#------------------------------------------------------------------------------ #$Date: 2009-05-03 21:56:13 +0300 (Sun, 03 May 2009) $ #$Revision: 691 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2219218.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2219218_Fobs loop_ _publ_author_name 'Fun, Hoong-Kun' 'Kia, Reza' _publ_section_title ; N,N'-Bis[2-chloro-5-(trifluoromethyl)benzylidene]ethane-1,2-diamine ; _journal_coeditor_code AT2608 _journal_issue 9 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o1722 _journal_page_last o1723 _journal_volume 64 _journal_year 2008 _space_group_IT_number 15 _symmetry_space_group_name_Hall '-C 2yc' _symmetry_space_group_name_H-M 'C 1 2/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 127.851 _cell_angle_gamma 90.000 _cell_length_a 35.7299 _cell_length_b 4.6663 _cell_length_c 27.1134 _exptl_crystal_F_000 1776.00 _reflns_d_resolution_high 0.6152 _[local]_cod_data_source_file at2608Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' clfm in C2/c (100K)' _shelx_refln_list_code 4 _shelx_F_calc_maximum 517.30 _shelx_F_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 2974.07 0.24 1.43 o 4 0 0 29.70 -6.99 6.99 o 6 0 0 2538.51 2788.94 35.46 o 8 0 0 74056.22 76609.71 690.28 o 10 0 0 6775.69 6849.08 67.76 o 12 0 0 3357.83 4030.12 47.30 o 14 0 0 40952.90 44769.20 407.85 o 16 0 0 245.18 365.61 13.18 o 18 0 0 16240.24 16075.67 154.88 o 20 0 0 13639.12 14329.26 136.11 o 22 0 0 191.29 252.80 11.82 o 24 0 0 767.59 750.24 26.65 o 26 0 0 5907.13 5925.92 95.97 o 28 0 0 6449.97 6698.68 115.59 o 30 0 0 3104.42 3379.20 113.96 o 32 0 0 322.04 298.73 26.74 o 34 0 0 1835.58 2085.78 62.78 o 36 0 0 1594.53 1515.16 54.45 o 38 0 0 541.95 602.02 38.26 o 40 0 0 1139.25 1193.39 76.23 o 42 0 0 755.05 1045.95 115.53 o 44 0 0 454.90 534.52 72.76 o 1 1 0 2218.40 2066.08 31.45 o 3 1 0 18536.45 18466.92 144.27 o 5 1 0 3639.88 3886.91 34.01 o 7 1 0 1483.64 1354.76 17.20 o 9 1 0 8216.84 7927.90 66.19 o 11 1 0 736.88 1022.89 13.67 o 13 1 0 26029.22 28079.30 178.59 o 15 1 0 349.76 263.32 7.38 o 17 1 0 12299.63 12565.82 84.22 o 19 1 0 2711.48 2647.72 27.33 o 21 1 0 5210.78 5058.45 49.20 o 23 1 0 1830.62 1604.69 23.94 o 25 1 0 6.57 2.55 6.17 o 27 1 0 993.85 904.10 20.63 o 29 1 0 2153.22 2067.07 40.36 o 31 1 0 625.91 540.57 23.25 o 33 1 0 25.67 31.97 13.27 o 35 1 0 8.25 16.45 13.74 o 37 1 0 1678.11 1789.52 47.46 o 39 1 0 267.09 273.32 23.86 o 41 1 0 2205.32 2446.17 68.13 o 43 1 0 400.71 437.52 52.69 o 45 1 0 1.77 -3.97 32.12 o 0 2 0 352.74 254.76 21.18 o 2 2 0 460.06 501.03 11.08 o 4 2 0 2734.53 2835.18 27.57 o 6 2 0 1838.62 1936.02 19.62 o 8 2 0 457.15 332.23 7.80 o 10 2 0 56.06 61.06 4.65 o 12 2 0 1083.57 1085.70 16.90 o 14 2 0 508.48 515.04 13.51 o 16 2 0 7159.17 7286.87 71.14 o 18 2 0 23.51 34.27 7.47 o 20 2 0 903.99 1104.93 28.08 o 22 2 0 321.74 282.52 17.76 o 24 2 0 10029.72 9857.11 134.39 o 26 2 0 755.50 866.13 30.76 o 28 2 0 39.24 49.60 13.27 o 30 2 0 2328.58 2256.05 50.33 o 32 2 0 159.11 112.17 19.35 o 34 2 0 1020.16 938.52 46.47 o 36 2 0 73.13 90.59 24.33 o 38 2 0 2012.67 2006.27 111.66 o 40 2 0 212.04 190.64 34.52 o 42 2 0 447.14 429.24 63.10 o 44 2 0 96.15 71.58 57.69 o 1 3 0 1005.47 802.97 26.39 o 3 3 0 2137.33 2414.04 30.60 o 5 3 0 862.88 760.47 13.22 o 7 3 0 9236.95 9264.85 74.24 o 9 3 0 2095.90 1981.95 22.30 o 11 3 0 1415.79 1432.10 20.78 o 13 3 0 15833.79 16346.64 145.66 o 15 3 0 17.71 19.78 8.75 o 17 3 0 1912.99 1918.25 44.60 o 19 3 0 401.27 409.99 25.13 o 21 3 0 9168.11 9324.92 149.03 o 23 3 0 941.65 970.42 40.51 o 25 3 0 4.99 10.83 18.12 o 27 3 0 2080.45 2142.07 62.87 o 29 3 0 877.57 905.76 43.15 o 31 3 0 12.01 5.88 14.97 o 33 3 0 50.46 81.52 19.48 o 35 3 0 462.26 488.65 42.22 o 37 3 0 1057.25 1154.84 60.62 o 39 3 0 774.72 801.13 67.90 o 41 3 0 52.45 134.83 54.88 o 0 4 0 1274.76 1652.75 87.56 o 2 4 0 696.26 753.60 22.90 o 4 4 0 9.28 10.84 8.59 o 6 4 0 545.22 504.13 14.87 o 8 4 0 8.61 14.87 5.62 o 10 4 0 6815.96 7138.10 79.11 o 12 4 0 4001.39 4172.15 78.30 o 14 4 0 1972.23 2034.96 68.81 o 16 4 0 56.47 40.09 12.70 o 18 4 0 1267.36 1187.43 39.26 o 20 4 0 775.71 796.62 35.80 o 22 4 0 73.88 60.49 17.05 o 24 4 0 34.26 29.87 15.29 o 26 4 0 757.65 753.83 38.76 o 28 4 0 464.56 495.79 37.38 o 30 4 0 12.95 25.23 18.02 o 32 4 0 0.63 17.72 19.60 o 34 4 0 106.05 54.35 26.22 o 36 4 0 229.66 194.67 42.12 o 38 4 0 334.58 292.60 51.31 o 1 5 0 1363.02 1468.20 79.77 o 3 5 0 904.44 913.65 43.64 o 5 5 0 232.66 217.62 29.11 o 7 5 0 48.18 48.52 14.32 o 9 5 0 3662.00 3941.66 77.47 o 11 5 0 1845.09 1936.07 43.81 o 13 5 0 4939.54 5250.40 90.51 o 15 5 0 380.12 379.53 36.62 o 17 5 0 277.74 271.40 19.07 o 19 5 0 86.89 77.13 14.90 o 21 5 0 1668.40 1785.37 49.22 o 23 5 0 109.31 106.67 18.86 o 25 5 0 4.50 15.55 15.95 o 27 5 0 51.19 79.11 17.96 o 29 5 0 880.36 884.45 63.89 o 31 5 0 114.02 126.49 32.18 o 33 5 0 105.72 65.16 27.58 o 4 6 0 238.03 322.86 32.40 o 6 6 0 0.90 8.66 14.66 o 8 6 0 1733.83 2037.05 64.12 o 10 6 0 292.16 273.16 22.16 o 12 6 0 695.63 730.60 34.79 o 14 6 0 242.96 229.73 62.52 o 16 6 0 135.82 183.34 21.05 o 18 6 0 726.35 782.51 37.23 o 20 6 0 470.01 416.36 32.95 o 22 6 0 213.90 169.07 22.42 o 24 6 0 281.62 288.10 40.03 o 26 6 0 3.63 8.44 23.86 o 28 6 0 237.36 346.88 77.64 o 5 7 0 342.78 397.71 44.69 o 7 7 0 50.71 55.86 31.84 o 9 7 0 71.94 93.74 25.76 o 11 7 0 267.04 291.34 31.91 o 13 7 0 69.28 74.10 25.36 o 15 7 0 25.34 32.04 25.73 o 17 7 0 48.12 34.38 31.28 o -45 1 1 140.78 98.25 32.06 o -43 1 1 1032.19 1053.68 45.63 o -41 1 1 142.44 194.38 21.95 o -39 1 1 3576.93 3758.77 90.60 o -37 1 1 1550.63 1583.92 44.01 o -35 1 1 37.87 75.47 15.10 o -33 1 1 433.51 447.93 27.27 o -31 1 1 7267.20 7358.73 92.77 o -29 1 1 4043.64 3977.13 59.17 o -27 1 1 171.34 229.02 11.97 o -25 1 1 11211.95 10662.71 93.40 o -23 1 1 11211.04 11386.53 93.50 o -21 1 1 617.81 516.52 12.58 o -19 1 1 70.52 80.17 5.86 o -17 1 1 26081.01 26027.44 168.26 o -15 1 1 3530.84 3850.93 34.88 o -13 1 1 13781.90 15623.03 111.44 o -11 1 1 3395.04 3528.31 34.06 o -9 1 1 17350.90 18047.79 150.34 o -7 1 1 54.19 60.32 4.15 o -5 1 1 1289.37 1582.18 17.79 o -3 1 1 239.37 219.49 5.49 o -1 1 1 15940.44 16806.82 189.32 o 1 1 1 1396.72 1362.58 15.59 o 3 1 1 125460.30 127754.27 1046.60 o 5 1 1 325.52 273.44 6.21 o 7 1 1 50383.63 52731.01 400.87 o 9 1 1 890.57 1005.68 13.71 o 11 1 1 6702.96 7412.67 53.78 o 13 1 1 11210.00 11954.15 78.04 o 15 1 1 776.21 824.80 11.26 o 17 1 1 4793.33 4936.19 37.63 o 19 1 1 3853.18 4051.81 38.02 o 21 1 1 4587.67 4887.06 51.87 o 23 1 1 16.27 1.40 5.73 o 25 1 1 674.48 647.04 16.78 o 27 1 1 1815.82 1864.02 35.10 o 29 1 1 73.70 69.38 12.31 o 31 1 1 133.99 104.21 15.93 o 33 1 1 2120.61 2086.21 49.71 o 35 1 1 284.65 261.39 21.90 o 37 1 1 13.95 10.70 14.87 o 39 1 1 183.65 163.92 21.28 o 41 1 1 619.59 581.44 36.46 o 43 1 1 1517.49 1646.94 114.73 o -44 2 1 174.54 165.22 48.95 o -42 2 1 103.31 79.70 31.53 o -40 2 1 99.52 68.12 28.05 o -38 2 1 928.07 976.79 54.17 o -36 2 1 132.58 89.05 21.51 o -34 2 1 312.25 317.63 30.58 o -32 2 1 101.19 57.17 19.66 o -30 2 1 816.82 840.65 30.80 o -28 2 1 366.33 356.51 31.68 o -26 2 1 965.03 847.61 28.81 o -24 2 1 70.25 97.16 13.76 o -22 2 1 11.07 2.86 8.07 o -20 2 1 27.62 28.22 7.85 o -18 2 1 14642.80 14669.30 142.07 o -16 2 1 3195.53 3385.26 41.00 o -14 2 1 5407.76 5684.07 57.15 o -12 2 1 640.36 740.34 14.22 o -10 2 1 11228.54 11129.41 87.23 o -8 2 1 2725.98 2526.54 24.89 o -6 2 1 3592.19 3813.71 33.56 o -4 2 1 22478.38 22354.20 182.57 o -2 2 1 85.27 55.19 5.54 o 0 2 1 16762.41 17115.40 179.99 o 2 2 1 13798.29 14038.68 129.84 o 4 2 1 4466.10 4094.19 37.74 o 6 2 1 34.23 78.03 4.48 o 8 2 1 6064.10 6727.44 52.87 o 10 2 1 472.63 456.20 9.27 o 12 2 1 6280.23 6540.80 59.12 o 14 2 1 274.93 258.37 10.09 o 16 2 1 2143.06 2044.97 28.48 o 18 2 1 115.27 80.97 9.51 o 20 2 1 3280.69 3311.32 53.65 o 22 2 1 1436.12 1574.42 36.39 o 24 2 1 3907.77 3923.27 58.43 o 26 2 1 1014.36 1065.21 48.04 o 28 2 1 832.24 874.86 30.94 o 30 2 1 93.87 87.39 17.50 o 32 2 1 2550.38 2646.79 69.07 o 34 2 1 70.65 53.95 20.24 o 36 2 1 1099.58 1186.67 57.49 o 38 2 1 40.12 39.05 26.07 o 40 2 1 796.50 701.35 50.91 o 42 2 1 876.90 894.89 87.35 o -41 3 1 431.17 423.05 65.85 o -39 3 1 0.07 21.05 26.29 o -37 3 1 87.77 41.35 26.95 o -35 3 1 1022.58 1166.44 47.31 o -33 3 1 1393.50 1585.51 48.60 o -31 3 1 10.45 7.83 14.94 o -29 3 1 259.22 237.01 24.45 o -27 3 1 46.13 44.45 16.86 o -25 3 1 48.83 35.99 15.40 o -23 3 1 303.90 298.41 24.95 o -21 3 1 350.10 355.17 27.03 o -19 3 1 707.34 721.48 29.12 o -17 3 1 670.65 534.10 21.34 o -15 3 1 5454.00 5413.66 70.88 o -13 3 1 974.34 1139.43 23.04 o -11 3 1 82.52 96.20 6.50 o -9 3 1 1165.06 1150.28 15.58 o -7 3 1 4839.22 4959.16 41.08 o -5 3 1 2259.41 2675.83 29.60 o -3 3 1 2343.66 2291.57 45.68 o -1 3 1 11958.88 13328.28 158.17 o 1 3 1 17.27 25.52 6.90 o 3 3 1 1688.35 1718.90 29.30 o 5 3 1 115.74 120.18 5.41 o 7 3 1 3262.95 3506.38 35.03 o 9 3 1 426.61 408.47 10.63 o 11 3 1 150.29 105.27 7.05 o 13 3 1 908.06 901.27 20.51 o 15 3 1 95.84 79.08 13.16 o 17 3 1 824.08 885.81 35.93 o 19 3 1 1400.63 1294.80 41.92 o 21 3 1 844.11 798.03 35.88 o 23 3 1 1.20 16.70 14.20 o 25 3 1 349.04 315.21 28.25 o 27 3 1 167.78 165.79 18.97 o 29 3 1 590.82 495.52 28.84 o 31 3 1 69.34 49.44 17.37 o 33 3 1 81.12 51.19 21.66 o 35 3 1 558.45 645.46 71.19 o 37 3 1 99.73 164.38 36.94 o 39 3 1 12.64 30.29 42.45 o 41 3 1 91.83 88.36 53.62 o -38 4 1 2474.61 2582.93 168.14 o -36 4 1 123.57 105.45 30.67 o -34 4 1 252.08 226.19 40.89 o -32 4 1 38.14 44.42 20.26 o -30 4 1 1119.71 1127.51 48.37 o -28 4 1 52.89 50.43 18.49 o -26 4 1 370.10 335.96 29.89 o -24 4 1 109.01 58.39 19.05 o -22 4 1 1097.87 1077.42 70.64 o -20 4 1 3.20 4.77 12.24 o -18 4 1 4948.08 5099.84 92.12 o -16 4 1 2464.05 2586.00 51.75 o -14 4 1 1605.52 1613.12 46.86 o -12 4 1 4058.46 4192.17 105.98 o -10 4 1 11231.38 11734.83 144.72 o -8 4 1 755.02 821.22 18.03 o -6 4 1 336.80 341.61 11.70 o -4 4 1 200.99 160.58 16.70 o -2 4 1 1592.18 1423.86 53.28 o 0 4 1 789.90 856.61 39.62 o 2 4 1 2.88 9.23 7.68 o 4 4 1 218.86 206.72 14.26 o 6 4 1 983.22 951.19 19.10 o 8 4 1 170.77 150.63 8.97 o 10 4 1 13.72 1.11 6.84 o 12 4 1 4414.62 4561.72 77.95 o 14 4 1 301.53 243.71 19.44 o 16 4 1 757.40 650.43 29.75 o 18 4 1 262.56 242.16 21.00 o 20 4 1 5453.78 5486.77 96.56 o 22 4 1 242.21 210.69 22.51 o 24 4 1 33.56 27.17 17.30 o 26 4 1 95.65 70.68 18.34 o 28 4 1 536.02 505.28 35.42 o 30 4 1 266.54 287.26 37.20 o 32 4 1 149.89 76.44 31.18 o 34 4 1 4.21 9.78 24.13 o 36 4 1 43.87 66.36 39.54 o 38 4 1 255.33 353.02 91.61 o -35 5 1 109.24 85.78 28.65 o -33 5 1 0.63 15.38 20.62 o -31 5 1 171.92 131.06 23.69 o -29 5 1 1.23 -0.86 15.02 o -27 5 1 427.97 421.78 31.68 o -25 5 1 39.12 57.65 17.58 o -23 5 1 691.93 869.22 37.60 o -21 5 1 631.68 684.74 59.25 o -19 5 1 649.58 703.27 35.14 o -17 5 1 0.10 -4.77 9.36 o -15 5 1 90.73 84.28 14.34 o -13 5 1 341.01 327.43 20.91 o -11 5 1 24.69 9.01 11.09 o -9 5 1 8.66 22.74 14.05 o -7 5 1 2408.01 2499.55 64.21 o -5 5 1 822.39 822.26 44.93 o -3 5 1 824.08 821.29 84.21 o -1 5 1 684.71 723.56 60.13 o 1 5 1 158.91 213.66 55.30 o 3 5 1 2566.31 2541.27 83.03 o 5 5 1 305.23 314.55 40.24 o 7 5 1 869.81 813.28 56.54 o 9 5 1 30.79 20.50 10.50 o 11 5 1 1928.47 2089.50 47.31 o 13 5 1 257.00 235.29 20.68 o 15 5 1 344.63 365.41 28.55 o 17 5 1 115.68 92.47 14.73 o 19 5 1 50.10 33.37 14.00 o 21 5 1 25.59 18.62 13.72 o 23 5 1 0.16 3.06 13.82 o 25 5 1 388.33 327.90 26.69 o 27 5 1 230.72 184.57 23.17 o 29 5 1 71.11 65.14 20.66 o 31 5 1 196.67 150.21 29.91 o 33 5 1 6.27 2.01 25.05 o -28 6 1 786.43 814.91 39.44 o -26 6 1 115.90 104.36 25.46 o -24 6 1 69.93 38.55 19.23 o -22 6 1 275.01 244.40 30.61 o -20 6 1 124.63 130.29 21.24 o -18 6 1 33.17 50.37 17.20 o -16 6 1 770.39 768.15 32.24 o -14 6 1 2831.21 3195.94 88.85 o -12 6 1 33.66 33.86 17.60 o -10 6 1 68.87 67.80 20.00 o -8 6 1 241.20 248.10 24.87 o -6 6 1 267.41 264.62 22.91 o -4 6 1 49.74 44.97 18.99 o 4 6 1 331.06 326.27 23.57 o 6 6 1 1969.28 2252.98 65.15 o 8 6 1 1135.89 1135.52 74.24 o 10 6 1 3.98 5.94 14.42 o 12 6 1 1715.15 1853.05 55.37 o 14 6 1 23.51 40.02 14.30 o 16 6 1 3.68 1.46 14.74 o 18 6 1 515.96 478.94 28.47 o 20 6 1 25.28 22.42 16.11 o 22 6 1 98.73 118.17 23.15 o 24 6 1 117.57 87.55 27.77 o 26 6 1 167.51 188.90 25.18 o -17 7 1 824.00 1007.37 48.13 o -15 7 1 28.77 25.12 21.37 o -13 7 1 4.82 10.97 21.78 o -11 7 1 123.60 108.92 41.06 o -9 7 1 154.87 91.95 25.59 o -7 7 1 33.54 10.05 28.49 o -5 7 1 30.81 24.02 26.53 o 3 7 1 217.08 219.24 34.07 o 5 7 1 100.59 144.11 34.07 o 7 7 1 7.56 35.47 31.28 o 9 7 1 10.09 22.35 24.12 o 11 7 1 0.18 15.79 21.69 o 13 7 1 0.04 -23.16 23.64 o 15 7 1 131.11 174.18 34.98 o -46 0 2 3.36 28.44 40.63 o -44 0 2 218.59 254.08 38.65 o -42 0 2 290.37 318.43 40.63 o -40 0 2 2949.91 3076.52 81.57 o -38 0 2 222.30 222.39 26.18 o -36 0 2 119.86 55.00 18.80 o -34 0 2 2311.05 2415.41 73.61 o -32 0 2 5185.68 4788.19 135.97 o -30 0 2 2713.36 2494.19 60.19 o -28 0 2 15564.85 15244.79 219.35 o -26 0 2 5416.47 5218.27 105.35 o -24 0 2 4528.26 4929.04 61.01 o -22 0 2 3912.98 3822.41 47.32 o -20 0 2 173.98 104.33 8.33 o -18 0 2 229.11 46.53 6.16 o -16 0 2 162.11 165.75 8.61 o -14 0 2 1961.44 2450.69 30.15 o -12 0 2 766.49 653.42 12.51 o -10 0 2 48297.46 50459.16 439.45 o -8 0 2 604.49 533.20 12.85 o -6 0 2 30866.90 32453.49 616.23 o -4 0 2 702.44 495.52 35.89 o 0 0 2 290.09 134.07 19.69 o 2 0 2 10926.67 11353.82 122.01 o 4 0 2 0.08 -2.01 2.01 o 6 0 2 15156.14 16006.85 146.31 o 8 0 2 5453.46 5562.38 54.25 o 10 0 2 38298.80 38537.99 320.52 o 12 0 2 3881.35 4240.26 46.24 o 14 0 2 4744.44 5569.96 59.47 o 16 0 2 949.44 895.23 18.28 o 18 0 2 31649.15 33293.80 276.64 o 20 0 2 58.12 69.29 8.84 o 22 0 2 473.60 558.61 20.54 o 24 0 2 1996.40 1848.77 39.98 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41 53.47 26.45 39.65 o -28 2 41 3.89 -1.82 33.08 o -26 2 41 55.22 96.39 36.92 o -24 2 41 89.10 134.73 48.58 o -22 2 41 494.29 543.78 99.43 o -46 0 42 133.97 67.01 42.71 o -44 0 42 43.28 49.49 48.04 o -42 0 42 3.34 21.94 47.76 o -40 0 42 1747.72 2118.70 132.66 o -38 0 42 428.78 544.62 79.04 o -36 0 42 262.82 274.82 68.71 o -34 0 42 230.76 246.62 42.61 o -32 0 42 887.50 1018.08 65.73 o -30 0 42 17.00 25.43 32.90 o -28 0 42 1026.04 1100.14 67.81 o -26 0 42 713.31 711.18 57.50 o -45 1 42 8.12 31.53 36.14 o -43 1 42 18.36 41.74 35.70 o -41 1 42 247.22 247.27 47.25 o -39 1 42 110.26 147.31 40.69 o -37 1 42 26.03 59.56 37.25 o -35 1 42 47.52 46.86 30.60 o -33 1 42 1.64 49.65 30.29 o -31 1 42 155.00 168.32 45.38 o -29 1 42 22.60 21.47 37.51 o -27 1 42 7.97 97.05 52.09 o -25 1 42 140.03 118.66 42.73 o -23 1 42 934.05 1042.93 141.88 o -38 2 42 61.37 26.14 41.00 o -36 2 42 1.69 18.99 40.20 o -34 2 42 37.42 35.03 41.51 o -32 2 42 7.56 -9.94 38.65 o -30 2 42 1104.00 1267.57 73.10 o -28 2 42 33.11 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