#------------------------------------------------------------------------------ #$Date: 2009-05-03 21:56:13 +0300 (Sun, 03 May 2009) $ #$Revision: 691 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2218983.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2218983_Fobs loop_ _publ_author_name 'Pereira Silva, P. S.' 'Martins, N. D.' 'Ramos Silva, M.' 'Matos Beja, A.' _publ_section_title ; Bis(triphenylguanidinium) tetrachloridocuprate(II) ; _journal_coeditor_code ER2054 _journal_issue 8 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1083 _journal_volume 64 _journal_year 2008 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 119.423 _cell_angle_gamma 90.000 _cell_length_a 11.5893 _cell_length_b 8.2404 _cell_length_c 22.3640 _exptl_crystal_F_000 806.00 _reflns_d_resolution_high 0.8364 _[local]_cod_data_source_file er2054Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' tpgcucl2 P21/c' _shelx_refln_list_code 4 _shelx_F_calc_maximum 181.77 _shelx_F_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 11775.18 16328.37 223.83 o 2 0 0 2553.06 2039.19 39.10 o 3 0 0 1572.94 1652.26 43.86 o 4 0 0 1089.33 1023.25 38.68 o 5 0 0 494.69 620.94 37.09 o 6 0 0 24.69 41.57 31.57 o 7 0 0 36.29 -19.46 37.21 o 8 0 0 403.01 303.71 54.46 o 9 0 0 290.73 301.29 206.37 o 10 0 0 1.43 -9.57 159.59 o 11 0 0 4.01 11.26 117.02 o 12 0 0 4.05 128.81 211.21 o 1 1 0 2618.39 1926.23 26.54 o 2 1 0 21809.16 19915.46 180.19 o 3 1 0 1221.33 1166.83 26.71 o 4 1 0 84.17 64.09 19.55 o 5 1 0 912.85 745.27 28.99 o 6 1 0 62.58 66.53 27.54 o 7 1 0 40.63 32.94 29.41 o 8 1 0 70.65 147.30 43.94 o 9 1 0 5.89 25.77 54.50 o 10 1 0 1.44 -7.52 66.75 o 11 1 0 1.48 -23.62 80.52 o 0 2 0 732.63 1256.11 51.39 o 1 2 0 16549.96 15918.65 184.14 o 2 2 0 3283.76 5828.43 299.61 o 3 2 0 53.94 183.27 27.94 o 4 2 0 302.48 342.33 23.38 o 5 2 0 1474.61 1380.78 35.87 o 6 2 0 952.55 967.95 37.57 o 7 2 0 1063.90 1093.23 51.48 o 8 2 0 345.04 323.06 56.74 o 9 2 0 179.36 275.22 80.93 o 10 2 0 26.36 25.79 87.61 o 11 2 0 1.42 -71.49 71.49 o 1 3 0 489.67 799.99 41.77 o 2 3 0 96.94 2026.53 334.82 o 3 3 0 9.12 54.04 24.06 o 4 3 0 550.32 593.39 32.25 o 5 3 0 2030.23 2068.84 51.84 o 6 3 0 83.31 79.57 31.86 o 7 3 0 25.42 -0.68 38.48 o 8 3 0 34.01 46.00 60.48 o 9 3 0 11.39 8.96 83.60 o 10 3 0 6.03 -46.36 76.07 o 11 3 0 2.81 103.52 86.71 o 0 4 0 6825.46 7143.14 139.45 o 1 4 0 9041.46 8834.03 126.67 o 2 4 0 2182.61 3021.12 65.28 o 3 4 0 889.47 971.20 39.93 o 4 4 0 297.56 260.80 33.03 o 5 4 0 144.48 126.98 35.58 o 6 4 0 90.13 136.18 40.62 o 7 4 0 4.67 34.58 63.89 o 8 4 0 98.17 53.22 74.88 o 9 4 0 61.77 13.39 77.39 o 10 4 0 23.87 -44.36 82.53 o 11 4 0 0.45 -59.20 192.43 o 1 5 0 1715.35 1975.83 58.78 o 2 5 0 524.54 465.55 42.96 o 3 5 0 723.33 737.22 47.56 o 4 5 0 383.25 338.21 44.08 o 5 5 0 0.84 22.46 50.52 o 6 5 0 96.22 36.78 61.84 o 7 5 0 41.04 4.84 60.88 o 8 5 0 93.44 -36.97 78.04 o 9 5 0 4.17 -78.30 78.30 o 10 5 0 5.10 124.04 90.58 o 0 6 0 1544.58 2308.17 113.66 o 1 6 0 180.48 259.73 45.06 o 2 6 0 140.68 237.53 48.50 o 3 6 0 643.78 790.88 64.67 o 4 6 0 140.69 100.67 55.83 o 5 6 0 170.30 217.99 74.59 o 6 6 0 163.44 119.07 67.95 o 7 6 0 394.62 364.47 94.22 o 8 6 0 146.63 187.17 87.33 o 9 6 0 41.82 82.33 89.90 o 1 7 0 260.72 328.65 66.16 o 2 7 0 138.31 49.31 75.75 o 3 7 0 161.68 217.17 63.15 o 4 7 0 16.69 75.99 62.24 o 5 7 0 212.38 230.48 74.94 o 6 7 0 288.93 390.88 87.84 o 7 7 0 6.73 -64.39 85.69 o 8 7 0 8.73 17.77 117.30 o 0 8 0 473.77 490.30 143.34 o 1 8 0 606.47 689.19 96.74 o 2 8 0 492.97 577.61 139.02 o 3 8 0 70.18 -4.51 74.30 o 4 8 0 346.29 339.57 88.82 o 5 8 0 142.77 79.34 77.89 o 6 8 0 21.62 2.93 87.96 o 1 9 0 0.78 25.78 90.31 o 2 9 0 9.78 -75.04 92.62 o 3 9 0 255.03 191.82 110.86 o 4 9 0 64.74 151.22 111.91 o -12 1 1 1.10 23.41 83.54 o -11 1 1 36.24 145.91 81.43 o -10 1 1 56.09 69.77 103.59 o -9 1 1 312.84 282.09 54.77 o -8 1 1 1125.08 1325.90 60.66 o -7 1 1 1609.23 1536.78 45.31 o -6 1 1 96.37 108.57 24.41 o -5 1 1 2498.45 2358.87 43.04 o -4 1 1 301.16 362.53 21.27 o -3 1 1 4468.95 3251.39 41.65 o -2 1 1 5198.24 5229.57 54.81 o -1 1 1 24.12 32.26 11.93 o 0 1 1 2966.90 3259.39 39.56 o 1 1 1 16776.09 13594.46 143.96 o 2 1 1 19219.38 14669.29 153.09 o 3 1 1 167.08 165.05 20.95 o 4 1 1 72.99 62.28 21.01 o 5 1 1 1227.38 1374.44 40.33 o 6 1 1 3383.25 2958.78 58.68 o 7 1 1 1245.75 1347.02 55.91 o 8 1 1 23.30 -38.55 38.55 o 9 1 1 22.38 1.32 97.63 o 10 1 1 11.22 -76.24 76.24 o 11 1 1 1.35 52.82 87.67 o -12 2 1 0.51 -41.00 106.44 o -11 2 1 5.31 -9.03 75.00 o -10 2 1 29.27 88.54 75.96 o -9 2 1 12.85 85.55 59.51 o -8 2 1 52.38 51.14 50.23 o -7 2 1 399.22 360.59 42.08 o -6 2 1 184.38 111.57 26.89 o -5 2 1 226.40 260.15 25.84 o -4 2 1 362.88 448.38 62.88 o -3 2 1 147.89 241.27 23.15 o -2 2 1 243.82 3047.51 115.78 o -1 2 1 9266.56 11228.91 132.74 o 0 2 1 342.75 405.82 25.38 o 1 2 1 260.43 753.83 48.15 o 2 2 1 5507.66 4821.70 66.81 o 3 2 1 269.91 286.37 24.63 o 4 2 1 12.99 21.31 19.36 o 5 2 1 129.10 143.28 23.85 o 6 2 1 43.08 9.60 27.44 o 7 2 1 13.58 18.23 39.84 o 8 2 1 8.71 24.43 51.98 o 9 2 1 109.37 58.33 77.54 o 10 2 1 78.99 47.72 72.45 o 11 2 1 0.32 -76.78 76.78 o -11 3 1 3.91 63.83 84.96 o -10 3 1 9.07 -80.22 112.04 o -9 3 1 89.89 169.04 124.53 o -8 3 1 740.05 625.88 70.35 o -7 3 1 519.61 608.17 52.09 o -6 3 1 466.18 405.58 34.13 o -5 3 1 125.11 107.53 28.07 o -4 3 1 105.45 274.03 58.00 o -3 3 1 106.88 471.68 53.70 o -2 3 1 2168.96 3277.52 61.11 o -1 3 1 6792.63 7888.28 109.79 o 0 3 1 1717.09 2071.92 50.71 o 1 3 1 484.88 692.41 52.79 o 2 3 1 113.42 188.85 37.63 o 3 3 1 2028.52 1877.48 45.82 o 4 3 1 1034.38 1069.92 39.75 o 5 3 1 1732.38 1676.98 47.20 o 6 3 1 1671.38 1608.96 57.74 o 7 3 1 1401.12 1306.64 70.56 o 8 3 1 317.54 283.23 74.30 o 9 3 1 56.48 1.25 79.87 o 10 3 1 8.56 -5.56 80.63 o 11 3 1 33.03 -23.26 84.85 o -11 4 1 24.56 50.89 88.77 o -10 4 1 23.60 15.49 83.27 o -9 4 1 1.44 -71.26 71.26 o -8 4 1 0.25 -55.77 68.62 o -7 4 1 44.60 9.78 45.44 o -6 4 1 15.48 -37.08 37.08 o -5 4 1 81.11 67.73 33.35 o -4 4 1 32.88 105.13 32.38 o -3 4 1 239.58 266.84 32.92 o -2 4 1 5.81 504.68 45.87 o -1 4 1 99.62 182.84 28.96 o 0 4 1 220.07 357.99 35.42 o 1 4 1 44.16 72.77 29.21 o 2 4 1 17.24 262.26 32.30 o 3 4 1 376.57 458.96 35.63 o 4 4 1 227.93 225.97 34.92 o 5 4 1 178.39 198.27 35.95 o 6 4 1 5.83 -6.00 42.34 o 7 4 1 64.10 6.93 50.50 o 8 4 1 87.40 -19.94 80.83 o 9 4 1 5.58 -40.56 81.44 o 10 4 1 71.89 88.89 89.92 o -10 5 1 54.07 168.20 89.85 o -9 5 1 59.16 53.22 83.29 o -8 5 1 188.77 183.39 128.34 o -7 5 1 488.89 554.93 75.29 o -6 5 1 24.18 -22.33 49.90 o -5 5 1 1.31 31.34 49.82 o -4 5 1 44.93 83.89 42.09 o -3 5 1 478.39 398.65 42.62 o -2 5 1 1773.13 2018.59 60.08 o -1 5 1 2114.33 2620.15 63.84 o 0 5 1 2760.91 3102.94 68.04 o 1 5 1 3261.83 3223.04 70.87 o 2 5 1 489.07 533.81 46.71 o 3 5 1 152.31 202.28 38.80 o 4 5 1 598.45 673.69 52.90 o 5 5 1 502.66 568.49 70.53 o 6 5 1 335.06 453.26 57.38 o 7 5 1 54.87 -35.17 62.74 o 8 5 1 10.20 -5.63 81.20 o 9 5 1 72.74 96.01 92.08 o 10 5 1 21.84 82.23 91.42 o -9 6 1 10.13 22.86 88.08 o -8 6 1 162.39 97.43 86.27 o -7 6 1 65.19 88.62 80.71 o -6 6 1 166.64 169.06 87.75 o -5 6 1 170.54 144.45 56.30 o -4 6 1 509.57 566.69 63.55 o -3 6 1 437.63 473.11 55.14 o -2 6 1 1850.94 1763.18 71.83 o -1 6 1 240.64 247.98 46.97 o 0 6 1 423.94 531.43 49.24 o 1 6 1 1391.11 1788.86 71.70 o 2 6 1 112.96 33.51 45.74 o 3 6 1 7.96 35.76 51.01 o 4 6 1 231.91 242.48 59.66 o 5 6 1 14.84 44.25 59.29 o 6 6 1 14.32 125.76 79.46 o 7 6 1 10.10 -70.03 70.03 o 8 6 1 0.05 17.64 84.74 o 9 6 1 10.11 -13.79 185.82 o -8 7 1 47.75 153.38 92.54 o -7 7 1 172.27 188.69 88.94 o -6 7 1 634.74 564.06 111.46 o -5 7 1 164.28 198.22 73.24 o -4 7 1 210.05 266.22 63.43 o -3 7 1 378.37 412.81 68.97 o -2 7 1 197.30 164.94 66.15 o -1 7 1 176.87 168.87 61.63 o 0 7 1 13.26 16.61 59.92 o 1 7 1 19.88 -14.36 56.00 o 2 7 1 813.41 859.31 76.02 o 3 7 1 709.37 688.68 77.78 o 4 7 1 334.29 401.07 72.35 o 5 7 1 318.19 359.97 78.06 o 6 7 1 330.65 219.10 94.61 o 7 7 1 113.88 149.46 107.63 o 8 7 1 75.11 -83.74 97.46 o -7 8 1 0.01 -83.53 83.53 o -6 8 1 0.12 68.90 97.90 o -5 8 1 51.02 85.37 78.81 o -4 8 1 449.30 613.76 123.02 o -3 8 1 62.69 28.23 94.85 o -2 8 1 384.75 320.95 96.02 o -1 8 1 0.11 18.94 74.33 o 0 8 1 354.63 401.27 88.69 o 1 8 1 357.44 368.52 94.66 o 2 8 1 30.64 93.59 72.37 o 3 8 1 817.61 709.75 118.42 o 4 8 1 147.05 114.42 86.41 o 5 8 1 5.86 25.46 89.54 o 6 8 1 35.57 -83.80 83.80 o -5 9 1 25.07 133.13 202.33 o -4 9 1 94.57 -31.29 150.70 o -3 9 1 44.19 5.91 99.68 o -2 9 1 73.59 213.84 108.06 o -1 9 1 28.16 68.43 92.54 o 0 9 1 211.65 193.18 96.93 o 1 9 1 985.47 955.34 157.46 o 2 9 1 385.94 337.46 100.75 o 3 9 1 158.72 236.96 109.52 o 4 9 1 66.84 31.53 93.31 o -12 0 2 5.09 -12.48 113.09 o -11 0 2 40.61 22.06 103.88 o -10 0 2 319.19 334.17 112.39 o -9 0 2 538.48 353.14 81.78 o -8 0 2 238.09 315.74 53.34 o -7 0 2 64.29 86.13 31.38 o -6 0 2 277.98 252.39 26.02 o -5 0 2 2268.63 2339.35 54.92 o -4 0 2 3998.16 3787.67 62.32 o -3 0 2 88.65 6716.24 508.03 o -2 0 2 9579.65 9296.42 117.51 o -1 0 2 29384.09 24449.13 479.08 o 0 0 2 510.09 522.83 15.76 o 2 0 2 1384.37 1297.57 32.17 o 3 0 2 2621.53 2194.29 52.69 o 4 0 2 1326.41 1324.88 45.54 o 5 0 2 959.79 1012.12 45.56 o 6 0 2 714.66 632.34 44.21 o 7 0 2 564.68 607.62 62.63 o 8 0 2 228.93 206.28 71.73 o 9 0 2 72.41 228.05 115.38 o 10 0 2 32.81 104.46 181.56 o 11 0 2 15.13 -45.11 219.02 o -12 1 2 2.12 18.05 81.41 o -11 1 2 0.71 -91.31 91.31 o -10 1 2 8.49 117.96 64.47 o -9 1 2 24.51 21.91 43.49 o -8 1 2 0.20 -21.04 33.43 o -7 1 2 7.45 -24.79 24.79 o -6 1 2 2352.99 2452.34 41.82 o -5 1 2 178.56 168.28 19.18 o -4 1 2 4597.07 3837.58 52.30 o -3 1 2 10832.91 9579.77 92.40 o -2 1 2 1537.66 1406.98 22.69 o -1 1 2 57.62 509.62 29.87 o 0 1 2 43.01 38.09 11.04 o 1 1 2 7729.61 6332.70 70.26 o 2 1 2 1082.38 1319.86 34.61 o 3 1 2 182.18 158.71 21.85 o 4 1 2 2247.98 2172.28 42.46 o 5 1 2 18.66 -6.82 23.66 o 6 1 2 112.24 77.21 29.61 o 7 1 2 34.38 -5.37 39.63 o 8 1 2 88.96 91.94 47.82 o 9 1 2 12.53 18.02 69.13 o 10 1 2 3.20 153.49 83.98 o 11 1 2 3.79 73.89 125.20 o -12 2 2 0.23 115.14 78.64 o -11 2 2 17.16 -53.72 69.02 o -10 2 2 236.06 250.08 79.42 o -9 2 2 398.50 349.26 60.76 o -8 2 2 472.00 572.61 50.14 o -7 2 2 1069.43 1050.01 40.46 o -6 2 2 2150.08 1935.24 45.72 o -5 2 2 992.49 1171.60 44.09 o -4 2 2 1926.42 2422.99 43.70 o -3 2 2 1113.81 1450.12 32.69 o -2 2 2 4423.76 4423.60 59.02 o -1 2 2 6145.07 9496.19 167.02 o 0 2 2 159.83 277.55 25.63 o 1 2 2 10577.94 9188.29 104.53 o 2 2 2 13048.04 11418.67 128.97 o 3 2 2 2113.55 2020.20 42.35 o 4 2 2 5038.99 4056.23 59.74 o 5 2 2 1794.71 1652.74 43.21 o 6 2 2 1275.82 1401.08 49.22 o 7 2 2 914.48 913.24 55.53 o 8 2 2 472.03 404.31 64.85 o 9 2 2 189.20 267.85 84.79 o 10 2 2 7.04 -44.66 72.00 o 11 2 2 0.99 -75.67 75.67 o -11 3 2 1.80 -42.27 77.42 o -10 3 2 44.93 84.94 75.95 o -9 3 2 59.48 -60.77 60.77 o -8 3 2 4.72 70.48 49.19 o -7 3 2 82.68 48.21 42.76 o -6 3 2 16.25 15.89 33.41 o -5 3 2 104.86 109.31 35.29 o -4 3 2 131.83 234.42 26.64 o -3 3 2 550.84 1231.72 60.33 o -2 3 2 1042.83 1134.99 37.24 o -1 3 2 1705.04 2065.85 50.34 o 0 3 2 3062.14 3365.99 61.14 o 1 3 2 232.07 503.49 49.16 o 2 3 2 2174.67 2240.98 48.41 o 3 3 2 561.69 471.75 32.53 o 4 3 2 2582.21 2463.82 54.85 o 5 3 2 19.82 -26.70 26.70 o 6 3 2 44.45 89.86 37.56 o 7 3 2 0.37 36.35 49.74 o 8 3 2 26.96 -81.97 91.21 o 9 3 2 23.08 10.70 79.86 o 10 3 2 3.59 -31.11 85.78 o -11 4 2 75.88 16.72 111.73 o -10 4 2 207.05 136.44 80.89 o -9 4 2 227.37 206.14 129.17 o -8 4 2 89.82 143.49 63.17 o -7 4 2 17.55 22.00 47.81 o -6 4 2 31.01 51.04 36.56 o -5 4 2 6.17 21.05 32.34 o -4 4 2 356.21 422.12 36.96 o -3 4 2 1131.18 1307.36 47.69 o -2 4 2 3560.02 3941.23 68.82 o -1 4 2 3785.69 5729.83 92.95 o 0 4 2 4348.56 4790.23 83.34 o 1 4 2 896.21 1353.30 68.89 o 2 4 2 1363.69 1245.57 44.76 o 3 4 2 100.91 94.62 30.41 o 4 4 2 426.34 516.33 40.19 o 5 4 2 2013.97 1950.58 76.17 o 6 4 2 526.54 433.71 53.47 o 7 4 2 187.94 147.20 57.64 o 8 4 2 9.06 64.16 80.85 o 9 4 2 18.60 26.51 85.01 o 10 4 2 9.42 19.78 88.15 o -10 5 2 1.00 -78.50 78.50 o -9 5 2 1.31 4.61 77.39 o -8 5 2 126.92 30.47 78.00 o -7 5 2 246.70 106.70 67.15 o -6 5 2 81.90 60.37 54.90 o -5 5 2 124.93 215.91 43.61 o -4 5 2 716.14 769.18 50.34 o -3 5 2 1423.82 1552.88 54.15 o -2 5 2 352.66 452.35 38.29 o -1 5 2 96.37 450.47 42.29 o 0 5 2 34.31 30.66 34.60 o 1 5 2 509.35 606.46 42.02 o 2 5 2 108.99 114.60 37.14 o 3 5 2 17.61 4.45 36.82 o 4 5 2 51.94 91.53 45.05 o 5 5 2 166.20 159.39 56.07 o 6 5 2 5.13 -5.36 48.55 o 7 5 2 143.77 201.10 77.17 o 8 5 2 79.46 28.15 86.74 o 9 5 2 5.65 62.11 93.87 o -9 6 2 112.41 45.41 86.82 o -8 6 2 149.48 196.81 85.86 o -7 6 2 203.81 162.58 83.56 o -6 6 2 492.62 447.24 74.85 o -5 6 2 1476.14 1581.92 95.25 o -4 6 2 315.79 389.52 59.60 o -3 6 2 71.26 161.20 46.75 o -2 6 2 349.48 303.37 51.74 o -1 6 2 521.19 496.89 47.30 o 0 6 2 298.36 297.52 47.36 o 1 6 2 3.53 92.92 44.39 o 2 6 2 13.42 114.01 47.38 o 3 6 2 21.73 79.09 49.94 o 4 6 2 276.10 187.69 63.48 o 5 6 2 302.32 426.24 70.84 o 6 6 2 403.95 331.49 76.49 o 7 6 2 308.23 189.20 83.22 o 8 6 2 141.00 75.84 107.21 o -8 7 2 29.22 64.88 125.84 o -7 7 2 218.31 323.94 83.65 o -6 7 2 182.89 143.10 77.21 o -5 7 2 21.16 42.90 61.34 o -4 7 2 267.53 319.48 97.37 o -3 7 2 197.27 133.47 65.94 o -2 7 2 147.17 119.29 65.49 o -1 7 2 38.84 218.64 61.56 o 0 7 2 21.56 4.96 53.15 o 1 7 2 533.27 687.10 70.64 o 2 7 2 102.68 80.59 63.17 o 3 7 2 373.87 403.16 78.26 o 4 7 2 772.94 615.10 82.53 o 5 7 2 489.92 419.66 90.00 o 6 7 2 0.22 11.22 89.15 o 7 7 2 28.78 -100.35 100.35 o -7 8 2 40.49 -10.07 86.41 o -6 8 2 97.07 196.74 90.76 o -5 8 2 92.12 265.97 93.11 o -4 8 2 372.30 220.00 90.49 o -3 8 2 289.83 254.48 91.10 o -2 8 2 35.65 68.69 75.11 o -1 8 2 183.46 420.00 88.73 o 0 8 2 318.90 286.01 84.80 o 1 8 2 382.32 364.92 85.84 o 2 8 2 106.15 74.77 78.56 o 3 8 2 698.66 451.99 90.43 o 4 8 2 378.27 335.76 98.91 o 5 8 2 48.73 -76.43 84.82 o 6 8 2 50.78 -101.65 101.65 o -5 9 2 57.42 154.53 143.21 o -4 9 2 58.39 54.23 90.54 o -3 9 2 72.22 213.26 94.01 o -2 9 2 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