#------------------------------------------------------------------------------ #$Date: 2009-05-03 21:56:13 +0300 (Sun, 03 May 2009) $ #$Revision: 691 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2218717.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2218717_Fobs loop_ _publ_author_name 'Nimthong, Ruthairat' 'Pakawatchai, Chaveng' 'Saithong, Saowanit' 'Charmant, Jonathan P. H.' _publ_section_title ; Iodido(N-phenylthiourea)bis(triphenylphosphine)copper(I) ; _journal_coeditor_code HG2408 _journal_issue 7 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m977 _journal_volume 64 _journal_year 2008 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 67.422 _cell_angle_beta 77.215 _cell_angle_gamma 73.224 _cell_length_a 10.9505 _cell_length_b 18.7294 _cell_length_c 21.3731 _exptl_crystal_F_000 1752.00 _reflns_d_resolution_high 0.8000 _[local]_cod_data_source_file hg2408Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' rl001-p-1 in P-1' _shelx_refln_list_code 4 _shelx_F_calc_maximum 648.26 _shelx_F_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 392.38 382.83 23.54 o 2 0 0 1327.21 1432.42 95.38 o 3 0 0 84071.81 77738.46 1859.21 o 4 0 0 22.63 -65.10 65.10 o 5 0 0 1906.76 1595.45 113.88 o 6 0 0 18.25 31.01 123.35 o 7 0 0 193.49 562.74 124.20 o 8 0 0 9073.50 9157.33 395.37 o 9 0 0 7568.72 7996.88 384.57 o 10 0 0 3165.02 3560.72 274.94 o 11 0 0 25.01 86.83 258.85 o 12 0 0 2066.92 2302.80 390.21 o 13 0 0 103.63 94.79 423.47 o -12 1 0 2.97 77.35 369.31 o -11 1 0 44.48 176.49 261.39 o -10 1 0 2027.70 2351.58 327.42 o -9 1 0 3.04 -197.98 197.98 o -8 1 0 10379.59 10575.60 427.96 o -7 1 0 977.25 792.92 124.34 o -6 1 0 3514.83 3403.35 192.90 o -5 1 0 21323.97 20377.39 555.86 o -4 1 0 17685.07 15838.36 433.95 o -3 1 0 28596.54 27226.19 679.95 o -2 1 0 313.09 359.33 44.41 o -1 1 0 75222.33 70927.19 1677.52 o 0 1 0 3762.09 -45.07 45.07 o 1 1 0 69472.11 70886.10 1686.05 o 2 1 0 585.23 754.78 99.23 o 3 1 0 73.45 193.42 119.24 o 4 1 0 80685.05 79408.13 1909.61 o 5 1 0 18884.24 18036.09 647.68 o 6 1 0 199.15 216.03 94.99 o 7 1 0 20769.36 20520.14 579.05 o 8 1 0 3709.93 4061.65 274.04 o 9 1 0 84.95 -8.68 210.07 o 10 1 0 248.85 381.68 226.26 o 11 1 0 52.18 -268.74 315.23 o 12 1 0 5.64 -300.70 366.57 o 13 1 0 1254.62 1566.51 422.14 o -12 2 0 2793.05 2883.59 779.12 o -11 2 0 1342.38 881.78 459.24 o -10 2 0 899.56 899.83 241.12 o -9 2 0 13934.55 13503.84 532.42 o -8 2 0 6228.60 6275.52 334.00 o -7 2 0 285.22 424.71 126.56 o -6 2 0 8953.49 8284.77 295.04 o -5 2 0 283.14 358.67 105.84 o -4 2 0 6912.46 6309.91 243.00 o -3 2 0 28778.80 26658.29 671.54 o -2 2 0 63867.79 62594.55 1501.27 o -1 2 0 4091.46 3805.86 147.29 o 0 2 0 90681.92 98782.65 2761.65 o 1 2 0 1262.42 1233.71 54.42 o 2 2 0 125.81 97.91 32.53 o 3 2 0 22198.68 22966.24 580.31 o 4 2 0 26219.55 25958.75 665.52 o 5 2 0 4176.60 4320.15 183.52 o 6 2 0 2142.72 2432.52 149.86 o 7 2 0 2580.28 2454.96 165.76 o 8 2 0 13854.98 14001.07 514.46 o 9 2 0 1479.26 1634.12 208.97 o 10 2 0 57.99 185.51 234.24 o 11 2 0 769.50 491.79 437.48 o 12 2 0 1147.11 1461.93 656.21 o 13 2 0 188.31 -43.78 412.17 o -12 3 0 401.79 -76.33 408.03 o -11 3 0 169.30 410.39 350.59 o -10 3 0 169.31 85.99 239.69 o -9 3 0 731.41 726.98 211.50 o -8 3 0 23386.49 21637.64 726.51 o -7 3 0 3244.49 3499.56 274.76 o -6 3 0 38.84 95.48 111.03 o -5 3 0 55089.99 51448.01 1417.44 o -4 3 0 13039.63 11173.10 334.46 o -3 3 0 19120.27 18847.32 493.54 o -2 3 0 8035.53 8401.37 239.17 o -1 3 0 1172.52 1174.47 83.92 o 0 3 0 3671.99 3724.87 145.39 o 1 3 0 11955.27 12980.09 392.47 o 2 3 0 63826.94 67733.84 1619.07 o 3 3 0 4925.36 4879.07 160.57 o 4 3 0 51460.13 49972.29 1223.81 o 5 3 0 20711.47 20731.35 557.00 o 6 3 0 2311.37 2194.26 181.61 o 7 3 0 4189.67 4057.55 224.15 o 8 3 0 593.16 819.24 168.93 o 9 3 0 1059.04 1409.64 400.02 o 10 3 0 25.16 331.21 276.51 o 11 3 0 14.51 -313.25 313.25 o 12 3 0 601.20 443.73 362.37 o 13 3 0 751.14 219.50 409.48 o -12 4 0 2243.20 2495.49 445.75 o -11 4 0 2518.48 2705.03 399.50 o -10 4 0 523.63 603.55 316.62 o -9 4 0 8036.09 7790.24 499.05 o -8 4 0 11516.39 11556.39 470.82 o -7 4 0 3671.01 3596.04 213.31 o -6 4 0 468.97 352.36 119.27 o -5 4 0 4673.15 4867.93 476.73 o -4 4 0 1263.33 1043.89 107.65 o -3 4 0 9545.97 9326.64 280.02 o -2 4 0 4228.29 3718.73 276.40 o -1 4 0 25811.66 26259.41 1403.92 o 0 4 0 65189.66 71387.73 2021.42 o 1 4 0 6299.32 6334.69 242.96 o 2 4 0 30.69 128.86 42.18 o 3 4 0 20091.91 20154.42 520.44 o 4 4 0 5761.88 5944.90 200.91 o 5 4 0 2340.79 2645.72 144.49 o 6 4 0 5348.92 5270.89 217.70 o 7 4 0 40.51 125.36 108.99 o 8 4 0 7697.06 7348.51 352.56 o 9 4 0 5126.23 5325.94 316.76 o 10 4 0 80.34 133.08 276.51 o 11 4 0 479.28 306.91 314.86 o 12 4 0 624.70 951.37 691.63 o 13 4 0 53.16 122.91 735.38 o -11 5 0 12.29 -115.49 367.38 o -10 5 0 606.15 858.77 329.81 o -9 5 0 49.50 201.15 366.65 o -8 5 0 8354.89 8552.53 500.61 o -7 5 0 17253.55 15998.30 499.85 o -6 5 0 1391.46 1456.93 143.51 o -5 5 0 37943.21 34676.93 949.67 o -4 5 0 26911.69 24914.57 656.67 o -3 5 0 3525.19 3804.48 426.08 o -2 5 0 13.85 102.27 108.47 o -1 5 0 7824.49 8026.31 382.42 o 0 5 0 74.00 54.72 77.45 o 1 5 0 9161.83 9199.25 261.97 o 2 5 0 23193.17 23918.03 608.05 o 3 5 0 22321.13 22960.52 590.86 o 4 5 0 10573.17 10986.41 324.94 o 5 5 0 12348.33 12697.18 372.20 o 6 5 0 12458.17 13352.75 395.50 o 7 5 0 3214.18 3615.56 194.81 o 8 5 0 1687.65 1828.08 371.96 o 9 5 0 917.72 1564.00 269.27 o 10 5 0 1916.25 1857.10 298.76 o 11 5 0 18.45 -278.66 321.38 o 12 5 0 160.38 -366.07 366.07 o 13 5 0 27.79 144.49 407.39 o -11 6 0 2459.47 1791.37 399.50 o -10 6 0 3377.14 3351.81 393.30 o -9 6 0 806.03 555.17 288.84 o -8 6 0 6624.67 7096.83 456.62 o -7 6 0 4070.36 4063.57 298.84 o -6 6 0 178.20 51.96 130.03 o -5 6 0 5007.65 4712.97 286.86 o -4 6 0 639.91 772.61 126.14 o -3 6 0 38204.41 36596.95 1117.48 o -2 6 0 7168.94 6813.74 285.95 o -1 6 0 12049.46 13323.42 449.79 o 0 6 0 39593.47 42445.66 1246.70 o 1 6 0 17367.42 17864.93 477.11 o 2 6 0 8153.90 8520.42 258.16 o 3 6 0 3769.08 4234.51 298.28 o 4 6 0 3727.39 3763.10 165.81 o 5 6 0 262.55 510.90 96.82 o 6 6 0 8161.96 8597.40 287.87 o 7 6 0 2050.67 2269.41 143.45 o 8 6 0 192.00 427.70 165.94 o 9 6 0 2419.85 2538.67 354.15 o 10 6 0 170.73 91.40 324.98 o 11 6 0 525.34 494.29 322.63 o 12 6 0 92.47 -193.82 367.38 o 13 6 0 13.60 204.83 417.85 o -11 7 0 144.86 264.90 403.49 o -10 7 0 585.13 787.71 357.87 o -9 7 0 1536.83 1132.06 311.62 o -8 7 0 372.67 227.57 269.32 o -7 7 0 8410.96 7638.79 393.76 o -6 7 0 4955.62 4837.37 311.08 o -5 7 0 2397.96 2383.16 325.06 o -4 7 0 18162.33 17444.76 607.02 o -3 7 0 25925.39 26030.60 835.66 o -2 7 0 5.44 99.81 148.33 o -1 7 0 350.68 860.46 170.41 o 0 7 0 10107.04 11422.13 740.91 o 1 7 0 23349.95 23858.66 621.10 o 2 7 0 5225.37 5305.76 198.25 o 3 7 0 13350.20 14752.30 418.10 o 4 7 0 8886.01 8983.39 286.79 o 5 7 0 4242.31 4290.90 206.12 o 6 7 0 9338.39 9324.20 306.97 o 7 7 0 34.90 -31.77 103.46 o 8 7 0 6.58 -41.98 139.46 o 9 7 0 2396.89 2479.63 320.11 o 10 7 0 12.24 390.52 292.45 o 11 7 0 171.38 42.64 324.48 o 12 7 0 276.39 116.11 402.06 o 13 7 0 33.08 -169.70 423.14 o -10 8 0 856.65 726.87 378.57 o -9 8 0 1608.78 1819.51 612.47 o -8 8 0 3311.32 3674.57 406.23 o -7 8 0 2236.00 2132.23 235.23 o -6 8 0 2022.13 1958.51 201.70 o -5 8 0 61.19 140.99 157.30 o -4 8 0 100.91 315.17 140.00 o -3 8 0 23204.83 21332.06 711.17 o -2 8 0 49992.62 51600.88 1542.80 o -1 8 0 314.64 385.42 178.24 o 0 8 0 8773.10 8963.88 469.96 o 1 8 0 48043.34 50734.10 1458.14 o 2 8 0 14.60 70.35 75.46 o 3 8 0 1820.79 1816.34 123.59 o 4 8 0 844.92 978.07 90.30 o 5 8 0 2853.91 3005.16 161.68 o 6 8 0 2554.79 2728.33 158.97 o 7 8 0 489.65 635.42 129.30 o 8 8 0 566.54 325.38 146.77 o 9 8 0 1414.86 1345.82 279.89 o 10 8 0 51.06 477.70 295.90 o 11 8 0 3.70 493.82 343.46 o 12 8 0 17.87 -277.99 520.81 o 13 8 0 35.65 -428.20 428.20 o -10 9 0 239.53 771.87 392.90 o -9 9 0 351.27 315.39 341.60 o -8 9 0 1216.22 1296.52 300.68 o -7 9 0 11280.58 10095.29 551.91 o -6 9 0 10605.81 10788.39 488.03 o -5 9 0 6199.25 5186.58 320.94 o -4 9 0 10950.12 10364.34 433.39 o -3 9 0 16287.88 15117.89 552.63 o -2 9 0 328.63 153.42 120.34 o -1 9 0 977.96 1116.86 199.29 o 0 9 0 28731.14 29843.66 936.50 o 1 9 0 31519.16 32730.30 1008.47 o 2 9 0 5621.18 5664.60 238.65 o 3 9 0 207.02 178.22 83.73 o 4 9 0 2251.60 1894.06 133.40 o 5 9 0 9094.62 8828.50 300.49 o 6 9 0 3096.54 2915.09 172.64 o 7 9 0 26.65 52.50 131.25 o 8 9 0 1258.03 1258.33 180.32 o 9 9 0 448.66 165.31 270.16 o 10 9 0 32.34 -86.09 310.40 o 11 9 0 900.82 745.79 599.97 o 12 9 0 110.64 546.00 660.38 o 13 9 0 272.81 187.38 466.64 o -10 10 0 83.64 -417.85 417.85 o -9 10 0 604.98 967.37 359.10 o -8 10 0 8218.42 8622.76 574.47 o -7 10 0 43.60 -123.96 449.53 o -6 10 0 1667.51 1438.65 221.01 o -5 10 0 801.76 1068.98 195.72 o -4 10 0 527.67 400.36 165.88 o -3 10 0 11155.06 11110.84 451.69 o -2 10 0 10843.35 10203.92 429.22 o -1 10 0 84.14 179.63 128.23 o 0 10 0 12032.01 12359.61 468.53 o 1 10 0 31595.47 33311.31 1034.75 o 2 10 0 359.78 327.63 92.18 o 3 10 0 598.16 599.39 107.04 o 4 10 0 3728.49 3629.90 187.38 o 5 10 0 11.92 -98.93 98.93 o 6 10 0 3362.36 3123.56 183.49 o 7 10 0 667.69 763.62 148.05 o 8 10 0 1.76 -3.17 159.56 o 9 10 0 431.93 397.35 274.30 o 10 10 0 189.52 -6.50 410.39 o 11 10 0 62.07 -95.95 356.50 o 12 10 0 4.36 382.93 400.40 o -9 11 0 45.85 326.11 574.97 o -8 11 0 1603.21 1016.63 345.71 o -7 11 0 12316.31 11296.25 615.50 o -6 11 0 1974.14 2555.19 415.68 o -5 11 0 1751.36 1959.49 389.19 o -4 11 0 8763.87 9331.12 431.11 o -3 11 0 7430.59 7128.77 356.60 o -2 11 0 23.48 -0.67 150.94 o -1 11 0 296.01 93.14 140.72 o 0 11 0 2359.04 2408.11 190.47 o 1 11 0 14210.37 14914.81 538.97 o 2 11 0 9633.89 10253.25 342.51 o 3 11 0 119.99 8.14 100.65 o 4 11 0 6.84 6.90 101.54 o 5 11 0 8920.23 9032.61 317.63 o 6 11 0 510.74 529.34 147.02 o 7 11 0 497.09 527.97 204.97 o 8 11 0 87.49 144.49 165.58 o 9 11 0 67.88 111.30 289.15 o 10 11 0 17.06 -299.56 577.05 o 11 11 0 98.36 -180.91 364.74 o 12 11 0 105.58 -308.20 420.54 o -9 12 0 532.08 192.94 687.46 o -8 12 0 7465.64 7375.59 616.63 o -7 12 0 139.16 67.29 320.98 o -6 12 0 703.53 1237.00 266.24 o -5 12 0 2121.17 1809.60 310.00 o -4 12 0 4431.36 4714.34 326.48 o -3 12 0 6600.08 7011.06 373.65 o -2 12 0 12985.54 13196.40 534.00 o -1 12 0 713.63 704.86 314.43 o 0 12 0 10094.00 10445.77 465.60 o 1 12 0 19722.88 21416.06 731.17 o 2 12 0 754.77 905.37 144.69 o 3 12 0 339.11 448.84 134.11 o 4 12 0 3917.19 3954.00 212.79 o 5 12 0 20.75 12.42 127.49 o 6 12 0 2394.38 2252.51 202.81 o 7 12 0 588.29 520.32 165.16 o 8 12 0 727.24 705.54 181.35 o 9 12 0 51.91 609.64 472.89 o 10 12 0 53.46 460.38 337.34 o 11 12 0 13.18 -72.80 382.58 o 12 12 0 190.22 782.18 666.63 o -8 13 0 656.08 890.64 390.35 o -7 13 0 10587.66 10433.22 645.09 o -6 13 0 426.41 423.71 266.65 o -5 13 0 64.47 -15.43 237.59 o -4 13 0 11821.68 11462.13 512.06 o -3 13 0 3662.78 3436.75 282.83 o -2 13 0 546.14 450.01 181.85 o -1 13 0 145.77 250.32 168.93 o 0 13 0 150.07 392.79 149.79 o 1 13 0 12099.05 13021.66 835.37 o 2 13 0 23.09 197.93 140.30 o 3 13 0 1708.11 1628.76 200.86 o 4 13 0 5512.21 5378.28 266.41 o 5 13 0 995.12 1403.66 218.89 o 6 13 0 1032.33 953.82 179.33 o 7 13 0 67.84 -93.52 176.86 o 8 13 0 602.36 812.13 195.42 o 9 13 0 24.21 202.99 310.33 o 10 13 0 81.11 363.51 352.38 o 11 13 0 3.16 -111.37 399.73 o 12 13 0 276.50 236.28 444.30 o -7 14 0 737.25 425.52 319.07 o -6 14 0 1799.88 1961.23 477.00 o -5 14 0 669.07 510.76 262.30 o -4 14 0 463.98 256.14 236.99 o -3 14 0 4351.58 3971.15 296.99 o -2 14 0 8330.47 8947.17 443.40 o -1 14 0 245.62 164.61 230.30 o 0 14 0 12272.40 13189.32 726.32 o 1 14 0 3511.95 3613.88 268.31 o 2 14 0 174.95 55.20 154.90 o 3 14 0 6135.24 6562.65 331.20 o 4 14 0 885.66 941.02 144.07 o 5 14 0 326.30 108.51 171.80 o 6 14 0 539.42 606.95 237.33 o 7 14 0 9.26 226.67 190.60 o 8 14 0 7.13 31.86 203.06 o 9 14 0 44.98 233.06 326.28 o 10 14 0 161.55 470.38 385.40 o 11 14 0 14.94 -21.60 411.21 o -7 15 0 3157.95 3359.08 570.80 o -6 15 0 1623.61 1534.88 621.03 o -5 15 0 1002.15 813.33 288.25 o -4 15 0 2446.98 2649.52 296.51 o -3 15 0 5533.42 5583.63 437.85 o -2 15 0 97.30 124.42 217.30 o -1 15 0 535.65 615.10 221.32 o 0 15 0 262.68 397.04 180.47 o 1 15 0 1635.16 1801.50 202.43 o 2 15 0 1161.69 1659.28 231.02 o 3 15 0 6.96 -54.63 164.28 o 4 15 0 232.19 444.01 217.06 o 5 15 0 820.31 473.57 189.65 o 6 15 0 100.81 77.71 314.89 o 7 15 0 456.59 315.57 203.94 o 8 15 0 32.94 472.55 218.69 o 9 15 0 737.98 1074.94 345.32 o 10 15 0 172.74 211.46 378.35 o 11 15 0 319.93 856.94 434.26 o -6 16 0 255.60 392.28 344.01 o -5 16 0 1.58 -176.91 364.04 o -4 16 0 949.26 1150.22 284.58 o -3 16 0 533.31 1164.58 258.52 o -2 16 0 5991.73 5552.92 393.57 o -1 16 0 348.19 650.43 212.46 o 0 16 0 474.32 543.55 205.47 o 1 16 0 4213.81 4455.03 327.14 o 2 16 0 386.40 131.02 185.32 o 3 16 0 4.42 203.32 178.15 o 4 16 0 60.82 269.17 233.09 o 5 16 0 1.28 -16.48 233.54 o 6 16 0 47.02 -3.68 231.88 o 7 16 0 120.53 217.05 217.87 o 8 16 0 35.38 0.42 269.18 o 9 16 0 251.85 572.38 362.10 o 10 16 0 675.23 963.86 400.40 o -5 17 0 3909.12 3250.64 355.36 o -4 17 0 1471.09 1664.25 306.10 o -3 17 0 808.71 1181.44 288.63 o -2 17 0 429.37 755.85 248.99 o -1 17 0 668.79 699.46 234.11 o 0 17 0 308.72 828.76 274.07 o 1 17 0 2.70 38.48 209.95 o 2 17 0 2085.74 2671.73 272.27 o 3 17 0 960.43 665.65 262.15 o 4 17 0 640.94 477.06 259.21 o 5 17 0 138.19 20.11 254.52 o 6 17 0 165.12 -258.63 258.63 o 7 17 0 13.82 -289.46 397.90 o 8 17 0 316.64 207.37 252.28 o 9 17 0 86.27 381.01 637.47 o 10 17 0 21.08 614.54 427.46 o -4 18 0 1329.44 955.49 336.27 o -3 18 0 188.32 363.90 281.53 o -2 18 0 2471.74 2952.16 317.46 o -1 18 0 2640.49 2800.00 296.61 o 0 18 0 1.43 298.29 244.89 o 1 18 0 2598.57 3012.97 285.22 o 2 18 0 135.27 89.14 298.15 o 3 18 0 791.05 997.01 414.56 o 4 18 0 52.25 227.71 464.56 o 5 18 0 2.55 13.33 281.07 o 6 18 0 47.38 -147.58 277.61 o 7 18 0 9.97 -13.90 286.17 o 8 18 0 84.53 286.53 303.23 o 9 18 0 382.48 2.12 410.41 o -3 19 0 927.83 1081.23 333.60 o -2 19 0 482.92 873.33 300.00 o -1 19 0 2184.99 1907.14 571.29 o 0 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