#------------------------------------------------------------------------------ #$Date: 2009-05-03 21:56:13 +0300 (Sun, 03 May 2009) $ #$Revision: 691 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2218766.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2218766_Fobs loop_ _publ_author_name 'Kurawa, Mukhtar A.' 'Adams, Christopher J.' 'Orpen, A. Guy' _publ_section_title ; Pentakis(2-oxo-2,3-dihydropyrimidin-1-ium) di-\m~3~-chlorido-tri-\m~2~-chlorido-hexachloridotricadmate(II) ; _journal_coeditor_code LH2641 _journal_issue 7 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m960 _journal_page_last m961 _journal_volume 64 _journal_year 2008 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 104.947 _cell_angle_gamma 90.000 _cell_length_a 17.5446 _cell_length_b 8.0898 _cell_length_c 27.2451 _exptl_crystal_F_000 2344.00 _reflns_d_resolution_high 0.7091 _[local]_cod_data_source_file lh2641Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' I in P2(1)/c' _shelx_refln_list_code 4 _shelx_F_calc_maximum 538.62 _shelx_F_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 133092.63 129900.19 1924.19 o 3 0 0 10983.21 13078.30 166.17 o 4 0 0 205.44 302.65 64.06 o 5 0 0 112193.00 109714.32 1337.06 o 6 0 0 325.99 237.88 30.56 o 7 0 0 19531.98 18716.19 225.47 o 8 0 0 9643.79 9900.03 234.33 o 9 0 0 261.40 416.02 91.39 o 10 0 0 112100.00 113723.02 1363.55 o 11 0 0 38486.54 38857.14 445.32 o 12 0 0 1303.07 1063.95 154.59 o 13 0 0 4402.94 3587.32 235.64 o 14 0 0 6043.01 5334.44 287.71 o 15 0 0 10911.50 10523.46 363.51 o 16 0 0 32218.51 35212.82 903.03 o 17 0 0 5588.58 5043.95 321.90 o 18 0 0 29767.28 30514.88 655.55 o 19 0 0 1009.77 862.53 269.12 o 20 0 0 5413.77 4742.77 424.07 o 21 0 0 11369.62 11956.62 504.75 o 22 0 0 15732.52 17339.69 968.21 o 23 0 0 832.76 1048.22 1097.67 o 1 1 0 104148.56 100917.10 434.10 o 2 1 0 5.39 70.55 32.22 o 3 1 0 28649.49 27651.95 143.13 o 4 1 0 50750.30 50641.75 430.65 o 5 1 0 4025.58 3805.97 90.84 o 6 1 0 74416.63 74830.66 533.68 o 7 1 0 41487.41 41307.68 396.57 o 8 1 0 3996.05 4345.37 76.72 o 9 1 0 12576.47 12651.32 137.00 o 10 1 0 4241.95 4038.85 77.43 o 11 1 0 3733.67 3612.97 102.03 o 12 1 0 24279.87 24325.62 240.49 o 13 1 0 10.69 26.10 52.88 o 14 1 0 1142.46 979.12 70.17 o 15 1 0 23859.08 24640.82 659.34 o 16 1 0 1482.61 1494.88 153.99 o 17 1 0 33076.23 34628.43 453.80 o 18 1 0 3229.94 3314.13 198.35 o 19 1 0 5376.05 5552.35 234.90 o 20 1 0 20839.34 22087.02 528.49 o 21 1 0 5651.16 5755.66 370.81 o 22 1 0 6335.33 5889.27 383.40 o 23 1 0 6084.40 6475.33 434.57 o 0 2 0 12322.70 16608.80 636.19 o 1 2 0 12911.57 12755.52 95.05 o 2 2 0 237.43 302.78 32.95 o 3 2 0 359.53 565.38 46.13 o 4 2 0 65916.07 68151.77 398.87 o 5 2 0 41449.13 42686.21 409.61 o 6 2 0 9307.09 9702.91 128.97 o 7 2 0 21662.95 22666.31 210.08 o 8 2 0 540.26 482.87 64.75 o 9 2 0 9640.53 9950.58 261.33 o 10 2 0 1733.24 1663.62 88.87 o 11 2 0 379.38 289.46 82.39 o 12 2 0 3726.68 3557.37 119.03 o 13 2 0 262.03 209.53 107.88 o 14 2 0 667.05 618.33 111.35 o 15 2 0 7569.78 7610.13 211.11 o 16 2 0 222.35 286.40 149.02 o 17 2 0 83.32 100.90 193.70 o 18 2 0 1097.53 920.01 204.06 o 19 2 0 33.52 46.28 217.14 o 20 2 0 426.03 402.74 303.18 o 21 2 0 488.30 480.68 339.26 o 22 2 0 133.93 168.11 319.99 o 23 2 0 916.96 1004.52 425.88 o 1 3 0 34375.53 33614.28 170.90 o 2 3 0 2220.45 1949.86 50.88 o 3 3 0 1176.69 988.27 47.53 o 4 3 0 60103.84 61881.46 484.26 o 5 3 0 52971.04 56028.20 312.39 o 6 3 0 38388.91 39782.35 536.34 o 7 3 0 28855.30 29467.68 513.65 o 8 3 0 33489.04 34249.14 1610.54 o 9 3 0 7259.08 7304.87 339.17 o 10 3 0 29697.03 30693.21 574.22 o 11 3 0 7134.79 7340.47 218.48 o 12 3 0 25497.88 25442.05 542.91 o 13 3 0 4133.76 4061.13 149.59 o 14 3 0 4354.84 4342.04 250.59 o 15 3 0 31499.18 33139.41 386.87 o 16 3 0 1959.88 1745.86 197.52 o 17 3 0 18265.45 18644.46 381.74 o 18 3 0 9248.71 9175.15 311.91 o 19 3 0 20885.11 22208.51 390.03 o 20 3 0 4072.35 4659.14 317.19 o 21 3 0 2208.76 1963.25 348.87 o 22 3 0 8989.76 9311.05 418.77 o 23 3 0 4411.62 4606.77 568.01 o 0 4 0 290111.28 289822.63 1818.24 o 1 4 0 60.99 62.04 21.76 o 2 4 0 86018.41 88315.97 479.64 o 3 4 0 16884.97 16995.94 187.92 o 4 4 0 1199.30 1155.98 60.46 o 5 4 0 59345.27 58924.88 743.64 o 6 4 0 8705.35 8935.28 282.86 o 7 4 0 42173.13 44246.42 516.92 o 8 4 0 4277.16 4392.84 115.22 o 9 4 0 697.39 575.70 51.46 o 10 4 0 13736.73 13638.78 247.30 o 11 4 0 8415.66 7857.11 255.95 o 12 4 0 6478.91 6745.69 161.46 o 13 4 0 2833.04 2971.40 124.93 o 14 4 0 6313.40 5758.43 218.33 o 15 4 0 3885.44 3861.58 221.26 o 16 4 0 16476.97 17167.03 489.68 o 17 4 0 4177.94 3884.65 266.08 o 18 4 0 17623.61 18317.32 551.53 o 19 4 0 463.12 117.33 289.56 o 20 4 0 4278.57 3974.09 365.20 o 21 4 0 11774.31 12208.42 442.43 o 22 4 0 13994.90 15009.76 504.45 o 1 5 0 73742.72 77249.13 859.90 o 2 5 0 23679.19 24801.29 269.23 o 3 5 0 1623.82 1437.30 103.54 o 4 5 0 6327.74 6234.06 139.33 o 5 5 0 663.54 553.53 70.83 o 6 5 0 9923.51 9736.73 171.29 o 7 5 0 13818.33 13700.88 395.31 o 8 5 0 17375.39 17462.22 286.04 o 9 5 0 445.86 429.18 93.88 o 10 5 0 1017.59 771.16 69.40 o 11 5 0 75.08 64.78 85.47 o 12 5 0 3508.34 3305.22 204.64 o 13 5 0 444.04 495.98 246.70 o 14 5 0 2698.54 2559.99 245.10 o 15 5 0 6232.84 5871.48 277.92 o 16 5 0 560.55 397.62 248.00 o 17 5 0 11569.53 12591.01 342.77 o 18 5 0 450.51 411.77 313.36 o 19 5 0 16.61 69.37 405.12 o 20 5 0 8597.52 8880.72 451.96 o 21 5 0 1896.89 1733.36 530.57 o 0 6 0 115.89 135.20 165.80 o 1 6 0 6131.48 5896.78 137.71 o 2 6 0 4509.68 4787.49 141.86 o 3 6 0 7316.79 6902.11 165.79 o 4 6 0 30387.47 31499.69 291.45 o 5 6 0 12049.75 11928.62 243.60 o 6 6 0 2799.08 2664.24 136.12 o 7 6 0 13545.29 13683.48 223.69 o 8 6 0 1615.65 1413.22 154.17 o 9 6 0 30951.66 31353.23 440.95 o 10 6 0 215.88 206.88 197.62 o 11 6 0 3537.79 3114.44 225.66 o 12 6 0 4274.53 3921.09 248.41 o 13 6 0 28.69 -4.76 101.72 o 14 6 0 4707.51 4402.17 274.79 o 15 6 0 16461.29 16205.61 506.00 o 16 6 0 403.06 244.53 363.58 o 17 6 0 207.11 110.57 355.48 o 18 6 0 5184.99 5626.11 449.94 o 19 6 0 5.08 44.18 105.44 o 20 6 0 593.35 570.96 605.61 o 1 7 0 1465.26 1307.51 143.90 o 2 7 0 12264.55 12534.20 262.91 o 3 7 0 22739.32 23153.05 289.46 o 4 7 0 383.15 233.34 170.97 o 5 7 0 7637.58 7962.40 173.33 o 6 7 0 9788.13 9503.91 219.55 o 7 7 0 753.07 589.12 178.34 o 8 7 0 39723.33 41451.74 768.88 o 9 7 0 442.04 477.53 218.99 o 10 7 0 16683.94 16480.41 401.99 o 11 7 0 324.32 242.88 215.81 o 12 7 0 3223.35 2725.45 244.73 o 13 7 0 6143.68 5952.93 259.27 o 14 7 0 7167.53 7104.01 359.33 o 15 7 0 1335.44 1292.65 397.50 o 16 7 0 8.07 -108.12 285.06 o 17 7 0 6141.27 6439.84 434.39 o 18 7 0 1153.28 1131.91 554.10 o 0 8 0 502.37 295.03 257.88 o 1 8 0 216.90 159.64 170.18 o 2 8 0 8431.63 9112.03 232.42 o 3 8 0 1362.19 1076.05 198.88 o 4 8 0 5540.67 5209.94 202.83 o 5 8 0 9399.72 9418.23 317.39 o 6 8 0 132.15 76.67 169.42 o 7 8 0 4085.97 4131.95 244.97 o 8 8 0 16.84 -5.03 226.54 o 9 8 0 3000.45 3225.62 275.00 o 10 8 0 682.14 350.83 262.37 o 11 8 0 564.84 620.80 379.37 o 12 8 0 3806.82 3688.58 366.61 o 13 8 0 1566.81 1382.78 418.08 o 14 8 0 4673.75 4542.45 460.87 o 15 8 0 1261.83 955.57 535.71 o 16 8 0 474.23 673.76 552.13 o 17 8 0 53.20 -92.99 569.07 o 1 9 0 3969.55 3897.34 249.12 o 2 9 0 8182.39 8174.04 249.88 o 3 9 0 157.91 43.82 76.98 o 4 9 0 334.76 77.89 80.61 o 5 9 0 189.14 100.38 276.18 o 6 9 0 393.49 597.70 324.64 o 7 9 0 291.81 343.35 397.44 o 8 9 0 3094.59 2481.37 514.21 o 9 9 0 177.85 164.54 450.30 o 10 9 0 2805.29 2273.71 462.82 o 11 9 0 228.27 85.49 258.17 o 12 9 0 379.93 361.95 481.61 o 13 9 0 170.93 -79.66 491.32 o 14 9 0 99.87 151.62 581.21 o 0 10 0 17.11 29.67 406.34 o 1 10 0 2459.55 2628.68 450.25 o 2 10 0 3009.20 2902.16 558.20 o 3 10 0 701.54 861.09 550.21 o 4 10 0 7405.22 7919.47 475.13 o 5 10 0 196.79 68.79 612.57 o 6 10 0 224.92 601.00 663.33 o 7 10 0 2483.03 2376.82 701.41 o 8 10 0 183.18 -65.74 509.55 o 9 10 0 5607.99 5822.67 680.79 o 10 10 0 1.51 -39.54 272.88 o 11 10 0 2012.01 2135.55 659.17 o 1 11 0 15.76 -35.96 1018.55 o 2 11 0 8748.29 9233.51 1050.02 o 3 11 0 7449.85 7674.67 1091.37 o 4 11 0 902.85 1450.97 1092.27 o 5 11 0 1063.87 740.77 1168.69 o 6 11 0 704.98 426.12 1210.94 o -23 1 1 752.86 891.06 470.63 o -22 1 1 1846.51 1676.13 455.71 o -21 1 1 2115.46 2198.94 359.29 o -20 1 1 6353.86 6418.78 286.93 o -19 1 1 71.30 73.38 250.57 o -18 1 1 2608.91 2592.49 215.89 o -17 1 1 27259.57 29236.96 546.12 o -16 1 1 483.27 469.63 166.68 o -15 1 1 4162.08 3605.61 175.34 o -14 1 1 3706.00 3316.91 144.58 o -13 1 1 18981.29 19177.40 311.82 o -12 1 1 169.94 148.64 71.69 o -11 1 1 46762.41 47393.76 380.06 o -10 1 1 7280.35 7443.06 109.05 o -9 1 1 21926.20 22152.81 171.32 o -8 1 1 22745.87 23192.70 195.86 o -7 1 1 4674.75 4779.54 70.42 o -6 1 1 132199.63 131849.13 581.68 o -5 1 1 992.03 1088.21 37.04 o -4 1 1 40214.59 40325.12 234.11 o -3 1 1 1559.15 1602.40 66.07 o -2 1 1 18874.18 18930.55 169.32 o -1 1 1 117749.54 115639.77 1073.22 o 0 1 1 26662.26 26568.51 147.36 o 1 1 1 27573.98 28016.22 147.05 o 2 1 1 5251.72 5400.77 60.15 o 3 1 1 49706.22 49697.65 205.85 o 4 1 1 38083.75 38041.12 208.86 o 5 1 1 67284.20 66259.43 481.10 o 6 1 1 28893.52 29054.32 199.93 o 7 1 1 52955.67 52813.51 448.06 o 8 1 1 9978.11 9729.53 93.60 o 9 1 1 3557.61 3632.46 72.24 o 10 1 1 48298.79 47074.47 418.15 o 11 1 1 1760.28 1511.30 68.90 o 12 1 1 18667.24 18405.19 281.00 o 13 1 1 1384.20 1125.58 69.83 o 14 1 1 8948.20 8557.87 227.96 o 15 1 1 2283.41 1941.94 96.02 o 16 1 1 7134.35 6635.19 241.26 o 17 1 1 963.07 881.67 223.48 o 18 1 1 4388.05 4002.64 221.75 o 19 1 1 372.74 398.12 285.28 o 20 1 1 948.95 931.15 418.59 o 21 1 1 4485.21 4533.82 412.14 o 22 1 1 59.93 169.94 405.04 o 23 1 1 6460.15 6736.99 432.26 o -23 2 1 9693.51 10532.23 508.77 o -22 2 1 3523.30 3558.41 388.60 o -21 2 1 12261.78 12474.15 360.86 o -20 2 1 564.43 362.68 262.72 o -19 2 1 5585.04 5532.81 221.24 o -18 2 1 12003.48 11589.25 330.71 o -17 2 1 153.04 101.78 77.20 o -16 2 1 25247.15 26158.44 367.71 o -15 2 1 7538.21 7434.35 156.44 o -14 2 1 6493.89 6262.04 136.10 o -13 2 1 11708.69 11200.26 185.69 o -12 2 1 59092.27 60447.18 663.18 o -11 2 1 16686.64 17288.81 151.52 o -10 2 1 61554.09 62528.77 784.58 o -9 2 1 60298.85 59398.17 728.13 o -8 2 1 969.01 1067.22 44.37 o -7 2 1 217407.03 216715.08 2077.83 o -6 2 1 25780.28 27539.62 243.12 o -5 2 1 146039.67 144377.28 622.39 o -4 2 1 30307.16 31929.98 217.13 o -3 2 1 42255.80 45358.93 191.83 o -2 2 1 32662.22 31635.59 242.11 o -1 2 1 20989.79 21342.91 112.50 o 0 2 1 152536.61 146385.81 965.88 o 1 2 1 47780.88 47162.05 168.08 o 2 2 1 88.40 88.28 33.97 o 3 2 1 1005.57 1114.25 50.14 o 4 2 1 2782.75 3024.16 72.37 o 5 2 1 60823.42 61157.80 502.30 o 6 2 1 193281.67 191605.53 1398.35 o 7 2 1 922.69 828.88 58.73 o 8 2 1 83750.05 83476.25 872.88 o 9 2 1 87305.62 87941.69 1302.91 o 10 2 1 4163.07 3958.06 84.64 o 11 2 1 95963.76 95117.95 577.11 o 12 2 1 473.18 490.53 84.86 o 13 2 1 18053.67 17840.72 262.48 o 14 2 1 163.58 158.94 112.38 o 15 2 1 6500.93 6606.17 189.90 o 16 2 1 21230.57 22686.43 304.65 o 17 2 1 6687.70 6773.12 191.46 o 18 2 1 4688.95 4517.30 200.59 o 19 2 1 4546.54 4701.20 236.92 o 20 2 1 17197.51 18267.56 439.16 o 21 2 1 4013.51 4122.58 322.82 o 22 2 1 12598.79 13932.57 402.50 o 23 2 1 702.44 824.71 481.36 o -23 3 1 4296.95 4695.86 542.21 o -22 3 1 7277.43 7486.71 423.19 o -21 3 1 116.27 65.50 329.08 o -20 3 1 431.47 422.29 288.31 o -19 3 1 1685.03 1385.97 255.71 o -18 3 1 1264.64 1080.99 220.83 o -17 3 1 2228.77 1773.94 205.91 o -16 3 1 757.21 799.85 197.42 o -15 3 1 746.18 712.18 182.24 o -14 3 1 1233.32 1173.19 125.38 o -13 3 1 2031.37 1911.18 104.65 o -12 3 1 2256.70 2114.80 97.48 o -11 3 1 54550.64 55606.10 809.38 o -10 3 1 596.88 657.49 75.83 o -9 3 1 25127.13 26136.12 678.29 o -8 3 1 33279.33 34989.64 607.95 o -7 3 1 13.18 36.80 52.46 o -6 3 1 123957.30 128276.58 1350.31 o -5 3 1 30376.46 32637.40 229.70 o -4 3 1 387.08 387.53 60.90 o -3 3 1 114.80 144.45 43.12 o -2 3 1 25421.14 27323.07 154.11 o -1 3 1 49803.04 49769.97 222.67 o 0 3 1 16392.17 15993.03 101.35 o 1 3 1 14772.46 15527.34 128.46 o 2 3 1 31035.89 30931.79 194.46 o 3 3 1 585.87 507.59 40.94 o 4 3 1 41085.07 41493.48 327.90 o 5 3 1 74525.19 76057.99 717.72 o 6 3 1 2723.51 2588.11 74.89 o 7 3 1 6842.27 6450.70 119.00 o 8 3 1 855.13 923.86 79.43 o 9 3 1 840.92 804.47 123.16 o 10 3 1 13222.51 12944.17 257.91 o 11 3 1 467.73 473.00 76.19 o 12 3 1 17346.58 17813.18 497.20 o 13 3 1 4706.02 4757.13 211.14 o 14 3 1 276.96 343.19 161.14 o 15 3 1 1088.57 809.89 173.44 o 16 3 1 5268.91 5196.17 249.13 o 17 3 1 777.53 795.35 219.79 o 18 3 1 2255.55 2300.02 235.84 o 19 3 1 793.39 571.41 263.82 o 20 3 1 22.64 -9.68 211.14 o 21 3 1 9876.17 9656.36 360.85 o 22 3 1 655.40 615.89 422.51 o -22 4 1 265.75 537.85 495.11 o -21 4 1 1933.70 1782.06 458.97 o -20 4 1 4184.21 4151.21 348.25 o -19 4 1 14037.95 14640.86 305.92 o -18 4 1 319.08 294.20 257.33 o -17 4 1 3170.65 3037.78 245.78 o -16 4 1 1183.02 1045.99 218.87 o -15 4 1 1622.57 1476.43 185.34 o -14 4 1 340.57 284.34 173.45 o -13 4 1 14.80 13.77 31.68 o -12 4 1 449.98 399.33 96.48 o -11 4 1 765.11 588.96 109.60 o -10 4 1 4333.66 4499.00 154.85 o -9 4 1 39237.61 39957.29 546.46 o -8 4 1 17309.04 17901.83 282.31 o -7 4 1 1186.41 1161.99 89.78 o -6 4 1 2217.30 1844.26 152.30 o -5 4 1 66.24 242.50 107.32 o -4 4 1 6024.97 5572.20 129.78 o -3 4 1 19454.60 19589.04 147.29 o -2 4 1 21566.94 22769.92 148.88 o -1 4 1 7312.00 7358.38 84.11 o 0 4 1 3210.41 3391.45 59.59 o 1 4 1 88313.98 90008.69 345.99 o 2 4 1 62725.68 63823.91 403.52 o 3 4 1 241.16 185.67 59.45 o 4 4 1 3906.02 3976.25 82.66 o 5 4 1 2642.25 2340.12 158.72 o 6 4 1 7901.65 8016.93 262.07 o 7 4 1 2100.97 2162.07 127.66 o 8 4 1 4075.37 4250.59 241.81 o 9 4 1 10635.02 10647.99 435.96 o 10 4 1 9057.17 9173.48 187.42 o 11 4 1 2781.39 2488.84 158.66 o 12 4 1 2184.88 2098.35 145.09 o 13 4 1 2532.20 2480.19 106.40 o 14 4 1 301.00 429.44 214.99 o 15 4 1 6480.17 6325.80 211.39 o 16 4 1 3500.82 3040.67 209.44 o 17 4 1 244.46 149.79 250.24 o 18 4 1 22211.88 24309.99 395.71 o 19 4 1 580.81 810.50 318.01 o 20 4 1 1925.57 1581.58 356.84 o 21 4 1 13.44 -34.62 160.32 o 22 4 1 26.62 359.71 569.10 o -21 5 1 3730.98 3477.29 511.55 o -20 5 1 5797.86 5174.22 390.55 o -19 5 1 5695.80 5641.50 357.23 o -18 5 1 2694.14 2970.95 294.71 o -17 5 1 15534.47 16901.25 386.43 o -16 5 1 379.91 366.96 249.48 o -15 5 1 7099.58 6694.57 252.00 o -14 5 1 4579.44 4601.03 235.47 o -13 5 1 15574.83 15259.51 363.56 o -12 5 1 230.46 146.41 189.73 o -11 5 1 5150.54 4810.60 153.50 o -10 5 1 3645.96 3352.91 135.20 o -9 5 1 16119.20 16569.85 234.59 o -8 5 1 1220.95 1189.22 101.56 o -7 5 1 159.01 15.87 29.85 o -6 5 1 12715.23 12227.91 223.69 o -5 5 1 3254.72 3205.98 109.63 o -4 5 1 20878.98 21065.63 291.58 o -3 5 1 17311.18 18042.78 290.22 o -2 5 1 51090.29 53734.10 618.53 o -1 5 1 18370.82 19204.05 261.44 o 0 5 1 707.12 676.88 92.70 o 1 5 1 103631.77 107217.48 544.61 o 2 5 1 47.67 15.20 48.53 o 3 5 1 27704.86 29351.07 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