#------------------------------------------------------------------------------ #$Date: 2009-05-05 17:46:52 +0300 (Tue, 05 May 2009) $ #$Revision: 697 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2218708.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2218708_Fobs loop_ _publ_author_name 'Zhang, Ya-Wen' 'Dong, Hua-Ze' 'Cheng, Lin' _publ_section_title ; Poly[{\m~2~-1,2-bis[4-(3-pyridyl)pyrimidin-2-ylsulfanyl]ethane}di-\m~2~-cyanido-dicopper(I)] ; _journal_coeditor_code HG2393 _journal_issue 7 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m868 _journal_volume 64 _journal_year 2008 _space_group_IT_number 15 _symmetry_space_group_name_Hall '-C 2yc' _symmetry_space_group_name_H-M 'C 1 2/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 105.660 _cell_angle_gamma 90.000 _cell_length_a 16.0249 _cell_length_b 16.2963 _cell_length_c 9.3103 _exptl_crystal_F_000 1176.00 _reflns_d_resolution_high 0.8108 _[local]_cod_data_source_file hg2393Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 1 in C2/c' _shelx_refln_list_code 4 _shelx_F_calc_maximum 607.62 _shelx_F_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 13192.16 14580.56 462.52 o 4 0 0 29638.28 33734.95 1065.59 o 6 0 0 82.28 75.70 23.47 o 8 0 0 35228.79 37947.60 1201.72 o 10 0 0 3129.37 2723.76 101.89 o 12 0 0 902.49 833.09 45.29 o 14 0 0 140.33 158.22 21.54 o 16 0 0 9.95 30.37 16.57 o 18 0 0 2028.73 2162.94 97.75 o 3 1 0 69352.66 70065.26 1281.70 o 5 1 0 81817.91 80117.23 1970.32 o 7 1 0 6677.79 6941.23 131.73 o 9 1 0 913.39 932.04 26.94 o 11 1 0 169.60 147.05 13.24 o 13 1 0 3602.79 3327.61 143.45 o 15 1 0 3059.85 2932.44 96.65 o 17 1 0 5.80 4.43 11.32 o 19 1 0 184.64 167.20 22.92 o 0 2 0 1679.78 1583.06 56.33 o 2 2 0 30230.51 31617.90 451.02 o 4 2 0 1286.76 1298.57 25.11 o 6 2 0 4119.61 4650.76 89.00 o 8 2 0 14093.69 14536.97 235.06 o 10 2 0 24510.79 24926.68 701.79 o 12 2 0 1911.90 1766.65 121.22 o 14 2 0 86.03 84.19 27.34 o 16 2 0 28.17 27.64 9.27 o 18 2 0 288.92 283.94 23.06 o 1 3 0 1888.30 2239.33 43.48 o 3 3 0 34111.68 36807.59 525.32 o 5 3 0 20298.33 21751.33 312.16 o 7 3 0 7146.06 7230.88 128.22 o 9 3 0 311.05 257.79 13.96 o 11 3 0 3063.45 2901.13 92.27 o 13 3 0 2423.85 2326.75 75.80 o 15 3 0 918.71 891.42 28.51 o 17 3 0 622.93 614.85 71.93 o 0 4 0 32962.48 33004.08 752.40 o 2 4 0 9470.71 10290.09 148.78 o 4 4 0 899.27 784.06 14.23 o 6 4 0 3450.92 3777.34 57.49 o 8 4 0 6569.62 6595.57 98.44 o 10 4 0 36.99 48.05 7.95 o 12 4 0 3152.38 3031.82 110.03 o 14 4 0 501.65 498.43 19.55 o 16 4 0 478.59 466.49 23.02 o 18 4 0 18.50 33.57 13.94 o 1 5 0 4956.08 5382.10 80.04 o 3 5 0 15356.72 17334.68 249.30 o 5 5 0 305.18 358.53 8.79 o 7 5 0 5702.64 6233.19 93.10 o 9 5 0 426.96 377.12 13.83 o 11 5 0 2327.00 2269.06 51.16 o 13 5 0 744.66 721.98 23.47 o 15 5 0 21.25 30.27 8.79 o 17 5 0 5.53 26.50 13.12 o 0 6 0 5346.56 5805.07 287.18 o 2 6 0 771.17 857.19 15.47 o 4 6 0 14761.25 17068.80 246.34 o 6 6 0 11222.31 12836.97 186.97 o 8 6 0 180.43 185.55 9.50 o 10 6 0 1152.20 1021.24 42.53 o 12 6 0 394.00 364.38 21.31 o 14 6 0 4211.15 4147.61 88.40 o 16 6 0 6.17 16.01 9.23 o 18 6 0 1.33 21.40 24.16 o 1 7 0 22.57 20.58 3.49 o 3 7 0 1162.81 1093.59 19.47 o 5 7 0 7480.38 8018.59 118.69 o 7 7 0 1255.30 1288.09 23.56 o 9 7 0 400.70 431.76 16.74 o 11 7 0 790.10 736.97 23.13 o 13 7 0 174.24 167.75 12.01 o 15 7 0 7.24 8.68 8.22 o 17 7 0 28.95 33.62 17.49 o 0 8 0 8725.35 8384.37 159.57 o 2 8 0 3252.94 3083.31 54.70 o 4 8 0 7079.80 8231.57 135.35 o 6 8 0 2200.90 2502.79 41.01 o 8 8 0 430.81 452.26 12.59 o 10 8 0 1630.68 1690.45 34.72 o 12 8 0 887.69 876.46 26.32 o 14 8 0 537.44 564.35 24.81 o 16 8 0 178.60 225.59 19.78 o 1 9 0 1907.27 1881.28 34.99 o 3 9 0 2153.09 1956.41 45.52 o 5 9 0 714.16 616.95 16.91 o 7 9 0 2817.13 2685.23 44.33 o 9 9 0 353.87 365.19 12.68 o 11 9 0 350.36 380.28 20.31 o 13 9 0 151.57 184.97 22.50 o 15 9 0 961.46 1025.44 39.82 o 17 9 0 628.90 650.43 32.41 o 0 10 0 5314.26 4983.09 124.64 o 2 10 0 7570.04 7909.75 133.02 o 4 10 0 1080.41 967.73 22.28 o 6 10 0 279.98 244.23 10.48 o 8 10 0 1422.29 1421.47 42.93 o 10 10 0 631.06 641.74 21.41 o 12 10 0 1775.35 1973.21 59.55 o 14 10 0 703.08 787.33 88.50 o 16 10 0 650.74 720.24 50.39 o 1 11 0 2480.40 2483.86 65.03 o 3 11 0 2422.32 2402.71 111.79 o 5 11 0 3345.32 3331.02 61.12 o 7 11 0 6101.30 6362.49 122.76 o 9 11 0 977.54 1009.77 39.58 o 11 11 0 256.08 311.92 29.96 o 13 11 0 493.19 495.25 26.09 o 15 11 0 129.16 181.75 18.55 o 0 12 0 55.50 62.36 11.36 o 2 12 0 6355.52 6830.38 198.68 o 4 12 0 561.74 514.84 19.56 o 6 12 0 496.89 480.13 18.64 o 8 12 0 392.26 400.68 16.62 o 10 12 0 2134.78 1944.99 58.54 o 12 12 0 965.79 992.18 37.67 o 14 12 0 161.33 177.57 17.76 o 1 13 0 547.15 546.94 29.27 o 3 13 0 2699.42 2787.88 68.22 o 5 13 0 2021.66 2073.69 50.31 o 7 13 0 865.31 886.78 27.37 o 9 13 0 52.31 60.73 12.19 o 11 13 0 32.95 41.14 11.48 o 13 13 0 70.64 66.55 18.50 o 0 14 0 6846.59 7218.35 257.63 o 2 14 0 24.01 15.54 8.43 o 4 14 0 41.72 43.90 9.08 o 6 14 0 104.22 113.69 10.78 o 8 14 0 971.56 905.80 35.04 o 10 14 0 68.69 86.35 13.18 o 12 14 0 164.61 146.35 24.85 o 1 15 0 223.51 212.27 19.22 o 3 15 0 53.14 79.43 10.12 o 5 15 0 184.49 164.27 13.31 o 7 15 0 17.45 17.96 8.85 o 9 15 0 89.01 73.98 13.56 o 11 15 0 46.48 45.25 14.50 o 0 16 0 187.63 185.56 26.23 o 2 16 0 160.84 157.69 24.79 o 4 16 0 12.92 16.46 12.01 o 6 16 0 402.03 369.45 19.07 o 8 16 0 72.52 75.43 14.30 o 10 16 0 91.82 78.88 14.43 o 1 17 0 19.84 18.26 11.71 o 3 17 0 24.96 25.92 10.59 o 5 17 0 23.62 40.04 10.36 o 7 17 0 193.34 185.46 21.26 o 9 17 0 15.89 13.57 13.13 o 0 18 0 203.88 287.45 31.48 o 2 18 0 463.82 507.91 48.74 o 4 18 0 211.38 205.27 17.35 o 6 18 0 40.67 37.73 11.06 o 8 18 0 67.51 90.56 17.08 o 1 19 0 46.05 77.62 15.89 o 3 19 0 185.48 141.98 15.44 o 5 19 0 243.02 248.46 17.59 o 0 20 0 533.74 628.47 47.22 o -19 1 1 67.15 65.48 18.26 o -17 1 1 206.15 233.13 20.50 o -15 1 1 1274.70 1234.25 42.65 o -13 1 1 23.76 25.34 9.08 o -11 1 1 395.21 419.72 20.09 o -9 1 1 245.01 258.22 14.15 o -7 1 1 11204.79 12143.01 226.06 o -5 1 1 6256.87 6369.42 119.62 o -3 1 1 6292.61 6523.85 129.85 o -1 1 1 1364.94 1381.17 33.58 o 1 1 1 80.01 67.68 3.57 o 3 1 1 61.30 85.54 3.52 o 5 1 1 473.94 531.00 19.69 o 7 1 1 1033.78 1000.57 20.40 o 9 1 1 2389.78 2288.62 71.71 o 11 1 1 1.98 8.62 8.69 o 13 1 1 928.26 939.65 35.21 o 15 1 1 10.82 13.42 9.59 o 17 1 1 84.80 87.10 15.02 o -18 2 1 0.71 9.39 12.59 o -16 2 1 59.78 55.75 11.74 o -14 2 1 382.14 345.31 20.20 o -12 2 1 1797.76 1522.68 45.59 o -10 2 1 6621.47 6586.22 156.49 o -8 2 1 268.89 269.87 9.48 o -6 2 1 2386.07 2390.15 47.76 o -4 2 1 12.46 15.89 2.44 o -2 2 1 44456.48 44399.32 738.41 o 0 2 1 19318.87 20355.27 326.51 o 2 2 1 2018.08 2312.80 34.90 o 4 2 1 27201.31 29067.18 466.11 o 6 2 1 754.01 745.21 14.17 o 8 2 1 7744.77 7512.00 111.45 o 10 2 1 63.88 50.27 7.58 o 12 2 1 1196.11 1184.91 86.43 o 14 2 1 98.06 107.45 13.64 o 16 2 1 496.62 449.24 25.19 o 18 2 1 486.78 523.33 30.36 o -19 3 1 139.24 151.87 19.63 o -17 3 1 576.74 567.54 33.50 o -15 3 1 4252.25 3938.96 157.26 o -13 3 1 44.28 48.70 10.73 o -11 3 1 199.25 152.70 19.05 o -9 3 1 379.87 391.11 12.70 o -7 3 1 15315.38 15463.26 248.67 o -5 3 1 10708.14 11553.32 192.30 o -3 3 1 1848.76 1987.81 30.63 o -1 3 1 19302.76 21191.10 395.37 o 1 3 1 1113.60 1114.67 16.29 o 3 3 1 65319.38 65997.27 1054.36 o 5 3 1 7241.51 7464.09 109.53 o 7 3 1 1187.77 1201.57 24.41 o 9 3 1 2671.35 2537.96 47.09 o 11 3 1 2277.46 2251.48 60.29 o 13 3 1 1413.34 1317.43 35.66 o 15 3 1 119.16 131.64 22.09 o 17 3 1 773.69 801.01 35.73 o -18 4 1 30.24 40.66 13.29 o -16 4 1 88.57 71.58 10.57 o -14 4 1 2.77 7.06 7.96 o -12 4 1 5923.41 5684.37 114.67 o -10 4 1 8213.16 8141.11 193.38 o -8 4 1 4376.64 4655.14 80.01 o -6 4 1 2019.48 2064.90 37.55 o -4 4 1 25.30 16.61 3.55 o -2 4 1 47463.72 47325.00 933.05 o 0 4 1 22251.58 22009.38 399.56 o 2 4 1 5805.24 6099.03 100.31 o 4 4 1 3159.38 3212.12 57.37 o 6 4 1 6334.21 6742.04 99.99 o 8 4 1 12958.32 13462.14 196.46 o 10 4 1 3778.76 3677.32 122.31 o 12 4 1 1272.74 1315.20 41.48 o 14 4 1 883.67 818.47 57.34 o 16 4 1 216.71 185.85 18.70 o 18 4 1 20.20 46.97 14.92 o -17 5 1 568.73 586.32 23.09 o -15 5 1 40.42 61.24 9.46 o -13 5 1 1536.03 1369.48 36.45 o -11 5 1 193.46 192.61 14.28 o -9 5 1 1190.93 1153.93 24.59 o -7 5 1 12323.80 12479.92 203.83 o -5 5 1 56110.96 57718.97 918.04 o -3 5 1 22459.78 23353.32 376.16 o -1 5 1 8421.81 8720.53 166.22 o 1 5 1 1808.53 1888.77 30.25 o 3 5 1 32312.98 32910.59 470.77 o 5 5 1 19507.15 20118.37 290.01 o 7 5 1 20005.66 21727.32 313.68 o 9 5 1 656.11 650.60 17.03 o 11 5 1 916.75 867.19 25.87 o 13 5 1 1964.83 1915.87 47.67 o 15 5 1 1271.70 1357.71 89.60 o 17 5 1 19.66 8.66 17.12 o -18 6 1 292.79 302.13 27.22 o -16 6 1 87.11 100.88 11.68 o -14 6 1 1506.98 1530.13 59.01 o -12 6 1 3688.77 3481.37 136.24 o -10 6 1 7201.04 6932.27 117.37 o -8 6 1 13028.29 13832.99 366.14 o -6 6 1 281.25 266.40 7.97 o -4 6 1 3248.44 2781.81 43.33 o -2 6 1 7777.40 7317.10 149.20 o 0 6 1 31294.15 31797.81 514.46 o 2 6 1 15407.26 15294.75 220.97 o 4 6 1 563.22 538.03 11.79 o 6 6 1 2351.25 2501.16 40.52 o 8 6 1 3955.14 3913.24 65.51 o 10 6 1 7733.85 7997.63 135.18 o 12 6 1 2655.32 2651.04 60.75 o 14 6 1 27.24 26.82 8.45 o 16 6 1 0.71 9.53 11.52 o -17 7 1 396.00 435.18 24.89 o -15 7 1 3060.53 3061.72 87.95 o -13 7 1 2707.68 2537.91 71.85 o -11 7 1 296.41 311.77 14.06 o -9 7 1 5343.58 5503.81 94.05 o -7 7 1 1743.99 1632.32 28.32 o -5 7 1 4078.42 3541.80 54.65 o -3 7 1 15687.29 16165.61 262.66 o -1 7 1 485.32 445.21 14.57 o 1 7 1 2530.45 2384.24 45.74 o 3 7 1 3198.09 3050.53 47.73 o 5 7 1 13790.11 13878.29 202.16 o 7 7 1 2566.91 2324.45 38.76 o 9 7 1 40.68 42.65 6.26 o 11 7 1 31.12 37.62 8.34 o 13 7 1 553.61 483.73 20.01 o 15 7 1 1574.60 1673.69 56.89 o 17 7 1 953.72 1046.05 43.19 o -16 8 1 546.97 498.09 31.48 o -14 8 1 449.64 445.89 45.84 o -12 8 1 43.64 44.42 9.00 o -10 8 1 578.71 537.06 15.60 o -8 8 1 7984.53 8746.96 130.16 o -6 8 1 22.48 21.99 4.97 o -4 8 1 4062.92 4176.41 78.14 o -2 8 1 3210.39 3105.08 65.33 o 0 8 1 21876.36 23533.20 383.44 o 2 8 1 15916.29 16459.33 508.01 o 4 8 1 457.04 442.69 11.11 o 6 8 1 461.74 399.91 10.90 o 8 8 1 616.25 619.18 20.55 o 10 8 1 4941.76 5204.06 91.51 o 12 8 1 772.62 829.57 26.68 o 14 8 1 564.67 573.32 22.84 o 16 8 1 4.22 0.00 13.46 o -17 9 1 106.28 117.87 26.09 o -15 9 1 544.53 500.74 30.65 o -13 9 1 873.49 849.35 38.52 o -11 9 1 139.13 116.79 12.96 o -9 9 1 792.80 818.00 23.83 o -7 9 1 83.28 62.19 7.21 o -5 9 1 7108.22 7383.63 124.74 o -3 9 1 7924.50 8273.21 138.52 o -1 9 1 29.46 40.03 7.21 o 1 9 1 866.67 861.98 20.59 o 3 9 1 1366.87 1308.44 23.77 o 5 9 1 5787.52 6165.90 93.64 o 7 9 1 5713.36 6106.62 119.25 o 9 9 1 84.62 93.29 9.92 o 11 9 1 33.04 44.36 8.79 o 13 9 1 53.61 43.59 11.44 o 15 9 1 566.45 551.99 44.46 o -16 10 1 31.14 30.22 19.88 o -14 10 1 126.79 112.65 13.94 o -12 10 1 376.67 359.90 20.76 o -10 10 1 1.21 0.00 7.05 o -8 10 1 782.72 824.07 20.89 o -6 10 1 0.03 0.00 5.37 o -4 10 1 4.86 0.00 5.23 o -2 10 1 216.16 222.61 13.95 o 0 10 1 1642.89 1662.10 40.71 o 2 10 1 1735.97 1810.47 42.97 o 4 10 1 7.13 0.00 4.44 o 6 10 1 238.65 217.92 10.55 o 8 10 1 41.14 42.63 6.61 o 10 10 1 289.07 264.67 16.17 o 12 10 1 26.80 48.79 12.70 o 14 10 1 53.96 40.03 11.81 o -15 11 1 7.84 6.79 11.48 o -13 11 1 7.40 7.90 10.58 o -11 11 1 8.73 18.86 10.44 o -9 11 1 30.87 19.44 7.49 o -7 11 1 197.93 177.44 9.56 o -5 11 1 6.24 2.14 9.82 o -3 11 1 7.27 6.81 5.39 o -1 11 1 1607.88 1656.87 40.83 o 1 11 1 382.00 360.83 13.44 o 3 11 1 392.64 380.67 15.67 o 5 11 1 181.76 178.14 29.95 o 7 11 1 30.08 32.59 7.94 o 9 11 1 0.37 0.00 7.11 o 11 11 1 36.46 31.11 21.40 o 13 11 1 4.02 5.96 20.16 o 15 11 1 27.35 45.02 13.53 o -14 12 1 102.53 92.24 14.43 o -12 12 1 43.38 52.65 12.69 o -10 12 1 11.32 13.40 8.56 o -8 12 1 115.96 126.16 8.93 o -6 12 1 120.55 119.78 14.04 o -4 12 1 1659.95 1595.83 40.59 o -2 12 1 876.91 819.44 25.62 o 0 12 1 3622.35 3534.77 77.01 o 2 12 1 3702.04 3622.94 78.64 o 4 12 1 147.34 149.27 10.73 o 6 12 1 19.73 19.61 7.29 o 8 12 1 1.69 0.00 8.41 o 10 12 1 53.32 57.04 18.78 o 12 12 1 69.18 50.53 18.50 o 14 12 1 0.45 0.00 13.53 o -13 13 1 500.95 564.41 41.97 o -11 13 1 26.93 43.47 10.73 o -9 13 1 466.12 495.89 24.58 o -7 13 1 281.44 307.91 15.46 o -5 13 1 1688.66 1714.60 43.64 o -3 13 1 2682.24 2581.94 60.07 o -1 13 1 164.05 157.17 11.73 o 1 13 1 601.05 555.56 21.30 o 3 13 1 994.80 1027.77 45.30 o 5 13 1 2070.43 2058.93 50.20 o 7 13 1 525.10 548.58 20.61 o 9 13 1 181.29 170.42 15.60 o 11 13 1 26.18 45.84 18.22 o 13 13 1 24.77 0.00 16.57 o -14 14 1 416.65 405.36 35.34 o -12 14 1 905.13 938.57 54.67 o -10 14 1 1591.58 1503.14 50.43 o -8 14 1 1858.97 1856.87 58.18 o -6 14 1 29.70 21.72 8.27 o -4 14 1 814.98 788.70 26.31 o -2 14 1 126.25 144.27 11.86 o 0 14 1 153.18 146.91 16.21 o 2 14 1 41.80 49.19 9.55 o 4 14 1 724.34 702.05 24.43 o 6 14 1 296.57 316.88 20.53 o 8 14 1 495.48 503.83 25.28 o 10 14 1 1272.95 1311.50 59.64 o 12 14 1 343.59 340.47 31.76 o -13 15 1 284.13 313.13 33.41 o -11 15 1 60.57 59.05 14.63 o -9 15 1 606.07 583.19 28.87 o -7 15 1 1882.79 1886.42 48.83 o -5 15 1 1337.69 1322.33 37.82 o -3 15 1 1034.94 1090.40 33.08 o -1 15 1 242.40 240.97 15.34 o 1 15 1 754.42 732.60 32.41 o 3 15 1 159.73 153.04 17.52 o 5 15 1 1449.91 1489.56 59.51 o 7 15 1 388.68 411.23 18.91 o 9 15 1 33.46 37.78 11.39 o 11 15 1 14.25 17.67 17.67 o -10 16 1 596.10 656.01 37.28 o -8 16 1 118.44 155.33 37.55 o -6 16 1 39.78 45.59 10.03 o -4 16 1 698.35 725.64 40.62 o -2 16 1 2494.36 2577.91 69.76 o 0 16 1 3903.24 4077.70 112.95 o 2 16 1 2360.80 2365.15 59.13 o 4 16 1 172.57 193.07 14.84 o 6 16 1 155.38 156.96 13.23 o 8 16 1 610.53 629.64 30.05 o 10 16 1 199.89 263.30 53.43 o -9 17 1 97.88 130.11 29.96 o -7 17 1 1250.15 1276.59 38.68 o -5 17 1 868.11 892.83 30.86 o -3 17 1 588.88 585.96 24.12 o -1 17 1 149.87 135.04 16.71 o 1 17 1 478.63 481.36 31.62 o 3 17 1 1918.15 1858.22 52.62 o 5 17 1 945.94 950.66 35.39 o 7 17 1 136.43 157.04 13.57 o 9 17 1 61.26 55.83 13.99 o -8 18 1 127.19 125.63 17.72 o -6 18 1 18.69 31.23 10.66 o -4 18 1 219.33 224.07 16.95 o -2 18 1 1163.89 1210.32 38.57 o 0 18 1 492.29 546.03 59.78 o 2 18 1 194.17 225.51 20.21 o 4 18 1 28.98 39.35 11.53 o 6 18 1 43.43 37.96 11.34 o -5 19 1 342.36 336.56 22.92 o -3 19 1 30.46 50.53 12.67 o -1 19 1 4.80 0.00 12.46 o 1 19 1 47.33 62.67 14.39 o 3 19 1 143.73 132.91 17.73 o 5 19 1 104.33 121.18 14.13 o 0 20 1 2.10 9.95 11.50 o -18 0 2 335.38 286.62 29.55 o -16 0 2 1928.64 1902.82 82.29 o -14 0 2 3685.32 3364.93 125.64 o -12 0 2 3331.09 3009.55 111.56 o -10 0 2 1517.99 1362.71 56.88 o -8 0 2 2198.77 3420.16 118.74 o -6 0 2 5170.73 5778.77 134.14 o -4 0 2 29497.56 31262.77 705.12 o -2 0 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