#------------------------------------------------------------------------------ #$Date: 2009-05-03 21:56:13 +0300 (Sun, 03 May 2009) $ #$Revision: 691 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2218845.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2218845_Fobs loop_ _publ_author_name 'Romanowski, Grzegorz' 'Lis, Tadeusz' _publ_section_title ; Di-\m-oxido-bis{[(R,R)-(+)-1-amino-2-(3-methoxy-2-oxidobenzylideneamino-\k^2^O^2^,N)-1,2-diphenylethane-\kN]oxidovanadium(V)} dihydrate ; _journal_coeditor_code XU2414 _journal_issue 7 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m886 _journal_page_last m887 _journal_volume 64 _journal_year 2008 _space_group_IT_number 19 _symmetry_space_group_name_Hall 'P 2ac 2ab' _symmetry_space_group_name_H-M 'P 21 21 21' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 9.3280 _cell_length_b 16.9500 _cell_length_c 25.4900 _exptl_crystal_F_000 1856.00 _reflns_d_resolution_high 0.7927 _[local]_cod_data_source_file xu2414Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' vo15 in P2(1)2(1)2(1)' _shelx_refln_list_code 4 _shelx_F_calc_maximum 390.63 _shelx_F_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 30855.14 32636.84 730.06 o 4 0 0 8432.30 8239.09 219.78 o 6 0 0 12819.97 12177.80 213.41 o 8 0 0 3346.08 3075.63 218.50 o 10 0 0 565.23 936.23 235.97 o 1 1 0 262.98 297.86 29.97 o 2 1 0 20050.52 18086.04 241.08 o 3 1 0 15.03 36.94 78.61 o 4 1 0 4149.68 3991.10 134.57 o 5 1 0 605.80 758.74 69.54 o 6 1 0 0.33 -17.94 50.73 o 7 1 0 8760.24 8444.05 162.95 o 8 1 0 171.85 150.10 154.30 o 9 1 0 1370.01 1542.26 181.25 o 10 1 0 1199.35 1090.57 149.56 o 11 1 0 172.60 82.70 120.89 o 0 2 0 74575.38 74771.99 1088.79 o 1 2 0 51.96 49.65 34.45 o 2 2 0 2132.81 2214.58 63.21 o 3 2 0 1395.48 1429.01 46.81 o 4 2 0 6845.79 6399.17 151.58 o 5 2 0 32.08 76.88 69.00 o 6 2 0 3242.68 3078.24 93.91 o 7 2 0 10.41 -1.31 27.92 o 8 2 0 571.89 745.75 137.83 o 9 2 0 138.80 176.50 245.10 o 10 2 0 234.05 349.21 145.60 o 11 2 0 52.76 48.15 175.23 o 1 3 0 705.66 733.65 44.91 o 2 3 0 52356.15 50255.57 493.77 o 3 3 0 13.13 -13.15 28.66 o 4 3 0 13.80 61.23 110.95 o 5 3 0 7.18 25.09 43.68 o 6 3 0 526.37 303.47 93.24 o 7 3 0 2825.74 2836.46 126.25 o 8 3 0 40.29 129.28 181.42 o 9 3 0 45.08 56.27 281.39 o 10 3 0 2.86 -39.12 145.19 o 11 3 0 25.03 91.95 158.16 o 0 4 0 89568.57 101457.74 936.94 o 1 4 0 118.83 65.52 42.66 o 2 4 0 1280.71 1150.37 66.25 o 3 4 0 27.36 13.35 44.57 o 4 4 0 1426.62 1264.47 124.15 o 5 4 0 16.11 46.86 102.75 o 6 4 0 7452.04 7263.76 171.60 o 7 4 0 31.75 42.89 72.58 o 8 4 0 526.50 789.83 166.83 o 9 4 0 769.52 804.05 267.34 o 10 4 0 659.27 588.18 238.11 o 11 4 0 62.35 166.14 156.53 o 1 5 0 1107.89 1064.84 76.15 o 2 5 0 872.45 722.08 62.79 o 3 5 0 207.73 132.68 72.74 o 4 5 0 984.41 1160.88 91.02 o 5 5 0 377.12 384.70 117.52 o 6 5 0 551.38 311.89 109.35 o 7 5 0 1101.04 1092.30 163.32 o 8 5 0 2198.79 2380.44 205.16 o 9 5 0 51.52 199.62 271.48 o 10 5 0 61.33 126.23 229.12 o 11 5 0 217.12 265.26 137.76 o 0 6 0 2584.97 2314.40 77.96 o 1 6 0 1.04 6.75 20.93 o 2 6 0 1683.57 1531.48 83.79 o 3 6 0 14.16 2.40 39.03 o 4 6 0 4688.20 4524.71 113.39 o 5 6 0 555.98 451.59 107.62 o 6 6 0 1219.21 948.97 132.06 o 7 6 0 199.01 251.78 150.43 o 8 6 0 78.21 51.06 185.43 o 9 6 0 48.69 297.73 186.49 o 10 6 0 207.21 301.19 193.15 o 1 7 0 73.37 114.19 68.64 o 2 7 0 1306.84 1001.80 85.74 o 3 7 0 429.05 342.33 101.75 o 4 7 0 4829.30 4668.37 122.12 o 5 7 0 39.45 39.04 92.99 o 6 7 0 27.09 0.24 20.40 o 7 7 0 39.91 -0.41 167.71 o 8 7 0 1207.74 1371.38 198.75 o 9 7 0 18.99 7.97 202.48 o 10 7 0 470.68 408.38 178.87 o 0 8 0 1766.24 1599.14 130.75 o 1 8 0 252.93 197.80 94.17 o 2 8 0 2642.46 2858.66 126.21 o 3 8 0 620.07 534.61 93.22 o 4 8 0 7100.94 7407.90 135.15 o 5 8 0 800.14 651.73 104.06 o 6 8 0 181.53 241.11 155.41 o 7 8 0 71.13 42.58 175.14 o 8 8 0 109.91 266.80 160.93 o 9 8 0 17.37 25.37 176.50 o 10 8 0 132.76 195.26 178.35 o 1 9 0 1455.51 1564.64 94.57 o 2 9 0 17905.06 17547.64 226.61 o 3 9 0 213.99 209.62 92.62 o 4 9 0 13811.87 13616.91 274.10 o 5 9 0 134.73 107.69 138.95 o 6 9 0 23.18 81.45 158.70 o 7 9 0 446.04 399.86 148.76 o 8 9 0 922.84 870.96 158.79 o 9 9 0 591.94 744.58 232.49 o 10 9 0 34.22 76.59 169.60 o 0 10 0 2484.65 2338.49 155.38 o 1 10 0 845.33 641.43 97.71 o 2 10 0 2167.83 2025.03 92.93 o 3 10 0 436.93 370.89 90.92 o 4 10 0 5403.14 5366.76 135.69 o 5 10 0 2006.76 1831.32 148.82 o 6 10 0 527.96 494.58 157.87 o 7 10 0 156.50 70.91 171.53 o 8 10 0 3.30 53.06 156.52 o 9 10 0 158.35 22.60 90.90 o 1 11 0 35.79 26.99 45.25 o 2 11 0 2474.58 2293.67 98.62 o 3 11 0 226.94 200.84 110.52 o 4 11 0 3808.20 3978.01 149.73 o 5 11 0 735.34 877.37 160.79 o 6 11 0 32.54 204.69 179.12 o 7 11 0 4.38 -44.74 145.62 o 8 11 0 532.68 421.32 192.68 o 0 12 0 209.26 145.20 143.92 o 1 12 0 116.67 11.93 104.28 o 2 12 0 110.88 176.58 112.74 o 3 12 0 58.26 141.31 160.84 o 4 12 0 1256.99 931.41 162.79 o 5 12 0 682.39 867.92 169.63 o 6 12 0 111.14 46.63 180.98 o 7 12 0 73.20 -3.11 168.57 o 8 12 0 136.16 181.02 320.36 o 1 13 0 27.19 56.95 99.35 o 2 13 0 4005.23 4152.30 136.47 o 3 13 0 1.66 -47.08 138.11 o 4 13 0 1793.45 1875.17 170.80 o 5 13 0 820.48 752.37 212.37 o 6 13 0 299.92 270.48 225.67 o 7 13 0 25.22 44.51 219.74 o 0 14 0 1367.37 1436.66 173.28 o 1 14 0 150.26 161.62 133.73 o 2 14 0 1739.84 1735.43 150.95 o 3 14 0 1.35 2.77 127.48 o 4 14 0 30.38 24.73 232.28 o 5 14 0 401.48 454.33 208.27 o 6 14 0 409.53 335.08 237.00 o 1 15 0 126.46 94.32 137.77 o 2 15 0 1498.15 1525.45 166.52 o 3 15 0 48.66 175.80 181.72 o 4 15 0 619.16 815.88 216.44 o 5 15 0 42.70 82.23 219.14 o 6 15 0 16.74 48.20 234.95 o 0 16 0 505.59 419.34 221.80 o 1 16 0 15.74 49.49 168.76 o 2 16 0 82.52 145.55 173.85 o 3 16 0 2.65 153.57 269.18 o 4 16 0 25.36 158.94 223.38 o 5 16 0 131.16 134.89 233.70 o 6 16 0 170.65 186.12 298.93 o 1 17 0 86.18 92.81 156.70 o 2 17 0 1789.81 2061.90 172.95 o 3 17 0 25.71 38.84 184.75 o 4 17 0 852.93 707.69 191.18 o 5 17 0 16.31 -4.42 41.66 o 0 18 0 3227.72 3022.99 197.94 o 1 18 0 37.51 -16.33 105.29 o 2 18 0 399.70 386.58 171.53 o 3 18 0 186.53 120.97 209.75 o 4 18 0 38.31 42.50 179.73 o 1 19 0 358.90 313.92 157.48 o 2 19 0 88.73 273.14 196.72 o 1 0 1 1124.69 941.46 27.50 o 2 0 1 1429.75 1393.00 32.70 o 3 0 1 672.51 729.20 84.93 o 4 0 1 798.26 709.86 84.11 o 5 0 1 743.09 841.62 72.65 o 6 0 1 5489.75 5286.94 105.94 o 7 0 1 592.07 557.37 109.33 o 8 0 1 35.89 94.26 180.91 o 9 0 1 1000.16 769.04 175.78 o 10 0 1 126.78 164.80 230.69 o 11 0 1 41.80 95.94 170.72 o -11 1 1 192.23 159.78 122.05 o -10 1 1 684.67 450.08 178.62 o -9 1 1 3150.78 3585.34 188.97 o -8 1 1 35.88 32.28 106.32 o -7 1 1 8775.01 8505.41 163.28 o -6 1 1 297.44 276.92 85.13 o -5 1 1 2790.98 2937.22 78.73 o -4 1 1 529.41 381.16 85.47 o -3 1 1 6452.13 5258.17 289.22 o -2 1 1 1157.56 1245.26 55.37 o -1 1 1 5081.53 5444.38 73.91 o 0 1 1 202.02 212.01 20.21 o 1 1 1 4471.27 4777.37 63.23 o 2 1 1 1002.54 1023.62 29.63 o 3 1 1 4558.69 4183.98 116.93 o 4 1 1 573.63 369.72 95.07 o 5 1 1 3045.34 3087.27 81.14 o 6 1 1 305.72 302.71 84.01 o 7 1 1 8402.79 8009.64 160.79 o 8 1 1 15.96 -0.04 130.75 o 9 1 1 2889.22 3232.22 171.04 o 10 1 1 737.10 530.99 222.30 o 11 1 1 209.54 176.71 124.01 o -11 2 1 2.94 -18.73 77.87 o -10 2 1 133.23 178.25 142.90 o -9 2 1 98.53 111.97 221.06 o -8 2 1 1321.29 1190.50 154.92 o -7 2 1 292.15 344.22 103.70 o -6 2 1 3009.01 2945.30 90.74 o -5 2 1 343.57 290.34 75.24 o -4 2 1 683.56 684.47 91.74 o -3 2 1 219.09 336.89 43.62 o -2 2 1 12469.87 12331.47 127.45 o -1 2 1 593.54 430.56 36.03 o 0 2 1 9219.17 9781.93 61.92 o 1 2 1 551.83 357.85 48.71 o 2 2 1 12983.44 12578.16 118.09 o 3 2 1 211.87 306.18 35.78 o 4 2 1 862.26 818.48 95.54 o 5 2 1 520.92 466.77 74.68 o 6 2 1 3224.24 3184.86 98.29 o 7 2 1 217.58 272.89 119.56 o 8 2 1 1347.90 1290.52 133.99 o 9 2 1 75.91 85.01 194.75 o 10 2 1 237.62 308.54 149.04 o 11 2 1 14.43 44.25 507.27 o -11 3 1 6.29 73.57 168.02 o -10 3 1 18.67 182.54 176.56 o -9 3 1 31.67 165.93 223.55 o -8 3 1 619.01 585.26 211.70 o -7 3 1 2582.69 2553.79 137.52 o -6 3 1 1332.36 1273.51 86.75 o -5 3 1 1845.91 1805.79 94.74 o -4 3 1 438.96 446.53 113.54 o -3 3 1 284.72 184.31 55.12 o -2 3 1 3780.18 3486.98 87.32 o -1 3 1 1686.63 1793.80 48.46 o 0 3 1 85.74 74.76 21.37 o 1 3 1 1820.67 1994.72 71.08 o 2 3 1 3966.00 3623.74 82.76 o 3 3 1 169.86 175.06 56.15 o 4 3 1 521.01 553.62 117.05 o 5 3 1 2099.90 2061.59 81.67 o 6 3 1 1300.46 1253.76 90.98 o 7 3 1 2710.31 2805.77 122.74 o 8 3 1 414.40 395.29 138.42 o 9 3 1 272.54 260.09 266.52 o 10 3 1 15.13 -15.35 47.30 o 11 3 1 7.26 -6.09 102.95 o -10 4 1 296.31 339.29 234.41 o -9 4 1 849.91 641.17 244.71 o -8 4 1 349.58 536.77 196.46 o -7 4 1 134.82 197.85 132.44 o -6 4 1 2472.66 2439.53 110.47 o -5 4 1 232.87 178.72 101.13 o -4 4 1 244.64 360.84 118.49 o -3 4 1 2646.33 2860.53 83.25 o -2 4 1 307.85 211.67 50.03 o -1 4 1 9285.38 9003.28 107.07 o 0 4 1 29660.94 29670.93 301.86 o 1 4 1 8681.14 8286.02 138.06 o 2 4 1 371.17 222.83 59.97 o 3 4 1 2515.07 2639.64 84.39 o 4 4 1 376.88 510.96 83.10 o 5 4 1 37.09 1.78 19.93 o 6 4 1 2542.08 2416.57 94.89 o 7 4 1 297.73 248.02 144.99 o 8 4 1 371.78 570.09 182.16 o 9 4 1 782.31 697.30 211.27 o 10 4 1 344.82 288.18 233.49 o 11 4 1 215.02 148.53 159.15 o -11 5 1 12.22 -25.08 431.63 o -10 5 1 199.22 249.23 221.82 o -9 5 1 1066.55 916.33 273.70 o -8 5 1 1853.03 1931.56 181.68 o -7 5 1 3148.78 3385.53 180.12 o -6 5 1 241.61 240.66 111.21 o -5 5 1 945.56 1080.11 122.04 o -4 5 1 667.06 764.24 90.81 o -3 5 1 3064.01 2661.85 85.58 o -2 5 1 367.98 385.95 52.61 o -1 5 1 835.64 845.42 60.81 o 0 5 1 202.74 198.29 26.90 o 1 5 1 413.84 319.83 59.01 o 2 5 1 282.56 309.57 62.22 o 3 5 1 2887.52 2472.43 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6 8 1 106.83 127.94 157.20 o 7 8 1 1751.58 1625.50 165.73 o 8 8 1 100.61 128.62 155.80 o 9 8 1 1.31 88.10 157.81 o 10 8 1 109.48 169.26 179.19 o -10 9 1 82.30 -6.80 36.49 o -9 9 1 186.94 168.30 248.37 o -8 9 1 489.26 579.14 159.87 o -7 9 1 1029.07 961.84 173.80 o -6 9 1 571.16 649.62 157.46 o -5 9 1 100.96 28.28 113.37 o -4 9 1 748.82 675.62 100.35 o -3 9 1 7632.49 7621.20 115.25 o -2 9 1 413.33 424.00 122.66 o -1 9 1 2098.99 1830.05 93.00 o 0 9 1 47.05 78.83 119.73 o 1 9 1 1915.24 1673.33 102.65 o 2 9 1 316.29 301.27 142.00 o 3 9 1 7764.54 7604.16 140.53 o 4 9 1 646.13 530.21 122.37 o 5 9 1 92.05 81.03 139.73 o 6 9 1 416.50 533.18 156.36 o 7 9 1 1148.24 1044.71 156.99 o 8 9 1 385.20 282.05 141.12 o 9 9 1 170.68 349.64 180.05 o 10 9 1 129.55 -30.16 309.72 o -9 10 1 209.85 197.63 222.94 o -8 10 1 39.00 54.77 145.47 o -7 10 1 523.06 387.39 189.86 o -6 10 1 322.49 426.79 171.72 o -5 10 1 6139.31 6165.08 163.52 o -4 10 1 136.06 46.99 44.06 o -3 10 1 2105.87 1877.45 104.93 o -2 10 1 216.63 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245.25 162.92 o -3 12 1 559.56 493.63 125.45 o -2 12 1 124.11 179.41 110.23 o -1 12 1 1369.63 1512.79 116.99 o 0 12 1 1408.42 1315.29 116.33 o 1 12 1 1513.24 1612.03 120.30 o 2 12 1 95.83 145.98 121.83 o 3 12 1 637.86 475.77 151.51 o 4 12 1 242.76 221.43 191.13 o 5 12 1 1925.49 2043.39 162.32 o 6 12 1 14.10 167.00 187.11 o 7 12 1 43.00 24.01 189.22 o 8 12 1 139.04 282.86 292.39 o -7 13 1 2.54 48.62 362.65 o -6 13 1 113.08 218.16 213.63 o -5 13 1 308.18 248.40 176.65 o -4 13 1 1084.28 1127.00 165.09 o -3 13 1 41.91 -38.77 151.35 o -2 13 1 24.83 18.64 83.02 o -1 13 1 108.68 61.00 141.42 o 0 13 1 30.16 32.97 95.31 o 1 13 1 160.89 99.92 146.18 o 2 13 1 50.58 65.35 127.76 o 3 13 1 28.62 35.84 116.75 o 4 13 1 809.44 932.66 199.79 o 5 13 1 304.43 305.46 235.56 o 6 13 1 109.38 62.00 239.69 o 7 13 1 3.32 30.15 286.32 o -7 14 1 1.84 194.31 313.03 o -6 14 1 284.99 139.12 221.08 o -5 14 1 843.14 1132.91 233.37 o -4 14 1 228.15 245.28 183.28 o -3 14 1 506.81 481.57 168.97 o -2 14 1 277.64 233.21 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1947.13 1467.04 188.39 o 1 0 28 697.29 685.55 205.45 o 2 0 28 150.60 234.39 135.75 o 3 0 28 140.33 42.02 121.77 o 4 0 28 223.90 153.21 144.81 o 5 0 28 95.80 99.83 131.70 o -5 1 28 135.84 17.57 125.64 o -4 1 28 327.80 353.44 160.27 o -3 1 28 14.57 -2.83 11.43 o -2 1 28 13.04 -57.83 86.42 o -1 1 28 366.80 374.21 140.61 o 0 1 28 161.75 219.71 141.32 o 1 1 28 293.96 517.12 192.54 o 2 1 28 8.02 21.95 186.70 o 3 1 28 19.45 -37.86 94.31 o 4 1 28 298.58 278.72 111.03 o 5 1 28 184.24 98.97 127.16 o -5 2 28 52.06 101.89 125.09 o -4 2 28 27.07 45.23 149.58 o -3 2 28 259.98 224.90 175.43 o -2 2 28 298.93 587.08 176.82 o -1 2 28 741.03 857.58 188.54 o 0 2 28 1771.05 1897.79 203.77 o 1 2 28 725.84 747.94 146.15 o 2 2 28 299.36 361.65 133.95 o 3 2 28 196.98 185.40 125.00 o 4 2 28 43.06 34.59 109.60 o 5 2 28 114.06 21.98 77.62 o -5 3 28 206.46 67.30 120.58 o -4 3 28 97.70 102.01 151.27 o -3 3 28 88.60 85.42 150.61 o -2 3 28 26.12 2.78 7.42 o -1 3 28 275.50 281.14 189.01 o 0 3 28 159.13 189.47 206.96 o 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164.62 139.45 o -1 7 28 178.09 237.40 155.98 o 0 7 28 208.83 286.53 155.01 o 1 7 28 167.48 139.37 146.32 o 2 7 28 155.16 100.92 145.77 o 3 7 28 226.94 245.07 129.83 o 4 7 28 108.10 84.91 102.55 o -2 8 28 29.24 8.89 128.49 o -1 8 28 272.00 285.77 142.21 o 0 8 28 34.20 52.33 147.21 o 1 8 28 156.33 142.28 145.81 o 2 8 28 16.62 20.91 123.92 o 3 8 28 112.62 89.97 109.54 o 0 9 28 200.44 232.39 123.15 o 1 9 28 68.35 114.45 123.06 o 2 9 28 50.21 -32.81 100.38 o 1 0 29 83.99 238.11 126.76 o 2 0 29 746.91 669.59 120.31 o 4 0 29 19.06 14.69 184.78 o -4 1 29 187.09 60.95 135.21 o -3 1 29 82.83 203.48 140.85 o -2 1 29 740.33 811.60 152.91 o -1 1 29 128.70 135.14 127.78 o 0 1 29 173.56 288.13 127.81 o 1 1 29 154.24 83.73 122.55 o 2 1 29 655.12 671.37 115.35 o 3 1 29 126.07 149.09 109.29 o -4 2 29 10.31 28.87 132.20 o -3 2 29 55.62 64.32 138.13 o -2 2 29 63.19 125.92 158.49 o -1 2 29 366.69 497.31 176.75 o 0 2 29 211.81 344.57 164.88 o 1 2 29 285.07 296.62 177.42 o 2 2 29 120.45 207.06 170.73 o 3 2 29 104.95 30.14 154.62 o 4 2 29 10.21 22.73 124.16 o -4 3 29 241.17 215.83 125.31 o -3 3 29 152.87 202.50 146.19 o -2 3 29 322.60 407.02 149.23 o -1 3 29 5.43 64.41 163.57 o 0 3 29 241.28 129.05 172.87 o 1 3 29 25.98 22.23 156.37 o 2 3 29 310.51 282.49 162.71 o 4 3 29 220.21 196.65 119.13 o -4 4 29 202.07 128.36 113.46 o -2 4 29 18.11 -32.67 99.71 o -1 4 29 27.76 39.11 155.57 o 0 4 29 751.05 886.56 160.30 o 1 4 29 68.57 108.84 156.27 o 2 4 29 18.42 13.41 157.64 o 3 4 29 150.03 188.07 136.84 o 4 4 29 105.53 80.04 114.71 o -3 5 29 38.98 31.09 124.17 o -2 5 29 240.64 205.10 134.17 o -1 5 29 29.97 177.50 157.06 o 0 5 29 261.63 453.60 148.14 o 1 5 29 28.18 59.02 151.90 o 2 5 29 238.68 182.21 135.14 o 3 5 29 77.39 109.65 118.22 o -3 6 29 56.70 110.84 114.42 o -2 6 29 11.56 65.33 133.60 o -1 6 29 12.96 61.71 138.54 o 0 6 29 1098.90 1052.39 140.60 o 1 6 29 37.17 24.44 147.11 o 2 6 29 35.82 6.31 125.50 o 3 6 29 28.35 51.14 117.44 o -2 7 29 58.15 100.60 112.00 o 0 7 29 208.08 237.53 127.44 o 1 7 29 202.78 83.02 135.01 o 2 7 29 156.17 78.08 120.06 o 3 7 29 455.03 244.65 103.05 o -1 8 29 35.29 127.25 110.95 o 0 8 29 187.50 242.41 110.24 o 1 8 29 84.15 92.89 111.99 o 0 0 30 262.05 196.72 149.58 o 1 0 30 710.33 702.01 106.88 o 2 0 30 37.57 0.83 138.65 o 3 0 30 121.33 65.12 127.91 o -3 1 30 193.22 182.34 125.41 o -2 1 30 2.66 31.76 135.42 o -1 1 30 113.67 64.70 143.03 o 0 1 30 57.11 129.50 108.16 o 1 1 30 53.33 107.21 105.35 o 2 1 30 1.32 -38.96 99.35 o -3 2 30 27.83 -0.58 13.47 o -2 2 30 23.70 97.77 128.57 o -1 2 30 17.28 -73.22 89.54 o 0 2 30 1687.28 1911.40 154.90 o 1 2 30 109.52 127.58 145.71 o 2 2 30 31.02 69.47 139.18 o 3 2 30 22.62 59.76 122.30 o -3 3 30 146.12 130.89 112.42 o -2 3 30 40.83 33.37 132.57 o -1 3 30 51.02 129.93 128.84 o 0 3 30 176.25 193.40 151.21 o 1 3 30 30.44 -11.46 58.08 o 2 3 30 42.01 95.92 131.28 o -3 4 30 203.40 164.91 107.94 o -2 4 30 681.27 485.63 127.66 o -1 4 30 211.52 240.28 126.80 o 0 4 30 13.86 88.09 144.38 o 1 4 30 299.78 252.62 140.24 o 2 4 30 591.92 587.43 129.64 o -3 5 30 9.76 29.44 97.43 o -2 5 30 68.05 38.94 116.57 o -1 5 30 93.04 74.35 115.07 o 0 5 30 3.03 20.58 126.05 o 1 5 30 100.76 67.61 122.18 o 2 5 30 68.67 80.99 112.00 o 3 5 30 5.37 48.07 97.60 o -2 6 30 137.69 107.96 97.94 o -1 6 30 3.85 -43.63 254.88 o 0 6 30 16.80 94.91 108.96 o 1 6 30 19.89 67.42 118.58 o -1 7 30 170.62 75.02 97.26 o 0 7 30 8.52 88.17 103.48 o 1 7 30 192.70 165.85 101.84 o 2 0 31 5.49 -33.35 169.89 o -2 1 31 563.14 316.44 108.63 o -1 1 31 210.40 179.16 118.95 o 0 1 31 12.35 -79.26 103.38 o 1 1 31 204.19 414.99 118.80 o -2 2 31 245.09 135.70 107.19 o -1 2 31 172.42 57.26 114.99 o 0 2 31 2.67 -3.21 10.20 o 1 2 31 124.69 145.74 117.52 o -2 3 31 208.38 109.08 97.67 o -1 3 31 1.65 -22.82 47.67 o 1 3 31 14.61 -3.02 25.14 o 2 3 31 203.71 114.40 102.57 o -2 4 31 193.22 112.42 92.41 o -1 4 31 56.87 95.27 101.55 o 1 4 31 52.67 45.07 106.04 o -1 5 31 91.77 11.02 95.76 o 1 5 31 47.94 61.70 96.58 o