277.05 332.47 11.18 o 4 3 0 58.64 59.73 3.21 o 5 3 0 78.90 93.83 8.70 o 6 3 0 20.46 14.71 2.10 o -7 4 0 637.62 600.00 19.09 o -6 4 0 696.81 715.81 14.80 o -5 4 0 1541.73 1601.73 30.18 o -4 4 0 3377.59 3423.02 62.02 o -3 4 0 1323.01 1316.45 24.50 o -2 4 0 4323.86 4370.82 78.40 o -1 4 0 6359.77 6174.01 110.24 o 0 4 0 2307.69 2346.61 60.95 o 1 4 0 2710.72 2223.53 58.04 o 2 4 0 2412.39 2301.76 60.56 o 3 4 0 1825.42 1950.34 52.29 o 4 4 0 879.64 1007.34 29.18 o 5 4 0 812.78 838.89 25.47 o -7 5 0 2.65 6.24 2.47 o -6 5 0 0.00 1.97 1.70 o -5 5 0 15.67 12.84 1.68 o -4 5 0 68.30 76.30 2.97 o -3 5 0 223.88 204.20 4.97 o -2 5 0 177.74 175.88 4.43 o -1 5 0 34.86 21.21 1.54 o 0 5 0 14.34 24.41 2.89 o 1 5 0 117.21 145.74 6.73 o 2 5 0 5.45 8.89 2.30 o 3 5 0 34.17 36.17 3.93 o 4 5 0 5.84 1.74 2.47 o -7 6 0 747.93 765.31 23.52 o -6 6 0 804.73 860.42 25.42 o -5 6 0 1354.24 1406.21 26.94 o -4 6 0 2058.77 2036.42 37.85 o -3 6 0 1538.44 1614.37 30.26 o -2 6 0 2023.83 1849.77 80.76 o -1 6 0 2442.36 2407.58 44.28 o 0 6 0 2475.88 2367.80 62.52 o 1 6 0 2754.89 2665.87 70.60 o 2 6 0 1486.63 1657.99 45.83 o 3 6 0 1342.07 1409.78 39.99 o -6 7 0 6.14 6.14 2.89 o -5 7 0 44.17 52.71 3.08 o -4 7 0 66.20 73.72 3.28 o -3 7 0 3.13 3.10 1.16 o -2 7 0 2.64 5.24 2.60 o -1 7 0 4.30 5.85 2.05 o 0 7 0 1.88 1.33 2.01 o 1 7 0 3.48 7.30 2.74 o 2 7 0 42.79 41.54 4.58 o -5 8 0 906.28 971.66 28.25 o -4 8 0 1421.65 1452.98 28.16 o -3 8 0 1890.04 1957.65 43.86 o -2 8 0 911.79 938.95 18.84 o -1 8 0 966.40 877.85 19.65 o 0 8 0 984.74 996.27 30.22 o 1 8 0 676.56 681.99 21.78 o -4 9 0 37.98 50.06 3.05 o -3 9 0 10.71 20.40 3.14 o -2 9 0 1.82 2.83 1.70 o -1 9 0 1.38 10.04 1.65 o 1 -9 1 4.74 9.35 2.65 o 2 -9 1 9.31 29.05 3.45 o 3 -9 1 6.38 10.09 2.45 o 4 -9 1 10.48 13.73 2.44 o -1 -8 1 636.24 664.23 21.11 o 0 -8 1 901.25 944.48 19.20 o 1 -8 1 1194.30 1202.75 23.54 o 2 -8 1 1655.38 1632.09 31.08 o 3 -8 1 2311.90 2437.15 45.41 o 4 -8 1 1628.82 1731.51 37.75 o 5 -8 1 732.81 809.61 16.95 o -3 -7 1 2.32 10.15 3.52 o -2 -7 1 19.07 25.54 3.89 o -1 -7 1 1.94 3.56 2.31 o 0 -7 1 20.09 30.40 3.38 o 1 -7 1 38.13 38.41 3.42 o 2 -7 1 66.52 61.54 4.20 o 3 -7 1 102.66 115.60 4.00 o 4 -7 1 264.94 293.49 7.11 o 5 -7 1 4.37 3.91 1.36 o 6 -7 1 107.52 106.03 4.51 o -4 -6 1 881.53 953.96 29.12 o -3 -6 1 1601.68 1481.94 41.90 o -2 -6 1 1564.67 1674.15 46.17 o -1 -6 1 1639.33 1848.28 50.02 o 0 -6 1 2769.49 2507.26 65.83 o 1 -6 1 2053.88 2002.80 36.98 o 2 -6 1 735.53 712.34 14.13 o 3 -6 1 1441.41 1460.13 47.02 o 4 -6 1 2363.89 2530.10 46.70 o 5 -6 1 1666.94 1828.55 50.02 o 6 -6 1 634.20 632.75 13.57 o 7 -6 1 734.28 724.68 22.34 o -4 -5 1 30.35 38.14 4.22 o -3 -5 1 16.30 12.19 2.85 o -2 -5 1 39.55 29.95 3.47 o -1 -5 1 72.52 80.40 4.94 o 0 -5 1 3.27 4.19 1.99 o 1 -5 1 45.19 40.25 1.89 o 2 -5 1 69.21 66.23 5.36 o 3 -5 1 73.94 72.68 3.21 o 4 -5 1 23.70 21.92 1.79 o 5 -5 1 2.02 7.68 1.36 o 6 -5 1 10.36 16.66 3.92 o 7 -5 1 2.33 5.98 2.51 o -5 -4 1 405.93 409.95 14.32 o -4 -4 1 922.88 939.33 27.21 o -3 -4 1 1392.75 1563.71 42.41 o -2 -4 1 2585.38 2520.56 65.83 o -1 -4 1 2804.53 3012.48 77.97 o 0 -4 1 2014.60 1837.24 48.08 o 1 -4 1 7132.94 6604.68 117.82 o 2 -4 1 3450.25 3616.26 64.97 o 3 -4 1 2670.65 2864.51 51.95 o 4 -4 1 3139.18 3286.22 59.71 o 5 -4 1 1085.69 1032.32 65.84 o 6 -4 1 969.43 942.36 26.96 o 7 -4 1 1044.88 1059.97 21.55 o -6 -3 1 0.58 0.35 1.47 o -5 -3 1 31.10 32.15 2.45 o -4 -3 1 12.90 18.70 2.41 o -3 -3 1 81.42 89.80 3.34 o -2 -3 1 129.53 118.61 4.94 o -1 -3 1 80.26 104.01 4.53 o 0 -3 1 588.32 550.68 15.26 o 1 -3 1 1453.64 1467.80 26.77 o 2 -3 1 112.67 152.68 4.94 o 3 -3 1 15.61 20.13 1.42 o 4 -3 1 33.63 37.22 2.12 o 5 -3 1 19.86 18.68 2.87 o 6 -3 1 73.66 76.36 3.58 o 7 -3 1 5.22 2.85 3.90 o -6 -2 1 782.63 862.88 18.07 o -5 -2 1 1865.43 1933.10 36.57 o -4 -2 1 1660.48 1598.31 105.43 o -3 -2 1 2367.56 2444.67 62.59 o -2 -2 1 7260.06 7537.43 114.69 o -1 -2 1 5494.31 5419.42 102.88 o 0 -2 1 2540.47 2429.61 122.36 o 1 -2 1 11835.66 10231.45 181.58 o 2 -2 1 5583.86 5781.25 103.12 o 3 -2 1 5585.84 5676.55 101.48 o 4 -2 1 5164.89 5543.85 99.56 o 5 -2 1 2073.41 1906.76 84.02 o 6 -2 1 1268.66 1258.07 24.65 o 7 -2 1 390.63 427.39 13.80 o -7 -1 1 1.71 2.16 4.18 o -6 -1 1 10.87 9.20 1.73 o -5 -1 1 45.01 56.24 2.92 o -4 -1 1 53.20 56.21 5.72 o -3 -1 1 31.03 35.89 3.14 o -2 -1 1 4.54 0.00 0.54 o -1 -1 1 2157.25 2264.26 34.76 o 0 -1 1 713.34 645.10 19.41 o 1 -1 1 587.75 601.54 9.49 o 2 -1 1 13.46 20.80 4.79 o 3 -1 1 200.83 198.40 14.98 o 4 -1 1 178.69 169.86 4.81 o 5 -1 1 83.82 81.72 3.41 o 6 -1 1 112.02 110.54 4.30 o 7 -1 1 1.02 1.98 1.60 o -7 0 1 553.84 524.09 11.96 o -6 0 1 1513.11 1478.47 28.52 o -5 0 1 1360.38 1345.28 30.73 o -4 0 1 587.04 562.55 10.78 o -3 0 1 9890.03 9892.33 150.25 o -2 0 1 17322.56 14114.78 212.80 o -1 0 1 7834.95 7383.67 111.75 o 1 0 1 5067.43 5104.68 90.89 o 2 0 1 3357.31 3428.81 61.61 o 3 0 1 2883.26 2893.30 52.48 o 4 0 1 2492.62 2213.97 91.47 o 5 0 1 1228.23 1115.73 21.88 o 6 0 1 858.95 795.53 16.60 o 7 0 1 658.15 636.00 14.27 o -7 1 1 18.42 23.18 3.38 o -6 1 1 302.83 249.65 6.40 o -5 1 1 138.93 130.01 12.22 o -4 1 1 1191.29 1288.71 30.91 o -3 1 1 0.03 0.00 0.72 o -2 1 1 5577.62 6060.40 107.85 o -1 1 1 10.57 8.38 0.43 o 0 1 1 418.84 376.39 10.23 o 1 1 1 610.39 604.78 13.28 o 2 1 1 804.87 845.52 20.40 o 3 1 1 30.32 25.98 5.10 o 4 1 1 290.55 261.99 14.66 o 5 1 1 10.45 11.00 1.69 o 6 1 1 0.85 1.09 1.83 o -7 2 1 1123.21 960.32 28.27 o -6 2 1 4049.83 3911.26 71.30 o -5 2 1 1693.25 1718.97 27.19 o -4 2 1 724.55 783.80 18.39 o -3 2 1 4375.84 4600.45 82.37 o -2 2 1 943.80 977.73 25.23 o -1 2 1 4884.94 4969.74 88.61 o 1 2 1 3112.98 2933.84 75.21 o 2 2 1 2168.49 2335.45 60.73 o 3 2 1 2302.46 2213.74 48.51 o 4 2 1 3335.65 3265.74 59.87 o 5 2 1 1322.70 1238.76 24.46 o 6 2 1 348.13 380.07 9.54 o -7 3 1 4.18 0.00 2.38 o -6 3 1 158.81 167.56 9.08 o -5 3 1 51.96 60.18 2.69 o -4 3 1 2.24 3.30 1.02 o -3 3 1 35.24 35.58 1.58 o -2 3 1 93.60 105.00 2.72 o -1 3 1 57.16 71.31 2.18 o 0 3 1 1730.04 1731.48 44.96 o 1 3 1 89.01 90.52 4.32 o 2 3 1 780.82 892.80 25.05 o 3 3 1 7.52 9.11 2.28 o 4 3 1 9.35 11.45 2.78 o 5 3 1 42.23 53.75 5.08 o -7 4 1 779.98 699.55 21.67 o -6 4 1 1098.19 1068.26 30.34 o -5 4 1 1202.50 1306.58 24.86 o -4 4 1 3479.49 3237.90 150.52 o -3 4 1 4650.06 4658.52 83.59 o -2 4 1 2762.38 2783.63 50.37 o -1 4 1 3077.39 3156.17 57.00 o 0 4 1 6244.59 6116.03 155.47 o 1 4 1 3912.99 4232.66 108.69 o 2 4 1 1864.70 1718.66 46.12 o 3 4 1 1174.25 1124.27 31.82 o 4 4 1 1550.60 1552.12 43.19 o 5 4 1 1085.57 1096.83 32.23 o -7 5 1 5.11 9.23 2.73 o -6 5 1 0.05 0.00 2.09 o -5 5 1 38.48 45.12 2.50 o -4 5 1 117.96 131.29 6.05 o -3 5 1 56.71 63.15 2.57 o -2 5 1 957.44 991.36 18.96 o -1 5 1 67.98 89.98 3.08 o 0 5 1 13.77 7.97 1.86 o 1 5 1 50.95 31.52 3.13 o 2 5 1 23.78 27.93 3.32 o 3 5 1 3.18 5.21 2.13 o 4 5 1 39.66 32.46 4.32 o -7 6 1 883.66 798.75 24.52 o -6 6 1 833.16 872.61 26.16 o -5 6 1 1579.63 1614.69 43.99 o -4 6 1 1817.19 1988.86 37.06 o -3 6 1 1509.68 1619.97 33.13 o -2 6 1 2683.04 2759.23 50.51 o -1 6 1 2367.71 2270.72 41.94 o 0 6 1 2726.16 2940.08 77.04 o 1 6 1 1852.11 1834.24 49.77 o 2 6 1 946.26 921.64 27.16 o 3 6 1 666.41 785.21 24.24 o -6 7 1 14.61 12.96 3.22 o -5 7 1 50.08 50.94 4.53 o -4 7 1 0.19 0.43 1.11 o -3 7 1 10.01 13.49 1.73 o -2 7 1 11.88 12.68 1.55 o -1 7 1 40.89 50.96 2.76 o 0 7 1 25.56 34.28 3.66 o 1 7 1 69.19 81.96 6.06 o 2 7 1 7.14 6.53 2.73 o -5 8 1 1095.43 1122.42 32.09 o -4 8 1 1369.42 1412.31 39.06 o -3 8 1 974.29 946.41 19.05 o -2 8 1 765.72 744.28 15.46 o -1 8 1 664.40 633.24 13.54 o 0 8 1 924.36 940.00 19.35 o -3 9 1 1.10 3.32 1.51 o 1 -9 2 27.54 39.10 4.34 o 2 -9 2 0.83 3.08 2.12 o 3 -9 2 0.00 4.39 2.08 o 4 -9 2 24.69 28.52 3.43 o -1 -8 2 850.73 957.59 28.66 o 0 -8 2 1082.20 976.27 28.59 o 1 -8 2 1887.40 1751.43 47.92 o 2 -8 2 2835.68 2719.31 72.02 o 3 -8 2 674.12 708.93 21.20 o 4 -8 2 188.36 192.53 7.87 o 5 -8 2 960.53 949.30 27.54 o -3 -7 2 0.95 0.00 3.20 o -2 -7 2 31.61 27.58 4.00 o -1 -7 2 6.49 10.60 2.38 o 0 -7 2 200.92 189.23 7.20 o 1 -7 2 331.25 330.61 20.88 o 2 -7 2 298.50 289.90 10.38 o 3 -7 2 32.83 41.61 2.77 o 4 -7 2 105.69 112.13 8.59 o 5 -7 2 0.09 0.81 3.78 o 6 -7 2 21.44 24.68 3.40 o -4 -6 2 598.17 548.95 18.68 o -3 -6 2 1216.65 1190.22 34.42 o -2 -6 2 2313.12 2461.10 65.88 o -1 -6 2 1365.25 1550.72 42.33 o 0 -6 2 330.21 322.52 10.96 o 1 -6 2 838.98 881.77 31.54 o 2 -6 2 4756.81 4753.98 85.47 o 3 -6 2 2161.65 2204.01 40.59 o 4 -6 2 985.58 1073.05 29.81 o 5 -6 2 1489.69 1608.21 30.64 o 6 -6 2 762.58 803.58 16.73 o -4 -5 2 86.08 83.03 6.07 o -3 -5 2 0.09 2.17 2.10 o -2 -5 2 615.87 629.68 19.15 o -1 -5 2 0.25 0.00 1.58 o 0 -5 2 630.50 536.97 15.99 o 1 -5 2 218.59 227.63 12.35 o 2 -5 2 145.67 167.16 7.94 o 3 -5 2 1.65 2.39 0.98 o 4 -5 2 7.08 10.30 1.32 o 5 -5 2 2.75 8.21 1.42 o 6 -5 2 58.36 55.74 4.49 o 7 -5 2 86.48 88.43 7.41 o -5 -4 2 656.78 736.03 22.39 o -4 -4 2 742.11 766.31 22.56 o -3 -4 2 1217.47 1168.27 32.38 o -2 -4 2 3630.29 4168.58 107.36 o -1 -4 2 3707.29 3597.42 92.62 o 0 -4 2 3913.12 3695.26 94.77 o 1 -4 2 6331.12 6575.20 117.19 o 2 -4 2 3713.76 3816.84 68.54 o 3 -4 2 2060.27 2286.10 41.80 o 4 -4 2 3691.71 4049.57 73.31 o 5 -4 2 2140.71 2243.79 45.99 o 6 -4 2 544.47 545.98 17.14 o 7 -4 2 881.15 914.23 19.55 o -6 -3 2 17.36 18.60 2.22 o -5 -3 2 23.46 29.41 2.35 o -4 -3 2 52.62 56.93 5.80 o -3 -3 2 100.37 108.37 3.03 o -2 -3 2 33.43 22.68 2.09 o -1 -3 2 62.21 52.13 2.49 o 0 -3 2 201.07 224.36 9.90 o 1 -3 2 187.70 164.59 6.52 o 2 -3 2 17.35 33.13 4.47 o 3 -3 2 321.44 327.10 14.84 o 4 -3 2 8.33 9.36 1.29 o 5 -3 2 13.79 12.01 1.59 o 6 -3 2 3.97 3.51 1.39 o 7 -3 2 9.05 3.25 1.61 o -6 -2 2 973.11 1005.87 20.44 o -5 -2 2 1338.56 1330.58 25.72 o -4 -2 2 1988.98 2044.97 47.97 o -3 -2 2 3806.85 4068.85 62.59 o -2 -2 2 9072.21 8996.71 136.70 o -1 -2 2 1245.06 1229.37 32.99 o 0 -2 2 3777.60 3641.40 105.98 o 1 -2 2 16675.44 12884.78 372.48 o 2 -2 2 4587.48 4526.55 80.91 o 3 -2 2 4365.47 4492.73 80.72 o 4 -2 2 2655.02 2717.68 49.73 o 5 -2 2 1338.64 1472.80 28.21 o 6 -2 2 743.97 741.52 15.57 o 7 -2 2 429.32 409.95 9.97 o -7 -1 2 3.75 6.03 2.45 o -6 -1 2 2.39 2.43 1.31 o -5 -1 2 61.99 56.13 3.27 o -4 -1 2 83.59 96.33 2.77 o -3 -1 2 6.25 4.66 0.77 o -2 -1 2 291.18 294.99 10.03 o -1 -1 2 103.32 105.61 5.79 o 0 -1 2 9.49 8.25 0.90 o 1 -1 2 0.72 0.31 1.89 o 2 -1 2 1070.36 1128.60 17.70 o 3 -1 2 14.22 14.26 3.55 o 4 -1 2 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