#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/89/2218962.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2218962_Fobs loop_ _publ_author_name 'Wang, Feng' 'Cao, Rui-Ge' 'Pan, Yi-Bing' 'Liu, Shu-Xia' _publ_section_title ; Trisodium bis{1-[iminio(morpholino)methyl]guanidinium} bis[hexahydrogenhexamolybdoaluminate(III)] chloride icosahydrate ; _journal_coeditor_code CV2425 _journal_issue 8 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1069 _journal_page_last m1070 _journal_volume 64 _journal_year 2008 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 81.698 _cell_angle_beta 75.314 _cell_angle_gamma 77.057 _cell_length_a 10.1070 _cell_length_b 11.3869 _cell_length_c 17.2548 _exptl_crystal_F_000 1364.00 _reflns_d_resolution_high 0.8225 _[local]_cod_data_source_file cv2425Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 2 in P-1' _shelx_refln_list_code 4 _shelx_F_calc_maximum 501.96 _shelx_F_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 13602.01 14472.93 469.32 o 2 0 0 372.12 291.41 16.53 o 3 0 0 2420.60 2400.60 72.89 o 4 0 0 26663.24 27158.67 1321.25 o 5 0 0 10854.48 11278.34 308.40 o 6 0 0 12064.42 12296.99 339.77 o 7 0 0 2109.31 2196.35 70.45 o 8 0 0 72.56 59.11 21.50 o 9 0 0 230.43 324.09 36.19 o 10 0 0 178.39 200.67 33.87 o 11 0 0 4928.70 5202.54 211.96 o -11 1 0 5.90 22.27 26.57 o -10 1 0 5078.13 5025.24 205.43 o -9 1 0 29078.25 31542.63 1042.84 o -8 1 0 4.03 39.58 20.51 o -7 1 0 2702.74 2624.76 112.55 o -6 1 0 210.60 265.39 62.97 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