#------------------------------------------------------------------------------ #$Date: 2016-04-03 01:51:43 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181109 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/89/2218989.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2218989_Fobs loop_ _publ_author_name 'Fang, Yan-Xiong' 'Huang, Hua-Rong' 'Du, Zhi-Yun' 'Huang, Bao-Hua' 'Zhang, Kun' _publ_section_title ; 5-Hydroxy-1-methyl-3,4-dihydro-2H-pyrrolium hydrogensulfate ; _journal_coeditor_code FB2100 _journal_issue 8 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o1622 _journal_volume 64 _journal_year 2008 _space_group_IT_number 19 _symmetry_space_group_name_Hall 'P 2ac 2ab' _symmetry_space_group_name_H-M 'P 21 21 21' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 6.5418 _cell_length_b 10.9638 _cell_length_c 11.6140 _exptl_crystal_F_000 416.00 _reflns_d_resolution_high 0.8120 _cod_data_source_file fb2100Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' FF in P2(1)2(1)2(1)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 88.14 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 515.46 627.13 23.75 o 4 0 0 2460.03 2515.69 93.03 o 6 0 0 13.31 19.05 2.43 o 8 0 0 227.59 249.60 12.09 o 1 1 0 38.50 22.78 0.53 o 2 1 0 4836.21 5140.37 132.61 o 3 1 0 369.55 461.30 12.74 o 4 1 0 140.53 142.75 4.81 o 5 1 0 135.82 164.21 5.64 o 6 1 0 4.57 6.33 1.57 o 7 1 0 11.67 11.79 1.88 o 8 1 0 0.01 -0.53 1.57 o 0 2 0 3283.33 3073.23 69.36 o 1 2 0 1844.47 1826.09 32.04 o 2 2 0 36.79 34.77 0.93 o 3 2 0 2909.68 3166.29 118.51 o 4 2 0 17.05 16.85 0.91 o 5 2 0 189.13 181.13 6.14 o 6 2 0 0.55 -0.24 1.28 o 7 2 0 86.85 105.16 4.68 o 1 3 0 130.52 138.77 3.02 o 2 3 0 79.72 61.36 1.88 o 3 3 0 11.89 8.88 0.95 o 4 3 0 45.36 56.00 2.83 o 5 3 0 45.29 50.07 2.77 o 6 3 0 266.94 267.09 8.86 o 7 3 0 33.49 37.47 2.84 o 0 4 0 694.80 633.76 14.34 o 1 4 0 27.32 30.77 1.28 o 2 4 0 5.38 12.27 0.56 o 3 4 0 51.94 51.70 1.82 o 4 4 0 2701.05 2656.65 59.31 o 5 4 0 1.42 0.90 1.36 o 6 4 0 122.12 117.24 5.06 o 7 4 0 40.04 36.28 2.94 o 1 5 0 11.52 22.31 1.18 o 2 5 0 0.55 0.08 0.31 o 3 5 0 0.63 1.85 0.85 o 4 5 0 80.59 72.83 2.50 o 5 5 0 52.98 50.88 3.97 o 6 5 0 46.02 43.82 3.94 o 7 5 0 3.03 3.90 2.07 o 0 6 0 389.40 426.02 9.78 o 1 6 0 2436.69 2462.06 38.61 o 2 6 0 4.27 5.31 1.14 o 3 6 0 252.92 235.90 6.15 o 4 6 0 1709.61 1686.93 39.36 o 7 6 0 42.89 51.31 4.72 o 1 7 0 937.35 926.32 14.99 o 2 7 0 503.16 502.56 12.06 o 3 7 0 31.32 39.62 1.83 o 5 7 0 0.51 -0.51 1.40 o 0 8 0 774.74 822.97 31.10 o 1 8 0 336.62 348.14 7.18 o 2 8 0 23.44 20.87 1.31 o 3 8 0 21.74 9.87 2.80 o 1 9 0 777.93 789.59 21.37 o 2 9 0 70.44 74.81 1.93 o 3 9 0 85.94 91.19 7.02 o 4 9 0 0.63 0.44 1.75 o 6 9 0 2.20 3.56 2.06 o 0 10 0 1324.92 1300.89 48.90 o 1 10 0 402.80 407.34 11.72 o 2 10 0 31.52 34.29 2.17 o 3 10 0 527.06 531.14 11.49 o 4 10 0 175.24 123.44 8.32 o 5 10 0 121.58 136.72 8.23 o 1 11 0 1.37 0.34 1.02 o 2 11 0 141.94 135.19 4.99 o 3 11 0 99.37 106.51 7.03 o 4 11 0 2.25 1.32 1.83 o 0 12 0 111.79 117.45 6.31 o 1 12 0 62.97 64.24 3.07 o 2 12 0 83.25 78.58 3.57 o 3 12 0 184.58 195.99 9.35 o 1 13 0 23.53 20.93 1.88 o 2 13 0 12.49 15.99 1.92 o 1 0 1 589.49 582.59 12.84 o 2 0 1 5162.33 5151.16 134.67 o 3 0 1 1438.97 1439.17 29.01 o 4 0 1 464.23 533.12 14.91 o 5 0 1 13.93 10.77 1.49 o 6 0 1 161.03 174.08 6.03 o 7 0 1 9.98 10.45 1.78 o 8 0 1 1.29 1.17 1.69 o -8 1 1 92.07 108.60 4.78 o -7 1 1 12.19 16.44 2.07 o -6 1 1 8.30 8.04 1.65 o -5 1 1 157.80 153.67 5.37 o -4 1 1 1122.67 1181.05 31.81 o -3 1 1 2872.58 3085.21 79.54 o -2 1 1 137.11 133.45 4.25 o -1 1 1 2532.35 2523.14 45.68 o 0 1 1 2596.64 2668.34 85.33 o 1 1 1 2508.99 2671.68 67.07 o 2 1 1 136.87 130.26 2.96 o 3 1 1 2884.44 3054.00 58.52 o 4 1 1 1130.93 1211.54 31.98 o 5 1 1 161.90 159.88 5.52 o 6 1 1 8.38 8.95 1.77 o 7 1 1 12.01 15.98 1.89 o 8 1 1 89.94 104.63 4.71 o -7 2 1 103.77 100.54 4.56 o -6 2 1 121.76 126.41 4.93 o -5 2 1 192.31 212.05 6.95 o -4 2 1 73.05 83.81 2.22 o -3 2 1 785.31 764.53 27.08 o -2 2 1 102.44 104.94 2.41 o -1 2 1 4030.19 3960.80 69.82 o 0 2 1 4413.42 4132.94 109.88 o 1 2 1 4034.50 4058.39 69.86 o 2 2 1 103.99 107.94 2.12 o 3 2 1 758.58 734.50 14.75 o 4 2 1 74.05 88.76 3.45 o 5 2 1 193.59 216.26 7.08 o 6 2 1 121.57 126.34 5.03 o 7 2 1 110.21 107.41 4.74 o -7 3 1 30.36 34.45 2.72 o -6 3 1 147.26 136.96 5.43 o -5 3 1 26.54 25.04 2.03 o -4 3 1 620.48 603.24 15.46 o -3 3 1 161.06 147.76 5.49 o -2 3 1 121.67 131.46 3.34 o -1 3 1 1532.17 1505.14 33.62 o 0 3 1 4081.84 3894.53 90.71 o 1 3 1 1528.63 1513.98 26.44 o 2 3 1 122.80 131.42 2.68 o 3 3 1 161.07 151.61 2.90 o 4 3 1 633.59 610.81 10.25 o 5 3 1 25.40 24.03 1.28 o 6 3 1 144.65 140.20 5.51 o 7 3 1 28.94 31.44 2.66 o -7 4 1 53.48 49.89 3.40 o -6 4 1 222.51 204.74 14.39 o -5 4 1 37.40 37.22 3.15 o -4 4 1 44.40 41.89 2.98 o -3 4 1 45.79 46.40 1.65 o -2 4 1 479.55 484.60 10.74 o -1 4 1 2055.69 2124.55 47.33 o 0 4 1 31.17 30.71 1.00 o 1 4 1 2038.36 2148.30 37.19 o 2 4 1 462.07 440.72 8.47 o 3 4 1 48.41 47.66 1.92 o 4 4 1 44.63 37.97 1.86 o 5 4 1 38.67 37.42 2.56 o 6 4 1 221.57 211.44 7.61 o 7 4 1 54.70 52.18 3.47 o -7 5 1 97.50 104.51 6.86 o -6 5 1 2.20 2.46 1.67 o -5 5 1 562.83 196.72 10.54 o -4 5 1 158.17 154.10 7.59 o -3 5 1 101.70 116.33 3.39 o -2 5 1 128.69 135.74 3.61 o -1 5 1 996.91 1027.95 28.92 o 0 5 1 56.69 48.58 1.09 o 1 5 1 1023.59 1043.38 18.23 o 2 5 1 126.97 126.80 3.70 o 3 5 1 110.58 122.13 2.69 o 4 5 1 152.42 157.51 3.46 o 6 5 1 2.25 1.77 1.96 o 7 5 1 98.68 104.90 6.94 o -6 6 1 69.16 13.25 3.82 o -3 6 1 402.76 410.89 9.88 o -2 6 1 31.97 27.87 1.36 o -1 6 1 328.39 333.09 6.75 o 0 6 1 41.56 44.46 0.88 o 1 6 1 343.40 332.26 7.08 o 2 6 1 35.93 32.18 1.04 o 3 6 1 411.53 403.65 9.98 o 6 6 1 70.25 25.06 4.73 o -6 7 1 10.05 3.96 1.95 o -3 7 1 45.10 42.47 1.87 o -2 7 1 13.86 10.52 0.96 o -1 7 1 310.41 327.97 6.74 o 0 7 1 2178.08 2294.73 33.34 o 1 7 1 306.75 329.71 5.65 o 2 7 1 14.11 9.56 1.54 o 3 7 1 43.90 40.95 1.97 o 6 7 1 10.07 4.63 4.07 o -3 8 1 162.14 168.89 4.93 o -2 8 1 1172.80 1172.04 23.10 o -1 8 1 157.97 153.38 3.51 o 0 8 1 92.74 91.82 2.17 o 1 8 1 156.64 155.20 3.64 o 2 8 1 1175.49 1187.25 28.10 o 3 8 1 167.66 174.77 5.08 o -4 9 1 63.05 53.37 2.39 o -3 9 1 718.80 654.92 26.16 o -2 9 1 1.36 3.29 2.07 o -1 9 1 538.10 553.85 15.42 o 0 9 1 2.40 3.12 1.90 o 1 9 1 538.50 561.33 11.54 o 2 9 1 1.32 1.93 0.93 o 3 9 1 716.05 714.12 16.56 o 4 9 1 63.25 53.61 4.36 o -5 10 1 151.38 145.10 4.80 o -4 10 1 4.82 7.03 1.27 o -3 10 1 87.88 87.99 3.17 o -2 10 1 107.74 109.31 4.15 o -1 10 1 600.37 562.26 15.63 o 0 10 1 176.49 179.00 5.76 o 1 10 1 594.38 558.85 15.67 o 2 10 1 111.27 108.35 5.01 o 3 10 1 87.16 89.81 3.03 o 4 10 1 4.69 8.12 4.04 o 5 10 1 153.36 139.23 8.47 o -4 11 1 153.85 168.34 7.55 o -3 11 1 18.85 17.33 2.03 o -2 11 1 10.53 10.82 1.68 o -1 11 1 52.79 51.43 2.57 o 0 11 1 242.11 245.30 7.63 o 1 11 1 51.80 53.95 2.62 o 2 11 1 10.39 10.83 1.67 o 3 11 1 19.21 18.90 1.56 o 4 11 1 156.44 157.08 6.76 o -3 12 1 49.92 56.72 3.90 o -2 12 1 177.12 177.08 10.03 o -1 12 1 51.31 43.96 2.42 o 0 12 1 82.70 78.66 3.40 o 1 12 1 49.45 41.56 2.39 o 2 12 1 179.66 179.61 6.29 o 3 12 1 51.25 58.92 5.26 o -2 13 1 3.76 7.35 1.73 o -1 13 1 60.60 68.22 3.31 o 0 13 1 85.83 81.36 3.67 o 1 13 1 60.31 66.41 3.27 o 2 13 1 3.69 8.30 1.86 o 0 0 2 1982.27 2054.89 141.57 o 1 0 2 3043.37 3059.39 67.68 o 2 0 2 1742.29 1778.87 45.19 o 3 0 2 0.24 0.45 0.44 o 4 0 2 2170.47 2268.51 43.75 o 5 0 2 4.59 2.30 1.04 o 6 0 2 1.47 4.67 1.36 o 7 0 2 5.69 4.65 1.61 o -7 1 2 102.10 101.96 4.32 o -6 1 2 83.23 87.63 5.10 o -5 1 2 75.78 76.03 3.23 o -4 1 2 219.94 249.16 7.38 o -3 1 2 161.03 151.22 4.11 o -2 1 2 541.42 600.36 11.89 o -1 1 2 5041.42 5191.94 76.56 o 0 1 2 154.53 153.21 2.45 o 1 1 2 5038.32 5109.53 81.33 o 2 1 2 561.89 602.08 14.73 o 3 1 2 164.69 153.04 5.45 o 4 1 2 217.86 240.51 8.52 o 5 1 2 79.67 76.97 3.41 o 6 1 2 79.03 78.96 5.20 o 7 1 2 97.96 95.65 4.21 o -7 2 2 177.68 196.77 7.12 o -6 2 2 21.40 20.01 1.90 o -5 2 2 1356.56 1388.92 36.87 o -4 2 2 136.11 151.65 5.05 o -3 2 2 1126.16 1136.86 22.07 o -2 2 2 256.68 245.17 12.18 o -1 2 2 7762.71 7659.60 249.36 o 0 2 2 1123.52 1088.97 16.19 o 1 2 2 7769.05 7447.02 166.03 o 2 2 2 256.85 257.53 6.44 o 3 2 2 1127.26 1157.72 22.47 o 4 2 2 138.98 151.10 3.76 o 5 2 2 1349.98 1366.70 37.05 o 6 2 2 20.87 20.14 2.01 o 7 2 2 179.87 199.41 7.32 o -7 3 2 52.61 58.28 3.42 o -6 3 2 7.66 5.58 1.69 o -5 3 2 46.61 46.38 2.68 o -4 3 2 8.27 4.51 1.22 o -3 3 2 750.59 806.62 17.50 o -2 3 2 1585.88 1791.64 45.10 o -1 3 2 335.59 365.14 5.68 o 0 3 2 207.81 217.73 3.69 o 1 3 2 340.67 368.12 5.66 o 2 3 2 1636.21 1828.88 31.89 o 3 3 2 746.23 752.92 12.63 o 4 3 2 8.13 5.95 0.84 o 5 3 2 47.37 42.57 3.09 o 6 3 2 5.43 2.90 1.83 o 7 3 2 51.33 55.57 3.46 o -7 4 2 40.91 38.05 2.98 o -6 4 2 91.22 76.05 7.30 o -5 4 2 483.59 517.96 20.27 o -4 4 2 312.06 321.28 12.43 o -3 4 2 201.05 221.92 8.37 o -2 4 2 879.37 939.95 31.67 o -1 4 2 2097.81 2132.29 44.78 o 0 4 2 1449.34 1333.39 21.12 o 1 4 2 2103.31 2135.25 47.27 o 2 4 2 880.06 915.38 16.44 o 3 4 2 200.47 205.16 4.27 o 4 4 2 304.31 279.51 7.09 o 5 4 2 484.90 484.95 8.60 o 6 4 2 93.38 81.66 4.11 o 7 4 2 41.67 43.70 3.16 o -7 5 2 234.30 255.25 12.50 o -6 5 2 171.72 169.41 8.87 o -5 5 2 218.81 213.19 9.97 o -4 5 2 160.06 162.40 7.82 o -3 5 2 406.28 434.34 14.39 o -2 5 2 797.07 828.21 18.93 o -1 5 2 85.28 100.26 2.32 o 0 5 2 1220.53 1309.57 20.74 o 1 5 2 76.69 85.40 2.01 o 2 5 2 784.70 816.08 14.80 o 3 5 2 413.32 401.06 7.79 o 4 5 2 162.80 163.73 3.62 o 5 5 2 225.73 208.68 5.86 o 6 5 2 170.57 170.80 9.08 o 7 5 2 232.01 248.73 12.67 o -7 6 2 6.28 4.85 2.18 o -6 6 2 4.49 2.45 1.75 o -3 6 2 443.29 449.69 17.83 o -2 6 2 1014.59 1043.85 23.68 o -1 6 2 95.43 91.81 2.91 o 0 6 2 284.65 267.17 4.58 o 1 6 2 93.46 83.65 4.06 o 2 6 2 1013.38 1031.79 18.52 o 3 6 2 442.19 438.32 8.37 o 6 6 2 4.85 0.76 1.95 o 7 6 2 6.66 5.23 2.23 o -3 7 2 86.61 86.40 2.86 o -2 7 2 188.67 183.57 4.23 o -1 7 2 24.36 24.50 1.50 o 0 7 2 594.59 591.50 9.71 o 1 7 2 24.80 25.18 0.87 o 2 7 2 188.76 186.81 5.18 o 3 7 2 84.41 85.29 3.03 o -4 8 2 548.42 555.91 13.62 o -3 8 2 551.26 544.28 13.12 o -2 8 2 99.79 96.32 3.56 o -1 8 2 654.40 689.67 13.64 o 0 8 2 1219.82 1287.27 20.57 o 1 8 2 653.91 693.05 13.99 o 2 8 2 99.71 91.77 5.57 o 3 8 2 553.51 539.54 13.32 o 4 8 2 553.01 554.61 13.72 o -4 9 2 35.36 38.45 2.04 o -3 9 2 108.17 115.32 3.21 o -2 9 2 264.52 243.67 5.40 o -1 9 2 320.16 328.48 6.86 o 0 9 2 7.81 9.15 1.29 o 1 9 2 330.25 330.39 7.25 o 2 9 2 264.13 239.99 5.82 o 3 9 2 109.48 113.46 4.65 o 4 9 2 36.18 43.04 2.27 o -5 10 2 3.52 2.01 1.27 o -4 10 2 242.25 252.89 6.14 o -3 10 2 20.00 26.33 2.15 o -2 10 2 217.01 214.30 6.86 o -1 10 2 13.18 15.75 1.42 o 0 10 2 645.91 679.44 18.65 o 1 10 2 14.55 17.95 1.21 o 2 10 2 218.70 213.58 5.56 o 3 10 2 21.94 26.64 1.75 o 4 10 2 242.49 246.97 7.27 o 5 10 2 4.24 1.42 2.18 o -4 11 2 3.59 2.62 1.72 o -3 11 2 8.12 9.98 1.71 o -2 11 2 493.86 512.65 14.44 o -1 11 2 0.46 -0.10 1.14 o 0 11 2 9.51 11.26 1.37 o 1 11 2 0.56 0.36 1.03 o 2 11 2 493.58 490.58 10.83 o 3 11 2 8.00 9.78 1.49 o 4 11 2 3.40 0.48 2.55 o -3 12 2 3.92 4.35 1.61 o -2 12 2 32.73 30.74 3.04 o -1 12 2 254.96 246.18 7.97 o 0 12 2 65.20 63.16 3.00 o 1 12 2 261.74 253.83 8.07 o 2 12 2 33.24 31.88 2.81 o 3 12 2 4.62 4.49 1.35 o -1 13 2 23.46 21.24 1.90 o 0 13 2 3.63 3.79 1.38 o 1 13 2 22.47 21.39 1.95 o 1 0 3 659.56 603.67 11.46 o 2 0 3 367.04 296.71 6.46 o 3 0 3 337.97 355.85 7.40 o 4 0 3 109.30 93.56 4.54 o 5 0 3 295.52 308.40 6.87 o 6 0 3 201.14 213.98 7.11 o 7 0 3 49.81 48.38 3.37 o -7 1 3 68.51 71.06 3.53 o -6 1 3 41.32 35.49 2.27 o -5 1 3 135.42 131.43 6.35 o -4 1 3 729.48 755.00 15.05 o -3 1 3 558.61 583.77 11.58 o -2 1 3 283.84 301.17 5.11 o -1 1 3 5614.54 5587.28 80.96 o 0 1 3 4628.75 4468.77 87.24 o 1 1 3 5574.17 5293.04 95.33 o 2 1 3 289.06 302.28 5.12 o 3 1 3 561.48 570.62 11.65 o 4 1 3 723.58 743.02 15.15 o 5 1 3 128.29 123.19 3.46 o 6 1 3 42.98 39.96 2.38 o 7 1 3 69.41 74.55 4.16 o -7 2 3 156.19 173.58 9.03 o -6 2 3 23.27 20.55 1.97 o -5 2 3 109.70 110.12 8.21 o -4 2 3 275.20 271.86 10.60 o -3 2 3 273.73 271.35 6.32 o -2 2 3 83.89 105.60 2.29 o -1 2 3 333.80 394.76 7.26 o 0 2 3 1881.49 1834.93 27.12 o 1 2 3 351.27 405.01 6.22 o 2 2 3 85.29 104.30 1.95 o 3 2 3 270.65 265.88 6.36 o 4 2 3 277.76 269.55 6.10 o 5 2 3 110.13 110.20 3.18 o 6 2 3 23.71 19.54 2.05 o 7 2 3 152.01 165.90 9.21 o -7 3 3 81.31 81.80 5.36 o -6 3 3 103.76 103.34 4.44 o -5 3 3 800.50 792.82 22.16 o -4 3 3 918.31 756.39 34.42 o -3 3 3 271.25 249.54 7.95 o -2 3 3 26.04 22.36 0.97 o -1 3 3 925.81 981.63 13.35 o 0 3 3 1163.23 1064.39 15.91 o 1 3 3 906.57 934.22 21.31 o 2 3 3 27.30 24.76 1.19 o 3 3 3 262.79 234.50 7.34 o 4 3 3 929.25 925.35 14.82 o 5 3 3 802.91 797.20 13.38 o 6 3 3 101.65 97.52 4.47 o 7 3 3 79.20 84.63 4.37 o -7 4 3 2.64 1.09 1.91 o -6 4 3 123.75 123.61 6.88 o -5 4 3 14.04 10.72 1.97 o -4 4 3 347.66 336.28 13.60 o -3 4 3 1591.79 1591.37 36.59 o -2 4 3 93.13 121.28 4.84 o -1 4 3 691.31 720.55 9.96 o 0 4 3 15.02 18.53 1.17 o 1 4 3 679.39 697.08 25.60 o 2 4 3 106.76 140.84 2.36 o 3 4 3 1603.71 1633.15 24.28 o 4 4 3 347.22 325.70 8.11 o 5 4 3 13.14 14.58 1.33 o 6 4 3 123.28 117.93 5.85 o 7 4 3 2.39 0.67 1.81 o -7 5 3 39.92 53.19 4.75 o -6 5 3 1.58 1.14 1.65 o -5 5 3 1225.20 1217.80 46.74 o -4 5 3 67.72 68.00 4.09 o -3 5 3 120.61 114.78 3.38 o -2 5 3 596.74 626.36 14.70 o -1 5 3 423.38 465.12 7.80 o 0 5 3 8.47 13.48 0.97 o 1 5 3 428.91 481.54 7.38 o 2 5 3 605.19 637.88 11.61 o 3 5 3 121.76 111.98 3.19 o 4 5 3 65.59 61.91 1.93 o 5 5 3 1225.86 1221.47 22.13 o 6 5 3 1.89 1.47 1.57 o 7 5 3 41.11 50.67 4.75 o -7 6 3 65.52 65.38 5.25 o -5 6 3 16.55 13.43 2.78 o -4 6 3 97.50 92.47 3.12 o -3 6 3 228.83 239.87 6.13 o -2 6 3 47.47 46.17 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1.61 o -1 2 13 4.75 7.32 2.32 o 0 2 13 252.51 265.40 5.48 o 1 2 13 5.14 7.76 2.38 o 2 2 13 23.85 23.01 2.00 o 3 2 13 10.29 11.60 1.80 o -2 3 13 41.86 43.26 2.08 o -1 3 13 8.83 7.74 1.26 o 0 3 13 79.19 78.54 2.37 o 1 3 13 7.82 6.13 1.30 o 2 3 13 43.49 47.28 2.47 o -2 4 13 40.19 40.75 2.03 o -1 4 13 77.67 85.60 3.05 o 0 4 13 9.02 5.66 1.38 o 1 4 13 75.82 86.89 3.31 o 2 4 13 40.44 41.11 2.35 o -1 5 13 24.80 20.55 2.16 o 0 5 13 14.45 14.04 4.36 o 1 5 13 23.75 22.12 1.89 o 0 0 14 1.14 1.74 1.62 o 1 0 14 54.02 48.79 1.93 o -1 1 14 111.23 109.07 3.63 o 0 1 14 29.56 34.38 1.94 o 1 1 14 111.08 114.05 3.10 o -1 2 14 23.86 24.10 2.07 o 0 2 14 7.29 11.79 1.51 o 1 2 14 24.82 26.04 1.50 o