#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/87/2218720.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2218720_Fobs loop_ _publ_author_name 'Knapp, Warren R.' 'LaDuca, Robert L.' _publ_section_title ; Di-4-pyridylmethanediol ; _journal_coeditor_code HG2417 _journal_issue 7 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o1347 _journal_volume 64 _journal_year 2008 _space_group_IT_number 96 _symmetry_space_group_name_Hall 'P 4nw 2abw' _symmetry_space_group_name_H-M 'P 43 21 2' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 7.6130 _cell_length_b 7.6130 _cell_length_c 17.5864 _exptl_crystal_F_000 424.00 _reflns_d_resolution_high 0.8307 _[local]_cod_data_source_file hg2417Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' tet in P4(3)2(1)2' _shelx_refln_list_code 4 _shelx_F_calc_maximum 91.69 _shelx_F_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, z+1/2' '-y+1/2, x+1/2, z+3/4' 'y+1/2, -x+1/2, z+1/4' '-x+1/2, y+1/2, -z+3/4' 'x+1/2, -y+1/2, -z+1/4' 'y, x, -z' '-y, -x, -z+1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 1 0 5.05 4.56 0.32 o 0 2 0 128.70 118.78 1.70 o 1 2 0 372.77 332.22 2.09 o 2 2 0 11.33 11.46 0.60 o 1 3 0 995.25 1034.56 6.10 o 2 3 0 3.15 3.28 0.36 o 3 3 0 1252.96 1281.44 10.33 o 0 4 0 496.28 534.43 5.57 o 1 4 0 292.59 281.08 2.59 o 2 4 0 481.40 516.76 3.82 o 3 4 0 52.98 52.27 1.80 o 4 4 0 17.33 19.58 1.82 o 1 5 0 45.17 43.25 1.19 o 2 5 0 165.68 155.38 2.66 o 3 5 0 423.53 416.07 5.15 o 4 5 0 416.24 422.15 5.43 o 5 5 0 1328.90 1355.93 20.93 o 0 6 0 7.75 6.48 1.27 o 1 6 0 288.83 294.99 4.13 o 2 6 0 0.00 0.63 0.83 o 3 6 0 46.86 41.01 2.09 o 4 6 0 44.59 47.30 2.36 o 5 6 0 2.70 0.89 1.43 o 6 6 0 5.17 2.56 3.45 o 1 7 0 29.95 27.14 1.69 o 2 7 0 100.00 93.61 2.86 o 3 7 0 189.74 198.31 4.72 o 4 7 0 11.55 13.23 1.97 o 5 7 0 24.91 23.47 3.01 o 0 8 0 152.28 144.67 5.28 o 1 8 0 51.29 53.05 2.64 o 2 8 0 0.39 3.31 1.69 o 3 8 0 63.33 54.04 3.88 o 4 8 0 38.48 40.50 4.50 o 1 9 0 30.90 38.12 4.35 o 0 1 1 523.85 528.92 2.83 o 1 1 1 1094.52 1052.95 4.97 o 0 2 1 8406.25 8068.45 40.56 o 1 2 1 727.52 684.28 2.70 o 2 2 1 11.49 10.19 0.41 o 0 3 1 0.48 0.01 0.27 o 1 3 1 608.77 623.07 2.83 o 2 3 1 703.52 698.83 3.05 o 3 3 1 554.04 552.38 3.80 o 0 4 1 419.37 437.13 3.42 o 1 4 1 957.57 958.41 4.11 o 2 4 1 41.56 45.25 0.69 o 3 4 1 62.32 61.64 1.22 o 4 4 1 10.35 10.96 1.05 o 0 5 1 89.91 86.70 1.41 o 1 5 1 94.17 87.60 1.17 o 2 5 1 112.78 110.95 1.60 o 3 5 1 397.70 394.47 3.34 o 4 5 1 29.12 28.73 1.08 o 5 5 1 0.15 0.84 1.06 o 0 6 1 16.21 13.52 1.04 o 1 6 1 134.81 130.40 1.87 o 2 6 1 101.94 99.39 1.74 o 3 6 1 88.38 85.14 1.95 o 4 6 1 49.35 51.15 1.78 o 5 6 1 70.34 73.40 2.37 o 6 6 1 420.74 457.64 10.12 o 0 7 1 53.71 37.58 2.07 o 1 7 1 43.66 47.29 1.54 o 2 7 1 19.18 21.00 1.44 o 3 7 1 24.37 19.61 1.37 o 4 7 1 16.46 15.40 1.43 o 5 7 1 91.86 97.41 3.44 o 0 8 1 0.34 -0.20 1.19 o 1 8 1 63.85 54.50 1.87 o 2 8 1 29.83 34.55 2.03 o 3 8 1 2.00 1.06 1.40 o 4 8 1 4.39 4.51 2.01 o 0 9 1 21.35 23.13 4.11 o 1 9 1 46.81 50.45 3.35 o 0 1 2 6676.10 6242.54 29.02 o 1 1 2 2480.34 2326.46 10.62 o 0 2 2 2135.69 1953.70 9.76 o 1 2 2 381.57 372.02 1.63 o 2 2 2 650.06 589.74 3.49 o 0 3 2 4704.98 4819.10 24.62 o 1 3 2 319.36 344.29 1.82 o 2 3 2 233.93 224.20 1.44 o 3 3 2 12.79 15.46 0.67 o 0 4 2 20.57 26.80 0.81 o 1 4 2 164.23 181.20 1.34 o 2 4 2 1.47 2.43 0.33 o 3 4 2 169.10 171.10 1.97 o 4 4 2 15.39 16.02 1.16 o 0 5 2 0.08 0.15 0.52 o 1 5 2 404.62 403.17 2.93 o 2 5 2 204.17 212.72 2.15 o 3 5 2 45.58 42.89 1.18 o 4 5 2 373.04 367.17 3.66 o 5 5 2 230.22 225.16 4.62 o 0 6 2 72.90 70.06 1.78 o 1 6 2 48.92 50.06 1.22 o 2 6 2 37.34 36.67 1.28 o 3 6 2 5.30 4.70 0.77 o 4 6 2 231.13 237.73 3.39 o 5 6 2 116.29 126.98 2.95 o 6 6 2 67.84 67.84 4.81 o 0 7 2 17.11 17.08 1.65 o 1 7 2 15.08 11.05 0.99 o 2 7 2 18.98 18.57 1.25 o 3 7 2 17.43 14.37 1.28 o 4 7 2 2.43 1.79 1.06 o 5 7 2 52.48 57.33 3.02 o 0 8 2 32.93 33.02 2.53 o 1 8 2 51.93 50.02 1.96 o 2 8 2 59.89 54.99 2.39 o 3 8 2 115.54 120.59 3.56 o 4 8 2 12.67 15.46 2.32 o 0 9 2 14.00 12.66 3.48 o 1 9 2 39.45 45.05 3.44 o 0 1 3 2329.80 2221.26 10.50 o 1 1 3 1058.46 1036.55 5.34 o 0 2 3 975.37 913.52 5.33 o 1 2 3 2220.93 2191.94 7.37 o 2 2 3 114.02 127.92 1.36 o 0 3 3 2078.27 2083.49 11.70 o 1 3 3 328.80 346.19 1.82 o 2 3 3 1205.83 1263.34 4.95 o 3 3 3 173.69 181.92 1.93 o 0 4 3 6.71 7.66 0.56 o 1 4 3 142.88 144.08 1.25 o 2 4 3 180.18 192.27 1.54 o 3 4 3 220.51 213.30 2.21 o 4 4 3 63.43 63.74 1.91 o 0 5 3 40.57 39.60 1.18 o 1 5 3 44.87 43.90 1.04 o 2 5 3 25.07 26.59 0.89 o 3 5 3 93.26 92.39 2.11 o 4 5 3 159.28 163.92 2.37 o 5 5 3 20.46 18.29 1.83 o 0 6 3 59.82 60.94 2.23 o 1 6 3 127.32 123.30 1.92 o 2 6 3 80.64 81.57 1.66 o 3 6 3 495.73 504.29 4.51 o 4 6 3 69.43 74.56 2.17 o 5 6 3 161.30 169.80 3.25 o 6 6 3 207.92 219.88 7.96 o 0 7 3 4.04 6.26 1.25 o 1 7 3 22.43 17.93 1.12 o 2 7 3 46.37 46.47 1.83 o 3 7 3 18.86 18.58 1.32 o 4 7 3 53.49 54.66 2.11 o 5 7 3 8.96 9.32 1.74 o 0 8 3 0.29 1.18 1.45 o 1 8 3 83.11 82.24 2.50 o 2 8 3 16.18 10.90 1.58 o 3 8 3 14.43 12.98 1.75 o 4 8 3 25.17 27.42 2.77 o 0 9 3 8.32 11.35 2.73 o 1 9 3 2.66 5.19 2.21 o 0 0 4 6470.78 6095.54 50.71 o 0 1 4 4500.58 4341.95 19.76 o 1 1 4 769.07 720.16 3.95 o 0 2 4 416.33 409.71 2.74 o 1 2 4 167.62 178.00 1.16 o 2 2 4 205.89 217.72 1.89 o 0 3 4 1202.89 1205.56 7.28 o 1 3 4 65.72 65.03 0.72 o 2 3 4 353.13 404.33 2.12 o 3 3 4 83.68 80.70 1.37 o 0 4 4 59.42 63.78 1.28 o 1 4 4 537.09 558.75 3.10 o 2 4 4 44.53 44.37 0.88 o 3 4 4 300.83 304.15 2.77 o 4 4 4 32.62 34.82 1.64 o 0 5 4 151.52 166.80 2.59 o 1 5 4 330.94 338.13 2.86 o 2 5 4 152.84 160.61 1.98 o 3 5 4 56.46 60.12 1.42 o 4 5 4 210.60 206.61 2.64 o 5 5 4 172.98 172.18 4.28 o 0 6 4 295.71 288.14 4.50 o 1 6 4 184.70 188.84 2.21 o 2 6 4 59.55 61.29 1.52 o 3 6 4 302.72 298.68 3.33 o 4 6 4 32.54 36.44 1.64 o 5 6 4 69.85 71.44 2.48 o 6 6 4 0.07 0.37 2.28 o 0 7 4 135.13 127.61 4.27 o 1 7 4 4.87 3.56 0.89 o 2 7 4 55.34 48.63 1.82 o 3 7 4 25.51 23.75 1.44 o 4 7 4 62.79 65.84 2.44 o 5 7 4 23.28 21.99 2.26 o 0 8 4 12.53 16.41 1.97 o 1 8 4 42.39 41.49 1.96 o 2 8 4 21.61 20.13 1.80 o 3 8 4 60.43 66.91 2.95 o 4 8 4 14.58 16.70 2.56 o 0 9 4 184.47 232.58 9.15 o 0 1 5 185.72 160.74 1.29 o 1 1 5 6.16 6.78 0.37 o 0 2 5 547.62 545.71 3.63 o 1 2 5 2.40 4.52 0.25 o 2 2 5 38.49 46.12 0.89 o 0 3 5 1562.43 1533.23 8.92 o 1 3 5 728.07 706.10 3.18 o 2 3 5 291.76 310.20 1.86 o 3 3 5 540.83 578.07 5.01 o 0 4 5 205.44 204.96 2.54 o 1 4 5 207.12 214.93 1.79 o 2 4 5 262.16 234.52 2.02 o 3 4 5 19.06 21.70 0.84 o 4 4 5 154.91 149.99 2.77 o 0 5 5 39.95 42.20 1.58 o 1 5 5 152.62 147.88 1.84 o 2 5 5 95.58 96.22 1.66 o 3 5 5 102.83 102.48 1.78 o 4 5 5 93.50 92.17 1.76 o 5 5 5 342.74 359.95 6.34 o 0 6 5 3.97 2.24 0.93 o 1 6 5 243.38 229.54 2.70 o 2 6 5 162.74 165.87 2.63 o 3 6 5 75.00 81.52 1.85 o 4 6 5 27.88 31.42 1.57 o 5 6 5 13.68 13.97 1.34 o 6 6 5 21.37 16.27 2.88 o 0 7 5 60.52 57.82 3.45 o 1 7 5 67.12 73.05 1.84 o 2 7 5 4.59 4.78 1.02 o 3 7 5 2.99 2.50 0.99 o 4 7 5 17.22 16.44 1.53 o 5 7 5 70.30 87.35 3.78 o 0 8 5 285.35 285.04 7.67 o 1 8 5 9.51 7.71 1.50 o 2 8 5 4.03 3.94 1.46 o 3 8 5 18.75 16.42 2.08 o 0 1 6 376.43 360.14 2.36 o 1 1 6 2011.19 2034.86 10.37 o 0 2 6 0.41 0.82 0.35 o 1 2 6 1031.09 1063.86 4.14 o 2 2 6 1060.50 1104.57 6.64 o 0 3 6 8.09 5.24 0.50 o 1 3 6 715.57 731.79 3.37 o 2 3 6 148.56 154.13 1.21 o 3 3 6 48.66 45.93 1.30 o 0 4 6 572.34 533.30 4.60 o 1 4 6 8.65 8.99 0.52 o 2 4 6 106.13 111.97 1.52 o 3 4 6 11.09 10.54 0.66 o 4 4 6 31.32 31.15 1.58 o 0 5 6 56.65 57.94 1.84 o 1 5 6 234.89 219.38 2.45 o 2 5 6 230.17 233.15 2.64 o 3 5 6 222.76 214.05 2.64 o 4 5 6 10.66 11.16 0.93 o 5 5 6 24.01 21.52 1.94 o 0 6 6 402.20 418.25 5.69 o 1 6 6 187.14 196.88 2.74 o 2 6 6 291.79 294.34 3.54 o 3 6 6 105.40 99.35 2.15 o 4 6 6 123.61 124.35 2.64 o 5 6 6 20.45 20.40 1.51 o 6 6 6 0.04 -0.85 2.33 o 0 7 6 141.38 140.29 4.06 o 1 7 6 129.90 124.96 2.73 o 2 7 6 17.49 10.89 1.32 o 3 7 6 11.15 11.08 1.38 o 4 7 6 84.53 90.18 3.25 o 5 7 6 36.87 36.19 2.84 o 0 8 6 49.92 46.02 4.28 o 1 8 6 9.93 9.18 1.54 o 2 8 6 38.73 40.78 2.68 o 3 8 6 15.46 15.22 2.51 o 0 1 7 887.88 848.32 4.92 o 1 1 7 17.80 18.38 0.62 o 0 2 7 974.20 991.79 5.87 o 1 2 7 588.73 597.70 2.81 o 2 2 7 488.87 571.23 4.23 o 0 3 7 9.77 10.75 0.61 o 1 3 7 1030.20 1052.87 4.71 o 2 3 7 58.62 52.92 0.83 o 3 3 7 998.59 1001.47 7.92 o 0 4 7 80.73 74.69 1.81 o 1 4 7 279.35 282.79 2.47 o 2 4 7 86.32 86.64 1.51 o 3 4 7 129.65 128.16 1.71 o 4 4 7 218.44 197.69 3.48 o 0 5 7 40.85 39.48 1.70 o 1 5 7 596.70 571.35 4.27 o 2 5 7 58.31 61.22 1.42 o 3 5 7 114.16 111.22 1.92 o 4 5 7 132.12 134.99 2.29 o 5 5 7 126.39 117.16 3.53 o 0 6 7 1432.47 1476.96 13.89 o 1 6 7 24.54 21.88 1.11 o 2 6 7 230.44 233.23 3.39 o 3 6 7 16.68 15.35 1.17 o 4 6 7 4.75 5.26 1.09 o 5 6 7 15.14 9.94 1.39 o 6 6 7 0.22 -2.46 2.46 o 0 7 7 0.37 -0.62 1.48 o 1 7 7 8.48 8.08 1.17 o 2 7 7 28.62 22.17 1.67 o 3 7 7 24.15 20.43 1.61 o 4 7 7 40.09 43.19 2.41 o 5 7 7 10.44 16.20 2.38 o 0 8 7 87.96 83.18 5.91 o 1 8 7 50.57 54.89 2.70 o 2 8 7 29.31 32.02 2.47 o 3 8 7 30.63 24.02 2.69 o 0 0 8 641.41 615.34 10.64 o 0 1 8 264.67 267.29 2.43 o 1 1 8 107.81 134.44 1.57 o 0 2 8 2.87 2.36 0.39 o 1 2 8 671.36 695.55 3.36 o 2 2 8 86.37 108.34 1.61 o 0 3 8 2.04 0.63 0.45 o 1 3 8 343.96 346.76 2.27 o 2 3 8 262.77 269.05 2.17 o 3 3 8 171.88 164.58 2.51 o 0 4 8 11.73 12.67 0.93 o 1 4 8 168.77 172.83 1.97 o 2 4 8 49.66 50.97 1.23 o 3 4 8 60.85 59.29 1.31 o 4 4 8 0.48 2.15 0.91 o 0 5 8 0.21 0.00 0.84 o 1 5 8 158.78 158.25 2.21 o 2 5 8 523.47 523.43 4.84 o 3 5 8 156.61 160.84 2.37 o 4 5 8 33.72 31.67 1.41 o 5 5 8 8.42 8.77 1.63 o 0 6 8 577.01 592.92 7.34 o 1 6 8 73.79 72.23 1.88 o 2 6 8 110.78 113.81 2.53 o 3 6 8 102.78 95.29 2.28 o 4 6 8 129.50 121.45 2.71 o 5 6 8 62.72 63.63 2.64 o 6 6 8 5.37 6.34 3.55 o 0 7 8 21.17 21.70 3.00 o 1 7 8 172.72 181.82 3.59 o 2 7 8 95.15 93.62 3.11 o 3 7 8 38.79 35.54 1.96 o 4 7 8 2.30 2.09 1.59 o 0 8 8 153.18 158.02 8.04 o 1 8 8 27.78 29.86 3.03 o 2 8 8 8.38 8.53 1.99 o 0 1 9 0.06 0.36 0.35 o 1 1 9 308.77 301.81 2.63 o 0 2 9 2.03 0.59 0.37 o 1 2 9 86.90 90.98 1.22 o 2 2 9 115.47 114.70 1.89 o 0 3 9 527.86 557.60 4.89 o 1 3 9 204.39 234.81 2.04 o 2 3 9 406.86 416.56 3.12 o 3 3 9 20.93 23.62 1.23 o 0 4 9 273.78 282.47 3.85 o 1 4 9 212.60 210.05 2.28 o 2 4 9 12.19 12.36 0.78 o 3 4 9 26.59 22.40 0.91 o 4 4 9 35.45 31.95 2.00 o 0 5 9 824.51 814.07 8.30 o 1 5 9 229.19 236.03 2.96 o 2 5 9 488.09 482.89 4.65 o 3 5 9 54.67 53.89 1.53 o 4 5 9 163.89 159.27 2.92 o 5 5 9 75.79 80.83 3.60 o 0 6 9 36.89 35.22 2.39 o 1 6 9 29.70 34.15 1.70 o 2 6 9 85.18 81.05 2.21 o 3 6 9 12.52 12.22 1.14 o 4 6 9 27.06 29.52 1.68 o 5 6 9 11.67 10.91 1.73 o 0 7 9 97.45 88.74 5.08 o 1 7 9 5.00 5.52 1.37 o 2 7 9 9.47 7.97 1.36 o 3 7 9 16.37 15.36 1.76 o 4 7 9 32.78 34.11 2.91 o 0 8 9 67.42 88.99 7.58 o 1 8 9 51.40 62.79 3.58 o 2 8 9 11.76 6.61 2.46 o 0 1 10 77.85 88.41 1.46 o 1 1 10 276.76 308.79 2.93 o 0 2 10 161.14 174.39 2.36 o 1 2 10 53.69 64.20 1.02 o 2 2 10 43.16 46.45 1.37 o 0 3 10 878.48 871.37 7.77 o 1 3 10 130.75 128.80 1.65 o 2 3 10 7.32 5.86 0.56 o 3 3 10 62.40 67.28 1.97 o 0 4 10 4.65 2.64 0.77 o 1 4 10 420.39 408.71 3.54 o 2 4 10 34.36 33.83 1.22 o 3 4 10 42.50 40.03 1.33 o 4 4 10 2.87 0.80 0.99 o 0 5 10 355.61 358.69 6.55 o 1 5 10 156.72 170.38 2.72 o 2 5 10 116.75 114.07 2.07 o 3 5 10 76.27 73.60 2.04 o 4 5 10 7.32 6.70 1.06 o 5 5 10 0.87 0.82 1.52 o 0 6 10 114.59 112.34 3.40 o 1 6 10 163.75 159.38 3.26 o 2 6 10 198.53 190.79 4.11 o 3 6 10 55.27 51.23 2.02 o 4 6 10 17.79 16.37 1.61 o 5 6 10 28.85 32.44 3.19 o 0 7 10 53.46 50.39 4.01 o 1 7 10 61.79 55.90 2.73 o 2 7 10 155.61 169.67 3.66 o 3 7 10 0.07 0.34 1.50 o 4 7 10 73.08 68.84 5.30 o 0 8 10 14.32 28.91 5.45 o 1 8 10 25.33 23.69 2.66 o 0 1 11 333.18 365.10 3.85 o 1 1 11 249.55 254.01 3.00 o 0 2 11 0.02 -0.17 0.56 o 1 2 11 225.65 232.63 2.24 o 2 2 11 25.26 27.36 1.24 o 0 3 11 45.83 47.39 1.74 o 1 3 11 2.22 1.31 0.47 o 2 3 11 41.96 47.83 1.15 o 3 3 11 22.52 22.82 1.46 o 0 4 11 3.87 5.03 0.93 o 1 4 11 528.44 523.59 4.50 o 2 4 11 68.52 69.79 1.74 o 3 4 11 59.76 54.84 1.63 o 4 4 11 10.80 7.48 1.33 o 0 5 11 40.03 45.09 2.43 o 1 5 11 360.37 368.67 4.29 o 2 5 11 25.08 21.88 1.28 o 3 5 11 25.08 24.17 1.45 o 4 5 11 72.49 74.14 2.37 o 5 5 11 13.32 12.14 2.60 o 0 6 11 150.17 144.51 4.31 o 1 6 11 263.05 254.31 4.24 o 2 6 11 1.42 0.76 1.01 o 3 6 11 87.20 90.07 2.62 o 4 6 11 7.02 6.68 1.67 o 5 6 11 12.02 10.90 2.80 o 0 7 11 60.42 65.58 3.90 o 1 7 11 0.31 0.70 1.31 o 2 7 11 7.36 6.65 1.50 o 3 7 11 5.77 7.65 2.26 o 0 0 12 578.16 609.74 12.56 o 0 1 12 102.00 103.17 2.17 o 1 1 12 180.20 180.90 2.97 o 0 2 12 34.45 31.51 1.46 o 1 2 12 65.23 64.32 1.30 o 2 2 12 133.22 129.21 2.71 o 0 3 12 14.00 13.78 1.04 o 1 3 12 105.64 104.86 1.76 o 2 3 12 14.27 16.33 0.95 o 3 3 12 51.49 45.01 2.13 o 0 4 12 15.14 13.29 1.32 o 1 4 12 31.49 30.49 1.38 o 2 4 12 17.50 17.49 1.13 o 3 4 12 44.96 45.84 1.77 o 4 4 12 39.20 37.19 2.76 o 0 5 12 0.14 0.74 0.97 o 1 5 12 109.59 102.44 2.31 o 2 5 12 36.41 32.40 1.67 o 3 5 12 42.15 34.68 1.77 o 4 5 12 41.01 33.66 1.99 o 5 5 12 67.54 70.64 7.04 o 0 6 12 22.42 26.20 2.51 o 1 6 12 6.64 4.11 1.17 o 2 6 12 5.20 4.79 1.14 o 3 6 12 32.02 25.81 2.01 o 4 6 12 13.22 11.12 2.37 o 0 7 12 6.13 5.43 2.21 o 1 7 12 75.38 68.85 3.47 o 2 7 12 22.68 17.02 2.32 o 0 1 13 35.21 34.35 1.54 o 1 1 13 368.89 346.23 4.52 o 0 2 13 134.07 130.83 2.80 o 1 2 13 124.61 125.96 1.95 o 2 2 13 46.27 38.93 1.91 o 0 3 13 21.26 18.50 1.36 o 1 3 13 189.94 181.55 2.48 o 2 3 13 12.77 11.07 0.98 o 3 3 13 62.53 62.97 2.54 o 0 4 13 225.44 228.65 4.24 o 1 4 13 98.61 98.56 2.14 o 2 4 13 381.17 369.31 5.12 o 3 4 13 31.71 30.49 1.76 o 4 4 13 61.58 61.00 3.70 o 0 5 13 61.62 68.48 2.92 o 1 5 13 156.29 154.27 3.58 o 2 5 13 56.37 60.00 2.30 o 3 5 13 4.93 1.63 1.18 o 4 5 13 3.36 2.52 1.64 o 5 5 13 6.55 6.68 4.64 o 0 6 13 0.87 0.41 1.45 o 1 6 13 24.90 28.44 1.81 o 2 6 13 85.64 85.54 3.61 o 3 6 13 20.74 19.78 2.50 o 4 6 13 6.13 10.45 3.24 o 0 7 13 0.00 0.03 2.12 o 1 7 13 39.89 43.13 3.31 o 0 1 14 251.34 263.69 4.00 o 1 1 14 163.85 154.84 3.06 o 0 2 14 327.51 318.46 5.18 o 1 2 14 17.84 16.12 1.02 o 2 2 14 222.28 221.96 4.54 o 0 3 14 21.60 18.86 1.53 o 1 3 14 74.82 73.28 1.74 o 2 3 14 45.19 41.31 1.69 o 3 3 14 186.72 178.57 6.17 o 0 4 14 279.74 292.74 5.55 o 1 4 14 99.69 97.14 2.45 o 2 4 14 31.06 27.69 1.73 o 3 4 14 112.71 122.72 3.26 o 4 4 14 5.11 4.74 2.00 o 0 5 14 5.67 3.58 1.81 o 1 5 14 58.02 60.23 2.55 o 2 5 14 62.71 59.62 2.57 o 3 5 14 31.86 40.17 2.53 o 4 5 14 4.61 2.04 2.24 o 0 6 14 1.14 1.89 1.85 o 1 6 14 1.81 1.96 1.32 o 2 6 14 11.72 13.64 2.22 o 3 6 14 9.32 14.06 3.08 o 0 1 15 88.75 82.90 2.47 o 1 1 15 29.08 29.60 1.77 o 0 2 15 37.43 35.08 1.97 o 1 2 15 330.32 326.86 3.68 o 2 2 15 7.11 4.65 1.52 o 0 3 15 72.79 68.68 2.60 o 1 3 15 138.09 140.96 2.68 o 2 3 15 109.73 118.09 2.99 o 3 3 15 10.65 4.90 1.87 o 0 4 15 31.05 33.53 2.55 o 1 4 15 139.50 140.67 3.15 o 2 4 15 20.47 16.54 1.59 o 3 4 15 53.53 58.05 2.77 o 4 4 15 205.11 200.45 8.42 o 0 5 15 40.82 46.58 3.55 o 1 5 15 9.72 7.84 1.46 o 2 5 15 20.19 17.53 1.93 o 3 5 15 25.86 18.56 2.48 o 4 5 15 45.97 45.98 4.74 o 0 6 15 11.27 10.82 4.11 o 1 6 15 5.49 4.03 2.59 o 2 6 15 5.68 6.90 2.68 o 0 0 16 43.63 40.01 4.35 o 0 1 16 51.02 53.26 2.33 o 1 1 16 82.05 86.79 2.85 o 0 2 16 16.47 16.20 1.73 o 1 2 16 301.64 301.31 4.09 o 2 2 16 18.06 14.20 2.02 o 0 3 16 140.51 144.57 4.21 o 1 3 16 27.29 25.37 1.71 o 2 3 16 23.84 17.71 1.76 o 3 3 16 13.75 12.39 2.36 o 0 4 16 116.49 112.64 4.47 o 1 4 16 0.47 0.55 1.21 o 2 4 16 67.42 77.64 2.94 o 3 4 16 76.34 77.80 3.96 o 4 4 16 21.31 21.35 5.09 o 0 5 16 18.74 23.46 3.84 o 1 5 16 45.21 44.99 3.86 o 2 5 16 40.89 45.31 3.70 o 3 5 16 1.32 1.70 2.43 o 0 6 16 0.01 -2.87 4.54 o 0 1 17 175.93 182.44 4.56 o 1 1 17 282.67 315.40 6.33 o 0 2 17 192.98 205.62 6.99 o 1 2 17 70.30 66.87 2.79 o 2 2 17 0.00 0.42 1.69 o 0 3 17 0.20 -0.69 1.53 o 1 3 17 31.34 31.14 2.07 o 2 3 17 62.75 52.58 2.69 o 3 3 17 1.77 2.25 2.60 o 0 4 17 20.94 11.94 3.41 o 1 4 17 0.18 0.43 1.42 o 2 4 17 77.49 74.06 4.03 o 3 4 17 96.15 97.72 5.82 o 0 5 17 8.86 4.40 3.58 o 1 5 17 3.31 -0.62 2.06 o 2 5 17 20.76 20.25 3.05 o 0 1 18 10.00 6.55 1.87 o 1 1 18 114.50 122.51 4.77 o 0 2 18 78.33 85.07 4.00 o 1 2 18 94.48 102.65 3.17 o 2 2 18 149.94 150.71 5.65 o 0 3 18 23.26 19.93 3.23 o 1 3 18 7.48 8.71 1.75 o 2 3 18 1.82 0.24 1.74 o 3 3 18 88.41 86.35 6.87 o 0 4 18 4.78 8.77 4.05 o 1 4 18 12.43 13.72 2.51 o 2 4 18 5.11 1.19 2.42 o 0 1 19 8.12 6.86 2.08 o 1 1 19 1.91 3.37 2.25 o 0 2 19 0.69 0.59 2.13 o 1 2 19 77.24 75.44 3.55 o 2 2 19 97.90 106.36 6.22 o 0 3 19 0.21 -0.34 2.36 o 1 3 19 12.69 12.53 2.15 o 2 3 19 18.31 21.44 3.02 o 0 4 19 15.02 14.64 5.03 o 0 0 20 7.18 9.14 5.55 o 0 1 20 37.77 34.52 4.08 o 1 1 20 73.45 83.51 6.10 o 0 2 20 111.29 116.11 7.40 o 1 2 20 23.43 15.09 2.64 o 2 2 20 0.30 3.31 3.07 o 0 3 20 0.52 0.25 5.90 o 0 1 21 0.52 3.41 6.32 o