#------------------------------------------------------------------------------ #$Date: 2016-04-03 01:50:10 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181104 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/84/2218470.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2218470_Fobs loop_ _publ_author_name 'Sim, Yoke Leng' 'Ariffin, Azhar' 'Ng, Seik Weng' _publ_section_title ; N-(2-Methoxyethyl)phthalimide ; _journal_coeditor_code LH2624 _journal_issue 6 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o1058 _journal_volume 64 _journal_year 2008 _space_group_IT_number 62 _symmetry_space_group_name_Hall '-P 2ac 2n' _symmetry_space_group_name_H-M 'P n m a' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 7.0514 _cell_length_b 9.3852 _cell_length_c 14.6024 _exptl_crystal_F_000 432.00 _reflns_d_resolution_high 0.7696 _cod_data_source_file lh2624Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' Pnma' _shelx_refln_list_code 4 _shelx_f_calc_maximum 195.03 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z' 'x+1/2, -y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, y, -z-1/2' 'x, -y-1/2, z' '-x-1/2, y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 38038.09 41219.03 634.19 o 4 0 0 3840.47 4354.62 139.81 o 6 0 0 0.66 -0.16 4.94 o 8 0 0 6.98 13.08 5.56 o 2 1 0 664.06 695.36 7.09 o 4 1 0 1455.79 1755.13 34.80 o 0 2 0 9232.40 8733.91 139.96 o 2 2 0 4.44 9.34 0.97 o 4 2 0 6.30 1.88 1.56 o 8 2 0 13.99 9.45 4.11 o 2 3 0 740.90 721.02 8.30 o 4 3 0 165.52 177.18 4.38 o 6 3 0 10.84 6.15 7.57 o 8 3 0 7.60 1.12 4.94 o 0 4 0 2488.44 2329.24 33.94 o 2 4 0 0.13 -0.24 0.44 o 4 4 0 333.81 377.01 5.51 o 6 4 0 921.40 1057.13 33.14 o 8 4 0 54.58 62.39 9.52 o 2 5 0 393.45 422.35 5.93 o 4 5 0 97.83 112.62 2.87 o 6 5 0 18.52 38.91 6.53 o 8 5 0 32.05 31.51 8.13 o 0 6 0 11.72 20.32 3.90 o 2 6 0 462.17 467.07 6.39 o 4 6 0 298.31 319.03 5.56 o 6 6 0 386.84 438.52 19.20 o 2 7 0 63.71 67.25 3.64 o 4 7 0 0.18 1.78 1.08 o 6 7 0 21.56 25.84 9.04 o 0 8 0 2199.99 2205.00 43.97 o 2 8 0 305.70 342.80 7.99 o 4 8 0 10.85 8.89 1.72 o 6 8 0 445.70 501.51 21.99 o 2 9 0 0.93 0.94 1.47 o 4 9 0 21.54 23.99 3.69 o 6 9 0 31.75 48.86 8.55 o 0 10 0 7.77 13.71 3.43 o 2 10 0 154.54 114.06 9.97 o 4 10 0 122.72 109.23 6.89 o 2 11 0 43.73 33.46 3.55 o 0 12 0 1072.53 1146.33 29.98 o 1 0 1 55.84 61.25 1.18 o 2 0 1 6769.81 7260.33 85.61 o 3 0 1 1426.15 1554.32 23.29 o 4 0 1 4907.65 5779.74 162.86 o 5 0 1 732.59 585.14 28.79 o 6 0 1 1543.98 343.66 22.28 o 7 0 1 191.33 68.50 11.76 o 8 0 1 398.02 8.90 3.37 o 9 0 1 1.15 13.32 4.07 o 0 1 1 2986.86 2819.43 55.25 o 1 1 1 3017.19 2937.63 21.57 o 2 1 1 8960.23 9429.47 122.30 o 3 1 1 137.14 132.09 2.11 o 4 1 1 1319.64 1498.93 20.32 o 7 1 1 232.97 194.31 17.88 o 8 1 1 1.34 4.39 2.30 o 9 1 1 55.14 13.54 2.79 o 1 2 1 400.21 389.43 4.06 o 2 2 1 228.40 250.30 2.57 o 3 2 1 221.99 232.54 2.51 o 4 2 1 39.60 49.47 1.33 o 5 2 1 22.49 31.25 1.62 o 6 2 1 0.24 -0.85 1.76 o 7 2 1 2.42 1.28 2.24 o 8 2 1 0.91 0.38 2.59 o 9 2 1 6.44 10.94 3.13 o 0 3 1 5985.21 5584.06 55.13 o 1 3 1 1727.92 1763.43 12.86 o 2 3 1 403.21 411.49 3.85 o 3 3 1 4.55 6.39 0.55 o 4 3 1 137.16 158.47 2.15 o 5 3 1 127.36 138.37 3.04 o 6 3 1 51.64 30.66 13.62 o 7 3 1 25.18 27.74 6.58 o 8 3 1 4.62 4.30 2.91 o 1 4 1 5.27 7.55 0.49 o 2 4 1 329.34 313.58 3.81 o 3 4 1 200.49 198.93 2.62 o 4 4 1 24.58 17.64 0.90 o 5 4 1 259.30 274.41 4.59 o 6 4 1 42.98 47.63 4.90 o 7 4 1 105.80 122.47 20.75 o 8 4 1 115.92 125.49 18.28 o 0 5 1 2546.67 2564.26 32.62 o 1 5 1 1316.36 1351.75 10.57 o 2 5 1 403.73 457.35 4.26 o 3 5 1 100.47 106.75 2.00 o 4 5 1 179.20 196.94 2.86 o 5 5 1 50.16 47.83 2.14 o 6 5 1 18.14 22.75 3.97 o 7 5 1 10.11 9.11 3.60 o 8 5 1 8.49 17.03 4.83 o 1 6 1 76.90 72.08 1.39 o 2 6 1 7.33 7.87 0.69 o 3 6 1 109.58 110.29 2.23 o 4 6 1 38.36 47.36 1.60 o 5 6 1 5.55 8.56 1.36 o 6 6 1 82.80 92.40 10.95 o 7 6 1 3.49 3.65 3.14 o 0 7 1 412.30 369.47 6.62 o 1 7 1 620.00 573.24 5.96 o 2 7 1 5.03 6.76 0.95 o 3 7 1 50.26 49.91 1.91 o 4 7 1 13.58 12.38 1.13 o 5 7 1 30.58 34.98 2.23 o 6 7 1 29.76 42.50 5.13 o 7 7 1 13.13 18.81 4.57 o 1 8 1 17.93 17.90 1.57 o 2 8 1 248.35 245.74 4.28 o 3 8 1 259.84 264.27 4.53 o 4 8 1 177.77 184.97 3.57 o 5 8 1 355.30 427.61 7.92 o 6 8 1 21.68 26.85 3.72 o 0 9 1 267.94 214.56 6.50 o 1 9 1 906.71 817.98 11.26 o 2 9 1 8.22 5.22 1.23 o 3 9 1 132.99 126.80 3.94 o 4 9 1 39.70 38.44 2.78 o 5 9 1 4.19 4.95 1.75 o 6 9 1 0.01 -0.19 2.38 o 1 10 1 14.67 11.98 1.81 o 2 10 1 0.30 2.59 1.21 o 3 10 1 5.10 7.21 1.47 o 4 10 1 10.88 9.94 2.20 o 5 10 1 1.50 0.09 1.69 o 0 11 1 182.52 150.63 6.14 o 1 11 1 20.61 20.38 2.08 o 2 11 1 2.45 1.57 1.31 o 3 11 1 12.71 13.93 1.92 o 1 12 1 0.83 0.54 1.39 o 0 0 2 1118.39 1082.01 27.44 o 1 0 2 30.89 41.32 2.07 o 2 0 2 64.02 82.15 3.54 o 3 0 2 160.93 175.05 4.06 o 4 0 2 968.49 1091.01 20.30 o 5 0 2 3.80 4.59 3.88 o 6 0 2 44.23 58.16 10.72 o 7 0 2 209.01 133.57 14.75 o 8 0 2 33.99 6.10 3.10 o 9 0 2 258.40 9.58 3.44 o 1 1 2 1623.72 1590.75 14.67 o 2 1 2 16.86 16.86 0.73 o 3 1 2 1042.57 1170.84 10.67 o 4 1 2 31.27 25.89 1.03 o 5 1 2 248.86 307.87 6.86 o 6 1 2 9.02 8.67 4.97 o 7 1 2 1.37 2.27 2.09 o 9 1 2 2.52 11.43 2.74 o 0 2 2 38.31 50.41 1.45 o 1 2 2 4337.88 4280.95 54.81 o 2 2 2 168.52 143.14 1.82 o 3 2 2 142.36 166.75 4.33 o 4 2 2 205.76 222.22 3.53 o 5 2 2 84.42 83.23 2.36 o 6 2 2 8.99 2.20 3.24 o 7 2 2 23.80 27.34 6.54 o 8 2 2 0.51 2.12 2.46 o 1 3 2 400.50 396.06 3.82 o 2 3 2 322.30 340.60 3.72 o 3 3 2 229.54 236.48 2.80 o 4 3 2 349.86 369.46 4.39 o 5 3 2 27.66 26.09 1.81 o 6 3 2 159.70 46.69 9.34 o 7 3 2 19.45 8.70 4.75 o 8 3 2 2.09 2.96 3.18 o 0 4 2 1037.64 1149.72 14.17 o 1 4 2 303.04 346.71 3.78 o 2 4 2 1544.50 1612.11 13.42 o 3 4 2 477.39 511.12 5.03 o 4 4 2 0.53 4.52 0.64 o 5 4 2 250.08 277.64 4.82 o 6 4 2 13.07 13.62 2.97 o 7 4 2 23.48 24.38 4.39 o 8 4 2 12.59 11.94 4.33 o 1 5 2 180.07 172.61 2.64 o 2 5 2 270.83 294.45 3.56 o 3 5 2 192.62 181.56 2.78 o 4 5 2 322.75 345.61 4.11 o 5 5 2 22.01 20.09 1.59 o 6 5 2 215.95 266.82 8.80 o 7 5 2 26.88 44.57 5.46 o 8 5 2 8.55 11.68 4.49 o 0 6 2 2.38 0.71 0.82 o 1 6 2 802.75 775.14 7.78 o 2 6 2 102.76 118.97 2.30 o 3 6 2 16.99 16.45 1.20 o 4 6 2 64.37 64.71 1.84 o 5 6 2 111.28 119.87 3.43 o 6 6 2 0.03 -0.03 2.12 o 7 6 2 65.97 79.59 7.11 o 1 7 2 110.66 102.36 2.29 o 2 7 2 62.18 61.09 1.90 o 3 7 2 150.83 151.25 3.33 o 4 7 2 98.33 101.59 2.38 o 5 7 2 49.44 60.17 2.71 o 6 7 2 70.90 80.89 6.95 o 7 7 2 3.11 2.26 3.34 o 0 8 2 157.52 150.11 5.04 o 1 8 2 608.24 492.32 6.95 o 2 8 2 281.73 263.90 4.51 o 3 8 2 485.18 471.55 6.49 o 4 8 2 4.81 4.95 1.13 o 5 8 2 144.40 156.07 4.23 o 6 8 2 0.60 1.29 1.97 o 1 9 2 151.47 132.07 3.58 o 2 9 2 73.05 74.12 3.69 o 3 9 2 343.33 350.36 6.10 o 4 9 2 162.59 169.60 4.83 o 5 9 2 252.40 304.65 6.31 o 6 9 2 116.57 140.56 7.55 o 0 10 2 56.52 53.00 4.40 o 1 10 2 39.77 50.64 2.68 o 2 10 2 130.30 112.31 5.23 o 3 10 2 18.31 14.52 1.77 o 4 10 2 0.06 0.71 1.60 o 5 10 2 86.85 85.87 4.55 o 1 11 2 14.05 15.32 1.90 o 2 11 2 7.70 6.16 1.55 o 3 11 2 0.66 1.99 1.36 o 0 12 2 3.18 3.02 2.27 o 1 12 2 61.36 63.99 3.43 o 1 0 3 471.54 433.58 24.75 o 2 0 3 2138.24 2175.38 33.88 o 3 0 3 53.93 47.23 2.11 o 4 0 3 843.19 980.08 22.46 o 5 0 3 26.09 19.49 4.91 o 7 0 3 38.52 45.78 10.96 o 8 0 3 4.93 6.71 3.14 o 9 0 3 12.75 10.63 3.45 o 0 1 3 445.64 409.45 6.10 o 1 1 3 0.71 1.06 0.48 o 2 1 3 33.74 32.07 1.82 o 3 1 3 18.77 21.08 0.83 o 4 1 3 570.52 621.18 9.47 o 5 1 3 77.01 99.54 3.73 o 6 1 3 0.02 -1.76 1.38 o 7 1 3 65.72 4.23 4.34 o 8 1 3 0.00 4.00 3.61 o 9 1 3 26.31 13.56 2.83 o 1 2 3 747.04 723.43 6.10 o 2 2 3 20.00 20.99 0.93 o 3 2 3 570.31 583.66 6.14 o 4 2 3 189.62 193.98 2.90 o 5 2 3 264.77 287.46 5.09 o 7 2 3 13.35 5.40 3.96 o 8 2 3 9.24 6.57 2.60 o 0 3 3 11.33 14.06 0.84 o 1 3 3 81.10 83.27 1.31 o 2 3 3 52.09 40.73 1.42 o 3 3 3 46.53 45.27 1.27 o 4 3 3 316.56 332.76 4.41 o 5 3 3 13.43 17.81 1.46 o 6 3 3 3.79 3.84 1.97 o 7 3 3 8.65 6.66 2.77 o 8 3 3 4.30 1.55 2.93 o 1 4 3 224.22 225.93 3.07 o 2 4 3 688.09 700.35 6.55 o 3 4 3 195.38 213.16 2.83 o 4 4 3 489.05 563.36 5.87 o 5 4 3 180.40 206.44 4.47 o 6 4 3 40.11 47.87 4.33 o 7 4 3 9.07 8.33 3.88 o 8 4 3 19.77 26.34 5.11 o 0 5 3 33.84 47.83 2.07 o 1 5 3 20.33 23.56 1.63 o 2 5 3 37.07 25.41 1.11 o 3 5 3 46.12 54.33 1.58 o 4 5 3 97.72 100.27 2.18 o 5 5 3 1.94 1.75 1.11 o 6 5 3 16.19 27.78 3.46 o 7 5 3 0.45 -0.20 3.08 o 8 5 3 14.96 21.96 5.07 o 1 6 3 222.47 215.61 3.31 o 2 6 3 0.96 0.45 0.61 o 3 6 3 426.45 435.58 4.91 o 4 6 3 15.58 16.65 1.09 o 5 6 3 459.28 515.85 7.65 o 6 6 3 52.60 75.16 4.96 o 7 6 3 25.35 32.14 4.97 o 0 7 3 2.84 0.53 0.96 o 1 7 3 5.08 9.91 1.01 o 2 7 3 30.33 32.34 1.52 o 3 7 3 24.45 33.37 1.51 o 4 7 3 44.51 43.95 1.74 o 5 7 3 14.53 16.27 1.75 o 6 7 3 29.90 43.78 3.51 o 7 7 3 11.12 13.06 4.28 o 1 8 3 20.92 20.23 1.51 o 2 8 3 412.45 379.28 5.66 o 3 8 3 0.23 -0.85 0.84 o 4 8 3 485.16 516.53 7.49 o 5 8 3 5.20 5.11 1.49 o 6 8 3 156.29 196.32 5.95 o 0 9 3 301.75 257.52 8.57 o 1 9 3 206.72 169.80 4.11 o 2 9 3 108.37 95.14 5.50 o 3 9 3 109.12 90.45 3.05 o 4 9 3 188.60 198.70 4.52 o 5 9 3 21.84 24.04 2.41 o 6 9 3 1.36 3.23 2.31 o 1 10 3 35.82 37.11 2.43 o 2 10 3 2.32 1.88 1.18 o 3 10 3 24.77 26.41 2.11 o 4 10 3 0.81 3.04 1.76 o 5 10 3 23.57 28.46 3.10 o 0 11 3 17.49 14.74 2.70 o 1 11 3 2.96 1.94 1.33 o 2 11 3 27.18 21.50 2.16 o 3 11 3 0.01 0.55 1.28 o 0 0 4 4310.03 4271.03 104.00 o 1 0 4 1112.01 1172.30 20.24 o 2 0 4 4765.14 4991.07 75.52 o 3 0 4 1054.93 1115.61 20.63 o 4 0 4 115.75 123.62 6.13 o 5 0 4 0.02 -0.14 1.10 o 6 0 4 4.19 2.26 2.73 o 7 0 4 65.65 64.82 12.19 o 8 0 4 22.75 5.41 4.12 o 1 1 4 121.10 112.32 2.11 o 2 1 4 170.33 172.59 3.11 o 3 1 4 0.61 0.43 0.63 o 4 1 4 28.05 26.00 0.99 o 5 1 4 101.79 115.81 3.55 o 6 1 4 20.27 22.67 8.47 o 7 1 4 1.65 3.64 2.03 o 8 1 4 24.38 10.65 3.97 o 0 2 4 1647.62 1611.66 18.61 o 1 2 4 1602.85 1598.10 12.51 o 2 2 4 56.49 56.51 1.35 o 3 2 4 131.47 140.01 2.28 o 4 2 4 78.35 98.57 1.97 o 5 2 4 80.84 91.13 3.37 o 6 2 4 55.97 71.54 5.49 o 7 2 4 64.05 31.60 13.95 o 8 2 4 23.50 9.92 3.66 o 1 3 4 82.30 79.12 1.51 o 2 3 4 516.27 514.98 5.20 o 3 3 4 8.19 6.65 0.81 o 4 3 4 406.72 452.34 5.61 o 5 3 4 232.14 237.93 4.66 o 6 3 4 41.15 47.19 4.35 o 7 3 4 10.64 9.66 2.53 o 8 3 4 0.00 2.63 2.94 o 0 4 4 116.68 127.56 2.55 o 1 4 4 869.19 846.18 7.77 o 2 4 4 231.18 217.09 2.95 o 3 4 4 184.59 186.36 3.14 o 4 4 4 39.02 51.37 1.75 o 5 4 4 0.13 0.90 1.00 o 6 4 4 0.02 -0.12 1.72 o 7 4 4 101.72 152.16 7.41 o 8 4 4 8.87 7.96 3.84 o 1 5 4 0.13 0.96 0.60 o 2 5 4 112.77 107.99 2.03 o 3 5 4 142.47 164.95 3.02 o 4 5 4 114.01 135.77 2.72 o 5 5 4 0.09 -0.22 1.04 o 6 5 4 2.77 2.40 2.16 o 7 5 4 75.01 96.27 5.92 o 8 5 4 4.94 5.65 4.20 o 0 6 4 417.93 391.21 6.98 o 1 6 4 467.91 413.40 5.12 o 2 6 4 97.92 106.62 2.28 o 3 6 4 307.25 290.86 3.85 o 4 6 4 130.98 151.82 2.81 o 5 6 4 178.45 188.05 4.57 o 6 6 4 0.35 -1.37 1.61 o 7 6 4 8.48 8.85 3.01 o 1 7 4 0.24 0.90 0.74 o 2 7 4 7.09 8.40 1.05 o 3 7 4 85.03 91.25 2.25 o 4 7 4 0.01 -0.41 0.84 o 5 7 4 4.15 4.76 1.47 o 6 7 4 41.31 51.14 3.78 o 7 7 4 113.14 147.40 13.93 o 0 8 4 610.48 532.70 9.34 o 1 8 4 540.98 484.11 6.20 o 2 8 4 553.83 497.33 6.83 o 3 8 4 299.59 281.35 4.67 o 4 8 4 5.88 4.99 1.27 o 5 8 4 51.35 54.21 2.86 o 6 8 4 5.93 8.42 2.54 o 1 9 4 3.02 3.58 1.20 o 2 9 4 2.87 1.75 1.14 o 3 9 4 13.81 14.31 1.75 o 4 9 4 27.60 31.53 2.25 o 5 9 4 15.30 21.41 2.32 o 0 10 4 66.87 61.79 5.11 o 1 10 4 119.20 114.98 7.01 o 2 10 4 1.50 2.24 1.23 o 3 10 4 28.23 37.39 2.98 o 4 10 4 11.01 14.38 2.56 o 1 11 4 9.47 10.15 1.74 o 2 11 4 76.28 78.22 4.19 o 3 11 4 1.21 0.08 1.36 o 1 0 5 756.62 727.86 11.36 o 2 0 5 166.53 172.07 4.63 o 3 0 5 520.63 519.21 10.40 o 4 0 5 300.07 327.75 7.62 o 5 0 5 915.70 1095.82 19.98 o 6 0 5 37.43 58.11 5.73 o 7 0 5 94.60 130.68 16.26 o 8 0 5 2.96 4.59 3.23 o 0 1 5 129.98 109.55 4.19 o 1 1 5 103.47 113.61 2.44 o 2 1 5 346.78 372.04 5.76 o 3 1 5 120.95 138.70 3.50 o 4 1 5 1.77 0.58 0.62 o 5 1 5 8.37 12.22 1.46 o 6 1 5 2.38 2.87 1.48 o 7 1 5 0.71 3.24 1.83 o 8 1 5 35.09 16.81 10.55 o 1 2 5 61.72 60.66 1.66 o 2 2 5 0.54 0.06 0.47 o 3 2 5 1317.09 1380.97 13.35 o 4 2 5 8.32 6.54 0.80 o 5 2 5 198.79 233.71 4.89 o 6 2 5 6.67 6.81 2.02 o 7 2 5 167.67 92.47 13.90 o 8 2 5 44.04 30.68 13.39 o 0 3 5 534.75 509.97 7.59 o 1 3 5 1415.75 1422.48 11.93 o 2 3 5 913.22 929.72 8.15 o 3 3 5 567.06 622.44 7.09 o 4 3 5 55.67 56.16 2.59 o 5 3 5 64.71 85.24 3.08 o 6 3 5 0.11 0.09 1.79 o 7 3 5 0.23 1.44 2.09 o 8 3 5 61.10 80.37 25.64 o 1 4 5 129.95 127.10 2.21 o 2 4 5 10.61 16.28 0.89 o 3 4 5 47.85 41.13 2.04 o 4 4 5 1.18 4.20 0.88 o 5 4 5 234.39 259.39 5.24 o 6 4 5 13.92 31.71 3.87 o 7 4 5 2.90 2.14 2.28 o 8 4 5 52.42 68.10 11.59 o 0 5 5 110.78 125.84 3.71 o 1 5 5 307.08 288.37 3.97 o 2 5 5 167.68 171.91 2.87 o 3 5 5 184.76 181.96 3.10 o 4 5 5 0.66 0.83 0.75 o 5 5 5 107.57 107.08 4.23 o 6 5 5 1.20 3.01 2.32 o 7 5 5 80.39 110.21 6.35 o 8 5 5 51.08 75.76 7.54 o 1 6 5 1.62 2.14 0.77 o 2 6 5 19.92 19.40 1.24 o 3 6 5 44.49 48.92 2.11 o 4 6 5 89.47 84.49 2.85 o 5 6 5 85.74 86.79 4.30 o 6 6 5 55.83 61.69 3.89 o 7 6 5 51.82 74.71 5.52 o 0 7 5 179.17 153.85 4.35 o 1 7 5 898.21 776.39 8.45 o 2 7 5 37.55 37.35 1.73 o 3 7 5 613.79 588.60 6.95 o 4 7 5 48.32 51.70 2.33 o 5 7 5 337.58 350.18 6.36 o 6 7 5 3.08 5.06 2.23 o 7 7 5 152.54 198.53 8.22 o 1 8 5 136.34 121.39 2.91 o 2 8 5 76.12 63.39 2.27 o 3 8 5 261.97 240.39 4.36 o 4 8 5 223.04 221.86 4.51 o 5 8 5 675.88 773.18 12.81 o 6 8 5 140.60 161.93 6.72 o 0 9 5 40.89 39.62 3.36 o 1 9 5 109.68 78.37 3.07 o 2 9 5 0.36 0.52 1.01 o 3 9 5 40.65 35.94 2.13 o 4 9 5 2.72 3.04 1.37 o 5 9 5 11.23 7.71 2.15 o 1 10 5 2.37 4.16 1.35 o 2 10 5 0.00 -0.70 1.11 o 3 10 5 153.84 166.83 4.77 o 4 10 5 3.56 3.74 1.97 o 0 11 5 44.32 39.30 3.92 o 1 11 5 209.87 225.73 5.49 o 2 11 5 111.68 102.65 5.00 o 3 11 5 116.72 119.44 4.24 o 0 0 6 2010.98 1943.22 50.67 o 1 0 6 2006.67 1956.72 27.86 o 2 0 6 536.72 509.49 10.80 o 3 0 6 80.43 89.35 3.64 o 4 0 6 278.66 303.40 7.56 o 5 0 6 49.54 49.78 4.93 o 6 0 6 61.01 66.76 6.07 o 7 0 6 76.16 101.45 19.91 o 8 0 6 24.62 11.82 4.22 o 1 1 6 128.75 125.50 2.28 o 2 1 6 74.80 81.20 2.37 o 3 1 6 210.43 217.27 4.43 o 4 1 6 338.75 379.69 5.76 o 5 1 6 0.17 -1.34 0.89 o 6 1 6 158.86 150.98 34.73 o 7 1 6 10.59 10.16 4.39 o 8 1 6 27.44 13.67 4.52 o 0 2 6 5.63 1.48 0.96 o 1 2 6 1891.52 1913.76 20.67 o 2 2 6 37.43 34.91 1.81 o 3 2 6 1054.65 1101.66 13.74 o 4 2 6 129.65 146.15 4.44 o 5 2 6 234.21 260.32 5.40 o 6 2 6 194.72 215.58 7.16 o 7 2 6 12.57 8.44 2.14 o 8 2 6 135.81 158.47 19.74 o 1 3 6 239.43 233.59 3.00 o 2 3 6 91.80 95.93 1.92 o 3 3 6 42.38 46.50 1.79 o 4 3 6 295.78 325.15 4.45 o 5 3 6 243.40 308.40 4.85 o 6 3 6 190.20 219.14 8.11 o 7 3 6 51.05 72.73 6.31 o 8 3 6 42.38 59.06 13.35 o 0 4 6 828.75 833.81 16.32 o 1 4 6 3.68 1.90 0.72 o 2 4 6 231.78 256.46 3.32 o 3 4 6 28.03 29.67 1.68 o 4 4 6 105.44 117.89 2.67 o 5 4 6 57.63 54.87 2.61 o 6 4 6 14.81 9.65 2.43 o 7 4 6 5.95 1.99 3.20 o 8 4 6 4.73 6.44 2.84 o 1 5 6 26.58 27.58 1.52 o 2 5 6 24.50 26.56 1.39 o 3 5 6 40.24 40.26 1.67 o 4 5 6 66.26 70.58 2.21 o 5 5 6 0.14 0.05 1.11 o 6 5 6 25.87 30.07 2.98 o 7 5 6 36.41 46.67 4.69 o 0 6 6 1366.52 1220.10 18.44 o 1 6 6 305.48 271.49 4.59 o 2 6 6 1161.36 1075.82 11.39 o 3 6 6 199.24 192.79 3.57 o 4 6 6 202.78 220.42 4.25 o 5 6 6 108.23 137.20 3.77 o 6 6 6 5.53 5.07 1.92 o 7 6 6 75.47 95.59 6.11 o 1 7 6 0.28 -0.15 0.80 o 2 7 6 33.23 34.65 1.76 o 3 7 6 318.28 321.02 5.01 o 4 7 6 35.18 41.03 2.07 o 5 7 6 221.54 236.28 5.40 o 6 7 6 39.91 52.64 4.25 o 0 8 6 12.67 14.63 2.46 o 1 8 6 1470.17 1276.55 13.52 o 2 8 6 67.58 65.04 2.50 o 3 8 6 523.16 485.26 7.85 o 4 8 6 24.37 25.60 2.14 o 5 8 6 60.62 69.56 3.69 o 6 8 6 8.75 6.76 3.02 o 1 9 6 1.68 1.42 1.09 o 2 9 6 5.05 4.63 1.28 o 3 9 6 127.98 119.86 4.77 o 4 9 6 35.45 33.50 2.63 o 5 9 6 44.60 50.51 3.85 o 0 10 6 2.40 2.23 1.90 o 1 10 6 89.02 96.30 3.66 o 2 10 6 9.31 9.52 1.70 o 3 10 6 89.19 91.11 3.83 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53.07 1.66 o 3 4 7 439.84 457.49 5.30 o 4 4 7 100.82 101.24 2.46 o 5 4 7 230.74 265.57 5.56 o 6 4 7 75.07 85.29 5.78 o 7 4 7 264.34 362.38 13.33 o 0 5 7 2.46 1.60 1.50 o 1 5 7 33.91 30.23 1.41 o 2 5 7 6.13 3.58 0.85 o 3 5 7 0.14 -0.33 0.79 o 4 5 7 198.26 204.22 4.14 o 5 5 7 0.41 0.39 1.15 o 6 5 7 196.02 208.12 6.39 o 7 5 7 1.73 0.88 2.84 o 1 6 7 78.49 75.53 2.55 o 2 6 7 340.22 313.90 5.14 o 3 6 7 4.77 4.77 1.09 o 4 6 7 474.20 504.26 7.43 o 5 6 7 51.07 63.69 2.97 o 6 6 7 247.90 313.31 7.90 o 7 6 7 0.57 0.77 2.49 o 0 7 7 295.21 257.38 6.78 o 1 7 7 462.25 423.81 6.85 o 2 7 7 281.65 254.80 4.80 o 3 7 7 322.83 322.55 5.57 o 4 7 7 463.11 456.51 7.30 o 5 7 7 56.96 58.05 3.98 o 6 7 7 316.70 356.46 10.74 o 1 8 7 68.55 59.14 2.60 o 2 8 7 20.63 14.24 1.61 o 3 8 7 8.13 7.44 1.44 o 4 8 7 34.65 38.96 2.65 o 5 8 7 56.24 58.78 3.91 o 6 8 7 15.60 26.82 4.12 o 0 9 7 236.08 206.10 6.54 o 1 9 7 8.61 7.09 1.63 o 2 9 7 105.16 95.28 3.65 o 3 9 7 16.15 15.50 1.95 o 4 9 7 2.51 2.56 1.56 o 5 9 7 0.03 -0.24 1.92 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3 8 2.92 3.76 2.69 o 0 4 8 158.73 148.60 4.81 o 1 4 8 2060.49 1930.44 19.85 o 2 4 8 27.55 24.89 1.30 o 3 4 8 437.00 428.31 5.18 o 4 4 8 15.24 18.21 1.41 o 5 4 8 21.97 18.47 2.25 o 6 4 8 17.19 16.46 2.68 o 7 4 8 133.25 172.22 9.10 o 1 5 8 50.43 47.96 1.89 o 2 5 8 2.41 3.50 1.03 o 3 5 8 2.49 1.84 1.00 o 4 5 8 58.95 65.26 2.60 o 5 5 8 56.28 59.32 2.82 o 6 5 8 228.12 281.28 7.39 o 7 5 8 0.83 -0.83 2.65 o 0 6 8 1677.30 1473.28 22.14 o 1 6 8 13.62 15.13 1.52 o 2 6 8 986.16 893.47 10.73 o 3 6 8 9.31 11.84 1.58 o 4 6 8 210.62 217.69 4.85 o 5 6 8 37.41 41.62 2.76 o 6 6 8 41.12 51.26 3.97 o 1 7 8 3.96 2.99 1.13 o 2 7 8 13.88 11.95 1.54 o 3 7 8 112.99 116.53 3.65 o 4 7 8 10.24 11.74 1.81 o 5 7 8 11.29 14.55 2.15 o 6 7 8 124.91 153.12 6.37 o 0 8 8 43.67 40.71 3.28 o 1 8 8 317.77 265.33 5.23 o 2 8 8 11.03 11.06 1.56 o 3 8 8 56.50 52.84 2.63 o 4 8 8 3.07 2.91 1.44 o 5 8 8 18.07 19.98 2.77 o 1 9 8 26.00 27.47 2.36 o 2 9 8 80.28 76.27 4.77 o 3 9 8 2.20 3.80 1.50 o 4 9 8 51.27 56.99 4.31 o 0 10 8 4.45 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4 9 3.58 3.88 1.70 o 6 4 9 104.46 120.66 6.22 o 7 4 9 2.32 1.74 3.30 o 0 5 9 578.56 526.76 10.39 o 1 5 9 146.14 127.52 2.97 o 2 5 9 535.55 524.69 7.28 o 3 5 9 0.62 -0.30 1.01 o 4 5 9 61.77 67.21 2.88 o 5 5 9 62.02 72.78 6.47 o 6 5 9 9.99 13.16 2.65 o 7 5 9 20.24 24.86 4.15 o 1 6 9 8.60 4.81 1.19 o 2 6 9 92.00 83.40 3.84 o 3 6 9 17.18 15.88 1.79 o 4 6 9 88.00 82.72 3.42 o 5 6 9 143.15 169.37 4.91 o 6 6 9 33.33 35.96 3.87 o 0 7 9 100.68 72.98 4.03 o 1 7 9 38.11 38.80 2.26 o 2 7 9 160.11 139.00 3.70 o 3 7 9 9.00 6.85 1.52 o 4 7 9 43.46 45.74 2.86 o 5 7 9 85.60 89.41 4.16 o 6 7 9 3.44 3.78 2.52 o 1 8 9 24.44 21.76 1.96 o 2 8 9 68.04 60.64 2.94 o 3 8 9 382.63 362.04 6.97 o 4 8 9 48.47 44.06 2.95 o 5 8 9 24.43 27.62 3.16 o 0 9 9 9.79 12.43 2.52 o 1 9 9 5.98 8.33 1.62 o 2 9 9 0.53 2.28 1.63 o 3 9 9 10.73 10.20 1.89 o 4 9 9 17.95 20.37 2.70 o 1 10 9 2.76 2.47 1.72 o 2 10 9 2.75 3.92 1.80 o 0 0 10 1280.99 1120.87 34.13 o 1 0 10 823.48 736.25 14.65 o 2 0 10 754.67 712.52 16.76 o 3 0 10 137.97 127.42 4.11 o 4 0 10 607.79 638.59 12.59 o 5 0 10 3.70 2.87 2.39 o 6 0 10 74.75 88.98 6.40 o 7 0 10 4.40 3.66 3.48 o 1 1 10 25.28 33.85 2.04 o 2 1 10 184.78 196.02 4.13 o 3 1 10 317.36 313.94 5.08 o 4 1 10 83.13 95.45 2.84 o 5 1 10 49.73 59.10 4.58 o 6 1 10 8.91 12.15 3.40 o 7 1 10 80.00 82.06 5.44 o 0 2 10 707.12 658.99 13.44 o 1 2 10 15.43 20.11 1.72 o 2 2 10 428.71 411.38 6.58 o 3 2 10 74.67 80.94 2.91 o 4 2 10 9.80 7.04 1.18 o 5 2 10 29.54 36.36 2.89 o 6 2 10 21.09 21.19 3.23 o 7 2 10 7.53 13.58 2.57 o 1 3 10 126.12 119.66 3.41 o 2 3 10 78.65 72.12 2.90 o 3 3 10 1128.50 1089.63 11.98 o 4 3 10 25.48 30.43 1.85 o 5 3 10 165.83 178.46 5.14 o 6 3 10 7.03 10.53 3.49 o 7 3 10 46.82 75.79 6.84 o 0 4 10 195.17 196.24 5.48 o 1 4 10 316.25 248.88 4.41 o 2 4 10 32.67 37.10 2.41 o 3 4 10 335.60 306.09 5.88 o 4 4 10 32.24 34.65 2.87 o 5 4 10 87.28 94.36 4.77 o 6 4 10 27.05 40.03 3.61 o 7 4 10 14.47 26.03 4.12 o 1 5 10 98.38 83.38 3.06 o 2 5 10 146.66 131.58 3.42 o 3 5 10 981.59 916.14 12.96 o 4 5 10 139.33 143.68 4.34 o 5 5 10 204.59 215.94 6.06 o 6 5 10 10.60 14.59 2.78 o 0 6 10 215.45 189.05 6.03 o 1 6 10 17.56 9.92 1.45 o 2 6 10 183.59 171.60 4.38 o 3 6 10 45.21 40.41 2.66 o 4 6 10 3.10 2.73 1.40 o 5 6 10 5.25 6.09 2.05 o 6 6 10 3.33 2.08 2.26 o 1 7 10 16.49 17.95 1.83 o 2 7 10 29.29 26.06 2.21 o 3 7 10 279.54 277.28 5.93 o 4 7 10 16.88 13.62 2.01 o 5 7 10 4.02 3.42 2.28 o 0 8 10 8.76 4.23 1.96 o 1 8 10 32.94 21.67 2.00 o 2 8 10 0.50 1.29 1.28 o 3 8 10 0.13 0.05 1.36 o 4 8 10 5.26 2.74 1.69 o 1 9 10 14.01 10.74 1.77 o 2 9 10 24.40 22.42 2.26 o 3 9 10 218.80 220.73 6.13 o 0 10 10 303.94 265.62 10.05 o 1 10 10 51.49 53.99 3.69 o 2 10 10 243.57 234.28 6.12 o 1 0 11 3.83 5.74 2.29 o 2 0 11 145.94 142.22 4.82 o 3 0 11 160.48 155.88 10.20 o 4 0 11 0.08 4.44 1.92 o 5 0 11 67.65 72.86 6.48 o 6 0 11 143.52 193.15 18.52 o 7 0 11 218.53 269.97 22.57 o 0 1 11 294.63 278.98 8.97 o 1 1 11 470.60 384.09 6.86 o 2 1 11 335.29 333.81 5.94 o 3 1 11 302.95 273.11 5.11 o 4 1 11 0.42 -0.43 1.11 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6.45 1.55 o 2 7 11 4.83 4.18 1.49 o 3 7 11 0.40 0.75 1.34 o 4 7 11 114.20 116.01 4.36 o 5 7 11 0.15 0.13 2.06 o 1 8 11 22.22 24.68 2.20 o 2 8 11 75.72 80.35 4.36 o 3 8 11 3.01 0.92 1.43 o 4 8 11 25.58 33.29 2.94 o 0 9 11 19.40 17.39 2.95 o 1 9 11 136.84 130.24 4.25 o 2 9 11 11.10 13.09 2.01 o 3 9 11 63.19 61.55 3.74 o 0 0 12 20.83 32.54 5.54 o 1 0 12 790.90 616.86 16.44 o 2 0 12 3.86 8.13 2.21 o 3 0 12 973.09 847.56 17.25 o 4 0 12 255.36 269.82 8.50 o 5 0 12 447.04 482.09 25.06 o 6 0 12 68.06 71.27 8.96 o 7 0 12 77.28 84.79 10.23 o 1 1 12 317.76 290.92 6.03 o 2 1 12 133.50 127.94 3.93 o 3 1 12 539.08 509.73 8.19 o 4 1 12 81.06 79.02 3.00 o 5 1 12 469.51 484.05 10.09 o 6 1 12 6.52 6.78 2.98 o 7 1 12 95.80 105.55 7.93 o 0 2 12 76.27 70.28 4.39 o 1 2 12 778.00 695.99 10.50 o 2 2 12 134.05 136.80 3.81 o 3 2 12 477.80 452.51 7.63 o 4 2 12 79.10 78.88 3.13 o 5 2 12 45.28 52.14 3.22 o 6 2 12 23.27 25.92 3.60 o 1 3 12 101.20 92.85 4.99 o 2 3 12 2.39 2.75 1.27 o 3 3 12 39.79 40.74 2.16 o 4 3 12 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o 4 7 13 2.90 4.68 2.07 o 1 8 13 52.38 53.63 3.65 o 2 8 13 2.76 1.14 1.78 o 0 0 14 40.97 71.38 8.22 o 1 0 14 185.97 162.09 8.18 o 2 0 14 336.04 367.81 10.54 o 3 0 14 259.98 245.27 9.57 o 4 0 14 73.30 82.30 9.60 o 5 0 14 259.07 296.20 11.43 o 6 0 14 85.08 106.94 8.86 o 1 1 14 10.16 6.98 1.69 o 2 1 14 1.53 1.99 1.46 o 3 1 14 36.81 32.35 2.75 o 4 1 14 20.86 24.51 2.33 o 5 1 14 88.61 92.93 4.75 o 6 1 14 39.21 57.64 4.75 o 0 2 14 526.18 448.72 14.45 o 1 2 14 87.20 73.47 3.57 o 2 2 14 22.86 20.01 2.27 o 3 2 14 0.39 0.46 1.47 o 4 2 14 3.55 1.55 1.60 o 5 2 14 40.57 51.67 3.79 o 1 3 14 7.76 4.72 1.55 o 2 3 14 4.08 2.89 1.70 o 3 3 14 8.14 6.08 1.86 o 4 3 14 10.03 9.60 2.24 o 5 3 14 20.26 28.36 3.40 o 0 4 14 1.21 0.27 1.97 o 1 4 14 11.88 5.60 1.64 o 2 4 14 86.65 89.20 3.66 o 3 4 14 0.14 0.45 1.45 o 4 4 14 0.61 -0.51 1.55 o 5 4 14 0.62 1.69 2.04 o 1 5 14 10.01 9.54 1.91 o 2 5 14 16.08 19.22 2.42 o 3 5 14 8.43 11.69 1.99 o 4 5 14 0.10 0.46 1.74 o 0 6 14 498.68 445.81 17.48 o 1 6 14 157.66 136.58 5.15 o 2 6 14 60.75 60.30 4.45 o 3 6 14 18.15 16.12 2.29 o 4 6 14 32.37 39.48 3.45 o 1 7 14 0.46 0.28 1.59 o 2 7 14 0.23 -0.28 1.65 o 3 7 14 25.77 33.28 2.95 o 0 8 14 71.72 76.00 6.00 o 1 8 14 146.91 167.67 5.70 o 1 0 15 16.77 19.39 4.54 o 2 0 15 2.75 2.23 2.28 o 3 0 15 27.93 31.20 3.91 o 4 0 15 11.92 13.39 2.85 o 5 0 15 2.16 -0.21 2.67 o 0 1 15 243.87 232.11 8.42 o 1 1 15 1.31 3.41 1.63 o 2 1 15 10.33 11.19 2.35 o 3 1 15 3.09 3.65 1.57 o 4 1 15 39.18 51.06 3.40 o 5 1 15 0.01 0.51 2.09 o 1 2 15 8.05 6.02 1.70 o 2 2 15 16.73 14.36 2.15 o 3 2 15 82.62 80.77 3.93 o 4 2 15 20.24 21.18 3.01 o 5 2 15 135.91 181.09 7.76 o 0 3 15 0.12 1.22 2.06 o 1 3 15 0.04 1.28 1.47 o 2 3 15 130.88 127.17 5.73 o 3 3 15 0.12 -0.71 1.50 o 4 3 15 25.09 26.69 2.83 o 5 3 15 10.73 12.12 2.65 o 1 4 15 20.75 18.23 2.40 o 2 4 15 8.24 3.85 1.72 o 3 4 15 73.28 82.08 3.76 o 4 4 15 10.77 9.17 2.28 o 0 5 15 8.39 7.39 2.82 o 1 5 15 58.67 57.86 4.62 o 2 5 15 62.15 57.20 3.97 o 3 5 15 44.97 50.80 3.52 o 4 5 15 8.59 7.82 2.46 o 1 6 15 10.89 11.15 2.20 o 2 6 15 1.44 0.70 1.76 o 3 6 15 76.59 80.48 5.16 o 0 7 15 105.15 114.45 7.04 o 1 7 15 20.12 18.25 2.65 o 0 0 16 27.88 32.05 4.98 o 1 0 16 0.86 0.12 1.85 o 2 0 16 13.39 14.36 2.80 o 3 0 16 10.96 7.32 2.50 o 4 0 16 2.38 0.71 2.63 o 1 1 16 0.44 -0.41 1.48 o 2 1 16 0.00 0.86 1.48 o 3 1 16 3.57 5.40 1.76 o 4 1 16 12.15 15.71 2.49 o 0 2 16 45.91 53.92 4.78 o 1 2 16 179.91 164.19 5.20 o 2 2 16 0.09 -1.39 1.49 o 3 2 16 103.89 100.66 4.55 o 4 2 16 53.75 51.91 4.27 o 1 3 16 0.05 -2.34 1.56 o 2 3 16 33.88 31.56 3.26 o 3 3 16 12.90 12.81 2.13 o 4 3 16 39.32 35.66 3.19 o 0 4 16 681.39 625.54 22.58 o 1 4 16 63.57 58.28 3.75 o 2 4 16 230.29 238.26 6.61 o 3 4 16 4.34 2.74 1.87 o 1 5 16 0.28 0.85 1.70 o 2 5 16 12.80 13.01 2.42 o 3 5 16 15.39 14.80 2.54 o 0 6 16 96.77 91.43 6.53 o 1 6 16 22.59 22.29 2.84 o 1 0 17 5.11 2.12 2.16 o 2 0 17 12.41 15.09 2.97 o 3 0 17 49.64 41.61 4.18 o 4 0 17 26.35 36.44 4.83 o 0 1 17 33.10 33.28 4.27 o 1 1 17 2.13 -0.26 1.49 o 2 1 17 1.97 1.85 1.63 o 3 1 17 12.37 11.09 2.17 o 1 2 17 3.71 4.52 1.88 o 2 2 17 1.33 0.57 1.69 o 3 2 17 41.43 37.91 3.42 o 0 3 17 78.79 102.67 8.37 o 1 3 17 1.51 1.44 2.15 o 2 3 17 168.54 181.27 6.44 o 3 3 17 7.17 7.67 2.08 o 1 4 17 8.54 8.55 2.20 o 2 4 17 119.70 116.33 6.76 o 0 5 17 40.54 53.91 8.77 o 1 5 17 11.75 15.24 2.63 o 0 0 18 66.41 60.48 14.93 o 1 0 18 0.55 0.05 2.11 o 2 0 18 0.03 -2.43 2.08 o 1 1 18 1.10 2.64 1.79 o 2 1 18 92.07 101.73 4.68 o 0 2 18 76.42 79.65 6.07 o 1 2 18 121.03 123.39 7.73 o 2 2 18 3.77 4.92 2.11 o 1 3 18 0.65 2.86 2.39 o