#------------------------------------------------------------------------------ #$Date: 2009-05-03 21:56:13 +0300 (Sun, 03 May 2009) $ #$Revision: 691 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2218811.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2218811_Fobs loop_ _publ_author_name 'Rieckborn, Timo Paul' 'Karakoc, Emine' 'Prosenc, Marc Heinrich' _publ_section_title ; Bis(1-{bis[2-(diphenylphosphinoyl)ethyl]phosphanyl}-2-(diphenylphosphanyl)ethane)dinitratoplatinum(II) methanol tetrasolvate ; _journal_coeditor_code SI2089 _journal_issue 7 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m898 _journal_page_last m899 _journal_volume 64 _journal_year 2008 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 66.200 _cell_angle_beta 77.479 _cell_angle_gamma 88.477 _cell_length_a 9.9905 _cell_length_b 14.3346 _cell_length_c 16.9916 _exptl_crystal_F_000 952.00 _reflns_d_resolution_high 0.7828 _[local]_cod_data_source_file si2089Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 30tr in P-1' _shelx_refln_list_code 4 _shelx_F_calc_maximum 278.19 _shelx_F_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 63.72 76.22 22.90 o 3 0 0 1384.07 1545.23 67.87 o 4 0 0 1331.79 1414.21 72.68 o 5 0 0 4545.07 4595.15 148.77 o 6 0 0 1720.57 1766.91 97.91 o 7 0 0 2371.11 2393.72 120.34 o 8 0 0 1434.44 1502.41 115.77 o 9 0 0 611.24 662.56 118.18 o 10 0 0 843.58 1034.65 192.28 o 11 0 0 1170.77 1159.37 193.31 o 12 0 0 763.49 656.75 222.12 o -12 1 0 853.44 1135.17 201.95 o -11 1 0 832.38 907.12 178.58 o -10 1 0 509.35 388.77 119.63 o -9 1 0 401.57 493.11 128.69 o -8 1 0 725.74 742.00 91.28 o -7 1 0 7349.23 7744.82 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