#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/91/2219132.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2219132_Fobs loop_ _publ_author_name 'Huang, Miao-Ling' 'Xie, Qing-Fan' 'Xian, Jing-Chun' 'Chen, Yan-Min' 'Zhou, Zi-Qiao' _publ_section_title ; A dinuclear copper complex: bis(\m-4-aminobenzoato)bis[aqua(1,10-phenanthroline)copper(II)] dichloride bis(4-aminobenzoic acid) dihydrate ; _journal_coeditor_code PV2085 _journal_issue 8 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1086 _journal_volume 64 _journal_year 2008 _space_group_IT_number 15 _symmetry_space_group_name_Hall '-C 2yc' _symmetry_space_group_name_H-M 'C 1 2/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 110.307 _cell_angle_gamma 90.000 _cell_length_a 25.7481 _cell_length_b 10.0988 _cell_length_c 20.9156 _exptl_crystal_F_000 2416.00 _reflns_d_resolution_high 0.8255 _[local]_cod_data_source_file pv2085Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' B in C2/c' _shelx_refln_list_code 4 _shelx_F_calc_maximum 977.76 _shelx_F_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 33490.52 39790.50 449.94 o 6 0 0 5273.98 5012.58 98.13 o 8 0 0 5573.71 5152.85 111.27 o 10 0 0 404.93 318.59 38.03 o 12 0 0 8369.99 8514.99 254.25 o 14 0 0 353.48 321.53 87.31 o 16 0 0 2074.13 2097.72 99.94 o 18 0 0 2774.14 2756.55 122.37 o 20 0 0 8894.53 9665.59 311.70 o 22 0 0 21.38 47.03 53.40 o 24 0 0 5687.85 5462.10 197.28 o 26 0 0 1944.82 1982.26 137.51 o 28 0 0 714.15 742.42 106.99 o 3 1 0 95894.34 94527.42 714.39 o 5 1 0 11902.69 12403.88 123.90 o 7 1 0 497.82 730.18 29.01 o 9 1 0 3184.28 3701.98 68.86 o 11 1 0 615.03 454.22 30.98 o 13 1 0 256.85 224.80 28.59 o 15 1 0 922.85 1035.77 51.57 o 17 1 0 5.43 5.22 23.96 o 19 1 0 3229.76 3206.71 114.40 o 21 1 0 1653.74 1665.83 78.04 o 23 1 0 10936.54 10349.42 191.49 o 25 1 0 1282.20 1238.99 79.90 o 27 1 0 634.44 608.79 67.81 o 29 1 0 1456.41 1711.57 100.93 o 0 2 0 371.08 150.52 12.68 o 2 2 0 71.32 97.63 10.10 o 4 2 0 112750.41 108212.84 660.76 o 6 2 0 2224.35 1802.37 31.85 o 8 2 0 318.16 138.07 12.80 o 10 2 0 12794.27 12944.45 113.89 o 12 2 0 246.12 248.70 26.49 o 14 2 0 179.48 185.85 21.93 o 16 2 0 3300.67 3239.41 96.97 o 18 2 0 1141.05 1013.23 58.68 o 20 2 0 8005.29 7991.20 155.34 o 22 2 0 3290.07 3078.84 103.62 o 24 2 0 3994.69 4041.48 138.37 o 26 2 0 2737.85 2549.10 107.74 o 28 2 0 2007.54 2139.56 107.34 o 1 3 0 98.03 237.21 13.91 o 3 3 0 350.91 476.41 18.80 o 5 3 0 23113.51 22008.59 166.22 o 7 3 0 18300.33 17471.10 143.09 o 9 3 0 34972.36 36084.97 259.78 o 11 3 0 3135.31 3326.90 56.45 o 13 3 0 5628.48 5683.94 119.10 o 15 3 0 1206.22 1156.22 55.84 o 17 3 0 1657.94 1872.92 93.64 o 19 3 0 13.36 -4.57 28.73 o 21 3 0 420.79 362.49 49.49 o 23 3 0 401.80 252.39 53.95 o 25 3 0 1453.54 1522.23 88.40 o 27 3 0 4002.07 3565.34 128.18 o 0 4 0 156.85 199.10 22.34 o 2 4 0 5977.19 5880.01 81.30 o 4 4 0 9960.90 9652.06 96.29 o 6 4 0 29192.37 32464.54 239.68 o 8 4 0 98233.66 102538.59 655.26 o 10 4 0 65.48 61.00 17.38 o 12 4 0 1712.15 1744.12 46.45 o 14 4 0 2025.11 2086.37 71.12 o 16 4 0 6356.89 6050.43 124.51 o 18 4 0 1761.51 1960.07 81.23 o 20 4 0 651.21 585.32 56.57 o 22 4 0 157.07 245.40 48.32 o 24 4 0 68.86 53.83 43.39 o 26 4 0 2297.37 2205.71 106.25 o 1 5 0 14115.12 15955.34 141.93 o 3 5 0 3980.61 4222.45 63.35 o 5 5 0 1330.39 1549.92 40.74 o 7 5 0 76.48 45.51 16.52 o 9 5 0 11676.58 11320.09 121.82 o 11 5 0 1359.76 1174.17 42.25 o 13 5 0 1032.35 920.31 38.66 o 15 5 0 478.04 359.48 35.83 o 17 5 0 754.82 931.88 70.37 o 19 5 0 479.13 529.49 53.95 o 21 5 0 1653.98 1666.08 84.39 o 23 5 0 563.97 615.01 64.84 o 25 5 0 5.29 -44.87 41.70 o 0 6 0 896.49 824.64 47.02 o 2 6 0 108.34 110.44 19.55 o 4 6 0 31.30 29.01 17.21 o 6 6 0 219.12 244.58 24.43 o 8 6 0 91.21 100.88 22.59 o 10 6 0 1233.17 1268.79 44.91 o 12 6 0 1198.82 1256.16 51.14 o 14 6 0 585.98 463.37 39.90 o 16 6 0 0.12 -34.36 29.82 o 18 6 0 0.48 14.45 36.16 o 20 6 0 1.00 19.55 39.20 o 22 6 0 325.81 293.98 53.14 o 24 6 0 8.39 27.74 45.51 o 1 7 0 132.79 158.11 24.26 o 3 7 0 3317.30 3411.29 104.56 o 5 7 0 23.14 22.44 20.43 o 7 7 0 4.90 -26.23 18.43 o 9 7 0 639.07 536.31 36.16 o 11 7 0 1.18 14.68 23.00 o 13 7 0 1086.14 1131.65 48.79 o 15 7 0 382.67 371.72 41.18 o 17 7 0 100.20 26.83 45.96 o 19 7 0 32.30 82.17 54.62 o 21 7 0 277.74 199.87 61.07 o 23 7 0 19.01 -7.71 76.88 o 0 8 0 1172.01 1330.57 89.17 o 2 8 0 2205.00 2250.20 78.47 o 4 8 0 363.96 298.07 45.06 o 6 8 0 36.62 13.11 27.91 o 8 8 0 2675.92 2444.81 72.49 o 10 8 0 572.68 572.35 52.09 o 12 8 0 3478.52 2963.59 82.64 o 14 8 0 192.02 252.47 46.29 o 16 8 0 4303.63 4012.38 237.45 o 18 8 0 83.84 66.16 52.99 o 20 8 0 340.25 297.27 70.81 o 22 8 0 136.99 125.51 60.33 o 1 9 0 75.13 152.26 47.22 o 3 9 0 1186.41 1181.31 64.63 o 5 9 0 235.80 299.03 42.88 o 7 9 0 5172.02 4836.78 118.67 o 9 9 0 2499.14 2468.32 123.15 o 11 9 0 16.24 17.49 36.70 o 13 9 0 690.08 671.75 59.02 o 15 9 0 15.75 -48.68 44.15 o 17 9 0 338.07 309.93 82.12 o 19 9 0 35.62 -15.42 68.38 o 0 10 0 1157.95 1165.92 102.04 o 2 10 0 1681.09 1660.60 111.88 o 4 10 0 936.44 1087.93 79.29 o 6 10 0 823.29 727.14 70.77 o 8 10 0 1424.15 1569.32 95.23 o 10 10 0 68.59 124.20 48.90 o 12 10 0 408.97 306.07 59.65 o 14 10 0 4.96 -12.65 59.55 o 16 10 0 69.43 80.53 107.67 o 1 11 0 641.03 660.42 90.39 o 3 11 0 1975.62 2040.87 135.72 o 5 11 0 2101.90 2154.10 134.98 o 7 11 0 1005.81 1274.53 114.04 o 9 11 0 270.28 341.77 78.36 o 11 11 0 566.92 619.59 93.71 o 0 12 0 4227.06 4441.62 269.63 o 2 12 0 1139.63 1236.66 121.85 o 4 12 0 1274.04 1432.22 147.93 o -29 1 1 180.67 141.78 62.56 o -27 1 1 25.32 38.62 42.92 o -25 1 1 564.02 532.49 59.64 o -23 1 1 11.78 -21.24 34.82 o -21 1 1 2144.19 2298.58 196.40 o -19 1 1 1672.86 1747.05 73.50 o -17 1 1 171.70 326.33 38.59 o -15 1 1 1637.98 1906.14 79.66 o -13 1 1 1684.98 1905.16 59.31 o -11 1 1 22.96 20.86 10.80 o -9 1 1 29.99 118.66 13.95 o -7 1 1 23.66 73.56 18.11 o -5 1 1 14984.02 14713.11 107.76 o -3 1 1 826.14 690.91 14.75 o -1 1 1 711.02 870.41 33.48 o 1 1 1 17238.46 15463.13 191.30 o 3 1 1 10657.14 12539.01 117.35 o 5 1 1 25240.07 27969.62 242.53 o 7 1 1 20399.80 21191.73 203.37 o 9 1 1 785.31 441.02 28.02 o 11 1 1 3836.84 3511.54 75.01 o 13 1 1 8377.68 9673.15 196.15 o 15 1 1 377.53 406.19 39.17 o 17 1 1 688.32 692.38 81.23 o 19 1 1 355.53 298.35 42.01 o 21 1 1 7.32 -23.85 31.69 o 23 1 1 281.87 196.14 44.89 o 25 1 1 585.75 483.75 61.39 o 27 1 1 58.14 -4.65 42.87 o -28 2 1 536.47 477.22 66.47 o -26 2 1 56.11 74.24 54.58 o -24 2 1 4382.11 4355.22 259.88 o -22 2 1 130.47 165.59 40.23 o -20 2 1 266.13 273.74 64.25 o -18 2 1 12564.06 12415.66 236.77 o -16 2 1 75.40 92.85 28.69 o -14 2 1 9469.64 10492.71 159.41 o -12 2 1 3187.47 3301.89 70.07 o -10 2 1 6294.32 6296.20 74.84 o -8 2 1 16021.57 17131.94 135.75 o -6 2 1 62.98 106.47 11.13 o -4 2 1 28198.57 29036.82 196.86 o -2 2 1 267.73 298.01 14.15 o 0 2 1 44607.34 47785.05 331.15 o 2 2 1 118743.74 117338.57 711.47 o 4 2 1 6167.89 6560.45 63.70 o 6 2 1 12831.44 12678.42 105.53 o 8 2 1 25393.16 27888.52 202.04 o 10 2 1 62.86 38.09 11.73 o 12 2 1 19792.00 20741.03 270.23 o 14 2 1 723.88 599.57 59.55 o 16 2 1 11670.26 11316.48 172.82 o 18 2 1 1.84 32.03 30.03 o 20 2 1 136.22 97.87 36.26 o 22 2 1 448.14 465.71 55.24 o 24 2 1 1544.43 1539.03 85.70 o 26 2 1 640.07 520.46 64.36 o 28 2 1 95.87 50.12 48.00 o -27 3 1 481.34 398.12 84.37 o -25 3 1 4044.88 3995.88 147.70 o -23 3 1 971.48 993.73 70.22 o -21 3 1 109.31 61.93 33.14 o -19 3 1 1595.06 1674.00 74.87 o -17 3 1 8918.55 8953.22 153.17 o -15 3 1 10.37 6.52 18.48 o -13 3 1 657.61 517.02 32.56 o -11 3 1 638.33 617.15 42.01 o -9 3 1 1206.94 1477.06 42.76 o -7 3 1 2759.29 2798.20 45.25 o -5 3 1 56392.43 58767.84 382.18 o -3 3 1 15736.68 17209.16 133.38 o -1 3 1 3892.35 4003.49 48.43 o 1 3 1 16518.08 15375.75 134.16 o 3 3 1 27043.80 26041.93 187.67 o 5 3 1 51245.91 50210.43 333.96 o 7 3 1 10252.04 9066.88 91.45 o 9 3 1 18004.38 19252.54 159.71 o 11 3 1 2563.44 2165.09 44.89 o 13 3 1 120.70 89.24 16.53 o 15 3 1 571.72 512.21 43.12 o 17 3 1 1213.20 1177.81 61.82 o 19 3 1 663.05 615.84 54.66 o 21 3 1 140.53 159.09 42.25 o 23 3 1 295.58 324.14 68.43 o 25 3 1 3001.00 2940.47 118.84 o 27 3 1 140.16 134.07 51.27 o -28 4 1 2137.01 2047.68 123.92 o -26 4 1 2719.31 2507.91 137.65 o -24 4 1 1821.79 2040.14 96.45 o -22 4 1 1653.55 1536.77 129.94 o -20 4 1 76.88 20.26 45.84 o -18 4 1 471.61 415.47 45.86 o -16 4 1 213.00 227.05 37.60 o -14 4 1 4312.52 4274.15 70.91 o -12 4 1 408.76 509.23 28.32 o -10 4 1 5706.69 6322.94 84.23 o -8 4 1 9212.07 9435.31 100.80 o -6 4 1 7822.37 8543.56 91.31 o -4 4 1 510.27 739.14 25.85 o -2 4 1 10274.41 10499.60 99.14 o 0 4 1 4658.23 3817.44 53.04 o 2 4 1 11194.07 9880.19 96.42 o 4 4 1 45679.43 44679.27 308.97 o 6 4 1 100326.72 100934.74 642.14 o 8 4 1 20666.38 21280.53 177.76 o 10 4 1 1222.30 1105.39 36.29 o 12 4 1 4382.68 4010.41 67.14 o 14 4 1 4.06 26.58 21.89 o 16 4 1 5.45 -11.51 27.85 o 18 4 1 667.46 599.45 82.41 o 20 4 1 829.47 766.69 61.64 o 22 4 1 2806.83 2706.90 126.48 o 24 4 1 1998.80 2024.81 127.98 o 26 4 1 1976.89 1959.29 102.68 o -27 5 1 1329.88 1683.55 101.01 o -25 5 1 1963.06 2203.95 103.22 o -23 5 1 2179.26 2208.52 97.90 o -21 5 1 7925.69 7915.95 164.92 o -19 5 1 1759.66 1831.59 81.90 o -17 5 1 685.58 730.14 55.63 o -15 5 1 3690.56 3661.54 108.02 o -13 5 1 1148.82 1329.50 45.24 o -11 5 1 784.19 754.45 35.07 o -9 5 1 4560.92 4432.05 85.65 o -7 5 1 938.98 852.51 32.29 o -5 5 1 30.45 92.00 16.63 o -3 5 1 10311.87 9796.93 102.66 o -1 5 1 7178.49 6927.17 82.11 o 1 5 1 4205.43 3606.72 59.38 o 3 5 1 7485.88 6190.76 78.62 o 5 5 1 4697.91 4039.14 63.75 o 7 5 1 16647.87 14560.37 141.11 o 9 5 1 21258.48 21258.27 187.84 o 11 5 1 1659.14 1731.08 48.44 o 13 5 1 2234.98 2475.38 58.89 o 15 5 1 663.54 676.44 61.93 o 17 5 1 2739.67 2881.99 127.46 o 19 5 1 559.65 572.47 59.11 o 21 5 1 1453.18 1426.05 126.94 o 23 5 1 1152.27 1072.18 79.16 o 25 5 1 1148.03 1171.83 86.21 o -24 6 1 1400.82 1506.42 90.52 o -22 6 1 5147.88 5111.04 141.23 o -20 6 1 6191.69 6381.94 148.77 o -18 6 1 2833.12 2895.44 99.00 o -16 6 1 9784.46 10309.19 151.85 o -14 6 1 3305.10 3494.70 75.46 o -12 6 1 201.36 197.48 26.37 o -10 6 1 1.92 -6.72 18.65 o -8 6 1 260.85 174.62 23.00 o -6 6 1 6904.14 6720.76 90.58 o -4 6 1 2580.74 2319.87 68.79 o -2 6 1 19986.10 19021.22 169.82 o 0 6 1 4889.51 4878.80 73.19 o 2 6 1 29317.46 29580.97 235.50 o 4 6 1 36105.32 36142.73 277.49 o 6 6 1 196.92 122.00 21.40 o 8 6 1 17111.59 17367.70 168.43 o 10 6 1 6919.40 6602.73 96.68 o 12 6 1 3730.29 3909.72 76.28 o 14 6 1 4435.98 4401.60 94.74 o 16 6 1 265.58 223.42 43.74 o 18 6 1 568.82 470.09 54.87 o 20 6 1 175.10 177.26 45.72 o 22 6 1 1870.25 1763.51 108.92 o 24 6 1 104.62 97.86 55.37 o -23 7 1 1851.59 2021.05 216.31 o -21 7 1 5967.01 6028.58 179.16 o -19 7 1 1651.08 1872.92 106.55 o -17 7 1 2315.41 2408.16 108.75 o -15 7 1 370.96 446.62 48.83 o -13 7 1 2265.96 2170.17 70.30 o -11 7 1 6596.05 6527.31 113.22 o -9 7 1 1395.73 1455.24 56.52 o -7 7 1 5376.85 5167.63 94.80 o -5 7 1 121.46 89.13 25.61 o -3 7 1 15299.63 15916.83 159.02 o -1 7 1 18385.54 18368.32 174.33 o 1 7 1 16272.44 16002.11 182.82 o 3 7 1 21649.87 21472.78 196.08 o 5 7 1 2965.46 2943.82 64.06 o 7 7 1 5445.39 5405.56 100.21 o 9 7 1 11229.08 10781.86 132.84 o 11 7 1 26.91 21.00 23.43 o 13 7 1 830.06 877.89 45.77 o 15 7 1 222.87 216.70 37.04 o 17 7 1 851.53 845.06 66.25 o 19 7 1 84.41 7.12 55.89 o 21 7 1 703.28 828.06 72.72 o 23 7 1 1069.11 936.87 94.07 o -22 8 1 2219.11 2128.97 124.31 o -20 8 1 2130.57 2165.61 276.49 o -18 8 1 947.31 1157.25 90.37 o -16 8 1 677.32 765.80 93.51 o -14 8 1 548.81 582.20 47.62 o -12 8 1 475.90 395.04 41.26 o -10 8 1 726.48 632.66 50.65 o -8 8 1 418.46 470.22 40.94 o -6 8 1 2516.97 2479.60 71.38 o -4 8 1 6766.60 6971.57 117.04 o -2 8 1 26164.24 27179.96 286.28 o 0 8 1 28167.80 28274.21 284.34 o 2 8 1 13301.64 12876.24 185.09 o 4 8 1 10606.77 10835.87 227.24 o 6 8 1 6569.47 6524.47 132.29 o 8 8 1 1739.63 1914.45 74.20 o 10 8 1 18.41 -22.68 25.23 o 12 8 1 1344.50 1347.70 62.57 o 14 8 1 12.16 5.98 43.10 o 16 8 1 290.96 268.33 61.44 o 18 8 1 411.65 451.75 70.99 o 20 8 1 622.75 554.22 109.29 o -19 9 1 1206.88 1346.33 180.05 o -17 9 1 2045.27 2071.07 204.48 o -15 9 1 621.85 602.93 85.62 o -13 9 1 551.88 609.69 58.45 o -11 9 1 97.17 66.00 36.34 o -9 9 1 462.48 467.04 51.25 o -7 9 1 111.32 60.18 52.76 o -5 9 1 2482.50 2490.42 89.72 o -3 9 1 1809.76 1772.10 75.54 o -1 9 1 331.15 262.19 41.82 o 1 9 1 176.45 264.00 52.83 o 3 9 1 1579.35 1621.47 75.88 o 5 9 1 2505.78 2576.16 88.11 o 7 9 1 1363.05 1411.25 70.59 o 9 9 1 5731.79 5649.08 129.88 o 11 9 1 2451.72 2384.94 110.46 o 13 9 1 326.61 303.24 51.05 o 15 9 1 1093.41 1028.44 106.82 o 17 9 1 4.79 -63.31 59.46 o 19 9 1 13.26 -52.06 71.01 o -16 10 1 372.32 183.67 119.43 o -14 10 1 467.36 551.83 91.73 o -12 10 1 86.98 227.05 58.00 o -10 10 1 481.04 503.56 65.53 o -8 10 1 33.29 25.39 41.61 o -6 10 1 1026.64 1041.87 91.38 o -4 10 1 2500.58 2471.87 109.40 o -2 10 1 24.21 11.57 40.40 o 0 10 1 626.90 674.42 88.63 o 2 10 1 535.81 775.54 70.91 o 4 10 1 789.39 932.34 75.25 o 6 10 1 4186.20 3975.34 227.62 o 8 10 1 832.31 925.98 78.57 o 10 10 1 1380.73 1291.76 98.89 o 12 10 1 1980.66 1762.20 131.23 o 14 10 1 1.07 -40.86 59.26 o -13 11 1 12.68 -29.32 58.82 o -11 11 1 0.12 -27.21 69.22 o -9 11 1 10.16 45.87 58.87 o -7 11 1 299.70 213.09 70.34 o -5 11 1 1254.75 1360.44 115.14 o -3 11 1 234.04 43.37 53.92 o -1 11 1 307.69 224.61 67.78 o 1 11 1 588.14 620.59 88.87 o 3 11 1 89.32 28.79 51.90 o 5 11 1 468.50 554.14 89.23 o 7 11 1 476.74 598.48 162.86 o 9 11 1 89.79 104.98 68.31 o 11 11 1 976.33 1206.62 110.97 o -6 12 1 0.56 -20.05 60.44 o -4 12 1 223.15 311.78 115.36 o -2 12 1 156.76 94.30 83.24 o 0 12 1 649.08 677.80 195.43 o 2 12 1 284.43 489.66 120.79 o 4 12 1 410.94 501.15 107.67 o -30 0 2 384.03 350.62 83.11 o -28 0 2 11.74 61.51 61.08 o -26 0 2 22.83 -13.33 52.82 o -24 0 2 13092.24 12549.38 302.82 o -22 0 2 36255.99 37260.96 580.92 o -20 0 2 9985.32 9454.32 653.26 o -18 0 2 29066.80 28120.07 441.86 o -16 0 2 41.95 82.50 37.49 o -14 0 2 836.24 790.36 59.88 o -12 0 2 9693.52 9781.90 187.40 o -10 0 2 5662.27 5858.31 85.16 o -8 0 2 13486.72 15576.81 233.08 o -6 0 2 2983.35 3262.50 53.25 o -4 0 2 12885.46 10963.06 145.50 o 2 0 2 34257.27 34350.91 387.85 o 4 0 2 69.09 268.81 23.19 o 6 0 2 96686.20 94587.49 1373.47 o 8 0 2 400.10 178.59 52.03 o 10 0 2 4235.49 5599.21 289.99 o 12 0 2 3373.26 2618.58 99.36 o 14 0 2 777.12 670.32 61.32 o 16 0 2 2695.26 2602.64 208.10 o 18 0 2 5737.87 5092.70 167.49 o 20 0 2 7798.71 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