#------------------------------------------------------------------------------ #$Date: 2016-04-03 01:52:01 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181110 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/90/2219008.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2219008_Fobs loop_ _publ_author_name 'Yao, Sumei' 'Liu, Jianhua' 'Han, Qiuxia' _publ_section_title ; Hexa-\m~2~-acetato-triaqua-\m~3~-oxido-triiron(III) nitrate acetic acid solvate ; _journal_coeditor_code HB2740 _journal_issue 8 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m989 _journal_volume 64 _journal_year 2008 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 90.851 _cell_angle_gamma 90.000 _cell_length_a 11.8351 _cell_length_b 14.7553 _cell_length_c 15.2500 _exptl_crystal_F_000 1460.00 _reflns_d_resolution_high 0.8255 _cod_data_source_file hb2740Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' NJY1 in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 274.07 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 2693.67 2273.97 81.16 o 2 0 0 9677.83 11196.00 334.26 o 3 0 0 10060.72 9815.08 257.77 o 4 0 0 6732.50 6471.56 172.45 o 5 0 0 17781.84 16540.93 374.36 o 6 0 0 343.64 636.63 127.07 o 7 0 0 2696.70 3181.89 135.97 o 8 0 0 7250.51 7519.11 237.95 o 9 0 0 6547.61 6766.67 386.71 o 10 0 0 2753.20 2990.54 258.68 o 11 0 0 702.36 772.30 147.10 o 12 0 0 4508.93 4379.50 298.90 o 13 0 0 512.62 433.26 133.96 o 14 0 0 4026.70 4386.43 323.19 o 1 1 0 40294.18 44201.47 1020.63 o 2 1 0 72.31 93.52 18.49 o 3 1 0 34887.81 36232.29 506.81 o 4 1 0 3227.71 3057.67 76.65 o 6 1 0 23.93 41.53 27.36 o 7 1 0 914.09 1067.90 59.97 o 8 1 0 2314.44 2309.93 88.70 o 9 1 0 957.01 999.23 78.60 o 10 1 0 2140.09 2034.66 114.87 o 11 1 0 1.51 16.07 89.60 o 12 1 0 65.16 73.23 151.60 o 13 1 0 2702.24 2827.44 275.72 o 14 1 0 6.43 0.00 78.93 o 0 2 0 1733.57 2166.45 82.51 o 1 2 0 1680.69 1768.59 59.18 o 2 2 0 5894.46 5820.67 110.97 o 3 2 0 1277.49 1171.10 57.53 o 4 2 0 3183.50 3455.28 80.50 o 5 2 0 1657.55 1673.95 59.57 o 6 2 0 1626.69 1399.80 60.67 o 7 2 0 167.37 81.76 39.42 o 8 2 0 1625.66 1774.31 106.60 o 9 2 0 481.64 403.77 66.90 o 10 2 0 23.04 20.99 50.36 o 11 2 0 677.62 762.37 86.58 o 12 2 0 6.90 65.59 89.40 o 13 2 0 211.72 214.17 87.86 o 14 2 0 65.55 39.71 99.71 o 1 3 0 678.19 717.09 26.67 o 2 3 0 31510.00 31886.05 569.20 o 3 3 0 792.54 872.38 56.47 o 4 3 0 801.20 729.99 38.52 o 5 3 0 1864.88 1823.66 62.29 o 6 3 0 251.84 214.97 33.19 o 7 3 0 60.68 0.00 27.64 o 8 3 0 7533.67 7281.82 177.07 o 9 3 0 196.71 286.30 61.03 o 10 3 0 7.62 2.79 44.58 o 11 3 0 382.82 478.22 75.70 o 12 3 0 1326.03 1350.70 133.97 o 13 3 0 182.95 211.09 84.07 o 14 3 0 10.10 0.00 106.88 o 0 4 0 6137.31 7521.48 145.03 o 1 4 0 34615.57 36692.70 411.03 o 2 4 0 6387.31 6744.68 122.71 o 3 4 0 14849.70 14374.65 229.58 o 4 4 0 9.48 0.00 52.76 o 5 4 0 92.92 56.31 23.66 o 6 4 0 3403.26 3382.22 93.06 o 7 4 0 2599.88 2485.48 84.64 o 8 4 0 3260.93 2910.88 98.08 o 9 4 0 19.98 0.00 41.27 o 10 4 0 81.02 45.56 51.54 o 11 4 0 3097.28 3154.37 147.71 o 12 4 0 46.72 105.03 64.03 o 13 4 0 57.64 191.47 79.40 o 2 5 0 8760.00 8990.79 135.94 o 3 5 0 845.31 731.91 43.12 o 4 5 0 14885.73 14216.29 239.42 o 5 5 0 9943.35 9925.27 217.62 o 6 5 0 675.73 566.30 44.73 o 7 5 0 12245.67 11931.87 224.16 o 8 5 0 2786.48 2667.53 165.97 o 9 5 0 3.63 0.00 42.03 o 10 5 0 4897.08 5040.26 234.87 o 11 5 0 897.76 933.37 95.36 o 12 5 0 938.05 875.74 132.53 o 13 5 0 344.88 214.80 129.90 o 0 6 0 53960.47 57231.91 903.18 o 1 6 0 5446.17 6029.35 103.14 o 2 6 0 2596.42 2554.98 56.51 o 3 6 0 11445.15 12640.26 186.54 o 4 6 0 716.14 598.33 53.37 o 5 6 0 17761.20 17135.86 335.03 o 6 6 0 949.41 1000.66 111.14 o 7 6 0 2113.82 2016.34 80.66 o 8 6 0 2399.65 2412.96 117.76 o 9 6 0 5154.02 5025.43 210.88 o 10 6 0 132.61 226.21 106.96 o 11 6 0 804.47 819.17 91.70 o 12 6 0 882.93 1004.09 135.57 o 13 6 0 78.37 152.97 90.94 o 1 7 0 5930.15 5868.52 98.84 o 2 7 0 6166.07 6819.92 109.91 o 3 7 0 9871.40 9549.08 154.70 o 4 7 0 15490.25 15900.60 234.18 o 5 7 0 367.91 312.47 47.98 o 6 7 0 1857.37 1862.71 95.00 o 7 7 0 680.63 604.11 71.06 o 8 7 0 287.42 229.24 58.42 o 9 7 0 1242.00 1099.24 117.34 o 10 7 0 1422.39 1796.05 160.88 o 11 7 0 31.85 0.00 97.64 o 12 7 0 267.92 220.18 100.71 o 13 7 0 459.03 393.42 172.03 o 0 8 0 1717.29 1932.30 105.25 o 1 8 0 6619.29 7206.11 118.47 o 2 8 0 717.65 830.98 47.04 o 3 8 0 45.28 47.10 24.45 o 4 8 0 377.99 466.97 37.95 o 5 8 0 142.65 119.67 43.66 o 6 8 0 2233.62 2433.54 155.27 o 7 8 0 904.37 1031.56 84.94 o 8 8 0 1.78 7.66 44.61 o 9 8 0 0.48 2.29 83.03 o 10 8 0 190.58 296.10 133.12 o 11 8 0 3.12 115.92 83.32 o 12 8 0 121.45 94.99 91.67 o 1 9 0 1098.16 1052.71 47.10 o 2 9 0 679.07 900.66 45.32 o 3 9 0 615.56 519.78 40.58 o 4 9 0 1021.37 1171.05 70.77 o 5 9 0 565.95 518.59 61.43 o 6 9 0 480.73 511.06 133.86 o 7 9 0 2282.57 2287.27 154.87 o 8 9 0 712.69 741.30 120.57 o 9 9 0 96.96 14.57 80.16 o 10 9 0 173.75 93.64 91.72 o 11 9 0 458.32 370.74 108.80 o 12 9 0 217.01 239.03 99.16 o 0 10 0 111.24 94.58 38.95 o 1 10 0 12087.82 12425.21 185.76 o 2 10 0 3207.20 3435.50 90.23 o 3 10 0 4542.76 4955.55 132.45 o 4 10 0 493.28 481.85 55.43 o 5 10 0 390.20 397.71 60.83 o 6 10 0 5203.73 5348.43 174.87 o 7 10 0 768.23 701.72 111.52 o 8 10 0 2059.80 2275.67 186.02 o 9 10 0 13.47 0.00 70.83 o 10 10 0 1264.22 1525.11 171.39 o 11 10 0 579.88 736.44 141.11 o 1 11 0 289.38 326.93 48.58 o 2 11 0 8429.19 8359.13 176.48 o 3 11 0 423.85 422.04 71.18 o 4 11 0 323.32 315.24 50.39 o 5 11 0 2088.29 2136.28 116.63 o 6 11 0 48.68 2.21 70.53 o 7 11 0 3939.53 3841.81 223.04 o 8 11 0 38.69 0.00 173.90 o 9 11 0 9.50 0.00 84.02 o 10 11 0 1319.17 1550.73 179.56 o 11 11 0 191.59 220.37 222.01 o 0 12 0 1817.72 1953.68 102.17 o 1 12 0 587.70 633.97 55.82 o 2 12 0 0.65 0.00 31.06 o 3 12 0 6.01 0.00 38.44 o 4 12 0 727.45 803.29 76.04 o 5 12 0 6.77 40.56 69.08 o 6 12 0 428.76 357.33 98.99 o 7 12 0 45.79 73.80 85.18 o 8 12 0 1096.61 1142.77 152.81 o 9 12 0 125.14 67.90 100.25 o 10 12 0 182.81 144.47 119.46 o 1 13 0 50.28 72.24 44.55 o 2 13 0 1694.57 1654.39 111.70 o 3 13 0 2122.12 2222.91 122.82 o 4 13 0 0.46 0.00 133.56 o 5 13 0 450.17 454.32 101.73 o 6 13 0 286.04 200.91 138.06 o 7 13 0 1563.51 1404.60 168.25 o 8 13 0 1.34 0.00 87.59 o 9 13 0 430.77 385.67 126.11 o 0 14 0 61.15 13.36 59.53 o 1 14 0 2302.42 2523.18 140.86 o 2 14 0 1829.83 1919.73 104.73 o 3 14 0 1847.63 1755.98 122.22 o 4 14 0 189.82 165.46 85.54 o 5 14 0 410.89 425.32 119.86 o 6 14 0 1854.85 1744.98 177.41 o 7 14 0 22.36 108.27 98.12 o 8 14 0 334.25 249.60 119.74 o 1 15 0 6.43 0.00 48.75 o 2 15 0 204.68 167.04 64.23 o 3 15 0 490.62 463.33 300.69 o 4 15 0 38.05 0.00 70.58 o 5 15 0 227.76 75.95 84.15 o 6 15 0 4.35 3.44 86.78 o 7 15 0 3.65 0.00 85.09 o 0 16 0 12.86 35.60 95.97 o 1 16 0 465.29 402.57 140.44 o 2 16 0 308.45 478.61 190.90 o 3 16 0 547.44 320.44 103.40 o 4 16 0 149.05 111.86 87.82 o 5 16 0 162.90 130.91 100.79 o 6 16 0 512.68 473.83 126.66 o 1 17 0 11.11 0.00 78.20 o 2 17 0 584.61 657.06 175.37 o 3 17 0 1911.89 1719.70 179.11 o 4 17 0 15.32 22.83 94.06 o -14 1 1 0.23 7.78 72.84 o -13 1 1 1134.74 1167.80 138.75 o -12 1 1 94.08 103.11 72.27 o -11 1 1 1109.88 1311.90 128.14 o -10 1 1 206.51 220.78 57.91 o -9 1 1 547.85 608.64 59.46 o -8 1 1 7264.17 7013.58 160.45 o -7 1 1 1882.22 1529.44 69.05 o -6 1 1 834.73 1117.56 55.79 o -5 1 1 10649.57 11190.75 192.80 o -4 1 1 13590.49 13620.51 217.10 o -3 1 1 30701.21 32146.47 448.72 o -2 1 1 637.62 681.39 27.91 o -1 1 1 11144.60 12846.52 258.32 o 0 1 1 10273.50 11439.21 430.95 o 1 1 1 54026.36 59666.53 1533.97 o 2 1 1 604.59 641.30 26.05 o 3 1 1 745.82 841.76 36.63 o 4 1 1 399.50 401.97 33.00 o 5 1 1 12771.21 12330.49 209.62 o 6 1 1 1261.52 1249.53 58.89 o 7 1 1 261.36 326.00 42.23 o 8 1 1 2016.24 1840.34 81.28 o 9 1 1 26.27 0.00 35.09 o 10 1 1 1946.06 2110.97 98.19 o 11 1 1 361.97 289.00 70.30 o 12 1 1 469.14 387.96 201.86 o 13 1 1 1334.90 1397.97 144.39 o 14 1 1 855.80 939.56 130.51 o -14 2 1 183.51 64.84 165.66 o -13 2 1 574.11 447.50 191.34 o -12 2 1 1503.13 1462.54 320.60 o -11 2 1 1117.10 1101.07 132.96 o -10 2 1 190.37 179.61 56.90 o -9 2 1 5400.85 5419.07 171.41 o -8 2 1 4575.14 4539.29 123.23 o -7 2 1 4969.35 5264.85 126.37 o -6 2 1 17025.81 18047.35 293.69 o -5 2 1 7548.29 7877.45 147.44 o -4 2 1 110.76 77.46 19.11 o -3 2 1 4964.08 4634.12 118.70 o -2 2 1 874.76 889.23 36.60 o -1 2 1 7368.51 8222.59 172.41 o 0 2 1 37899.41 42224.18 658.01 o 1 2 1 9318.25 10242.26 224.29 o 2 2 1 883.48 974.56 40.16 o 3 2 1 14710.30 14730.45 226.79 o 4 2 1 5748.94 5188.70 106.14 o 5 2 1 13836.78 14764.34 243.23 o 6 2 1 3161.62 3061.26 88.20 o 7 2 1 2514.67 2486.49 121.71 o 8 2 1 520.75 552.56 54.03 o 9 2 1 2955.34 3052.02 107.11 o 10 2 1 355.45 261.17 60.59 o 11 2 1 11.57 0.00 48.64 o 12 2 1 120.79 158.54 62.74 o 13 2 1 708.53 644.40 107.89 o 14 2 1 881.32 864.21 188.99 o -14 3 1 474.37 357.21 209.42 o -13 3 1 0.03 0.00 68.04 o -12 3 1 446.30 516.85 160.48 o -11 3 1 1.87 0.00 48.00 o -10 3 1 86.26 31.95 49.72 o -9 3 1 263.88 260.78 57.78 o -8 3 1 704.43 613.14 66.79 o -7 3 1 178.57 180.95 36.96 o -6 3 1 133.72 220.03 32.20 o -5 3 1 3413.28 3354.68 105.92 o -4 3 1 200.21 159.13 21.06 o -3 3 1 4207.67 4646.07 98.43 o -2 3 1 1622.45 1601.44 52.93 o -1 3 1 81.71 110.92 26.73 o 0 3 1 2051.01 2398.46 68.37 o 1 3 1 405.01 427.48 27.34 o 2 3 1 711.48 804.52 39.18 o 3 3 1 1988.13 2071.06 69.43 o 4 3 1 9328.33 9964.28 192.08 o 5 3 1 128.45 153.35 35.30 o 6 3 1 107.79 108.26 28.06 o 7 3 1 22.51 0.00 55.79 o 8 3 1 148.83 98.57 36.77 o 9 3 1 286.78 281.81 47.59 o 10 3 1 99.53 69.74 51.00 o 11 3 1 3.86 0.00 44.25 o 12 3 1 139.07 145.69 62.46 o 13 3 1 2.16 0.00 86.57 o 14 3 1 10.98 61.56 111.66 o -13 4 1 1.41 13.37 73.07 o -12 4 1 1791.40 1536.13 201.46 o -11 4 1 4.48 18.03 98.27 o -10 4 1 307.96 278.72 62.00 o -9 4 1 533.30 525.44 77.63 o -8 4 1 1256.42 1179.15 85.78 o -7 4 1 10983.18 11231.80 213.93 o -6 4 1 2280.64 1992.24 106.13 o -5 4 1 4935.84 5226.74 117.27 o -4 4 1 10665.84 11792.25 203.60 o -3 4 1 3490.96 3326.70 115.75 o -2 4 1 224.76 220.45 23.36 o -1 4 1 388.77 508.01 27.93 o 0 4 1 44287.48 47876.07 528.76 o 1 4 1 501.73 478.75 23.13 o 2 4 1 339.27 387.73 85.80 o 3 4 1 2992.41 3064.58 89.77 o 4 4 1 91.78 226.90 34.12 o 5 4 1 1481.17 1373.26 56.40 o 6 4 1 1968.29 2046.88 72.80 o 7 4 1 865.98 932.97 58.01 o 8 4 1 580.34 647.02 56.45 o 9 4 1 3068.58 2890.59 167.45 o 10 4 1 1.58 5.33 46.06 o 11 4 1 84.47 33.47 51.72 o 12 4 1 325.34 349.21 159.83 o 13 4 1 63.61 128.78 90.32 o -13 5 1 464.50 475.15 102.17 o -12 5 1 192.85 112.10 69.47 o -11 5 1 427.02 443.15 114.96 o -10 5 1 1992.04 2133.79 122.83 o -9 5 1 192.75 181.26 54.01 o -8 5 1 4819.60 4989.35 173.81 o -7 5 1 43.78 57.16 41.11 o -6 5 1 2607.54 2559.44 80.06 o -5 5 1 664.81 676.95 50.23 o -4 5 1 22298.32 22896.15 419.99 o -3 5 1 6217.74 5314.55 114.03 o -2 5 1 76.55 64.06 19.45 o -1 5 1 2217.43 2565.54 81.11 o 0 5 1 103.96 130.59 19.26 o 1 5 1 13531.27 13634.98 173.22 o 2 5 1 15060.01 15885.59 217.22 o 3 5 1 1536.72 1814.72 74.14 o 4 5 1 1455.69 1885.79 90.43 o 5 5 1 875.69 907.36 60.27 o 6 5 1 2028.37 2001.97 74.41 o 7 5 1 1153.15 1278.07 66.55 o 8 5 1 1568.46 1722.73 80.89 o 9 5 1 977.22 1062.45 213.57 o 10 5 1 1354.00 1250.64 103.70 o 11 5 1 1798.58 1745.26 359.39 o 12 5 1 708.00 871.04 130.11 o 13 5 1 124.79 173.85 89.75 o -13 6 1 43.11 133.24 114.69 o -12 6 1 370.37 293.15 116.75 o -11 6 1 2117.29 2140.96 132.35 o -10 6 1 75.44 33.33 49.77 o -9 6 1 2048.46 2102.57 117.37 o -8 6 1 1374.85 1503.33 140.26 o -7 6 1 3957.98 3943.13 139.68 o -6 6 1 14194.58 14059.10 317.08 o -5 6 1 24.51 6.39 27.33 o -4 6 1 1838.28 1592.23 66.68 o -3 6 1 4314.62 4160.33 94.18 o -2 6 1 19954.78 21291.59 240.37 o -1 6 1 12634.68 13824.67 180.00 o 0 6 1 168.63 257.45 23.47 o 1 6 1 2896.92 2771.39 59.04 o 2 6 1 4502.89 5019.15 93.91 o 3 6 1 13217.59 13221.51 258.18 o 4 6 1 1388.12 1374.76 95.11 o 5 6 1 49.06 74.44 44.95 o 6 6 1 15390.24 14930.77 316.94 o 7 6 1 4734.49 4307.84 166.02 o 8 6 1 4821.01 5015.50 200.57 o 9 6 1 207.61 204.17 53.97 o 10 6 1 2480.19 2580.92 258.80 o 11 6 1 230.55 4.60 101.98 o 12 6 1 778.51 803.70 129.44 o 13 6 1 175.72 168.59 139.10 o -13 7 1 203.91 83.66 86.23 o -12 7 1 16.06 112.23 83.32 o -11 7 1 257.79 197.08 65.07 o -10 7 1 196.92 213.41 74.65 o -9 7 1 124.57 138.70 58.16 o -8 7 1 965.74 843.08 83.60 o -7 7 1 8754.97 8608.80 227.28 o -6 7 1 1446.07 1520.27 90.01 o -5 7 1 759.59 774.63 94.17 o -4 7 1 6488.14 6470.53 140.66 o -3 7 1 11338.03 12400.74 187.84 o -2 7 1 16.91 7.72 17.63 o -1 7 1 5260.49 5335.53 93.13 o 0 7 1 10276.88 11751.34 162.99 o 1 7 1 4285.55 4075.00 78.71 o 2 7 1 705.07 653.89 41.48 o 4 7 1 2549.81 2459.68 93.42 o 5 7 1 12489.38 12046.95 260.55 o 6 7 1 54.29 25.36 35.74 o 7 7 1 4057.15 3571.88 148.05 o 8 7 1 2680.31 2460.90 181.66 o 9 7 1 14.37 142.72 111.90 o 10 7 1 936.35 1054.78 338.60 o 11 7 1 1082.46 1385.56 156.53 o 12 7 1 105.83 0.00 105.05 o 13 7 1 510.63 677.31 130.29 o -12 8 1 233.87 203.92 92.06 o -11 8 1 3.91 33.16 74.62 o -10 8 1 1984.97 1803.93 164.73 o -9 8 1 644.00 666.16 84.60 o -8 8 1 1340.72 1219.99 98.11 o -7 8 1 4880.96 4795.79 161.91 o -6 8 1 396.19 489.88 56.64 o -5 8 1 10227.85 10399.39 234.40 o -4 8 1 1185.81 1000.86 72.70 o -3 8 1 2436.11 2543.21 92.45 o -2 8 1 27.67 46.27 20.66 o -1 8 1 15973.25 16944.13 224.53 o 0 8 1 12676.26 13423.20 186.39 o 1 8 1 62.09 95.87 23.32 o 2 8 1 1009.01 1091.53 44.56 o 3 8 1 29.66 67.30 25.36 o 4 8 1 11915.08 11845.41 212.12 o 5 8 1 2388.58 2318.22 109.92 o 6 8 1 990.97 1086.82 80.08 o 7 8 1 1.13 0.00 67.28 o 8 8 1 58.73 0.00 71.99 o 9 8 1 2316.91 2324.97 178.65 o 10 8 1 42.97 0.00 85.97 o 11 8 1 34.17 0.00 70.64 o 12 8 1 140.68 271.92 104.09 o -12 9 1 85.61 75.60 93.67 o -11 9 1 827.47 950.37 146.42 o -10 9 1 1025.96 1161.67 147.36 o -9 9 1 3766.95 4108.85 228.72 o -8 9 1 241.95 231.13 62.19 o -7 9 1 41.64 86.04 63.60 o -6 9 1 77.97 92.00 52.64 o -5 9 1 4755.70 5035.22 138.53 o -4 9 1 4973.43 5232.76 120.00 o -3 9 1 76.53 72.97 38.29 o -2 9 1 15718.87 15791.11 217.16 o -1 9 1 742.02 839.61 45.29 o 0 9 1 7082.09 7543.70 126.94 o 1 9 1 0.70 0.00 24.36 o 2 9 1 2408.58 2809.97 71.52 o 3 9 1 6286.87 6155.73 124.37 o 4 9 1 288.34 258.19 38.08 o 5 9 1 127.12 107.28 46.82 o 6 9 1 26.80 0.00 65.41 o 7 9 1 2573.83 2691.68 180.51 o 8 9 1 940.08 1035.93 310.81 o 9 9 1 128.93 0.00 83.15 o 10 9 1 382.58 241.47 107.76 o 11 9 1 1.86 11.17 91.31 o 12 9 1 621.86 717.98 137.48 o -11 10 1 15.99 0.92 91.25 o -10 10 1 7.12 69.53 89.79 o -9 10 1 1905.86 1590.57 166.61 o -8 10 1 20.50 0.00 67.60 o -7 10 1 209.30 190.04 58.45 o -6 10 1 28.84 0.00 36.96 o -5 10 1 341.91 231.31 50.56 o -4 10 1 3678.18 3982.34 123.75 o -3 10 1 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