#------------------------------------------------------------------------------ #$Date: 2009-05-05 17:46:52 +0300 (Tue, 05 May 2009) $ #$Revision: 697 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2218802.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2218802_Fobs loop_ _publ_author_name 'Chen, Hong-Xian' 'Li, Zhong-Shu' 'Sun, Bai-Wang' _publ_section_title ; 4,4,5,5-Tetramethyl-2-(4-pyridyl)imidazolidin-1-oxyl-3-oxide trichloroacetic acid solvate ; _journal_coeditor_code RZ2217 _journal_issue 7 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o1197 _journal_volume 64 _journal_year 2008 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 115.329 _cell_angle_gamma 90.000 _cell_length_a 10.0029 _cell_length_b 21.0361 _cell_length_c 9.2796 _exptl_crystal_F_000 820.00 _reflns_d_resolution_high 0.8409 _[local]_cod_data_source_file rz2217Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 1 in P2(1)/c' _shelx_refln_list_code 4 _shelx_F_calc_maximum 206.34 _shelx_F_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 7147.53 6673.40 326.69 o 3 0 0 16777.05 16225.68 349.02 o 4 0 0 6960.88 7039.89 189.99 o 5 0 0 2537.18 2568.03 97.07 o 6 0 0 284.49 292.27 30.16 o 7 0 0 360.14 356.33 39.98 o 8 0 0 0.25 16.59 27.38 o 9 0 0 0.12 41.85 29.05 o 10 0 0 412.47 558.02 85.96 o 1 1 0 18.27 19.29 3.39 o 2 1 0 862.66 902.67 16.93 o 3 1 0 13.81 13.95 6.76 o 4 1 0 1065.40 1006.47 29.47 o 5 1 0 2300.68 2461.47 64.20 o 6 1 0 2.08 14.33 15.69 o 7 1 0 402.53 374.30 27.05 o 8 1 0 69.16 73.30 21.55 o 9 1 0 29.93 24.85 20.93 o 10 1 0 306.78 288.23 46.77 o 1 2 0 347.01 312.84 7.63 o 2 2 0 465.36 440.23 12.84 o 3 2 0 50.01 46.75 6.78 o 4 2 0 766.98 746.04 32.21 o 5 2 0 196.05 182.62 17.83 o 6 2 0 262.59 268.96 19.90 o 7 2 0 473.30 507.25 32.23 o 8 2 0 110.88 138.96 20.18 o 9 2 0 184.60 230.69 32.55 o 10 2 0 12.18 43.49 31.52 o 1 3 0 557.09 591.17 17.62 o 2 3 0 2562.57 2460.16 50.81 o 3 3 0 3246.54 3363.21 59.01 o 4 3 0 72.81 78.19 14.37 o 5 3 0 119.58 130.12 11.89 o 6 3 0 807.53 721.44 37.96 o 7 3 0 611.16 565.92 31.48 o 8 3 0 117.96 104.59 22.85 o 9 3 0 130.15 163.81 30.14 o 10 3 0 150.48 128.04 35.60 o 0 4 0 42574.42 37565.52 495.98 o 1 4 0 127.46 152.28 9.61 o 2 4 0 606.60 627.69 23.45 o 3 4 0 112.68 124.57 10.95 o 4 4 0 2708.12 2714.93 57.23 o 5 4 0 51.92 83.26 14.71 o 6 4 0 74.92 99.69 17.47 o 7 4 0 183.07 176.04 18.80 o 8 4 0 132.07 145.05 19.74 o 9 4 0 7.29 32.83 20.96 o 10 4 0 153.53 73.49 51.19 o 1 5 0 13.04 20.89 4.35 o 2 5 0 2553.50 2819.43 97.70 o 3 5 0 3512.28 3599.82 57.87 o 4 5 0 3639.85 3866.39 76.32 o 5 5 0 70.78 82.10 14.17 o 6 5 0 242.88 211.99 15.68 o 7 5 0 98.18 102.59 16.27 o 8 5 0 144.67 149.38 20.87 o 9 5 0 297.78 280.77 53.41 o 10 5 0 82.09 71.98 37.64 o 0 6 0 1570.29 1610.10 45.69 o 1 6 0 74.25 60.63 6.04 o 2 6 0 4.16 9.28 6.06 o 3 6 0 3360.83 3532.94 134.06 o 4 6 0 52.91 53.44 10.82 o 5 6 0 47.54 63.72 17.55 o 6 6 0 726.37 646.52 31.28 o 7 6 0 13.33 12.85 11.56 o 8 6 0 210.68 207.53 24.68 o 9 6 0 27.39 73.78 66.24 o 10 6 0 2.20 45.28 74.95 o 1 7 0 1430.53 1424.11 44.24 o 2 7 0 117.78 126.03 10.74 o 3 7 0 5941.58 5765.30 216.27 o 4 7 0 46.79 48.94 7.20 o 5 7 0 317.27 292.35 14.25 o 6 7 0 197.48 189.08 16.97 o 7 7 0 997.60 988.31 46.55 o 8 7 0 4.22 45.04 25.98 o 9 7 0 145.42 142.93 37.58 o 10 7 0 88.37 64.78 57.98 o 0 8 0 2050.58 2144.30 66.23 o 1 8 0 6738.55 7406.83 133.63 o 2 8 0 6096.46 5698.57 120.90 o 3 8 0 1934.13 1963.39 81.89 o 4 8 0 903.64 955.96 32.98 o 5 8 0 52.59 38.04 11.29 o 6 8 0 449.90 410.16 41.02 o 7 8 0 2.05 14.81 26.25 o 8 8 0 102.51 118.51 31.15 o 9 8 0 16.07 0.00 20.65 o 10 8 0 21.19 22.65 32.38 o 1 9 0 281.66 316.39 17.59 o 2 9 0 3.12 39.53 10.31 o 3 9 0 422.22 403.65 20.30 o 4 9 0 9.00 30.10 15.03 o 5 9 0 21.91 23.50 14.62 o 6 9 0 1.47 60.46 33.22 o 7 9 0 41.44 56.75 25.55 o 8 9 0 50.41 9.50 24.34 o 9 9 0 20.73 45.55 35.40 o 10 9 0 13.91 0.00 27.42 o 0 10 0 603.06 594.42 32.79 o 1 10 0 1504.13 1610.50 42.57 o 2 10 0 95.91 77.58 14.29 o 3 10 0 79.21 96.99 15.91 o 4 10 0 68.49 122.15 18.82 o 5 10 0 256.46 232.94 21.40 o 6 10 0 294.70 258.75 34.85 o 7 10 0 217.44 242.01 37.79 o 8 10 0 68.84 163.55 37.28 o 9 10 0 256.58 205.37 43.98 o 1 11 0 2158.78 2132.16 56.56 o 2 11 0 64.48 90.26 14.59 o 3 11 0 1.21 17.60 11.86 o 4 11 0 457.26 425.59 28.94 o 5 11 0 1441.21 1282.51 81.29 o 6 11 0 245.88 248.26 37.96 o 7 11 0 415.64 380.55 42.34 o 8 11 0 257.72 387.18 51.01 o 9 11 0 22.01 7.77 36.50 o 0 12 0 2921.88 2979.75 108.25 o 1 12 0 53.75 56.13 18.94 o 2 12 0 190.19 171.23 16.08 o 3 12 0 1389.22 1494.85 54.32 o 4 12 0 166.26 180.97 31.27 o 5 12 0 16.63 20.20 18.53 o 6 12 0 462.03 508.04 51.02 o 7 12 0 22.12 30.20 49.22 o 8 12 0 29.93 107.74 68.56 o 9 12 0 5.89 10.05 26.40 o 1 13 0 79.75 92.83 11.56 o 2 13 0 1018.18 1005.84 29.64 o 3 13 0 34.26 42.48 14.07 o 4 13 0 122.09 149.41 20.98 o 5 13 0 41.42 68.49 29.70 o 6 13 0 134.87 145.10 32.18 o 7 13 0 10.17 0.00 25.30 o 8 13 0 77.95 41.99 29.47 o 9 13 0 39.65 90.86 37.35 o 0 14 0 3.43 0.00 16.68 o 1 14 0 912.94 911.70 35.82 o 2 14 0 1264.09 1196.44 54.54 o 3 14 0 676.34 703.61 38.94 o 4 14 0 145.62 126.72 27.46 o 5 14 0 17.51 73.53 27.93 o 6 14 0 451.93 488.12 52.06 o 7 14 0 3.79 72.43 61.04 o 8 14 0 0.63 0.00 27.58 o 1 15 0 119.48 129.85 15.17 o 2 15 0 105.62 130.95 26.10 o 3 15 0 239.87 239.26 29.23 o 4 15 0 1080.11 968.39 47.82 o 5 15 0 0.56 0.00 25.04 o 6 15 0 165.38 112.69 33.64 o 7 15 0 46.93 46.15 31.72 o 8 15 0 123.02 136.23 41.04 o 0 16 0 960.71 888.92 56.91 o 1 16 0 1163.99 1115.91 44.25 o 2 16 0 53.57 52.01 20.57 o 3 16 0 1147.68 1070.67 54.52 o 4 16 0 322.52 296.33 26.66 o 5 16 0 7.59 7.29 25.02 o 6 16 0 7.83 37.56 37.36 o 7 16 0 3.06 0.00 30.95 o 8 16 0 0.01 1.47 45.98 o 1 17 0 102.61 120.33 18.21 o 2 17 0 556.65 529.34 38.55 o 3 17 0 3.51 0.00 12.94 o 4 17 0 115.97 134.07 20.30 o 5 17 0 0.94 42.70 31.07 o 6 17 0 8.42 41.71 28.87 o 7 17 0 48.09 27.80 32.91 o 0 18 0 343.50 250.36 37.78 o 1 18 0 569.25 541.48 32.87 o 2 18 0 1959.76 1996.15 91.88 o 3 18 0 41.45 68.15 20.38 o 4 18 0 0.08 73.89 36.25 o 5 18 0 4.70 8.27 26.24 o 6 18 0 80.65 40.17 27.88 o 7 18 0 28.70 16.57 31.40 o 1 19 0 177.86 200.77 32.14 o 2 19 0 14.14 40.68 25.07 o 3 19 0 432.17 469.65 39.37 o 4 19 0 0.27 29.24 27.55 o 5 19 0 22.60 43.46 30.56 o 6 19 0 34.04 25.49 27.66 o 0 20 0 73.41 77.42 62.79 o 1 20 0 830.04 847.06 74.59 o 2 20 0 8.20 34.98 24.11 o 3 20 0 0.33 9.86 19.28 o 4 20 0 13.71 0.00 25.14 o 5 20 0 7.61 89.44 69.08 o 6 20 0 39.17 21.44 31.24 o 1 21 0 14.68 8.66 27.70 o 2 21 0 20.06 12.95 23.17 o 3 21 0 12.07 0.35 16.05 o 4 21 0 69.06 70.31 32.38 o 5 21 0 46.10 65.10 36.10 o 0 22 0 536.08 613.87 82.84 o 1 22 0 90.47 154.84 58.81 o 2 22 0 10.56 54.84 39.42 o 3 22 0 60.44 95.34 61.66 o 4 22 0 105.03 154.22 46.09 o 5 22 0 1.90 0.00 31.56 o 1 23 0 6.05 0.00 41.89 o 2 23 0 6.10 4.23 19.97 o 3 23 0 0.02 2.19 25.74 o 4 23 0 0.45 0.00 24.50 o 0 24 0 1.39 6.73 35.20 o 1 24 0 201.39 199.52 42.87 o 2 24 0 4.48 0.00 29.82 o 3 24 0 144.43 85.98 36.49 o -11 1 1 232.77 194.32 59.89 o -10 1 1 7.68 39.96 24.95 o -9 1 1 75.74 114.97 21.95 o -8 1 1 17.13 11.72 14.83 o -7 1 1 216.08 197.87 20.85 o -6 1 1 5.50 77.13 33.16 o -5 1 1 0.59 5.99 13.58 o -4 1 1 827.76 983.29 35.71 o -3 1 1 301.27 305.48 12.87 o -2 1 1 15788.14 15100.07 351.92 o -1 1 1 616.98 537.77 16.49 o 0 1 1 1010.71 850.43 27.18 o 1 1 1 6651.32 6324.91 195.42 o 2 1 1 4991.85 5188.40 83.08 o 3 1 1 6786.93 7428.75 235.47 o 4 1 1 1356.67 1418.69 59.58 o 5 1 1 72.44 64.05 12.24 o 6 1 1 186.13 203.44 21.51 o 7 1 1 61.59 97.46 19.94 o 8 1 1 42.57 77.55 24.97 o 9 1 1 47.90 57.32 29.65 o 10 1 1 88.14 116.93 35.43 o -11 2 1 1.32 0.00 28.37 o -10 2 1 261.29 305.90 46.25 o -9 2 1 446.07 397.93 33.71 o -8 2 1 524.94 497.32 32.47 o -7 2 1 403.29 454.87 27.57 o -6 2 1 1537.41 1547.90 49.21 o -5 2 1 64.44 83.44 10.73 o -4 2 1 1485.40 1497.73 34.87 o -3 2 1 1586.45 1727.41 64.00 o -2 2 1 1108.64 1042.02 32.05 o -1 2 1 11335.28 9861.17 160.14 o 0 2 1 7.38 7.01 1.78 o 1 2 1 38471.39 38495.26 407.98 o 2 2 1 13851.41 14430.82 212.45 o 3 2 1 8443.34 8646.80 195.06 o 4 2 1 4522.05 4681.90 104.40 o 5 2 1 178.90 182.32 16.61 o 6 2 1 28.44 38.73 23.46 o 7 2 1 1042.73 896.42 61.85 o 8 2 1 24.15 0.00 14.54 o 9 2 1 94.01 104.34 24.91 o 10 2 1 4.13 0.00 21.33 o -11 3 1 497.90 562.01 132.07 o -10 3 1 174.27 173.99 34.52 o -9 3 1 47.28 89.10 32.52 o -8 3 1 78.62 94.20 17.46 o -7 3 1 559.95 526.94 28.33 o -6 3 1 2012.16 1981.38 56.55 o -5 3 1 392.05 400.61 39.53 o -4 3 1 969.44 943.83 23.63 o -3 3 1 229.85 292.17 15.78 o -2 3 1 2919.37 2767.91 62.86 o -1 3 1 262.23 220.50 10.46 o 0 3 1 2170.87 2094.79 63.37 o 1 3 1 19424.70 20582.49 353.39 o 2 3 1 2609.33 2701.33 47.97 o 3 3 1 579.63 589.97 25.55 o 4 3 1 861.41 749.97 28.32 o 5 3 1 1107.13 1103.94 38.62 o 6 3 1 153.48 119.32 15.62 o 7 3 1 219.39 209.24 22.63 o 8 3 1 405.73 399.26 34.60 o 9 3 1 11.78 19.58 19.43 o 10 3 1 8.60 30.92 36.17 o -11 4 1 27.11 98.93 54.81 o -10 4 1 57.38 28.86 24.35 o -9 4 1 6.12 24.36 20.77 o -8 4 1 935.11 958.46 55.20 o -7 4 1 320.15 302.44 21.36 o -6 4 1 490.21 469.22 22.48 o -5 4 1 2674.29 2747.76 61.51 o -4 4 1 2287.05 2331.79 73.76 o -3 4 1 1095.35 1072.78 29.81 o -2 4 1 515.14 476.01 15.12 o -1 4 1 4.82 20.84 9.23 o 0 4 1 865.50 946.72 20.27 o 1 4 1 2848.63 2939.78 44.24 o 2 4 1 10225.60 10625.22 237.26 o 3 4 1 1460.51 1560.29 38.20 o 4 4 1 91.84 118.52 11.87 o 5 4 1 228.00 228.24 17.91 o 6 4 1 143.69 148.14 16.91 o 7 4 1 77.08 119.32 19.90 o 8 4 1 67.34 114.47 21.01 o 9 4 1 4.66 16.26 20.83 o 10 4 1 55.23 68.84 78.48 o -10 5 1 110.54 82.97 36.07 o -9 5 1 190.63 230.73 31.68 o -8 5 1 268.04 314.46 33.08 o -7 5 1 40.67 78.24 12.65 o -6 5 1 3.06 0.00 8.05 o -5 5 1 150.52 139.33 14.45 o -4 5 1 17.65 20.51 8.36 o -3 5 1 3102.87 2788.51 58.23 o -2 5 1 8.26 16.45 6.30 o -1 5 1 1.08 21.54 9.86 o 0 5 1 7638.38 7859.60 111.65 o 1 5 1 812.38 720.64 23.38 o 2 5 1 683.28 763.84 18.38 o 3 5 1 1281.84 1431.27 34.87 o 4 5 1 0.05 19.08 9.40 o 5 5 1 219.62 238.69 18.42 o 6 5 1 847.17 745.44 32.93 o 7 5 1 293.67 283.81 24.12 o 8 5 1 7.79 2.76 12.65 o 9 5 1 104.97 112.83 76.77 o 10 5 1 33.02 1.19 30.91 o -10 6 1 7.47 0.00 27.93 o -9 6 1 78.08 70.59 21.87 o -8 6 1 292.34 298.79 28.87 o -7 6 1 47.20 106.24 27.30 o -6 6 1 804.07 689.16 23.10 o -5 6 1 1129.67 1156.61 59.78 o -4 6 1 1825.16 1927.91 58.23 o -3 6 1 16.64 18.78 6.30 o -2 6 1 2045.25 2102.58 36.59 o -1 6 1 52.48 85.84 12.24 o 0 6 1 396.57 310.37 12.73 o 1 6 1 7872.54 7994.98 117.69 o 2 6 1 1707.69 1701.42 34.23 o 3 6 1 19.42 29.04 16.21 o 4 6 1 94.27 71.37 10.91 o 5 6 1 2799.68 2835.66 74.22 o 6 6 1 552.27 493.72 27.69 o 7 6 1 621.34 569.04 39.02 o 8 6 1 0.29 19.51 20.48 o 9 6 1 9.68 0.00 33.49 o -10 7 1 64.50 109.19 48.37 o -9 7 1 24.35 86.73 37.77 o -8 7 1 44.91 50.61 37.79 o -7 7 1 22.33 46.53 17.49 o -6 7 1 613.56 597.25 31.08 o -5 7 1 3.98 18.61 15.11 o -4 7 1 81.61 91.06 8.30 o -3 7 1 2149.40 2059.76 34.22 o -2 7 1 93.50 60.86 8.05 o -1 7 1 2028.95 1993.90 40.13 o 0 7 1 5736.25 5583.00 95.50 o 1 7 1 1570.51 1604.25 32.69 o 2 7 1 319.91 262.69 19.17 o 3 7 1 2685.78 2702.38 79.86 o 4 7 1 33.75 36.27 15.04 o 5 7 1 342.67 324.30 22.04 o 6 7 1 0.01 4.79 14.38 o 7 7 1 93.24 110.77 15.48 o 8 7 1 23.16 19.84 32.84 o 9 7 1 0.08 42.17 31.96 o -10 8 1 56.11 114.22 42.85 o -9 8 1 1.52 0.00 28.17 o -8 8 1 94.47 173.92 37.16 o -7 8 1 74.66 82.64 18.17 o -6 8 1 1670.10 1532.96 111.56 o -5 8 1 0.05 11.05 17.78 o -4 8 1 1215.21 1112.09 49.29 o -3 8 1 2130.73 2362.04 54.37 o -2 8 1 597.26 569.14 17.74 o -1 8 1 806.35 753.09 23.45 o 0 8 1 3233.26 3236.58 85.66 o 1 8 1 213.23 208.35 14.30 o 2 8 1 61.64 95.49 12.47 o 3 8 1 1643.57 1531.43 48.38 o 4 8 1 284.97 254.42 17.83 o 5 8 1 175.80 174.76 26.78 o 6 8 1 288.00 255.05 21.96 o 7 8 1 22.17 21.21 18.97 o 8 8 1 46.59 0.18 28.18 o 9 8 1 156.44 115.73 57.23 o -10 9 1 7.08 16.12 29.67 o -9 9 1 2.25 23.56 31.14 o -8 9 1 5.87 53.12 44.62 o -7 9 1 825.84 907.87 67.94 o -6 9 1 372.64 357.02 38.91 o -5 9 1 128.62 154.53 24.09 o -4 9 1 974.89 864.09 24.87 o -3 9 1 52.05 26.38 12.45 o -2 9 1 1254.32 1316.33 31.99 o -1 9 1 176.20 196.85 13.15 o 0 9 1 744.15 666.78 28.55 o 1 9 1 3058.00 3108.95 67.95 o 2 9 1 405.09 440.74 29.30 o 3 9 1 82.58 101.57 14.59 o 4 9 1 2764.16 2669.86 82.51 o 5 9 1 129.38 113.60 16.68 o 6 9 1 6.69 0.00 21.68 o 7 9 1 126.60 188.21 33.32 o 8 9 1 37.92 0.62 32.19 o 9 9 1 9.92 11.18 30.55 o -10 10 1 62.77 43.27 34.97 o -9 10 1 39.49 44.81 34.22 o -8 10 1 0.35 16.90 82.82 o -7 10 1 55.26 106.25 62.93 o -6 10 1 966.30 997.09 67.41 o -5 10 1 231.58 274.42 31.10 o -4 10 1 1393.11 1387.70 44.55 o -3 10 1 1845.71 1910.19 53.01 o -2 10 1 1528.09 1551.17 39.26 o -1 10 1 463.48 549.12 21.55 o 0 10 1 58.39 56.24 14.34 o 1 10 1 1012.90 949.55 29.11 o 2 10 1 524.70 498.24 26.48 o 3 10 1 2.20 14.49 11.69 o 4 10 1 76.79 112.55 15.14 o 5 10 1 797.84 711.12 37.21 o 6 10 1 64.10 61.05 30.51 o 7 10 1 11.25 78.03 27.92 o 8 10 1 50.21 80.87 38.98 o 9 10 1 183.66 273.68 51.19 o -10 11 1 6.22 0.00 31.11 o -9 11 1 20.47 49.29 55.63 o -8 11 1 6.60 26.89 23.99 o -7 11 1 245.07 290.94 40.24 o -6 11 1 101.63 116.81 30.87 o -5 11 1 68.87 89.84 25.51 o -4 11 1 85.06 87.92 15.55 o -3 11 1 703.69 722.17 29.72 o -2 11 1 4.04 19.36 14.28 o -1 11 1 0.09 23.62 18.97 o 0 11 1 345.95 360.87 28.06 o 1 11 1 0.40 29.68 12.31 o 2 11 1 0.18 16.53 16.27 o 3 11 1 8.92 29.26 11.46 o 4 11 1 585.16 597.62 34.48 o 5 11 1 82.74 77.79 15.94 o 6 11 1 164.45 120.63 16.25 o 7 11 1 73.87 97.35 34.53 o 8 11 1 49.59 0.00 26.15 o 9 11 1 2.57 0.00 30.70 o -9 12 1 121.93 122.95 38.71 o -8 12 1 4.27 0.00 30.20 o -7 12 1 710.05 668.34 61.13 o -6 12 1 1446.38 1372.44 84.12 o -5 12 1 280.45 318.17 34.99 o -4 12 1 55.72 38.49 27.39 o -3 12 1 889.98 912.53 36.72 o -2 12 1 3707.72 3942.24 92.23 o -1 12 1 121.59 139.12 14.27 o 0 12 1 44.41 34.28 14.07 o 1 12 1 28.66 67.42 15.56 o 2 12 1 110.26 115.04 16.52 o 3 12 1 706.90 769.00 37.99 o 4 12 1 623.11 566.46 46.76 o 5 12 1 436.13 394.99 28.79 o 6 12 1 25.72 1.22 15.91 o 7 12 1 3.59 0.00 22.21 o 8 12 1 11.16 0.00 23.16 o -9 13 1 21.13 44.36 33.35 o -8 13 1 151.47 199.77 43.67 o -7 13 1 109.03 165.50 36.91 o -6 13 1 217.86 274.23 38.97 o -5 13 1 572.45 528.34 47.52 o -4 13 1 0.00 0.00 15.57 o -3 13 1 88.18 103.72 15.08 o -2 13 1 269.95 246.58 39.87 o -1 13 1 1547.17 1561.92 49.67 o 0 13 1 612.03 628.74 27.46 o 1 13 1 68.20 72.89 20.86 o 2 13 1 8.82 17.99 12.39 o 3 13 1 53.29 33.67 14.47 o 4 13 1 875.55 811.97 44.10 o 5 13 1 823.62 768.80 41.71 o 6 13 1 0.28 36.21 27.47 o 7 13 1 164.03 111.58 34.55 o 8 13 1 71.91 60.67 35.55 o -9 14 1 69.21 34.72 36.07 o -8 14 1 18.86 27.87 37.33 o -7 14 1 0.13 0.00 20.31 o -6 14 1 1004.79 993.66 74.21 o -5 14 1 0.80 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0.00 28.37 o -4 14 9 24.40 29.34 25.46 o -3 14 9 132.68 130.18 31.75 o -9 0 10 1.95 0.00 63.11 o -8 0 10 26.29 2.53 33.24 o -7 0 10 85.12 74.37 46.84 o -6 0 10 55.74 87.54 44.41 o -5 0 10 370.98 362.45 78.75 o -4 0 10 29.83 29.57 54.78 o -3 0 10 28.35 18.93 59.17 o -2 0 10 1031.06 1011.67 127.33 o -1 0 10 4.20 37.59 44.54 o -9 1 10 18.25 38.22 30.34 o -8 1 10 19.62 14.06 24.64 o -7 1 10 87.82 55.18 30.10 o -6 1 10 223.46 236.10 42.94 o -5 1 10 6.17 24.68 28.57 o -4 1 10 64.86 40.13 30.74 o -3 1 10 207.54 235.45 45.08 o -2 1 10 149.45 173.15 42.90 o -1 1 10 8.71 5.06 26.19 o -9 2 10 174.60 199.27 54.08 o -8 2 10 226.63 304.92 45.90 o -7 2 10 151.47 190.14 41.00 o -6 2 10 168.97 202.51 39.95 o -5 2 10 325.90 335.36 44.99 o -4 2 10 34.67 0.00 23.77 o -3 2 10 21.00 83.48 45.95 o -2 2 10 20.35 37.99 30.36 o -1 2 10 28.81 59.47 30.86 o -8 3 10 0.63 0.00 23.86 o -7 3 10 12.09 24.54 51.53 o -6 3 10 17.45 76.82 33.79 o -5 3 10 0.03 10.14 22.46 o -4 3 10 104.89 116.24 53.84 o -3 3 10 44.12 57.78 32.38 o -2 3 10 8.67 7.41 26.92 o -1 3 10 2.02 0.00 25.82 o -8 4 10 0.70 0.00 41.19 o -7 4 10 33.85 54.67 33.73 o -6 4 10 34.09 67.84 31.66 o -5 4 10 23.45 20.41 33.98 o -4 4 10 13.33 48.60 28.63 o -3 4 10 59.60 74.00 57.01 o -2 4 10 318.71 302.04 54.00 o -1 4 10 35.55 6.21 28.33 o -8 5 10 46.60 123.15 57.11 o -7 5 10 1.71 16.16 23.99 o -6 5 10 0.02 70.30 30.93 o -5 5 10 73.93 150.15 53.14 o -4 5 10 36.32 0.00 21.76 o -3 5 10 15.14 42.52 31.30 o -2 5 10 44.27 40.00 32.74 o -1 5 10 120.88 116.91 40.59 o -8 6 10 206.59 141.72 58.29 o -7 6 10 111.91 111.22 36.84 o -6 6 10 67.00 60.91 35.94 o -5 6 10 384.64 360.70 49.37 o -4 6 10 13.32 34.85 27.48 o -3 6 10 6.03 33.14 34.53 o -2 6 10 142.94 137.41 51.21 o -1 6 10 30.83 0.00 29.59 o -8 7 10 3.20 0.00 31.03 o -7 7 10 38.05 0.00 38.09 o -6 7 10 0.01 24.89 26.32 o -5 7 10 0.67 0.00 28.83 o -4 7 10 198.32 285.99 47.69 o -3 7 10 16.72 56.59 37.95 o -2 7 10 1.48 54.39 39.06 o -7 8 10 78.10 77.29 38.55 o -6 8 10 2.89 22.52 29.87 o -5 8 10 2.64 0.00 26.31 o -4 8 10 119.70 137.08 42.14 o -3 8 10 10.40 45.53 37.95 o -2 8 10 1.85 0.00 28.61 o -7 9 10 112.08 62.97 39.35 o -6 9 10 36.06 72.30 41.89 o -5 9 10 267.12 205.80 55.93 o -4 9 10 133.36 155.24 64.59 o -3 9 10 145.37 104.34 39.42 o -6 10 10 112.18 54.62 35.73 o -5 10 10 49.49 15.54 28.87 o -4 10 10 101.33 43.93 34.80 o -5 1 11 30.24 93.77 35.08 o -5 2 11 58.58 76.66 38.25 o