#------------------------------------------------------------------------------ #$Date: 2009-05-03 21:56:13 +0300 (Sun, 03 May 2009) $ #$Revision: 691 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2218609.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2218609_Fobs loop_ _publ_author_name 'Wang, Xiang' 'Li, Yan' 'Liu, Ming-Guo' _publ_section_title ; Diethyl 3-amino-4-[(triphenylphosphoranylidene)amino]thieno[2,3-b]thiophene-2,5-dicarboxylate ; _journal_coeditor_code BT2711 _journal_issue 7 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o1180 _journal_volume 64 _journal_year 2008 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 68.140 _cell_angle_beta 71.043 _cell_angle_gamma 68.969 _cell_length_a 13.1260 _cell_length_b 15.3616 _cell_length_c 16.6497 _exptl_crystal_F_000 1200.00 _reflns_d_resolution_high 0.8107 _[local]_cod_data_source_file bt2711Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 070411am in P-1' _shelx_refln_list_code 4 _shelx_F_calc_maximum 362.78 _shelx_F_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 8911.36 9377.49 168.21 o 2 0 0 8641.75 9361.43 172.30 o 3 0 0 20.54 24.31 5.43 o 4 0 0 1367.87 1406.62 42.43 o 5 0 0 188.75 245.23 20.53 o 6 0 0 0.17 14.27 7.61 o 7 0 0 733.61 733.70 35.80 o 8 0 0 160.77 155.43 21.17 o 9 0 0 305.52 365.52 33.67 o 10 0 0 54.71 78.22 26.36 o 11 0 0 132.20 116.98 87.72 o 12 0 0 1.55 25.00 31.01 o 13 0 0 80.25 82.55 31.75 o 14 0 0 315.20 349.88 58.49 o -14 1 0 20.68 2.22 27.67 o -13 1 0 48.51 69.14 34.62 o -12 1 0 35.88 31.66 22.61 o -11 1 0 65.98 101.14 29.39 o -10 1 0 918.39 955.79 79.84 o -9 1 0 210.08 218.40 36.61 o -8 1 0 1295.45 1262.67 70.64 o -7 1 0 95.61 76.54 14.56 o -6 1 0 2578.98 2575.22 72.69 o -5 1 0 180.06 178.64 17.46 o -4 1 0 478.00 514.98 23.00 o -3 1 0 31605.18 31770.68 560.91 o -2 1 0 2855.42 2598.44 72.19 o -1 1 0 4950.28 5157.90 119.20 o 0 1 0 620.60 432.65 77.22 o 1 1 0 651.10 632.47 15.86 o 2 1 0 3264.26 3270.63 83.58 o 3 1 0 1213.31 1207.92 35.18 o 4 1 0 496.02 548.57 24.36 o 5 1 0 2099.30 2178.45 62.20 o 6 1 0 723.07 887.78 49.73 o 7 1 0 788.28 692.51 35.42 o 8 1 0 2097.61 2120.70 71.96 o 9 1 0 330.06 376.44 51.80 o 10 1 0 57.03 70.94 17.40 o 11 1 0 220.27 199.95 38.58 o 12 1 0 152.03 222.79 42.20 o 13 1 0 269.39 283.98 48.78 o 14 1 0 53.20 98.83 43.48 o -14 2 0 1.16 35.92 24.19 o -13 2 0 31.71 46.69 27.77 o -12 2 0 4.87 23.79 29.85 o -11 2 0 163.60 163.92 36.80 o -10 2 0 343.74 305.11 80.70 o -9 2 0 854.15 878.98 49.52 o -8 2 0 88.53 52.90 35.78 o -7 2 0 95.93 126.24 16.75 o -6 2 0 1036.28 1026.86 39.69 o -5 2 0 700.24 665.08 28.14 o -4 2 0 14.60 6.22 5.47 o -3 2 0 0.51 12.91 6.10 o -2 2 0 4600.10 4706.40 94.48 o -1 2 0 16360.78 17613.20 313.58 o 0 2 0 10853.44 12657.12 226.24 o 1 2 0 30.49 40.49 5.37 o 2 2 0 3226.27 3469.44 73.36 o 3 2 0 15057.35 15389.92 345.35 o 4 2 0 5505.01 5599.12 129.70 o 5 2 0 5230.29 5061.67 145.90 o 6 2 0 907.55 1016.38 41.53 o 7 2 0 557.75 548.54 34.41 o 8 2 0 372.13 408.63 34.08 o 9 2 0 441.33 426.56 39.19 o 10 2 0 375.82 359.65 36.19 o 11 2 0 69.82 73.58 18.98 o 12 2 0 196.02 203.65 57.11 o 13 2 0 79.99 107.69 45.66 o 14 2 0 52.85 38.71 29.58 o 15 2 0 49.62 90.51 34.76 o -13 3 0 43.92 16.52 37.83 o -12 3 0 3.00 3.62 23.24 o -11 3 0 89.02 62.39 27.39 o -10 3 0 474.41 510.89 62.49 o -9 3 0 42.95 52.85 16.41 o -8 3 0 359.59 368.67 68.43 o -7 3 0 1439.25 1461.82 236.91 o -6 3 0 2320.77 2356.01 77.49 o -5 3 0 83.53 85.31 11.20 o -4 3 0 4856.73 5161.17 111.34 o -3 3 0 38.65 56.97 8.67 o -2 3 0 6301.45 6541.06 171.38 o -1 3 0 63822.20 64280.57 1111.24 o 0 3 0 3983.09 3359.73 70.28 o 1 3 0 3710.37 3528.04 89.91 o 2 3 0 213.66 174.01 12.25 o 3 3 0 657.64 691.21 23.20 o 4 3 0 3574.32 3915.25 112.80 o 5 3 0 517.80 617.15 88.67 o 6 3 0 51.29 61.65 14.69 o 7 3 0 78.43 108.76 21.39 o 8 3 0 40.36 35.54 27.94 o 9 3 0 298.46 281.39 56.43 o 10 3 0 349.93 317.75 41.78 o 11 3 0 34.95 47.41 20.55 o 12 3 0 727.39 783.43 69.69 o 13 3 0 325.84 467.00 88.74 o 14 3 0 3.57 62.84 40.62 o 15 3 0 30.28 11.72 25.35 o -13 4 0 3.07 22.66 39.60 o -12 4 0 68.54 118.37 32.91 o -11 4 0 0.27 0.00 18.43 o -10 4 0 128.67 80.31 29.69 o -9 4 0 32.82 46.43 16.97 o -8 4 0 1957.30 1985.24 83.54 o -7 4 0 0.69 0.00 15.47 o -6 4 0 4130.72 3928.24 174.55 o -5 4 0 1028.61 986.97 34.68 o -4 4 0 19.45 9.68 9.63 o -3 4 0 3.49 0.00 6.89 o -2 4 0 6587.96 6380.64 128.49 o -1 4 0 5469.39 5839.20 118.05 o 0 4 0 13349.43 13518.47 248.79 o 1 4 0 31.76 32.51 6.34 o 2 4 0 1099.24 1142.29 35.02 o 3 4 0 5723.68 5403.84 111.91 o 4 4 0 992.08 1050.52 33.46 o 5 4 0 792.26 940.33 48.01 o 6 4 0 3499.34 3726.55 120.27 o 7 4 0 340.75 412.71 41.32 o 8 4 0 238.68 232.30 32.33 o 9 4 0 1451.87 1412.43 75.28 o 10 4 0 285.68 219.61 35.76 o 11 4 0 31.60 74.73 24.96 o 12 4 0 178.64 205.93 36.95 o 13 4 0 76.50 66.74 27.53 o 14 4 0 335.72 321.29 72.11 o 15 4 0 0.97 0.14 28.76 o -12 5 0 1.69 0.00 19.95 o -11 5 0 171.51 209.84 43.37 o -10 5 0 217.79 209.58 43.21 o -9 5 0 83.24 71.25 18.22 o -8 5 0 124.79 99.87 20.58 o -7 5 0 579.73 548.11 43.57 o -6 5 0 529.80 545.53 78.45 o -5 5 0 6.45 2.36 20.31 o -4 5 0 333.89 457.86 44.64 o -3 5 0 1006.52 885.86 29.28 o -2 5 0 7.47 4.09 4.33 o -1 5 0 3183.25 3457.10 79.87 o 0 5 0 2132.57 1965.33 45.98 o 1 5 0 177.47 187.86 16.47 o 2 5 0 282.94 366.58 21.61 o 3 5 0 1491.54 1383.90 51.58 o 4 5 0 1092.12 1104.73 37.90 o 5 5 0 1609.32 1653.28 48.57 o 6 5 0 36.74 54.04 14.92 o 7 5 0 207.65 182.27 28.73 o 8 5 0 208.83 212.36 31.13 o 9 5 0 1744.68 1562.90 80.74 o 10 5 0 65.89 110.81 49.69 o 11 5 0 421.77 455.23 71.63 o 12 5 0 52.18 105.41 29.81 o 13 5 0 87.63 88.77 29.39 o 14 5 0 5.74 0.95 27.94 o 15 5 0 4.56 0.00 25.49 o -12 6 0 21.72 61.08 28.01 o -11 6 0 244.53 205.65 43.62 o -10 6 0 681.38 694.83 108.10 o -9 6 0 0.25 14.90 16.09 o -8 6 0 289.79 241.71 31.26 o -7 6 0 100.93 150.02 31.94 o -6 6 0 587.15 603.78 45.16 o -5 6 0 195.03 191.58 30.31 o -4 6 0 604.76 613.14 45.74 o -3 6 0 34.31 32.39 6.69 o -2 6 0 1711.27 1843.02 65.23 o -1 6 0 709.11 792.83 27.90 o 0 6 0 633.93 731.42 26.20 o 1 6 0 1884.52 1859.02 46.46 o 2 6 0 203.67 159.68 27.33 o 3 6 0 2321.94 2309.15 70.40 o 4 6 0 551.11 400.38 27.99 o 5 6 0 5074.62 5267.99 119.35 o 6 6 0 176.12 219.98 21.33 o 7 6 0 64.34 52.40 16.08 o 8 6 0 848.08 838.09 56.23 o 9 6 0 2314.37 2317.43 148.03 o 10 6 0 90.06 111.43 28.05 o 11 6 0 88.54 113.85 34.62 o 12 6 0 284.76 329.02 50.72 o 13 6 0 60.76 44.84 32.03 o 14 6 0 70.02 48.93 26.46 o 15 6 0 7.80 0.00 28.63 o -11 7 0 5.50 8.95 57.80 o -10 7 0 184.96 155.63 51.22 o -9 7 0 2.82 0.00 19.56 o -8 7 0 0.78 0.00 13.75 o -7 7 0 548.62 578.35 49.07 o -6 7 0 4.07 13.79 12.03 o -5 7 0 152.69 125.20 21.04 o -4 7 0 242.38 285.72 29.24 o -3 7 0 0.13 6.97 11.02 o -2 7 0 2237.21 2221.79 56.60 o -1 7 0 148.97 116.97 13.48 o 0 7 0 0.01 2.95 5.22 o 1 7 0 34.73 47.39 8.48 o 2 7 0 1027.68 1092.94 48.10 o 3 7 0 978.28 1004.45 40.92 o 4 7 0 33.85 68.11 18.11 o 5 7 0 1474.65 1592.80 53.90 o 6 7 0 4.44 15.22 7.55 o 7 7 0 237.22 271.18 47.16 o 8 7 0 158.64 136.50 39.46 o 9 7 0 561.35 532.81 56.68 o 10 7 0 155.58 207.70 38.67 o 11 7 0 407.23 493.21 58.87 o 12 7 0 261.10 286.65 46.15 o 13 7 0 284.50 353.12 54.44 o 14 7 0 45.01 57.64 45.19 o 15 7 0 43.77 84.20 23.42 o -11 8 0 16.50 64.15 24.02 o -10 8 0 1.90 0.00 17.87 o -9 8 0 0.83 18.94 39.58 o -8 8 0 34.05 43.66 19.10 o -7 8 0 252.13 229.43 33.02 o -6 8 0 318.73 369.56 38.16 o -5 8 0 301.20 262.79 30.93 o -4 8 0 1209.53 1252.08 86.51 o -3 8 0 965.87 896.86 45.28 o -2 8 0 1044.72 916.32 56.49 o -1 8 0 1575.61 1577.10 47.30 o 0 8 0 376.94 390.22 24.57 o 1 8 0 468.44 481.33 25.56 o 2 8 0 58.56 56.04 11.49 o 3 8 0 1447.80 1341.65 51.22 o 4 8 0 18.01 8.21 8.23 o 5 8 0 1501.81 1483.55 80.82 o 6 8 0 587.36 570.16 34.77 o 7 8 0 1.93 11.51 15.06 o 8 8 0 140.79 132.21 45.87 o 9 8 0 2488.33 2104.24 122.34 o 10 8 0 133.27 91.91 26.34 o 11 8 0 74.35 122.46 32.90 o 12 8 0 109.10 96.85 31.00 o 13 8 0 64.01 63.61 34.83 o 14 8 0 5.39 0.00 21.41 o 15 8 0 66.40 109.22 43.28 o -10 9 0 62.81 29.35 20.64 o -9 9 0 0.05 8.29 16.87 o -8 9 0 149.02 184.93 32.51 o -7 9 0 33.30 34.34 17.44 o -6 9 0 3.06 3.56 13.62 o -5 9 0 4.61 16.35 14.38 o -4 9 0 367.31 374.97 37.64 o -3 9 0 2.15 9.32 20.00 o -2 9 0 25.24 24.65 12.17 o -1 9 0 10.44 21.10 8.31 o 0 9 0 433.34 420.81 25.69 o 1 9 0 61.93 84.39 12.71 o 2 9 0 566.39 545.95 28.83 o 3 9 0 1477.29 1405.92 67.68 o 4 9 0 3286.11 3377.69 96.41 o 5 9 0 10.16 15.01 9.55 o 6 9 0 1.62 21.79 10.89 o 7 9 0 23.48 23.06 18.71 o 8 9 0 2.70 42.56 20.72 o 9 9 0 0.41 0.00 19.02 o 10 9 0 262.21 311.78 49.68 o 11 9 0 173.96 214.09 40.51 o 12 9 0 7.86 25.38 23.56 o 13 9 0 256.83 321.07 51.74 o 14 9 0 2.60 9.56 21.93 o -9 10 0 10.75 30.59 20.18 o -8 10 0 10.80 12.36 17.75 o -7 10 0 0.80 14.95 17.26 o -6 10 0 1.81 9.95 15.83 o -5 10 0 15.46 45.71 17.92 o -4 10 0 58.28 49.21 20.53 o -3 10 0 268.69 322.98 34.85 o -2 10 0 537.48 446.87 48.46 o -1 10 0 11.95 22.33 12.18 o 0 10 0 868.26 822.04 37.28 o 1 10 0 91.42 106.14 15.45 o 2 10 0 770.84 702.71 33.68 o 3 10 0 1101.47 1016.01 48.86 o 4 10 0 138.17 128.96 20.05 o 5 10 0 242.95 231.85 26.40 o 6 10 0 946.28 961.66 46.65 o 7 10 0 303.69 300.28 45.25 o 8 10 0 1135.01 1199.43 272.28 o 9 10 0 203.15 292.10 46.91 o 10 10 0 334.40 385.74 55.37 o 11 10 0 4.83 16.55 19.96 o 12 10 0 10.37 24.73 26.16 o 13 10 0 104.69 146.77 63.93 o 14 10 0 39.33 83.38 48.12 o -8 11 0 214.51 245.94 39.85 o -7 11 0 25.08 75.49 24.48 o -6 11 0 75.95 39.93 20.04 o -5 11 0 85.13 52.17 21.11 o -4 11 0 47.05 48.97 19.37 o -3 11 0 35.23 20.60 15.97 o -2 11 0 196.40 209.52 31.49 o -1 11 0 564.11 668.54 65.14 o 0 11 0 89.13 54.81 21.84 o 1 11 0 301.17 315.39 33.49 o 2 11 0 800.91 729.13 46.59 o 3 11 0 178.29 142.03 22.23 o 4 11 0 189.26 208.09 26.76 o 5 11 0 65.52 56.68 19.19 o 6 11 0 77.80 51.28 19.50 o 7 11 0 188.09 204.38 39.30 o 8 11 0 49.08 60.99 36.33 o 9 11 0 410.26 359.18 53.34 o 10 11 0 99.42 100.07 32.13 o 11 11 0 41.31 50.31 27.09 o 12 11 0 6.01 39.10 23.12 o 13 11 0 4.97 23.21 23.17 o 14 11 0 5.54 20.78 21.43 o -7 12 0 2.31 17.23 25.81 o -6 12 0 75.07 75.28 97.39 o -5 12 0 34.03 28.12 26.89 o -4 12 0 28.87 33.98 25.00 o -3 12 0 247.91 298.87 49.64 o -2 12 0 134.21 79.76 33.74 o -1 12 0 516.46 482.23 58.91 o 0 12 0 4.54 4.40 14.50 o 1 12 0 543.63 491.12 107.35 o 2 12 0 89.86 95.33 22.00 o 3 12 0 0.12 0.00 11.20 o 4 12 0 7.85 10.60 12.69 o 5 12 0 101.82 110.96 25.83 o 6 12 0 92.46 99.19 29.64 o 7 12 0 164.41 180.71 38.29 o 8 12 0 119.58 124.72 33.11 o 9 12 0 79.99 93.42 34.06 o 10 12 0 313.62 278.17 51.18 o 11 12 0 477.31 561.02 71.82 o 12 12 0 47.08 39.15 47.23 o 13 12 0 187.53 263.95 47.59 o -6 13 0 30.13 40.14 27.58 o -5 13 0 0.06 15.20 23.37 o -4 13 0 9.94 22.95 24.33 o -3 13 0 0.73 0.00 20.51 o -2 13 0 14.53 37.79 27.40 o -1 13 0 20.83 17.12 19.39 o 0 13 0 0.05 21.94 30.53 o 1 13 0 165.93 231.71 40.74 o 2 13 0 283.68 313.57 43.48 o 3 13 0 47.45 25.60 15.74 o 4 13 0 68.71 92.24 20.33 o 5 13 0 97.02 91.21 21.55 o 6 13 0 90.90 98.90 29.71 o 7 13 0 51.07 56.08 27.19 o 8 13 0 362.79 421.99 58.43 o 9 13 0 204.43 265.53 90.92 o 10 13 0 0.66 16.94 25.02 o 11 13 0 82.30 120.07 37.55 o 12 13 0 59.30 52.76 43.82 o -5 14 0 0.72 0.00 27.32 o -4 14 0 0.12 0.00 51.12 o -3 14 0 61.47 156.78 38.85 o -2 14 0 1.35 44.55 23.52 o -1 14 0 0.55 0.00 19.58 o 0 14 0 24.28 6.79 22.63 o 1 14 0 844.65 925.72 104.76 o 2 14 0 3.04 0.00 26.85 o 3 14 0 782.31 813.37 60.15 o 4 14 0 0.01 0.00 15.35 o 5 14 0 231.94 252.58 41.36 o 6 14 0 43.52 88.57 29.71 o 7 14 0 6.79 18.53 25.75 o 8 14 0 67.24 116.60 35.47 o 9 14 0 3.18 0.00 26.51 o 10 14 0 36.94 0.00 25.39 o 11 14 0 55.40 145.54 39.85 o 12 14 0 1.02 0.00 23.66 o -4 15 0 0.75 45.62 29.51 o -3 15 0 106.62 157.84 39.62 o -2 15 0 0.45 0.00 45.39 o -1 15 0 33.95 50.12 24.24 o 0 15 0 9.14 21.62 26.31 o 1 15 0 0.16 0.00 20.72 o 2 15 0 0.78 6.16 20.67 o 3 15 0 129.66 112.53 33.23 o 4 15 0 16.06 28.47 19.33 o 5 15 0 28.22 22.75 17.77 o 6 15 0 164.32 144.61 41.03 o 7 15 0 312.26 244.92 56.77 o 8 15 0 96.45 111.84 35.18 o 9 15 0 108.93 144.26 42.69 o 10 15 0 2.06 6.37 26.22 o 11 15 0 48.42 81.17 29.49 o -2 16 0 0.06 30.02 29.44 o -1 16 0 0.09 0.00 45.26 o 0 16 0 38.37 85.20 30.50 o 1 16 0 17.82 15.34 23.07 o 2 16 0 9.06 13.51 31.90 o 3 16 0 39.86 67.88 41.10 o 4 16 0 67.96 90.24 28.82 o 5 16 0 780.54 818.94 83.56 o 6 16 0 163.15 131.27 42.32 o 7 16 0 40.09 30.99 40.55 o 8 16 0 46.99 108.60 33.55 o 9 16 0 7.30 0.00 24.56 o 1 17 0 37.33 59.00 30.39 o 2 17 0 30.80 27.74 46.75 o 3 17 0 1.16 20.36 27.81 o 4 17 0 1.98 0.00 30.40 o 5 17 0 13.32 31.90 39.53 o 6 17 0 3.96 8.83 39.87 o 7 17 0 0.82 0.00 20.64 o -6 -17 1 14.93 5.31 23.07 o -5 -17 1 30.39 30.12 38.30 o -4 -17 1 24.81 30.28 52.14 o -3 -17 1 22.68 53.79 26.79 o -2 -17 1 80.10 96.40 32.74 o -8 -16 1 66.06 75.88 74.56 o -7 -16 1 42.50 33.89 33.60 o -6 -16 1 136.32 137.64 38.39 o -5 -16 1 93.98 139.34 37.61 o -4 -16 1 27.13 41.02 66.45 o -3 -16 1 16.21 27.40 25.25 o -2 -16 1 160.17 186.76 43.01 o -1 -16 1 5.47 33.23 25.05 o 0 -16 1 22.10 27.30 24.37 o 1 -16 1 5.81 27.37 25.69 o -10 -15 1 26.28 28.12 27.64 o -9 -15 1 35.64 71.67 33.62 o -8 -15 1 49.85 7.56 28.58 o -7 -15 1 90.32 107.07 31.78 o -6 -15 1 244.05 249.68 49.20 o -5 -15 1 1.04 17.43 23.21 o -4 -15 1 3.52 22.81 18.68 o -3 -15 1 84.84 119.36 34.56 o -2 -15 1 28.48 24.49 24.94 o -1 -15 1 51.16 26.30 24.24 o 0 -15 1 48.57 25.88 25.55 o 1 -15 1 10.55 36.68 40.48 o 2 -15 1 91.35 111.28 64.00 o 3 -15 1 35.11 11.13 26.63 o -11 -14 1 149.05 143.37 43.72 o -10 -14 1 33.80 22.36 28.76 o -9 -14 1 33.60 0.44 49.21 o -8 -14 1 22.70 89.91 34.16 o -7 -14 1 85.85 70.43 39.33 o -6 -14 1 133.15 215.56 44.62 o -5 -14 1 107.60 143.45 27.70 o -4 -14 1 71.95 54.10 22.21 o -3 -14 1 17.33 33.86 18.33 o -2 -14 1 148.60 147.69 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37.89 o 9 5 19 39.54 104.96 46.62 o 0 6 19 66.90 45.53 46.21 o 1 6 19 0.22 0.00 29.99 o 2 6 19 162.90 201.47 62.98 o 3 6 19 142.06 172.98 61.48 o 4 6 19 0.87 21.67 32.44 o 5 6 19 73.57 90.92 49.07 o 6 6 19 153.95 125.82 47.71 o 7 6 19 158.51 91.87 45.26 o 8 6 19 34.37 47.30 33.81 o 9 6 19 35.01 9.81 35.99 o 10 6 19 21.33 21.13 43.35 o 0 7 19 0.01 0.00 34.90 o 1 7 19 50.60 16.49 41.17 o 2 7 19 11.25 6.95 41.03 o 3 7 19 15.56 95.28 48.25 o 4 7 19 7.61 4.19 26.04 o 5 7 19 1.87 0.00 22.38 o 6 7 19 0.08 13.22 34.76 o 7 7 19 35.96 91.47 40.48 o 8 7 19 31.33 0.00 28.22 o 9 7 19 177.69 180.07 53.43 o 10 7 19 26.56 0.00 41.03 o 0 8 19 4.97 15.81 42.80 o 1 8 19 149.51 71.40 55.48 o 2 8 19 19.02 64.29 59.70 o 3 8 19 8.94 11.93 32.03 o 4 8 19 33.18 0.00 33.26 o 5 8 19 1.35 0.00 42.12 o 6 8 19 195.30 233.37 71.15 o 7 8 19 263.08 221.23 57.80 o 8 8 19 26.97 43.62 31.90 o 9 8 19 2.52 1.09 29.85 o 10 8 19 18.10 49.75 39.39 o 1 9 19 2.93 31.49 40.76 o 2 9 19 64.60 105.31 37.51 o 3 9 19 0.18 22.88 34.90 o 4 9 19 0.39 15.35 22.89 o 5 9 19 133.64 129.93 34.28 o 6 9 19 150.31 236.36 65.57 o 7 9 19 9.26 36.40 31.90 o 8 9 19 52.10 36.26 32.58 o 9 9 19 49.04 122.54 44.03 o 10 9 19 36.66 74.29 38.30 o 1 10 19 58.42 119.00 54.25 o 2 10 19 0.29 0.00 34.90 o 3 10 19 37.83 0.00 26.68 o 4 10 19 3.37 19.64 25.22 o 5 10 19 77.74 76.94 33.16 o 6 10 19 183.50 162.21 62.02 o 7 10 19 6.96 27.94 36.67 o 8 10 19 27.77 64.61 37.08 o 9 10 19 0.00 0.00 27.94 o 10 10 19 116.37 153.90 54.52 o 2 11 19 0.08 74.43 49.62 o 3 11 19 4.76 15.54 41.98 o 4 11 19 1.75 0.00 31.35 o 5 11 19 148.63 117.87 36.05 o 6 11 19 110.41 243.04 72.11 o 7 11 19 0.94 42.67 33.53 o 8 11 19 5.38 8.32 33.67 o 9 11 19 0.35 21.40 34.49 o 10 11 19 54.75 125.41 52.62 o 3 12 19 23.04 23.31 39.80 o 4 12 19 57.05 119.95 57.25 o 5 12 19 78.54 123.95 35.37 o 6 12 19 18.04 7.50 22.59 o 7 12 19 119.19 129.50 51.12 o 8 12 19 26.81 28.22 37.62 o 9 12 19 53.96 69.93 34.90 o 6 13 19 0.80 19.49 25.44 o 7 13 19 17.51 43.35 37.89 o 4 3 20 11.75 30.94 38.44 o 5 3 20 27.41 37.35 34.49 o 3 4 20 8.96 0.00 34.21 o 4 4 20 55.60 9.81 34.21 o 5 4 20 8.46 0.00 32.17 o 6 4 20 131.38 188.93 55.34 o 2 5 20 20.94 40.62 41.03 o 3 5 20 42.05 95.01 41.44 o 4 5 20 1.92 55.48 36.53 o 5 5 20 12.57 26.72 33.53 o 6 5 20 5.15 7.77 33.26 o 7 5 20 35.71 5.86 32.58 o 2 6 20 29.16 17.45 38.85 o 3 6 20 0.78 28.90 35.30 o 4 6 20 110.80 131.27 48.53 o 5 6 20 196.64 338.33 76.74 o 6 6 20 61.42 166.71 48.66 o 7 6 20 8.62 0.00 34.49 o 8 6 20 58.81 90.78 32.85 o 2 7 20 29.68 55.34 41.58 o 3 7 20 98.99 147.08 56.57 o 4 7 20 0.01 0.00 33.67 o 5 7 20 41.50 39.94 38.99 o 6 7 20 0.15 0.00 24.40 o 7 7 20 142.97 226.28 54.12 o 8 7 20 0.49 0.00 32.03 o 3 8 20 22.76 56.30 43.07 o 4 8 20 11.29 69.25 41.30 o 5 8 20 107.62 134.42 49.48 o 6 8 20 0.21 26.85 31.90 o 7 8 20 15.20 13.77 35.85 o 8 8 20 116.88 179.39 55.34 o 3 9 20 27.81 21.18 27.76 o 4 9 20 51.02 4.62 26.03 o 5 9 20 0.21 8.18 25.15 o 6 9 20 2.86 76.20 38.30 o 7 9 20 60.28 183.34 50.03 o 8 9 20 69.27 15.40 38.44 o 4 10 20 15.07 10.36 23.76 o 5 10 20 55.56 117.39 31.36 o 6 10 20 2.55 0.00 21.19 o 7 10 20 36.97 34.62 36.26 o