#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/87/2218768.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2218768_Fobs loop_ _publ_author_name 'Yang, Bo' _publ_section_title ; 1-Hydroxyethyl-2-methyl-5-nitroimidazolium 3-carboxy-4-hydroxybenzenesulfonate ; _journal_coeditor_code LH2643 _journal_issue 7 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o1338 _journal_page_last o1339 _journal_volume 64 _journal_year 2008 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 100.413 _cell_angle_gamma 90.000 _cell_length_a 8.8438 _cell_length_b 13.0249 _cell_length_c 14.1483 _exptl_crystal_F_000 808.00 _reflns_d_resolution_high 0.7828 _[local]_cod_data_source_file lh2643Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' I in P2(1)/n' _shelx_refln_list_code 4 _shelx_F_calc_maximum 304.83 _shelx_F_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 1.74 2.00 0.19 o 4 0 0 60.56 40.14 1.00 o 6 0 0 8.39 13.75 0.98 o 8 0 0 171.65 137.83 3.51 o 10 0 0 9.39 5.54 1.21 o 1 1 0 2716.55 2868.92 27.68 o 2 1 0 1787.48 1785.34 17.21 o 3 1 0 2207.24 2151.46 20.67 o 4 1 0 2968.02 3482.63 33.38 o 5 1 0 1224.48 1420.32 13.94 o 6 1 0 18.00 24.27 0.87 o 7 1 0 1805.31 1912.90 21.67 o 8 1 0 99.88 87.97 2.62 o 9 1 0 15.32 14.91 1.00 o 10 1 0 1.18 0.00 0.72 o 11 1 0 126.29 135.11 3.72 o 0 2 0 2276.86 2228.39 30.38 o 1 2 0 103.64 106.08 1.75 o 2 2 0 10096.12 10653.20 102.40 o 3 2 0 591.13 638.36 6.38 o 4 2 0 4765.15 5103.40 48.72 o 5 2 0 0.50 0.10 0.26 o 6 2 0 189.20 166.57 2.73 o 7 2 0 269.50 245.43 3.58 o 8 2 0 7.54 12.52 0.86 o 9 2 0 110.74 96.83 2.11 o 10 2 0 177.45 174.51 3.20 o 11 2 0 10.78 16.71 1.30 o 1 3 0 4544.24 4755.36 53.32 o 2 3 0 78.52 106.18 2.02 o 3 3 0 2082.77 2180.25 21.01 o 4 3 0 70.05 74.28 1.10 o 5 3 0 337.10 344.94 3.78 o 6 3 0 67.48 60.53 1.38 o 7 3 0 266.23 264.08 3.80 o 8 3 0 451.73 383.74 5.24 o 9 3 0 15.52 15.03 1.02 o 10 3 0 0.67 1.44 0.83 o 0 4 0 3187.48 3547.45 47.96 o 1 4 0 2001.02 2177.83 24.55 o 2 4 0 429.84 420.78 17.16 o 3 4 0 3256.65 3958.34 37.86 o 4 4 0 1191.56 1339.86 13.16 o 5 4 0 127.70 102.81 1.49 o 6 4 0 1231.12 1245.35 13.30 o 7 4 0 69.97 62.94 1.53 o 8 4 0 0.57 2.10 0.64 o 9 4 0 7.08 8.16 0.88 o 10 4 0 13.37 16.12 1.28 o 1 5 0 234.27 261.40 9.25 o 2 5 0 1085.15 1232.71 14.09 o 3 5 0 795.38 728.51 7.74 o 4 5 0 0.42 3.52 0.34 o 5 5 0 177.30 181.96 2.28 o 6 5 0 11.46 8.23 0.61 o 7 5 0 14.60 12.88 0.83 o 8 5 0 58.34 59.48 1.74 o 9 5 0 25.83 26.06 1.35 o 10 5 0 2.35 1.72 0.93 o 0 6 0 14.32 29.34 0.88 o 1 6 0 628.48 684.51 6.84 o 2 6 0 183.80 213.54 2.80 o 3 6 0 1013.43 1152.68 12.09 o 4 6 0 1095.88 1113.20 11.09 o 5 6 0 979.56 926.93 11.35 o 6 6 0 25.37 26.85 0.98 o 7 6 0 241.08 216.89 3.64 o 8 6 0 175.73 163.73 3.12 o 9 6 0 0.75 2.57 0.85 o 10 6 0 86.72 90.45 2.50 o 1 7 0 3742.43 4176.90 40.03 o 2 7 0 156.89 164.49 2.28 o 3 7 0 849.55 923.68 10.82 o 4 7 0 17.88 22.51 0.80 o 5 7 0 905.42 957.64 10.35 o 6 7 0 518.44 484.84 6.15 o 7 7 0 355.64 361.79 5.39 o 8 7 0 97.75 92.34 2.26 o 9 7 0 13.68 15.30 1.23 o 10 7 0 1.49 1.46 1.01 o 0 8 0 2.06 0.77 0.35 o 1 8 0 240.15 251.11 3.03 o 2 8 0 14.18 21.52 0.70 o 3 8 0 193.04 226.24 3.44 o 4 8 0 40.70 39.18 1.21 o 5 8 0 15.12 12.61 0.98 o 6 8 0 294.26 302.46 4.21 o 7 8 0 5.11 4.74 0.79 o 8 8 0 381.91 395.64 6.01 o 9 8 0 203.24 238.06 4.29 o 1 9 0 133.56 104.72 1.59 o 2 9 0 479.92 463.74 5.29 o 3 9 0 421.37 439.24 6.10 o 4 9 0 1.88 0.91 0.43 o 5 9 0 202.70 170.43 2.68 o 6 9 0 179.91 192.14 3.05 o 7 9 0 4.98 4.86 0.82 o 8 9 0 111.41 101.85 2.48 o 9 9 0 14.37 13.27 1.29 o 0 10 0 3.66 4.70 0.75 o 1 10 0 1761.87 1847.00 20.59 o 2 10 0 215.23 171.08 2.58 o 3 10 0 69.99 59.48 1.25 o 4 10 0 9.87 10.91 0.80 o 5 10 0 2.27 6.45 0.96 o 6 10 0 16.76 18.02 1.05 o 7 10 0 2.84 3.89 0.84 o 8 10 0 15.93 19.54 1.32 o 1 11 0 1.82 4.32 0.62 o 2 11 0 94.45 100.87 1.87 o 3 11 0 73.63 74.72 1.60 o 4 11 0 175.59 158.14 8.70 o 5 11 0 99.05 83.25 3.27 o 6 11 0 6.93 6.82 0.82 o 7 11 0 70.87 87.68 3.04 o 8 11 0 29.53 32.97 1.60 o 0 12 0 33.58 33.55 1.59 o 1 12 0 65.99 60.89 1.97 o 2 12 0 409.48 369.27 4.90 o 3 12 0 161.95 152.77 2.58 o 4 12 0 138.65 135.91 2.44 o 5 12 0 11.61 9.95 1.45 o 6 12 0 3.62 3.71 0.86 o 7 12 0 104.91 117.09 2.95 o 1 13 0 5.89 5.40 0.74 o 2 13 0 275.16 270.52 3.94 o 3 13 0 16.18 23.98 1.09 o 4 13 0 11.45 9.31 1.04 o 5 13 0 26.72 27.47 1.55 o 6 13 0 6.74 0.59 0.81 o 0 14 0 15.49 19.09 2.92 o 1 14 0 9.73 11.85 1.79 o 2 14 0 21.08 20.08 2.12 o 3 14 0 33.26 34.32 2.50 o 4 14 0 7.28 15.24 1.99 o 5 14 0 174.51 169.58 5.64 o 6 14 0 0.70 2.36 2.50 o 1 15 0 5.42 1.77 1.37 o 2 15 0 78.37 80.67 3.78 o 3 15 0 6.69 5.06 1.79 o 4 15 0 34.71 34.41 2.80 o 0 16 0 25.24 26.79 3.54 o 1 16 0 54.16 58.55 4.48 o 2 16 0 9.01 8.66 2.03 o 3 16 0 11.47 13.17 2.46 o -11 0 1 71.80 75.23 3.00 o -9 0 1 7.78 16.83 2.22 o -7 0 1 508.26 467.11 8.44 o -5 0 1 4167.51 4422.29 59.93 o -3 0 1 116.21 107.94 1.87 o -1 0 1 116.05 90.68 1.41 o 1 0 1 438.19 355.99 16.26 o 3 0 1 16782.32 17831.87 242.37 o 5 0 1 83.68 67.17 1.46 o 7 0 1 0.02 0.00 0.74 o 9 0 1 0.12 0.00 0.87 o -11 1 1 14.75 22.91 1.38 o -10 1 1 14.06 16.56 1.13 o -9 1 1 38.36 36.37 1.35 o -8 1 1 686.22 645.27 8.07 o -7 1 1 254.89 231.06 3.39 o -6 1 1 501.39 482.07 9.50 o -5 1 1 1098.16 1250.88 12.35 o -4 1 1 196.94 149.58 1.80 o -3 1 1 2109.65 2383.44 22.90 o -2 1 1 12481.01 13042.21 125.18 o -1 1 1 1276.04 1316.52 14.40 o 0 1 1 1175.36 1247.04 15.46 o 1 1 1 3497.13 3608.93 40.72 o 2 1 1 856.20 921.11 9.00 o 3 1 1 1844.14 2014.32 19.42 o 4 1 1 6819.90 7447.15 71.05 o 5 1 1 7.41 5.56 0.34 o 6 1 1 486.07 533.24 6.57 o 7 1 1 38.79 33.83 1.15 o 8 1 1 47.43 45.30 1.34 o 9 1 1 21.60 22.01 1.12 o 10 1 1 39.21 42.73 1.58 o -11 2 1 0.12 0.93 0.85 o -10 2 1 6.51 7.03 0.94 o -9 2 1 124.85 105.56 2.23 o -8 2 1 2.27 3.80 0.67 o -7 2 1 1215.68 1126.52 13.15 o -6 2 1 325.08 301.70 6.28 o -5 2 1 919.29 879.99 8.85 o -4 2 1 2436.96 2632.91 25.36 o -3 2 1 53.05 50.07 1.04 o -2 2 1 2.91 2.27 0.26 o -1 2 1 22948.77 19382.17 369.73 o 0 2 1 2628.64 2745.32 26.41 o 1 2 1 5411.92 5644.04 67.10 o 2 2 1 2545.13 2497.19 28.08 o 3 2 1 5.78 6.57 0.31 o 4 2 1 2158.52 2516.20 24.24 o 5 2 1 1897.87 2046.86 21.21 o 6 2 1 92.12 119.50 2.04 o 7 2 1 754.29 727.62 8.84 o 8 2 1 0.39 0.70 0.59 o 9 2 1 172.72 166.49 2.96 o 10 2 1 47.48 58.49 1.82 o -11 3 1 41.75 45.87 1.77 o -10 3 1 8.61 10.16 1.00 o -9 3 1 0.00 0.55 0.65 o -8 3 1 43.46 45.37 1.36 o -7 3 1 484.24 489.63 6.25 o -6 3 1 325.20 350.89 3.94 o -5 3 1 6.00 3.71 0.36 o -4 3 1 11.37 4.19 0.31 o -3 3 1 1869.80 2137.77 20.65 o -2 3 1 2756.98 2892.27 31.48 o -1 3 1 3407.44 3587.15 34.29 o 0 3 1 30.20 26.96 0.41 o 1 3 1 89.22 85.96 1.27 o 2 3 1 745.35 738.03 8.53 o 3 3 1 69.72 42.31 0.72 o 4 3 1 74.95 69.85 1.05 o 5 3 1 22.60 20.47 0.80 o 6 3 1 1674.78 1741.94 19.68 o 7 3 1 838.31 816.02 9.82 o 8 3 1 40.93 33.79 1.23 o 9 3 1 26.12 20.04 1.12 o 10 3 1 109.56 129.27 2.70 o -10 4 1 69.48 70.15 1.96 o -9 4 1 35.46 36.80 1.72 o -8 4 1 96.64 100.79 2.06 o -7 4 1 631.93 600.81 7.48 o -6 4 1 171.10 156.44 2.10 o -5 4 1 2128.32 2161.97 21.04 o -4 4 1 35.05 47.32 0.86 o -3 4 1 452.82 469.74 5.14 o -2 4 1 226.94 238.91 2.56 o -1 4 1 8908.26 9019.44 88.35 o 0 4 1 195.99 179.85 1.92 o 1 4 1 3852.10 4119.83 41.71 o 2 4 1 1368.28 1397.46 14.38 o 3 4 1 1466.10 1554.85 17.73 o 4 4 1 113.08 137.69 1.74 o 5 4 1 14.25 19.23 0.62 o 6 4 1 1153.71 1088.84 12.62 o 7 4 1 11.86 14.97 0.93 o 8 4 1 0.71 4.08 0.93 o 9 4 1 110.42 108.49 2.30 o 10 4 1 7.45 9.62 1.15 o -10 5 1 10.02 12.88 1.19 o -9 5 1 0.84 2.90 0.96 o -8 5 1 492.75 489.03 6.43 o -7 5 1 53.65 45.04 1.31 o -6 5 1 143.88 126.10 1.97 o -5 5 1 203.25 194.56 2.40 o -4 5 1 2816.29 2944.81 28.40 o -3 5 1 1374.93 1493.72 16.58 o -2 5 1 1481.20 1492.20 14.50 o -1 5 1 6550.73 7256.98 69.25 o 0 5 1 185.21 184.58 2.02 o 1 5 1 5.25 0.77 0.21 o 2 5 1 4965.25 5422.86 55.04 o 3 5 1 1117.60 1146.01 13.21 o 4 5 1 22.21 15.78 0.75 o 5 5 1 30.33 23.96 0.84 o 6 5 1 616.15 611.82 7.49 o 7 5 1 297.44 269.10 5.36 o 8 5 1 4.28 6.06 0.85 o 9 5 1 56.87 54.26 1.78 o 10 5 1 14.41 17.88 1.38 o -10 6 1 15.82 15.76 1.30 o -9 6 1 172.88 199.45 3.71 o -8 6 1 3.74 5.68 0.83 o -7 6 1 748.19 725.94 9.62 o -6 6 1 196.66 166.13 2.70 o -5 6 1 79.70 69.90 1.24 o -4 6 1 4.60 7.90 0.44 o -3 6 1 142.99 156.52 1.92 o -2 6 1 713.74 842.11 8.37 o -1 6 1 629.42 575.66 6.18 o 0 6 1 1354.60 1340.54 15.27 o 1 6 1 2.18 3.05 0.30 o 2 6 1 1540.75 1817.24 18.71 o 3 6 1 777.04 809.89 22.49 o 4 6 1 257.92 340.22 4.36 o 5 6 1 502.65 473.03 5.09 o 6 6 1 89.40 89.91 1.95 o 7 6 1 81.39 77.33 1.92 o 8 6 1 7.11 10.01 0.99 o 9 6 1 147.82 149.86 3.39 o 10 6 1 23.42 26.92 1.56 o -10 7 1 15.88 21.39 1.49 o -9 7 1 19.16 18.00 1.56 o -8 7 1 204.29 197.35 3.56 o -7 7 1 73.00 70.07 1.83 o -6 7 1 211.00 197.08 2.79 o -5 7 1 920.24 898.68 9.76 o -4 7 1 1131.92 1126.92 11.95 o -3 7 1 772.98 806.15 8.14 o -2 7 1 744.95 927.56 9.24 o -1 7 1 114.28 97.35 2.30 o 0 7 1 2211.65 2504.67 28.31 o 1 7 1 13.83 18.33 0.60 o 2 7 1 307.86 235.01 2.87 o 3 7 1 218.18 202.24 2.78 o 4 7 1 24.48 28.15 2.19 o 5 7 1 58.26 61.94 1.31 o 6 7 1 25.89 28.84 1.17 o 7 7 1 137.07 128.48 2.73 o 8 7 1 46.20 47.66 1.64 o 9 7 1 0.06 0.75 0.85 o -9 8 1 9.06 15.49 1.27 o -8 8 1 17.03 19.71 1.23 o -7 8 1 124.31 131.13 2.84 o -6 8 1 653.05 667.04 7.58 o -5 8 1 1078.59 1084.54 12.46 o -4 8 1 1.08 0.64 0.39 o -3 8 1 13.13 9.24 0.53 o -2 8 1 518.92 519.00 5.77 o -1 8 1 279.51 302.01 3.85 o 0 8 1 2.43 8.55 0.50 o 1 8 1 320.76 319.54 3.74 o 2 8 1 10.05 10.99 0.52 o 3 8 1 363.85 320.16 3.84 o 4 8 1 464.91 458.82 7.01 o 5 8 1 244.76 207.54 6.53 o 6 8 1 201.37 201.54 3.42 o 7 8 1 1.49 1.26 0.70 o 8 8 1 0.51 0.99 0.79 o 9 8 1 176.87 213.46 4.02 o -9 9 1 73.72 79.83 3.33 o -8 9 1 94.94 101.95 2.45 o -7 9 1 11.17 9.02 0.93 o -6 9 1 460.92 400.72 5.45 o -5 9 1 125.26 116.15 2.08 o -4 9 1 614.53 624.91 7.03 o -3 9 1 625.39 626.02 6.97 o -2 9 1 174.50 173.24 2.77 o -1 9 1 10.36 9.05 3.16 o 0 9 1 263.34 246.79 4.07 o 1 9 1 226.88 202.80 2.62 o 2 9 1 60.43 58.03 1.17 o 3 9 1 112.00 103.20 1.68 o 4 9 1 347.76 334.06 4.40 o 5 9 1 24.73 14.89 0.99 o 6 9 1 201.84 200.79 3.43 o 7 9 1 31.74 36.47 1.45 o 8 9 1 15.07 19.19 1.27 o 9 9 1 14.10 15.61 1.36 o -8 10 1 0.33 3.80 0.97 o -7 10 1 0.71 2.04 0.75 o -6 10 1 84.83 81.02 2.04 o -5 10 1 61.98 43.39 1.19 o -4 10 1 141.61 130.09 2.06 o -3 10 1 132.93 106.00 2.03 o -2 10 1 314.56 300.04 4.93 o -1 10 1 7.89 7.57 0.77 o 0 10 1 17.72 11.12 0.98 o 1 10 1 465.22 427.71 8.58 o 2 10 1 128.18 116.33 1.84 o 3 10 1 177.83 136.47 2.07 o 4 10 1 220.90 209.98 2.91 o 5 10 1 382.64 347.59 10.32 o 6 10 1 207.77 217.13 4.81 o 7 10 1 0.06 0.00 0.71 o 8 10 1 75.78 81.26 2.45 o -8 11 1 4.80 4.03 1.03 o -7 11 1 44.96 50.33 1.90 o -6 11 1 2.59 1.88 0.69 o -5 11 1 57.62 54.74 1.50 o -4 11 1 182.17 169.43 2.72 o -3 11 1 27.58 27.15 1.25 o -2 11 1 1.03 1.72 0.64 o -1 11 1 966.78 958.09 35.59 o 0 11 1 44.04 35.72 1.35 o 1 11 1 861.88 809.25 9.56 o 2 11 1 139.87 159.80 2.79 o 3 11 1 320.83 309.80 5.20 o 4 11 1 0.71 0.00 0.50 o 5 11 1 2.48 3.23 0.61 o 6 11 1 3.90 3.91 0.88 o 7 11 1 124.05 125.66 2.79 o 8 11 1 22.46 29.12 1.57 o -7 12 1 2.41 2.16 1.60 o -6 12 1 1.16 0.12 1.27 o -5 12 1 77.63 78.11 2.33 o -4 12 1 57.54 48.17 3.78 o -3 12 1 615.78 519.37 8.10 o -2 12 1 110.86 90.00 5.23 o -1 12 1 0.02 0.53 0.55 o 0 12 1 255.13 252.40 5.25 o 1 12 1 168.70 173.34 2.75 o 2 12 1 390.12 384.01 5.07 o 3 12 1 3.80 2.79 0.85 o 4 12 1 436.22 445.27 5.83 o 5 12 1 26.75 27.91 1.38 o 6 12 1 16.13 14.96 1.25 o 7 12 1 8.90 5.35 2.66 o -7 13 1 4.46 3.87 2.05 o -6 13 1 0.17 0.00 1.16 o -5 13 1 4.56 4.75 1.66 o -4 13 1 18.71 20.38 2.01 o -3 13 1 152.74 120.61 11.07 o -2 13 1 138.75 143.67 3.21 o -1 13 1 71.17 75.10 2.20 o 0 13 1 237.41 232.37 5.87 o 1 13 1 0.13 0.07 0.75 o 2 13 1 35.10 36.63 2.50 o 3 13 1 84.54 86.80 2.42 o 4 13 1 0.67 1.37 0.80 o 5 13 1 0.41 1.56 1.51 o 6 13 1 0.24 0.94 1.23 o -6 14 1 15.17 18.83 1.87 o -5 14 1 5.09 2.52 2.33 o -4 14 1 11.13 10.81 1.31 o -3 14 1 11.99 12.58 1.27 o -2 14 1 15.82 17.28 1.65 o -1 14 1 15.15 15.44 1.24 o 0 14 1 259.87 260.72 9.36 o 1 14 1 1.28 0.73 0.87 o 2 14 1 24.84 23.11 1.44 o 3 14 1 24.60 31.98 1.60 o 4 14 1 36.68 46.13 1.91 o 5 14 1 8.61 8.61 2.92 o -4 15 1 14.43 12.95 2.11 o -3 15 1 62.17 62.82 3.43 o -2 15 1 1.21 1.74 1.50 o -1 15 1 1.05 0.57 1.39 o 0 15 1 9.39 9.21 1.77 o 1 15 1 60.88 57.10 3.17 o 2 15 1 25.96 28.06 2.45 o 3 15 1 125.61 143.60 7.32 o 4 15 1 7.35 9.69 3.26 o -3 16 1 2.44 1.40 1.79 o -2 16 1 18.17 26.83 2.64 o -1 16 1 4.74 5.49 1.84 o 0 16 1 0.62 0.62 1.55 o 1 16 1 1.62 3.14 1.74 o 2 16 1 1.11 0.00 1.91 o -10 0 2 8.24 9.20 1.35 o -8 0 2 126.42 102.89 2.88 o -6 0 2 758.40 692.18 16.49 o -4 0 2 100.67 114.16 2.07 o -2 0 2 1582.96 1720.40 26.88 o 0 0 2 1201.45 1434.94 26.40 o 2 0 2 4645.49 4953.09 76.26 o 4 0 2 8.87 1.00 0.48 o 6 0 2 5.62 9.02 3.09 o 8 0 2 388.54 363.09 7.10 o 10 0 2 28.58 33.90 2.07 o -11 1 2 20.22 26.99 1.44 o -10 1 2 0.01 0.30 0.73 o -9 1 2 187.51 183.70 3.11 o -8 1 2 126.46 103.96 2.05 o -7 1 2 184.40 165.59 2.66 o -6 1 2 143.26 134.45 2.41 o -5 1 2 157.76 135.36 1.76 o -4 1 2 120.09 158.70 1.90 o -3 1 2 148.72 116.97 1.41 o -2 1 2 626.03 691.70 7.25 o -1 1 2 60.81 64.87 0.81 o 0 1 2 0.01 2.97 0.34 o 1 1 2 2989.24 3228.94 30.85 o 2 1 2 281.48 347.47 4.12 o 3 1 2 1251.06 1308.27 13.57 o 4 1 2 53.52 55.99 1.28 o 5 1 2 1131.68 1035.03 11.89 o 6 1 2 70.50 67.23 1.44 o 7 1 2 122.50 106.45 2.02 o 8 1 2 3.40 3.80 0.68 o 9 1 2 79.91 86.02 2.02 o 10 1 2 2.06 2.47 0.84 o -11 2 2 14.62 15.26 1.24 o -10 2 2 120.56 131.37 2.74 o -9 2 2 8.60 8.65 0.88 o -8 2 2 107.37 90.42 1.91 o -7 2 2 90.18 81.26 1.75 o -6 2 2 103.88 100.26 1.50 o -5 2 2 73.28 107.48 1.49 o -4 2 2 376.70 431.26 4.51 o -3 2 2 4343.32 4668.96 44.58 o -2 2 2 1675.54 1918.59 18.41 o -1 2 2 83.72 89.06 1.01 o 0 2 2 3373.95 3495.06 33.64 o 1 2 2 1227.64 1317.08 12.69 o 2 2 2 4984.08 5198.35 50.28 o 3 2 2 408.31 465.52 4.73 o 4 2 2 1786.37 1916.42 18.57 o 5 2 2 0.00 0.83 0.79 o 6 2 2 78.58 76.12 1.57 o 7 2 2 179.76 161.82 2.68 o 8 2 2 34.88 37.65 1.30 o 9 2 2 23.98 22.04 1.16 o 10 2 2 1.26 1.04 0.91 o -11 3 2 1.26 2.75 0.94 o -10 3 2 0.17 0.00 0.74 o -9 3 2 385.03 344.32 4.93 o -8 3 2 18.96 18.45 0.97 o -7 3 2 1437.32 1424.36 16.37 o -6 3 2 5.76 5.94 0.48 o -5 3 2 227.46 217.11 2.57 o -4 3 2 134.56 149.14 1.84 o -3 3 2 1814.63 1740.87 17.94 o -2 3 2 210.55 271.64 3.03 o -1 3 2 931.10 1001.54 9.73 o 0 3 2 4686.05 4821.48 46.12 o 1 3 2 2805.75 2772.64 28.20 o 2 3 2 506.54 543.93 5.44 o 3 3 2 1478.47 1581.75 17.99 o 4 3 2 144.55 175.47 2.07 o 5 3 2 1930.25 2089.97 21.67 o 6 3 2 31.85 26.59 0.97 o 7 3 2 377.09 360.20 4.88 o 8 3 2 80.41 70.31 1.70 o 9 3 2 41.95 41.59 1.46 o 10 3 2 51.64 50.32 2.61 o -10 4 2 52.99 56.85 1.76 o -9 4 2 80.82 69.25 2.39 o -8 4 2 256.02 246.91 3.73 o -7 4 2 779.86 777.21 9.37 o -6 4 2 1313.58 1321.31 19.77 o -5 4 2 353.17 427.54 4.61 o -4 4 2 207.13 177.15 2.14 o -3 4 2 535.53 548.79 6.50 o -2 4 2 3038.65 3192.04 30.59 o -1 4 2 1196.02 1332.88 12.90 o 0 4 2 58.25 45.64 0.83 o 1 4 2 1601.66 1875.33 22.18 o 2 4 2 2382.64 2471.80 23.76 o 3 4 2 1498.13 1604.13 15.59 o 4 4 2 393.54 385.40 8.10 o 5 4 2 84.97 68.29 1.47 o 6 4 2 301.20 292.10 4.01 o 7 4 2 346.17 331.91 4.57 o 8 4 2 250.07 242.24 3.72 o 9 4 2 5.24 4.10 0.86 o 10 4 2 4.70 5.77 1.06 o -10 5 2 3.53 4.83 0.98 o -9 5 2 185.73 198.48 3.35 o -8 5 2 71.95 67.75 1.70 o -7 5 2 0.03 0.00 0.52 o -6 5 2 13.75 16.78 0.72 o -5 5 2 480.06 472.75 7.68 o -4 5 2 173.69 167.00 2.20 o -3 5 2 1399.20 1616.54 15.74 o -2 5 2 709.05 724.81 7.22 o -1 5 2 904.97 910.19 8.94 o 0 5 2 953.70 1018.39 9.95 o 1 5 2 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