#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/87/2218732.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2218732_Fobs loop_ _publ_author_name 'Chen, Rui-Zhan' 'Guo, Fei-Jun' 'Meng, Fan-Lei' _publ_section_title ; (5,5'-Dicarboxybiphenyl-2,2'-dicarboxylato-\k^2^O^2^,O^2'^)bis(1,10-phenanthroline-\k^2^N,N')zinc(II) dihydrate ; _journal_coeditor_code HY2133 _journal_issue 7 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m855 _journal_volume 64 _journal_year 2008 _space_group_IT_number 15 _symmetry_space_group_name_Hall '-C 2yc' _symmetry_space_group_name_H-M 'C 1 2/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 96.429 _cell_angle_gamma 90.000 _cell_length_a 16.9009 _cell_length_b 9.4735 _cell_length_c 22.1262 _exptl_crystal_F_000 1624.00 _reflns_d_resolution_high 0.8055 _[local]_cod_data_source_file hy2133Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' C2C in C2/c' _shelx_refln_list_code 4 _shelx_F_calc_maximum 439.16 _shelx_F_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 110331.22 117646.27 1512.99 o 4 0 0 73.07 126.34 26.35 o 6 0 0 5886.10 5234.43 132.56 o 8 0 0 7228.13 7550.17 183.02 o 10 0 0 1320.00 1209.73 89.53 o 12 0 0 8370.74 8544.16 430.35 o 14 0 0 3511.53 3276.80 330.06 o 16 0 0 6.15 -136.99 136.99 o 18 0 0 11.05 -67.55 145.33 o 20 0 0 4.85 108.42 165.13 o 1 1 0 13424.38 14672.92 134.10 o 3 1 0 23366.58 23824.21 194.79 o 5 1 0 383.01 419.79 26.41 o 7 1 0 1523.28 1332.85 76.13 o 9 1 0 2570.22 3100.18 94.70 o 11 1 0 48.88 19.60 72.79 o 13 1 0 122.70 58.26 92.96 o 15 1 0 2482.64 2622.18 348.51 o 17 1 0 958.42 774.64 165.47 o 19 1 0 614.06 600.85 167.52 o 0 2 0 13150.40 13584.05 257.08 o 2 2 0 24654.85 26707.65 465.65 o 4 2 0 4883.71 5089.45 96.72 o 6 2 0 1756.79 1731.30 68.26 o 8 2 0 968.48 910.45 64.87 o 10 2 0 592.01 571.34 62.99 o 12 2 0 816.26 1019.25 205.89 o 14 2 0 354.38 362.62 111.70 o 16 2 0 1285.95 1091.44 171.23 o 18 2 0 57.01 205.73 180.25 o 20 2 0 62.96 13.25 113.20 o 1 3 0 6284.30 6649.57 152.27 o 3 3 0 643.05 653.26 44.01 o 5 3 0 6899.94 7419.87 96.44 o 7 3 0 149.74 211.56 39.05 o 9 3 0 89.16 67.19 33.60 o 11 3 0 2415.09 2154.14 129.98 o 13 3 0 411.46 338.97 84.18 o 15 3 0 33.59 -59.43 59.43 o 17 3 0 0.40 36.41 106.48 o 19 3 0 78.11 186.02 120.07 o 0 4 0 2225.88 1997.65 135.11 o 2 4 0 776.43 645.62 76.20 o 4 4 0 21389.20 21505.07 249.05 o 6 4 0 5136.18 5277.47 120.07 o 8 4 0 2439.49 2359.15 149.83 o 10 4 0 70.64 109.10 57.93 o 12 4 0 2.11 51.70 53.10 o 14 4 0 151.97 247.76 75.16 o 16 4 0 354.69 340.92 105.56 o 18 4 0 300.08 296.59 107.21 o 1 5 0 6029.29 5920.87 354.35 o 3 5 0 176.46 117.92 34.46 o 5 5 0 336.23 383.90 41.90 o 7 5 0 1520.34 1509.01 110.55 o 9 5 0 133.39 127.23 50.40 o 11 5 0 339.78 481.77 80.13 o 13 5 0 1470.52 1371.11 127.55 o 15 5 0 564.10 545.32 167.01 o 17 5 0 88.10 158.39 68.16 o 0 6 0 10596.07 10366.67 372.59 o 2 6 0 10890.11 10414.18 210.63 o 4 6 0 8116.11 8360.22 197.20 o 6 6 0 5137.38 5054.55 164.17 o 8 6 0 616.20 582.87 75.32 o 10 6 0 1032.71 1085.07 143.54 o 12 6 0 1774.56 1701.45 212.22 o 14 6 0 417.01 279.17 79.84 o 16 6 0 871.92 806.66 111.76 o 1 7 0 4405.65 4442.89 187.75 o 3 7 0 4078.04 3868.24 138.81 o 5 7 0 478.11 543.24 68.73 o 7 7 0 1549.96 1445.17 182.34 o 9 7 0 316.23 393.34 70.17 o 11 7 0 1766.05 1634.90 177.81 o 13 7 0 1296.24 1265.54 133.14 o 15 7 0 43.58 110.84 64.91 o 0 8 0 843.37 1023.53 168.47 o 2 8 0 2151.25 1999.71 152.83 o 4 8 0 317.47 263.34 56.46 o 6 8 0 38.34 106.88 47.31 o 8 8 0 45.25 60.94 45.89 o 10 8 0 421.00 444.03 81.25 o 12 8 0 481.13 539.21 91.64 o 14 8 0 490.46 385.56 87.61 o 1 9 0 0.07 -34.89 34.89 o 3 9 0 111.73 144.89 48.54 o 5 9 0 2.98 -38.70 43.71 o 7 9 0 15.72 40.27 63.34 o 9 9 0 1.33 38.87 50.49 o 11 9 0 11.68 22.43 117.91 o 13 9 0 3.31 3.15 72.87 o 0 10 0 191.59 87.15 93.20 o 2 10 0 320.10 417.73 85.17 o 4 10 0 101.02 173.78 70.44 o 6 10 0 19.37 -48.79 48.79 o 8 10 0 8.17 25.85 94.87 o 10 10 0 235.00 362.45 99.39 o 1 11 0 95.55 493.52 128.23 o 3 11 0 257.74 342.15 120.31 o 5 11 0 302.06 218.72 99.87 o 7 11 0 242.18 50.67 79.23 o -19 1 1 332.71 392.35 146.61 o -17 1 1 36.23 -57.04 111.75 o -15 1 1 34.00 96.02 103.46 o -13 1 1 880.04 865.54 285.33 o -11 1 1 5012.86 4720.01 219.28 o -9 1 1 2364.89 2747.53 156.61 o -7 1 1 13756.17 15523.75 302.85 o -5 1 1 4307.78 4702.28 127.91 o -3 1 1 31502.67 31877.38 276.77 o -1 1 1 849.75 799.54 24.80 o 1 1 1 12652.74 14504.04 114.97 o 3 1 1 59.20 51.01 21.89 o 5 1 1 36.43 42.00 20.09 o 7 1 1 4095.76 4217.38 89.61 o 9 1 1 1997.77 2075.37 84.90 o 11 1 1 6672.44 6305.22 125.78 o 13 1 1 1152.30 1355.30 111.11 o 15 1 1 266.87 424.19 135.93 o 17 1 1 320.22 448.65 200.16 o 19 1 1 9.83 -22.01 118.04 o -20 2 1 138.80 49.17 170.76 o -18 2 1 662.88 540.34 219.66 o -16 2 1 743.47 719.76 146.93 o -14 2 1 1331.25 1206.48 159.70 o -12 2 1 13.17 -19.95 54.55 o -10 2 1 5390.60 5309.64 171.89 o -8 2 1 4414.88 4266.27 275.74 o -6 2 1 90.35 119.32 40.36 o -4 2 1 2012.01 2296.76 77.68 o -2 2 1 1274.01 1079.96 35.82 o 0 2 1 605.69 575.27 44.33 o 2 2 1 66609.19 70898.80 389.09 o 4 2 1 29332.72 28954.29 212.72 o 6 2 1 1405.85 1590.51 45.62 o 8 2 1 4416.96 4033.10 79.61 o 10 2 1 2279.73 2217.86 97.70 o 12 2 1 2532.60 2470.99 114.22 o 14 2 1 224.34 224.74 110.32 o 16 2 1 1836.14 1981.83 236.54 o 18 2 1 536.47 687.18 161.23 o 20 2 1 146.83 -8.03 107.93 o -19 3 1 265.79 370.47 141.12 o -17 3 1 1122.45 1132.01 167.93 o -15 3 1 1967.51 2139.05 199.24 o -13 3 1 1345.11 1763.81 136.02 o -11 3 1 3323.24 3216.35 143.51 o -9 3 1 975.01 954.82 86.80 o -7 3 1 15826.22 15945.24 256.65 o -5 3 1 27205.46 26831.41 312.38 o -3 3 1 23521.01 24359.69 268.59 o -1 3 1 183.72 188.57 30.48 o 1 3 1 29782.74 29264.71 291.10 o 3 3 1 9472.34 10108.89 120.09 o 5 3 1 36785.16 41103.34 295.28 o 7 3 1 23480.22 25340.44 290.76 o 9 3 1 1991.03 1991.11 93.55 o 11 3 1 2689.49 2560.71 179.54 o 13 3 1 1907.64 2037.35 143.94 o 15 3 1 486.09 566.58 101.64 o 17 3 1 933.98 989.80 173.71 o 19 3 1 246.37 404.43 137.99 o -18 4 1 260.58 312.48 103.79 o -16 4 1 365.46 234.43 104.89 o -14 4 1 230.18 467.27 91.38 o -12 4 1 766.81 854.96 103.31 o -10 4 1 279.28 299.67 60.89 o -8 4 1 4913.59 4626.93 151.61 o -6 4 1 1487.84 1331.18 48.56 o -4 4 1 792.56 969.01 67.21 o -2 4 1 2008.27 1860.98 128.54 o 0 4 1 1211.02 1231.09 66.63 o 2 4 1 184.76 171.85 34.86 o 4 4 1 166.36 131.18 25.66 o 6 4 1 2880.57 2672.96 70.35 o 8 4 1 399.06 405.74 53.72 o 10 4 1 1056.18 1066.31 84.03 o 12 4 1 602.10 624.66 162.28 o 14 4 1 1155.23 894.95 110.63 o 16 4 1 1341.49 1386.77 144.86 o 18 4 1 157.93 196.68 116.31 o -17 5 1 106.11 188.35 71.71 o -15 5 1 613.08 593.44 103.28 o -13 5 1 655.70 703.92 111.75 o -11 5 1 70.08 147.86 60.41 o -9 5 1 2179.81 2316.90 130.04 o -7 5 1 595.28 524.11 105.33 o -5 5 1 9947.22 10048.22 208.19 o -3 5 1 2425.36 2260.11 92.77 o -1 5 1 2055.95 1812.94 101.88 o 1 5 1 501.80 519.38 67.92 o 3 5 1 5656.81 5548.59 138.48 o 5 5 1 373.75 497.78 41.25 o 7 5 1 65.19 48.88 31.92 o 9 5 1 2063.38 2017.99 109.19 o 11 5 1 403.09 426.42 80.01 o 13 5 1 859.31 757.45 122.95 o 15 5 1 9.89 88.67 63.99 o 17 5 1 167.69 212.16 69.94 o -16 6 1 8.50 81.34 61.77 o -14 6 1 63.96 132.73 61.83 o -12 6 1 184.95 153.07 67.01 o -10 6 1 240.46 264.28 67.21 o -8 6 1 38.27 45.65 39.54 o -6 6 1 931.92 1037.84 90.37 o -4 6 1 959.25 1060.91 82.76 o -2 6 1 632.10 604.84 75.03 o 0 6 1 14.04 -25.09 32.45 o 2 6 1 534.52 610.76 81.51 o 4 6 1 736.38 769.13 58.92 o 6 6 1 196.52 209.70 50.37 o 8 6 1 0.14 -22.86 46.33 o 10 6 1 458.54 504.81 97.85 o 12 6 1 2.44 61.87 50.69 o 14 6 1 105.64 260.34 69.69 o 16 6 1 17.95 13.66 55.95 o -15 7 1 39.10 4.57 58.66 o -13 7 1 8.00 31.59 68.09 o -11 7 1 221.29 122.12 61.68 o -9 7 1 2697.73 2895.67 151.43 o -7 7 1 1188.01 1195.20 104.97 o -5 7 1 2.43 -41.89 68.45 o -3 7 1 3433.77 3290.08 127.61 o -1 7 1 795.13 788.26 98.96 o 1 7 1 42.54 101.72 45.74 o 3 7 1 41.67 39.50 31.90 o 5 7 1 220.27 225.77 62.50 o 7 7 1 19.23 45.66 37.66 o 9 7 1 735.33 867.98 129.89 o 11 7 1 57.62 34.19 48.58 o 13 7 1 12.42 -9.70 48.92 o 15 7 1 17.81 117.89 71.43 o -14 8 1 151.02 172.89 73.38 o -12 8 1 597.96 535.07 90.60 o -10 8 1 291.06 359.63 73.41 o -8 8 1 1055.90 922.79 101.61 o -6 8 1 3153.37 3051.62 147.51 o -4 8 1 1870.44 1883.13 117.53 o -2 8 1 566.27 509.33 83.98 o 0 8 1 388.85 439.42 86.82 o 2 8 1 415.76 437.31 66.30 o 4 8 1 8.27 55.28 39.69 o 6 8 1 221.65 313.65 61.29 o 8 8 1 594.20 767.85 144.57 o 10 8 1 679.36 725.08 99.45 o 12 8 1 191.43 138.91 90.22 o 14 8 1 43.37 -63.87 68.63 o -13 9 1 354.84 275.57 84.54 o -11 9 1 595.14 565.99 93.96 o -9 9 1 751.73 830.17 107.83 o -7 9 1 866.83 1039.51 109.29 o -5 9 1 620.84 725.68 85.00 o -3 9 1 209.10 250.56 130.42 o -1 9 1 2247.60 2515.72 183.67 o 1 9 1 2556.63 2558.37 139.32 o 3 9 1 361.56 371.26 64.56 o 5 9 1 146.53 311.02 60.62 o 7 9 1 1033.88 1129.33 120.28 o 9 9 1 830.57 837.05 128.41 o 11 9 1 339.99 423.33 104.67 o 13 9 1 392.70 206.77 89.72 o -10 10 1 7.53 -61.30 82.77 o -8 10 1 91.85 38.14 92.99 o -6 10 1 718.35 817.00 125.24 o -4 10 1 1382.63 1237.92 147.10 o -2 10 1 484.48 651.87 104.79 o 0 10 1 125.65 100.44 69.00 o 2 10 1 703.29 776.11 141.26 o 4 10 1 1544.25 1442.20 227.06 o 6 10 1 1193.42 1132.57 141.15 o 8 10 1 156.41 89.46 66.88 o 10 10 1 144.80 98.84 72.68 o -7 11 1 58.60 120.31 104.46 o -5 11 1 133.83 90.70 83.40 o -3 11 1 140.28 140.14 69.64 o -1 11 1 122.48 292.32 140.11 o 1 11 1 35.40 366.75 105.08 o 3 11 1 112.75 -57.96 73.60 o 5 11 1 185.76 25.44 88.61 o 7 11 1 105.76 194.74 103.00 o -20 0 2 440.51 476.42 239.78 o -18 0 2 819.71 998.51 276.47 o -16 0 2 100.92 271.68 189.32 o -14 0 2 538.70 720.58 203.50 o -12 0 2 3674.85 3693.39 290.02 o -10 0 2 26192.36 27359.50 698.06 o -8 0 2 50.16 -16.47 89.86 o -6 0 2 2676.51 3034.31 181.19 o -4 0 2 1824.43 1693.65 125.10 o -2 0 2 48185.61 52045.95 444.61 o 0 0 2 59760.66 65348.38 751.85 o 2 0 2 16750.40 18473.80 166.11 o 4 0 2 952.09 935.16 48.35 o 6 0 2 3168.98 3197.77 92.95 o 8 0 2 35894.66 36253.00 384.16 o 10 0 2 2459.14 2433.24 167.74 o 12 0 2 5521.60 5757.54 317.44 o 14 0 2 2323.64 2384.83 296.70 o 16 0 2 124.55 99.04 149.70 o 18 0 2 725.69 932.00 264.17 o 20 0 2 92.46 9.80 174.31 o -19 1 2 484.79 518.32 154.69 o -17 1 2 399.11 526.27 149.75 o -15 1 2 1062.41 1245.67 181.24 o -13 1 2 1332.11 1180.73 246.97 o -11 1 2 180.34 107.23 79.10 o -9 1 2 2878.01 2942.98 155.68 o -7 1 2 14904.00 15292.74 302.08 o -5 1 2 181.08 224.31 26.16 o -3 1 2 10601.25 11094.92 128.50 o -1 1 2 1525.86 1468.98 28.19 o 1 1 2 7636.82 7792.80 113.82 o 3 1 2 417.21 369.17 26.23 o 5 1 2 27136.00 27730.87 215.69 o 7 1 2 3046.13 3602.53 79.86 o 9 1 2 234.68 364.78 37.63 o 11 1 2 4795.72 4860.78 112.12 o 13 1 2 2136.21 2282.25 128.44 o 15 1 2 1418.80 1359.21 305.35 o 17 1 2 1833.60 1951.31 224.97 o 19 1 2 305.70 323.46 178.48 o -20 2 2 40.15 97.56 124.74 o -18 2 2 114.68 190.13 121.42 o -16 2 2 1985.34 1836.02 205.96 o -14 2 2 757.08 759.51 135.87 o -12 2 2 25.40 28.73 72.75 o -10 2 2 343.11 329.07 68.02 o -8 2 2 1285.14 1284.78 89.85 o -6 2 2 118.59 131.54 41.35 o -4 2 2 86483.99 91591.95 660.92 o -2 2 2 192865.86 206001.09 1316.63 o 0 2 2 227.40 277.54 28.61 o 2 2 2 5467.94 6000.76 124.62 o 4 2 2 3221.05 3299.38 64.91 o 6 2 2 4460.86 4743.59 84.16 o 8 2 2 1327.11 1356.32 53.62 o 10 2 2 1184.68 1174.19 123.56 o 12 2 2 2.94 -4.44 37.46 o 14 2 2 65.10 41.76 67.02 o 16 2 2 18.60 73.67 102.66 o 18 2 2 83.89 222.99 127.05 o 20 2 2 33.04 190.57 122.64 o -19 3 2 90.26 212.97 136.67 o -17 3 2 0.01 5.04 170.24 o -15 3 2 457.41 495.87 120.19 o -13 3 2 93.35 167.18 70.78 o -11 3 2 13.30 -42.46 42.46 o -9 3 2 1551.66 1577.83 103.95 o -7 3 2 392.70 391.80 57.43 o -5 3 2 21590.98 23036.34 284.95 o -3 3 2 4073.68 3958.06 77.43 o -1 3 2 500.10 576.08 34.72 o 1 3 2 299.84 331.17 45.92 o 3 3 2 14923.25 15179.27 167.80 o 5 3 2 3079.64 3244.34 72.39 o 7 3 2 1188.88 1564.69 54.45 o 9 3 2 508.36 528.20 59.65 o 11 3 2 13.20 24.17 38.20 o 13 3 2 422.64 454.70 71.36 o 15 3 2 42.38 -11.25 110.03 o 17 3 2 276.98 235.86 115.52 o 19 3 2 7.46 69.25 147.62 o -18 4 2 111.93 128.91 85.59 o -16 4 2 270.76 333.69 134.38 o -14 4 2 431.07 347.33 111.96 o -12 4 2 264.50 262.50 71.48 o -10 4 2 29.97 -21.27 43.28 o -8 4 2 313.31 272.41 71.13 o -6 4 2 3375.45 3384.95 71.44 o -4 4 2 1699.12 1683.09 79.21 o -2 4 2 6127.67 5820.46 111.70 o 0 4 2 1437.86 1348.92 64.30 o 2 4 2 896.60 794.56 49.41 o 4 4 2 13933.07 14661.04 169.55 o 6 4 2 1740.35 1772.34 71.82 o 8 4 2 4111.58 3922.72 121.69 o 10 4 2 109.82 121.23 38.13 o 12 4 2 268.61 243.81 56.94 o 14 4 2 359.67 334.36 80.89 o 16 4 2 988.64 857.98 121.05 o 18 4 2 0.97 124.89 119.26 o -17 5 2 222.77 212.16 91.37 o -15 5 2 735.79 672.06 104.74 o -13 5 2 1663.41 1751.03 142.17 o -11 5 2 130.34 222.35 60.78 o -9 5 2 29.21 92.68 62.29 o -7 5 2 2239.47 2321.16 115.66 o -5 5 2 3440.40 3408.65 121.76 o -3 5 2 6332.06 6144.99 148.99 o -1 5 2 6160.95 5980.05 142.96 o 1 5 2 13301.86 13589.20 226.44 o 3 5 2 416.06 440.06 43.89 o 5 5 2 1916.10 1855.88 69.64 o 7 5 2 3439.37 3428.65 125.93 o 9 5 2 4740.24 4698.22 145.27 o 11 5 2 243.35 334.58 59.67 o 13 5 2 656.09 797.13 101.74 o 15 5 2 282.95 191.06 85.10 o 17 5 2 154.87 272.44 123.48 o -18 6 2 40.21 101.12 106.34 o -16 6 2 687.44 600.51 102.91 o -14 6 2 415.55 282.81 81.86 o -12 6 2 736.20 1077.54 115.57 o -10 6 2 693.03 749.92 92.51 o -8 6 2 865.62 875.96 92.71 o -6 6 2 1476.10 1393.52 101.06 o -4 6 2 2562.52 2279.48 101.94 o -2 6 2 2682.98 2734.01 153.14 o 0 6 2 5534.18 5816.11 195.54 o 2 6 2 11328.73 10946.35 223.53 o 4 6 2 4920.72 5062.52 119.80 o 6 6 2 2835.52 2789.13 107.98 o 8 6 2 679.95 885.94 80.95 o 10 6 2 2239.03 2057.55 137.85 o 12 6 2 421.21 476.28 84.14 o 14 6 2 541.00 559.53 95.57 o 16 6 2 305.42 265.59 89.87 o -15 7 2 219.62 120.94 79.76 o -13 7 2 390.09 573.86 95.22 o -11 7 2 808.47 832.53 103.11 o -9 7 2 651.25 729.51 92.43 o -7 7 2 59.54 71.48 44.54 o -5 7 2 793.15 827.51 84.08 o -3 7 2 1416.76 1267.79 103.87 o -1 7 2 5556.98 5592.51 160.03 o 1 7 2 1408.31 1493.11 123.85 o 3 7 2 923.98 917.49 77.25 o 5 7 2 496.32 556.13 71.72 o 7 7 2 539.86 542.91 77.90 o 9 7 2 363.05 366.36 71.90 o 11 7 2 2154.31 2170.69 152.61 o 13 7 2 740.90 616.79 99.08 o 15 7 2 3.92 -22.99 117.39 o -14 8 2 204.84 195.82 100.26 o -12 8 2 363.31 297.84 83.38 o -10 8 2 900.89 822.60 110.29 o -8 8 2 1204.42 1094.83 110.81 o -6 8 2 566.06 600.82 79.07 o -4 8 2 1528.26 1348.16 102.37 o -2 8 2 678.68 652.19 73.72 o 0 8 2 850.80 703.93 102.53 o 2 8 2 1810.03 2023.19 161.32 o 4 8 2 138.29 87.54 72.44 o 6 8 2 238.39 240.75 56.21 o 8 8 2 55.30 28.03 44.82 o 10 8 2 109.98 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