#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/87/2218729.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2218729_Fobs loop_ _publ_author_name 'Liu, Jian-Lan' 'Yao, Bing-Qian' 'Zhang, Shao-Ming' _publ_section_title ; Bis(1-amino-4-methylpyridinium) bis(1,2-dicyanoethene-1,2-dithiolato-\k^2^S,S')nickelate(II) ; _journal_coeditor_code HK2475 _journal_issue 7 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m970 _journal_volume 64 _journal_year 2008 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 93.116 _cell_angle_beta 104.519 _cell_angle_gamma 108.813 _cell_length_a 7.6778 _cell_length_b 9.0947 _cell_length_c 9.6649 _exptl_crystal_F_000 286.00 _reflns_d_resolution_high 0.8409 _[local]_cod_data_source_file hk2475Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' vb in P-1' _shelx_refln_list_code 4 _shelx_F_calc_maximum 121.88 _shelx_F_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 1614.60 1780.73 9.05 o 2 0 0 1278.71 1224.06 7.93 o 3 0 0 418.76 418.43 5.52 o 5 0 0 16.64 19.39 1.79 o 6 0 0 95.83 93.21 3.97 o 7 0 0 58.27 56.96 3.55 o -8 1 0 0.30 0.79 1.32 o -7 1 0 82.99 90.33 4.20 o -5 1 0 7.87 7.17 1.18 o -4 1 0 86.52 84.63 2.79 o -3 1 0 128.00 107.40 2.64 o -2 1 0 5535.47 5018.31 24.73 o -1 1 0 1867.29 1336.50 191.40 o 0 1 0 2214.90 2148.78 391.34 o 3 1 0 468.54 476.47 6.40 o 4 1 0 264.50 263.41 5.46 o 5 1 0 22.35 23.03 2.06 o 7 1 0 140.07 114.10 5.11 o -8 2 0 6.94 9.90 2.00 o -7 2 0 64.37 57.14 3.26 o -6 2 0 216.13 198.46 5.29 o -5 2 0 54.16 65.18 2.76 o -4 2 0 89.58 89.54 2.76 o -3 2 0 219.20 235.39 3.79 o -2 2 0 11543.15 10539.19 1111.13 o -1 2 0 1519.84 1000.16 126.51 o 0 2 0 353.12 370.63 73.13 o 1 2 0 677.15 813.68 6.90 o 4 2 0 402.03 404.15 7.29 o 5 2 0 128.71 112.98 4.35 o 6 2 0 2.07 2.44 1.38 o 7 2 0 277.89 259.42 7.90 o -8 3 0 69.57 65.57 3.79 o -7 3 0 189.77 160.82 17.70 o -6 3 0 337.48 305.62 29.61 o -5 3 0 845.98 760.97 66.52 o -4 3 0 456.77 379.10 48.25 o -3 3 0 221.22 213.13 31.44 o -2 3 0 185.03 197.73 21.59 o -1 3 0 1830.45 1535.05 103.39 o 0 3 0 472.53 491.90 96.87 o 1 3 0 137.60 171.82 3.64 o 2 3 0 15.47 17.68 1.47 o 4 3 0 12.65 12.16 1.67 o 5 3 0 96.57 89.60 4.17 o 6 3 0 12.76 10.49 2.06 o 7 3 0 0.86 0.15 1.38 o -8 4 0 86.59 92.47 4.35 o -7 4 0 244.18 215.02 21.99 o -6 4 0 279.91 269.16 25.73 o -5 4 0 491.72 569.58 86.65 o -4 4 0 2771.80 3095.11 346.56 o -3 4 0 1.69 0.97 0.20 o -2 4 0 279.65 221.65 15.28 o -1 4 0 25.12 24.55 3.81 o 0 4 0 107.52 134.67 36.73 o 1 4 0 49.43 60.69 2.53 o 2 4 0 40.75 46.94 2.50 o 3 4 0 161.07 184.48 5.23 o 4 4 0 551.71 540.66 9.66 o 5 4 0 21.04 20.09 2.35 o 6 4 0 24.72 22.47 2.73 o -7 5 0 12.93 14.30 1.33 o -6 5 0 814.02 757.09 85.38 o -5 5 0 212.85 234.81 37.06 o -4 5 0 1134.02 1153.05 231.92 o -3 5 0 1880.30 2014.50 422.01 o -2 5 0 658.53 432.60 23.95 o -1 5 0 166.27 162.80 24.85 o 0 5 0 338.74 391.44 86.35 o 1 5 0 84.75 120.68 3.91 o 2 5 0 560.68 617.74 9.43 o 3 5 0 42.08 48.56 3.08 o 4 5 0 411.89 379.39 8.72 o 5 5 0 159.09 142.41 5.90 o -8 6 0 24.34 19.33 2.32 o -7 6 0 0.19 0.25 0.57 o -6 6 0 19.93 16.79 1.31 o -5 6 0 376.14 410.90 74.20 o -4 6 0 248.59 279.81 62.48 o -3 6 0 1094.24 1096.49 194.10 o -2 6 0 825.51 575.95 89.68 o -1 6 0 632.07 634.13 127.52 o 0 6 0 901.56 1014.31 214.31 o 1 6 0 124.44 166.30 5.02 o 2 6 0 4.66 4.55 1.35 o 3 6 0 624.73 663.48 11.40 o 4 6 0 245.62 227.13 7.29 o 5 6 0 175.61 159.07 6.64 o -8 7 0 13.86 9.96 1.94 o -7 7 0 0.64 0.00 0.91 o -6 7 0 71.86 61.77 2.37 o -5 7 0 28.88 25.89 6.37 o -4 7 0 5.45 11.77 3.86 o -3 7 0 356.57 321.24 38.86 o -2 7 0 456.26 352.43 27.63 o -1 7 0 344.97 384.74 68.65 o 0 7 0 41.37 42.68 7.36 o 1 7 0 370.60 458.67 8.99 o 2 7 0 1.21 2.20 1.29 o 3 7 0 65.28 62.78 3.97 o 4 7 0 120.94 106.69 5.46 o -7 8 0 20.37 17.30 2.35 o -6 8 0 29.68 28.29 2.64 o -5 8 0 64.87 78.12 16.96 o -4 8 0 15.53 14.91 3.39 o -3 8 0 11.24 11.19 1.15 o -2 8 0 58.39 40.40 3.11 o -1 8 0 284.26 297.68 46.96 o 0 8 0 175.15 241.50 6.73 o 1 8 0 5.16 7.05 1.70 o 2 8 0 5.97 5.73 1.70 o 3 8 0 1.00 1.44 1.50 o -7 9 0 32.16 34.11 3.20 o -6 9 0 7.01 6.82 1.70 o -5 9 0 10.29 11.78 2.76 o -4 9 0 0.40 0.92 0.63 o -3 9 0 29.08 25.35 1.95 o -2 9 0 208.00 175.35 8.94 o -1 9 0 10.29 11.71 2.48 o 0 9 0 124.56 152.46 5.85 o 1 9 0 0.48 0.00 0.97 o 2 9 0 16.94 16.22 2.64 o -5 10 0 67.22 69.24 4.32 o -4 10 0 46.90 52.80 8.52 o -3 10 0 5.28 7.07 1.53 o -2 10 0 52.42 42.06 3.07 o -1 10 0 86.34 96.73 4.85 o 0 10 0 56.73 65.18 4.26 o 0 -10 1 48.22 62.28 4.05 o 1 -10 1 7.21 6.02 1.75 o 2 -10 1 0.39 0.35 0.62 o 3 -10 1 2.19 1.73 1.23 o 4 -10 1 0.57 0.73 1.09 o 5 -10 1 63.11 67.33 4.32 o -2 -9 1 127.73 165.53 6.64 o -1 -9 1 95.37 122.97 5.43 o 0 -9 1 98.12 113.13 4.94 o 1 -9 1 4.71 5.65 1.04 o 2 -9 1 35.83 30.59 4.49 o 3 -9 1 72.95 72.29 11.38 o 4 -9 1 20.24 20.09 2.29 o 5 -9 1 39.57 39.80 3.20 o 6 -9 1 66.45 66.74 4.17 o -3 -8 1 74.74 73.79 4.49 o -2 -8 1 146.90 174.79 6.32 o -1 -8 1 207.13 262.59 7.23 o 0 -8 1 246.79 271.86 53.43 o 1 -8 1 208.68 204.53 25.38 o 2 -8 1 55.98 54.57 3.63 o 3 -8 1 101.77 113.54 20.90 o 4 -8 1 23.64 23.52 4.92 o 5 -8 1 9.19 8.99 1.70 o 6 -8 1 0.17 0.00 0.82 o 7 -8 1 23.82 26.32 2.79 o -4 -7 1 3.53 3.70 1.65 o -3 -7 1 80.86 89.24 4.58 o -2 -7 1 192.66 239.44 6.79 o -1 -7 1 493.51 663.54 10.49 o 0 -7 1 701.97 794.31 179.38 o 1 -7 1 698.22 702.60 118.77 o 2 -7 1 314.30 258.74 15.22 o 3 -7 1 353.05 149.53 166.93 o 4 -7 1 9.98 12.82 3.80 o 5 -7 1 7.88 7.70 1.50 o 6 -7 1 15.17 13.48 1.94 o 7 -7 1 58.87 47.06 3.38 o 8 -7 1 10.38 12.72 2.23 o -5 -6 1 47.73 50.23 3.85 o -4 -6 1 9.55 9.14 1.94 o -3 -6 1 66.73 80.52 4.08 o -2 -6 1 132.92 153.84 5.05 o -1 -6 1 125.30 174.43 4.99 o 0 -6 1 246.63 221.42 43.19 o 1 -6 1 2083.51 1880.71 253.18 o 2 -6 1 631.38 482.07 20.36 o 3 -6 1 749.31 857.82 189.96 o 4 -6 1 513.62 559.33 124.73 o 5 -6 1 151.49 161.57 31.20 o 6 -6 1 77.64 67.42 3.58 o 7 -6 1 84.54 69.18 3.88 o 8 -6 1 38.59 37.60 3.20 o -6 -5 1 73.89 65.36 4.41 o -5 -5 1 36.97 37.98 3.20 o -4 -5 1 5.16 5.99 1.56 o -3 -5 1 14.61 18.98 2.06 o -2 -5 1 11.78 15.98 1.73 o -1 -5 1 6.84 9.78 1.60 o 0 -5 1 16.81 15.26 2.85 o 1 -5 1 185.27 131.79 19.58 o 2 -5 1 2085.03 1547.09 125.64 o 3 -5 1 666.58 742.04 97.98 o 4 -5 1 757.39 785.47 143.34 o 5 -5 1 133.53 120.54 19.86 o 6 -5 1 182.27 168.27 19.77 o 7 -5 1 107.20 98.82 4.44 o 8 -5 1 50.08 34.75 3.00 o -6 -4 1 65.08 59.02 3.97 o -5 -4 1 16.14 16.92 2.29 o -4 -4 1 36.71 39.63 2.79 o -3 -4 1 39.96 41.51 2.53 o -2 -4 1 139.51 175.08 4.49 o -1 -4 1 735.31 734.37 112.27 o 0 -4 1 4.96 4.90 0.76 o 1 -4 1 52.08 36.31 1.26 o 2 -4 1 58.97 57.28 6.85 o 3 -4 1 123.04 117.07 24.51 o 4 -4 1 849.86 923.87 82.57 o 5 -4 1 277.31 312.77 45.67 o 6 -4 1 91.95 71.80 8.45 o 7 -4 1 3.88 1.56 1.03 o 8 -4 1 9.55 11.93 1.97 o -7 -3 1 21.93 21.94 2.91 o -6 -3 1 86.02 81.93 4.38 o -5 -3 1 346.57 342.20 7.87 o -4 -3 1 157.44 155.66 4.85 o -3 -3 1 229.93 204.78 4.96 o -2 -3 1 725.95 546.01 7.05 o -1 -3 1 13.02 19.15 4.96 o 0 -3 1 2943.44 2842.59 537.42 o 1 -3 1 26.12 36.68 1.68 o 2 -3 1 20.49 41.86 10.53 o 3 -3 1 799.76 887.37 103.53 o 4 -3 1 320.38 387.65 69.22 o 5 -3 1 163.28 167.29 28.67 o 6 -3 1 11.83 5.82 1.06 o 7 -3 1 2.75 1.12 0.79 o -7 -2 1 101.74 94.06 4.85 o -6 -2 1 31.77 31.08 2.76 o -5 -2 1 233.32 227.54 6.08 o -4 -2 1 296.62 293.99 6.17 o -3 -2 1 2169.94 2434.04 15.77 o -2 -2 1 1609.78 1343.72 291.39 o -1 -2 1 2690.97 2594.44 286.37 o 0 -2 1 172.75 149.77 1.67 o 1 -2 1 2264.58 2089.22 110.93 o 2 -2 1 3.32 5.41 1.41 o 3 -2 1 172.47 193.48 33.80 o 4 -2 1 288.79 252.95 4.47 o 6 -2 1 0.94 2.70 1.00 o 7 -2 1 0.86 2.23 1.20 o -7 -1 1 0.83 0.00 1.00 o -6 -1 1 20.51 21.68 2.23 o -5 -1 1 150.06 171.17 4.96 o -4 -1 1 253.06 235.86 5.17 o -3 -1 1 2677.74 2980.61 16.24 o -2 -1 1 14853.57 11220.29 2441.36 o -1 -1 1 10605.01 8784.39 2001.56 o 0 -1 1 851.52 906.14 109.73 o 1 -1 1 61.56 94.33 14.09 o 2 -1 1 428.32 368.93 3.73 o 3 -1 1 5.14 2.53 0.44 o 4 -1 1 234.63 193.12 4.11 o 5 -1 1 578.65 609.14 8.34 o 6 -1 1 425.14 434.67 7.93 o 7 -1 1 164.99 154.02 5.38 o -8 0 1 34.47 43.98 3.53 o -7 0 1 1.34 0.73 1.09 o -6 0 1 0.43 0.00 0.79 o -5 0 1 2.13 1.06 0.73 o -4 0 1 592.94 579.00 7.64 o -3 0 1 1039.52 1074.71 8.99 o -2 0 1 7681.42 6134.52 765.78 o -1 0 1 549.53 537.61 4.14 o 0 0 1 2791.87 1720.10 11.34 o 2 0 1 151.04 180.60 2.94 o 3 0 1 108.38 104.75 2.79 o 4 0 1 1294.68 1418.55 11.84 o 5 0 1 887.75 837.27 10.31 o 6 0 1 622.12 623.68 9.99 o 7 0 1 170.61 155.87 5.67 o 8 0 1 155.79 138.54 5.90 o -8 1 1 28.25 26.59 2.79 o -6 1 1 27.49 27.20 2.17 o -5 1 1 9.34 9.22 1.26 o -4 1 1 241.97 210.71 4.44 o -3 1 1 725.50 863.76 7.73 o -2 1 1 2483.51 2268.23 201.24 o -1 1 1 880.70 855.52 88.19 o 0 1 1 332.09 484.55 4.00 o 1 1 1 876.33 1139.72 7.34 o 5 1 1 165.30 162.21 4.94 o 6 1 1 506.90 458.79 9.05 o 7 1 1 161.42 162.18 6.08 o -8 2 1 144.07 147.55 5.64 o -7 2 1 190.03 197.55 5.93 o -6 2 1 11.08 12.62 1.40 o -5 2 1 1.06 3.81 0.75 o -4 2 1 360.51 322.92 35.68 o -3 2 1 52.56 59.07 8.89 o -2 2 1 696.94 759.84 137.52 o -1 2 1 2422.13 1955.93 217.53 o 0 2 1 11.35 17.10 0.97 o 1 2 1 284.24 340.05 4.64 o 2 2 1 16.77 26.38 1.59 o 4 2 1 0.50 1.20 0.82 o 5 2 1 87.10 94.71 4.08 o 6 2 1 5.11 3.26 1.47 o 7 2 1 161.23 135.45 5.85 o -8 3 1 149.87 153.75 5.67 o -7 3 1 304.19 323.37 7.43 o -6 3 1 301.50 269.86 27.35 o -5 3 1 927.78 895.27 84.09 o -4 3 1 111.45 154.16 25.73 o -3 3 1 38.36 48.85 8.46 o -2 3 1 1154.01 1071.42 147.52 o -1 3 1 20.45 23.96 4.20 o 0 3 1 29.20 49.53 1.91 o 1 3 1 518.81 700.88 7.70 o 2 3 1 486.26 521.68 7.34 o 3 3 1 243.11 295.31 6.17 o 4 3 1 143.30 148.93 4.91 o 5 3 1 18.11 13.78 2.00 o -9 4 1 22.53 23.68 2.79 o -8 4 1 101.58 101.49 4.61 o -7 4 1 355.98 352.39 27.17 o -6 4 1 462.53 440.23 44.40 o -5 4 1 446.22 402.64 58.58 o -4 4 1 2094.45 2521.25 330.16 o -3 4 1 18.98 29.50 7.18 o -2 4 1 608.21 496.03 40.26 o -1 4 1 744.59 707.61 111.82 o 0 4 1 399.99 554.94 7.14 o 1 4 1 1592.28 2096.75 15.04 o 2 4 1 1041.53 1218.77 12.43 o 3 4 1 252.56 253.98 6.26 o 4 4 1 373.93 356.77 8.05 o 5 4 1 43.58 44.62 3.29 o 6 4 1 1.29 0.82 1.35 o -8 5 1 5.91 4.67 1.41 o -7 5 1 0.68 0.63 0.59 o -6 5 1 707.54 707.92 80.53 o -5 5 1 290.97 289.06 47.03 o -4 5 1 472.77 480.06 85.34 o -3 5 1 850.62 794.63 138.29 o -2 5 1 764.88 645.06 43.26 o -1 5 1 479.54 500.02 85.72 o 0 5 1 248.21 339.05 6.26 o 1 5 1 300.97 377.27 7.05 o 2 5 1 2860.00 3289.55 22.35 o 3 5 1 265.49 261.83 6.90 o 4 5 1 216.74 199.43 6.52 o 5 5 1 106.26 93.74 4.96 o -8 6 1 2.92 4.85 1.44 o -7 6 1 2.26 1.50 0.71 o -6 6 1 37.66 36.91 4.61 o -5 6 1 550.21 572.23 105.11 o -4 6 1 273.77 283.72 58.72 o -3 6 1 189.53 178.72 8.58 o -2 6 1 237.01 183.21 3.88 o -1 6 1 0.92 1.22 0.75 o 0 6 1 94.08 112.22 4.05 o 1 6 1 160.90 205.69 5.76 o 2 6 1 200.40 206.63 6.17 o 3 6 1 992.89 970.57 14.10 o 4 6 1 118.28 116.12 5.43 o -8 7 1 103.51 87.04 4.49 o -7 7 1 0.33 0.93 0.82 o -6 7 1 6.09 5.64 0.99 o -5 7 1 8.00 7.82 1.40 o -4 7 1 153.88 156.97 30.59 o -3 7 1 113.65 96.80 4.05 o -2 7 1 109.01 89.72 4.60 o -1 7 1 73.97 76.97 12.76 o 0 7 1 638.84 809.77 11.60 o 1 7 1 72.97 80.87 4.05 o 2 7 1 15.31 11.87 2.14 o 3 7 1 38.81 32.14 3.11 o 4 7 1 54.86 49.97 4.00 o -7 8 1 17.99 18.33 1.69 o -6 8 1 11.59 13.69 3.61 o -5 8 1 56.92 63.74 14.41 o -4 8 1 173.73 168.95 21.09 o -3 8 1 351.26 289.50 19.06 o -2 8 1 4.65 4.63 0.87 o -1 8 1 16.91 14.77 1.42 o 0 8 1 41.22 50.00 3.35 o 1 8 1 385.61 442.55 9.81 o 2 8 1 5.39 3.23 1.65 o -7 9 1 53.59 61.89 4.08 o -6 9 1 33.00 38.64 8.06 o -5 9 1 82.38 93.39 15.14 o -4 9 1 99.12 100.57 5.13 o -3 9 1 95.07 75.40 2.82 o -2 9 1 498.39 440.76 13.63 o -1 9 1 11.20 9.75 1.85 o 0 9 1 15.85 21.18 2.61 o 1 9 1 0.80 1.41 1.38 o -6 10 1 15.28 12.48 2.23 o -5 10 1 1.45 1.30 0.82 o -4 10 1 145.63 145.98 11.47 o -3 10 1 36.02 33.67 2.12 o -2 10 1 208.72 181.05 7.11 o -1 10 1 474.17 473.48 10.78 o 0 -10 2 3.95 5.30 1.14 o 1 -10 2 43.72 42.17 2.28 o 2 -10 2 29.34 33.43 3.00 o 3 -10 2 0.26 0.00 0.94 o 4 -10 2 18.04 18.86 2.53 o 5 -10 2 59.78 60.40 4.17 o -2 -9 2 125.20 168.50 6.58 o -1 -9 2 75.43 105.96 4.96 o 0 -9 2 9.22 8.73 1.44 o 1 -9 2 8.42 8.04 1.22 o 2 -9 2 19.63 12.14 2.47 o 3 -9 2 9.61 9.55 1.79 o 4 -9 2 34.29 29.55 2.79 o 5 -9 2 18.90 20.53 2.47 o 6 -9 2 21.45 22.33 2.64 o -3 -8 2 163.75 206.98 7.17 o -2 -8 2 210.51 276.81 7.73 o -1 -8 2 350.15 466.66 9.37 o 0 -8 2 234.71 272.85 54.57 o 1 -8 2 59.80 60.24 7.08 o 2 -8 2 48.48 46.89 1.96 o 3 -8 2 0.29 0.18 0.76 o 4 -8 2 55.09 50.50 3.29 o 5 -8 2 146.14 135.48 5.43 o 6 -8 2 35.45 38.69 3.20 o 7 -8 2 30.12 29.26 3.00 o -4 -7 2 23.14 22.97 2.76 o -3 -7 2 74.21 94.74 4.64 o -2 -7 2 152.26 200.55 6.11 o -1 -7 2 508.26 493.46 84.94 o 0 -7 2 591.03 613.34 112.52 o 1 -7 2 430.54 370.40 42.14 o 2 -7 2 192.95 172.71 11.15 o 3 -7 2 298.40 375.78 89.21 o 4 -7 2 81.76 68.74 3.55 o 5 -7 2 238.43 203.28 6.26 o 6 -7 2 138.44 133.31 5.38 o 7 -7 2 90.72 84.51 4.58 o -5 -6 2 0.96 0.97 1.26 o -4 -6 2 5.50 4.17 1.53 o -3 -6 2 0.35 1.70 1.09 o -2 -6 2 6.21 4.47 1.75 o -1 -6 2 287.37 270.11 45.85 o 0 -6 2 327.72 298.52 59.08 o 1 -6 2 996.03 769.04 110.43 o 2 -6 2 385.38 313.05 15.96 o 3 -6 2 127.05 153.54 40.27 o 4 -6 2 152.68 135.51 4.61 o 5 -6 2 126.19 109.60 4.41 o 6 -6 2 138.66 120.88 4.91 o 7 -6 2 144.35 137.13 5.55 o 8 -6 2 121.36 111.22 5.35 o -6 -5 2 13.96 13.40 2.38 o -5 -5 2 3.38 2.79 1.41 o -4 -5 2 18.96 18.71 2.20 o -3 -5 2 20.46 25.82 2.23 o -2 -5 2 126.58 124.48 34.24 o -1 -5 2 28.75 33.06 9.53 o 0 -5 2 188.74 190.15 36.86 o 1 -5 2 14.27 8.70 0.97 o 2 -5 2 744.49 802.35 69.37 o 3 -5 2 122.22 127.01 16.41 o 4 -5 2 40.32 33.66 4.24 o 5 -5 2 28.61 22.53 2.03 o 6 -5 2 0.56 0.32 0.73 o 7 -5 2 29.01 31.46 2.76 o 8 -5 2 88.50 75.00 4.35 o -6 -4 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15.29 o -4 -1 9 66.34 70.91 3.79 o -3 -1 9 8.89 6.35 1.29 o -2 -1 9 4.34 1.82 0.88 o -1 -1 9 29.27 27.17 2.38 o 0 -1 9 101.63 117.59 4.88 o 1 -1 9 214.13 243.32 7.26 o 2 -1 9 420.98 495.13 10.78 o 3 -1 9 336.85 416.17 10.43 o -7 0 9 7.25 6.46 1.15 o -6 0 9 14.50 14.53 2.82 o -5 0 9 11.59 12.53 1.27 o -4 0 9 20.55 18.51 1.38 o -3 0 9 7.38 7.05 1.32 o -2 0 9 125.46 81.69 3.88 o -1 0 9 4.58 4.35 1.15 o 0 0 9 12.91 15.04 1.97 o 1 0 9 86.05 115.24 5.08 o 2 0 9 217.14 243.38 7.70 o 3 0 9 203.93 205.42 7.49 o -7 1 9 0.11 0.06 0.85 o -6 1 9 3.01 3.35 0.84 o -5 1 9 37.83 38.59 1.98 o -4 1 9 2.54 1.84 0.66 o -3 1 9 18.78 11.57 1.59 o -2 1 9 0.22 0.56 0.71 o -1 1 9 7.63 9.25 1.56 o 0 1 9 1.52 0.91 0.91 o 1 1 9 15.32 14.31 2.12 o 2 1 9 4.87 5.55 1.73 o -7 2 9 11.46 10.60 1.91 o -6 2 9 10.80 12.60 1.97 o -5 2 9 79.19 88.27 4.29 o -4 2 9 302.77 305.40 47.74 o -3 2 9 153.49 146.76 54.18 o -2 2 9 110.89 110.39 4.44 o -1 2 9 25.81 31.81 2.59 o 0 2 9 0.44 0.06 0.94 o 1 2 9 57.58 53.96 3.70 o 2 2 9 38.50 32.23 3.17 o -7 3 9 17.40 17.65 2.44 o -6 3 9 107.07 124.26 5.41 o -5 3 9 79.13 97.88 4.61 o -4 3 9 237.02 297.37 7.55 o -3 3 9 228.01 196.87 86.25 o -2 3 9 294.22 305.45 7.34 o -1 3 9 233.95 264.70 7.20 o 0 3 9 57.98 67.95 3.97 o 1 3 9 1.83 1.94 1.44 o -6 4 9 5.21 8.20 1.82 o -5 4 9 15.53 17.04 2.29 o -4 4 9 60.15 75.44 4.08 o -3 4 9 201.07 240.35 6.93 o -2 4 9 281.70 369.40 8.49 o -1 4 9 480.30 502.82 9.93 o 0 4 9 388.50 385.85 9.25 o -6 5 9 0.24 0.00 0.79 o -5 5 9 0.23 0.06 0.91 o -4 5 9 4.24 4.29 1.47 o -3 5 9 32.88 43.36 3.32 o -2 5 9 133.74 156.07 5.96 o -5 6 9 9.32 9.64 2.06 o -4 6 9 19.93 25.56 2.82 o -3 6 9 33.51 39.80 3.41 o -2 -5 10 41.38 48.82 3.64 o -1 -5 10 4.25 4.32 1.38 o 0 -5 10 0.10 0.00 0.73 o 1 -5 10 18.08 15.69 2.29 o -4 -4 10 16.47 16.13 2.38 o -3 -4 10 90.55 98.73 5.05 o -2 -4 10 106.69 109.81 5.23 o -1 -4 10 66.90 42.51 3.32 o 0 -4 10 29.38 27.32 2.76 o 1 -4 10 1.89 1.15 1.09 o 2 -4 10 23.03 28.11 2.94 o -4 -3 10 6.32 9.37 1.82 o -3 -3 10 91.51 94.80 4.82 o -2 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10 95.68 112.45 5.20 o -5 2 10 117.39 155.52 5.82 o -4 2 10 168.33 123.70 4.91 o -3 2 10 131.47 113.33 4.76 o -2 2 10 47.57 48.56 3.32 o -1 2 10 0.34 0.91 0.88 o 0 2 10 1.27 1.82 1.23 o -6 3 10 37.37 44.30 3.53 o -5 3 10 72.88 88.51 4.61 o -4 3 10 156.39 217.20 6.79 o -2 3 10 234.51 231.01 6.93 o -1 3 10 39.40 43.01 3.32 o 0 3 10 9.44 10.46 2.00 o -5 4 10 14.33 19.74 2.56 o -4 4 10 66.63 91.45 4.70 o -3 -3 11 48.72 47.91 3.64 o -2 -3 11 98.14 54.73 3.88 o -1 -3 11 142.39 155.99 6.46 o 0 -3 11 39.73 50.94 3.82 o -3 -2 11 20.89 14.83 2.17 o -2 -2 11 68.68 63.48 4.11 o -1 -2 11 110.20 139.27 6.05 o 0 -2 11 52.89 60.84 4.20 o -4 -1 11 2.76 4.44 1.38 o -3 -1 11 0.34 0.24 0.71 o -2 -1 11 10.72 8.78 1.76 o -1 -1 11 25.14 31.26 3.00 o 0 -1 11 1.95 1.53 1.18 o -4 0 11 4.91 3.79 1.26 o -3 0 11 6.24 5.11 1.41 o -2 0 11 5.36 4.79 1.41 o -1 0 11 15.14 17.24 2.35 o 0 0 11 14.55 19.15 2.56 o -4 1 11 22.79 17.63 2.14 o -3 1 11 0.86 0.71 0.85 o -2 1 11 5.20 6.02 1.53 o -1 1 11 43.01 47.85 3.61 o -3 2 11 16.62 19.48 2.35 o -2 2 11 8.82 8.99 1.82 o