#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/93/2219327.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2219327_Fobs loop_ _publ_author_name 'Nakaema, Kosuke' 'Okamoto, Akiko' 'Maruyama, Satoshi' 'Noguchi, Keiichi' 'Yonezawa, Noriyuki' _publ_section_title ; 2,2'-Dimethoxybiphenyl ; _journal_coeditor_code FL2209 _journal_issue 9 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o1731 _journal_volume 64 _journal_year 2008 _space_group_IT_number 92 _symmetry_space_group_name_Hall 'P 4abw 2nw' _symmetry_space_group_name_H-M 'P 41 21 2' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 7.3931 _cell_length_b 7.3931 _cell_length_c 20.1623 _exptl_crystal_F_000 456.00 _reflns_d_resolution_high 0.8305 _[local]_cod_data_source_file fl2209Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' Yonezawa_080204_01_' _shelx_refln_list_code 4 _shelx_F_calc_maximum 104.92 _shelx_F_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-y+1/2, x+1/2, z+1/4' '-x, -y, z+1/2' 'y+1/2, -x+1/2, z+3/4' '-x+1/2, y+1/2, -z+1/4' 'y, x, -z' 'x+1/2, -y+1/2, -z+3/4' '-y, -x, -z+1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 1 0 758.92 743.53 3.10 o 0 2 0 52.73 44.18 0.28 o 1 2 0 1992.55 1932.05 6.76 o 2 2 0 145.34 138.16 0.54 o 1 3 0 282.22 274.04 0.82 o 2 3 0 44.11 51.13 0.22 o 3 3 0 10.10 7.53 0.17 o 0 4 0 749.16 829.49 4.18 o 1 4 0 636.26 680.08 2.35 o 2 4 0 858.11 929.46 3.30 o 3 4 0 18.57 17.55 0.17 o 4 4 0 53.25 53.45 0.61 o 1 5 0 395.80 389.66 1.79 o 2 5 0 0.99 0.76 0.14 o 3 5 0 21.19 21.92 0.31 o 4 5 0 1.20 0.86 0.17 o 5 5 0 292.25 292.75 2.45 o 0 6 0 383.20 390.90 2.82 o 1 6 0 9.02 7.53 0.26 o 2 6 0 34.79 30.27 0.48 o 3 6 0 208.28 217.60 1.52 o 4 6 0 176.92 169.92 1.33 o 5 6 0 224.62 226.36 1.56 o 6 6 0 249.49 260.23 4.02 o 1 7 0 13.70 15.75 0.29 o 2 7 0 50.75 50.68 0.55 o 3 7 0 30.88 29.37 0.48 o 4 7 0 34.03 35.10 0.49 o 5 7 0 4.20 6.91 0.29 o 0 8 0 241.73 261.10 1.98 o 1 8 0 61.61 60.79 0.50 o 2 8 0 24.74 19.76 0.31 o 3 8 0 1.11 0.75 0.20 o 0 1 1 138.36 142.06 0.40 o 1 1 1 54.06 63.80 0.26 o 0 2 1 3751.94 3715.07 15.51 o 1 2 1 187.63 183.44 0.37 o 2 2 1 1035.03 998.92 3.12 o 0 3 1 35.05 31.08 0.12 o 1 3 1 1117.22 1143.75 2.69 o 2 3 1 378.01 393.70 0.82 o 3 3 1 3.02 3.34 0.10 o 0 4 1 2.05 1.68 0.10 o 1 4 1 397.25 426.78 0.98 o 2 4 1 155.26 169.89 0.39 o 3 4 1 64.36 64.68 0.26 o 4 4 1 21.95 24.33 0.30 o 0 5 1 19.60 16.13 0.22 o 1 5 1 64.26 65.83 0.28 o 2 5 1 210.57 196.51 0.74 o 3 5 1 309.31 297.97 1.19 o 4 5 1 48.92 48.64 0.34 o 5 5 1 621.92 618.95 3.66 o 0 6 1 49.97 51.70 0.43 o 1 6 1 46.50 44.63 0.29 o 2 6 1 322.22 325.04 1.35 o 3 6 1 60.15 59.04 0.45 o 4 6 1 47.16 45.43 0.41 o 5 6 1 35.67 36.12 0.34 o 6 6 1 41.64 43.52 0.53 o 0 7 1 246.30 249.26 1.35 o 1 7 1 136.45 126.33 0.56 o 2 7 1 112.50 108.55 0.57 o 3 7 1 19.16 17.44 0.29 o 4 7 1 29.86 29.34 0.35 o 5 7 1 22.85 23.71 0.26 o 0 8 1 149.22 147.24 0.86 o 1 8 1 46.23 48.22 0.31 o 2 8 1 12.54 10.74 0.19 o 3 8 1 2.45 1.60 0.15 o 0 1 2 6150.67 6171.06 43.82 o 1 1 2 1150.08 1094.71 3.41 o 0 2 2 2228.02 2093.00 7.74 o 1 2 2 725.79 703.61 1.48 o 2 2 2 66.08 64.89 0.22 o 0 3 2 16.59 17.47 0.12 o 1 3 2 199.14 182.73 0.39 o 2 3 2 302.90 323.44 0.67 o 3 3 2 0.37 0.42 0.07 o 0 4 2 480.27 468.38 1.67 o 1 4 2 799.38 857.99 2.11 o 2 4 2 476.02 471.03 1.05 o 3 4 2 2.25 1.65 0.08 o 4 4 2 63.19 54.53 0.45 o 0 5 2 147.63 128.47 0.63 o 1 5 2 40.47 37.94 0.20 o 2 5 2 597.48 606.69 2.29 o 3 5 2 90.26 90.30 0.50 o 4 5 2 48.35 45.58 0.33 o 5 5 2 87.74 83.63 0.65 o 0 6 2 2.48 2.30 0.19 o 1 6 2 150.68 142.89 0.61 o 2 6 2 18.04 18.81 0.26 o 3 6 2 293.43 297.14 1.31 o 4 6 2 20.05 21.97 0.29 o 5 6 2 54.31 56.89 0.40 o 6 6 2 77.29 72.18 0.70 o 0 7 2 8.97 10.01 0.23 o 1 7 2 127.34 129.32 0.60 o 2 7 2 13.68 11.94 0.20 o 3 7 2 2.53 2.08 0.17 o 4 7 2 6.81 6.54 0.20 o 5 7 2 66.59 72.61 0.46 o 0 8 2 104.24 107.13 0.70 o 1 8 2 7.05 7.59 0.15 o 2 8 2 6.13 6.07 0.16 o 3 8 2 5.38 5.33 0.18 o 0 1 3 1338.97 1318.22 4.34 o 1 1 3 5799.62 5704.74 29.76 o 0 2 3 113.47 109.87 0.35 o 1 2 3 97.38 100.74 0.23 o 2 2 3 89.37 87.64 0.27 o 0 3 3 149.08 155.44 0.47 o 1 3 3 236.22 257.92 0.53 o 2 3 3 630.55 683.94 1.48 o 3 3 3 245.84 228.98 0.74 o 0 4 3 300.34 312.55 1.04 o 1 4 3 99.64 108.07 0.28 o 2 4 3 61.93 66.20 0.19 o 3 4 3 24.49 27.02 0.16 o 4 4 3 3.29 2.14 0.17 o 0 5 3 38.32 37.78 0.29 o 1 5 3 110.35 113.25 0.41 o 2 5 3 186.12 188.50 0.76 o 3 5 3 176.52 172.83 0.76 o 4 5 3 261.14 253.22 1.07 o 5 5 3 29.45 34.07 0.39 o 0 6 3 2.86 2.63 0.18 o 1 6 3 323.04 332.24 1.29 o 2 6 3 225.42 227.71 1.01 o 3 6 3 15.88 14.50 0.23 o 4 6 3 63.40 61.17 0.43 o 5 6 3 152.24 151.40 0.74 o 6 6 3 12.31 12.91 0.36 o 0 7 3 582.46 583.78 3.46 o 1 7 3 0.36 1.01 0.13 o 2 7 3 21.40 20.74 0.25 o 3 7 3 53.61 52.28 0.37 o 4 7 3 7.24 7.48 0.20 o 5 7 3 11.13 13.19 0.23 o 0 8 3 5.85 6.74 0.34 o 1 8 3 14.18 16.97 0.20 o 2 8 3 0.67 0.95 0.12 o 3 8 3 43.15 41.03 0.33 o 0 0 4 488.47 524.15 3.11 o 0 1 4 715.39 709.37 2.13 o 1 1 4 1327.24 1261.58 4.09 o 0 2 4 4554.68 4542.85 20.72 o 1 2 4 382.55 357.82 0.69 o 2 2 4 898.26 962.18 2.92 o 0 3 4 3.42 6.35 0.09 o 1 3 4 478.00 501.81 1.06 o 2 3 4 78.44 76.19 0.18 o 3 3 4 1.09 1.62 0.09 o 0 4 4 0.03 0.38 0.06 o 1 4 4 114.36 99.43 0.26 o 2 4 4 261.71 273.31 0.65 o 3 4 4 20.17 18.31 0.16 o 4 4 4 158.67 155.87 0.88 o 0 5 4 65.72 56.44 0.36 o 1 5 4 55.10 53.96 0.26 o 2 5 4 116.46 110.88 0.53 o 3 5 4 0.31 0.53 0.11 o 4 5 4 295.08 296.26 1.21 o 5 5 4 20.36 16.06 0.35 o 0 6 4 328.68 307.07 1.75 o 1 6 4 324.25 330.22 1.32 o 2 6 4 12.18 11.72 0.22 o 3 6 4 69.88 68.79 0.44 o 4 6 4 9.88 9.92 0.20 o 5 6 4 88.65 86.15 0.54 o 6 6 4 57.96 55.63 0.67 o 0 7 4 99.88 90.12 0.71 o 1 7 4 75.57 72.60 0.46 o 2 7 4 12.69 11.73 0.22 o 3 7 4 35.78 36.28 0.30 o 4 7 4 34.75 37.66 0.33 o 5 7 4 5.93 5.31 0.19 o 0 8 4 11.47 10.68 0.29 o 1 8 4 75.48 73.17 0.46 o 2 8 4 3.94 4.53 0.17 o 3 8 4 113.96 120.91 0.68 o 0 1 5 11009.01 11089.09 69.75 o 1 1 5 3512.34 3410.50 14.15 o 0 2 5 113.95 117.55 0.36 o 1 2 5 1084.16 1112.86 2.49 o 2 2 5 733.80 769.18 2.29 o 0 3 5 1292.79 1313.33 4.61 o 1 3 5 42.34 48.99 0.14 o 2 3 5 76.70 88.78 0.21 o 3 3 5 294.01 285.07 0.95 o 0 4 5 318.28 341.51 1.08 o 1 4 5 8.52 8.86 0.09 o 2 4 5 90.51 81.04 0.25 o 3 4 5 94.44 98.83 0.40 o 4 4 5 9.46 10.77 0.23 o 0 5 5 3.26 3.26 0.17 o 1 5 5 9.99 10.47 0.14 o 2 5 5 183.11 187.14 0.78 o 3 5 5 98.35 95.64 0.47 o 4 5 5 181.27 187.19 0.83 o 5 5 5 137.72 120.79 0.89 o 0 6 5 22.18 25.77 0.37 o 1 6 5 501.85 504.87 2.05 o 2 6 5 23.16 24.28 0.28 o 3 6 5 63.13 62.53 0.42 o 4 6 5 134.85 131.54 0.69 o 5 6 5 60.20 57.80 0.38 o 6 6 5 75.50 80.26 0.79 o 0 7 5 55.53 66.74 0.59 o 1 7 5 42.88 38.81 0.34 o 2 7 5 48.72 48.61 0.39 o 3 7 5 2.48 2.16 0.16 o 4 7 5 5.64 4.26 0.16 o 5 7 5 0.98 0.99 0.18 o 0 8 5 3.54 2.34 0.19 o 1 8 5 20.63 22.52 0.26 o 2 8 5 9.36 11.14 0.25 o 3 8 5 9.96 10.53 0.23 o 0 1 6 96.26 83.91 0.26 o 1 1 6 2297.02 2281.96 8.93 o 0 2 6 48.06 48.51 0.19 o 1 2 6 665.29 694.04 1.52 o 2 2 6 206.04 189.78 0.54 o 0 3 6 866.91 932.25 3.10 o 1 3 6 650.57 669.28 1.49 o 2 3 6 202.10 213.46 0.46 o 3 3 6 278.17 266.35 0.91 o 0 4 6 57.42 40.66 0.22 o 1 4 6 482.00 471.98 1.16 o 2 4 6 12.47 12.63 0.12 o 3 4 6 112.08 111.67 0.49 o 4 4 6 32.41 35.54 0.43 o 0 5 6 188.19 182.96 1.06 o 1 5 6 126.99 121.28 0.50 o 2 5 6 58.88 55.10 0.32 o 3 5 6 67.83 68.60 0.42 o 4 5 6 762.62 742.82 3.18 o 5 5 6 21.83 20.18 0.35 o 0 6 6 76.85 78.33 0.65 o 1 6 6 439.38 424.53 1.93 o 2 6 6 85.88 81.26 0.52 o 3 6 6 0.62 1.13 0.14 o 4 6 6 23.66 24.36 0.27 o 5 6 6 15.55 16.65 0.28 o 6 6 6 9.04 11.02 0.32 o 0 7 6 259.16 248.74 1.54 o 1 7 6 36.03 34.67 0.32 o 2 7 6 26.78 28.08 0.32 o 3 7 6 123.32 122.79 0.68 o 4 7 6 4.59 2.98 0.14 o 5 7 6 25.54 26.67 0.42 o 0 8 6 58.87 58.95 0.50 o 1 8 6 35.27 38.55 0.32 o 2 8 6 20.19 20.30 0.27 o 3 8 6 5.74 8.38 0.20 o 0 1 7 117.97 118.12 0.34 o 1 1 7 548.24 595.76 1.83 o 0 2 7 1556.98 1581.98 5.66 o 1 2 7 671.19 691.48 1.51 o 2 2 7 511.63 560.80 1.68 o 0 3 7 208.01 212.54 0.65 o 1 3 7 1546.93 1625.81 4.47 o 2 3 7 112.65 105.08 0.27 o 3 3 7 118.49 136.16 0.55 o 0 4 7 235.50 219.33 0.80 o 1 4 7 297.84 287.51 0.72 o 2 4 7 213.12 211.72 0.69 o 3 4 7 178.39 170.40 0.68 o 4 4 7 0.64 0.51 0.17 o 0 5 7 34.58 32.42 0.36 o 1 5 7 155.07 146.40 0.65 o 2 5 7 353.31 359.35 1.45 o 3 5 7 444.53 449.11 1.86 o 4 5 7 0.95 2.13 0.16 o 5 5 7 13.83 16.08 0.34 o 0 6 7 413.82 424.32 2.52 o 1 6 7 55.41 52.46 0.39 o 2 6 7 44.09 45.85 0.38 o 3 6 7 16.36 15.43 0.24 o 4 6 7 0.10 0.25 0.12 o 5 6 7 8.40 7.58 0.17 o 6 6 7 129.93 144.37 1.43 o 0 7 7 35.98 38.18 0.45 o 1 7 7 8.57 6.71 0.21 o 2 7 7 39.11 35.49 0.34 o 3 7 7 7.64 7.16 0.21 o 4 7 7 15.36 18.83 0.24 o 0 8 7 1.73 1.20 0.17 o 1 8 7 14.15 16.89 0.22 o 2 8 7 17.68 19.98 0.27 o 0 0 8 26.15 28.39 0.60 o 0 1 8 428.00 418.11 1.37 o 1 1 8 1880.88 1888.43 7.25 o 0 2 8 60.50 63.91 0.25 o 1 2 8 51.53 49.77 0.14 o 2 2 8 95.84 105.30 0.34 o 0 3 8 120.16 135.85 0.51 o 1 3 8 112.50 116.55 0.29 o 2 3 8 94.83 85.07 0.25 o 3 3 8 19.35 18.60 0.20 o 0 4 8 331.04 347.72 1.45 o 1 4 8 163.10 170.57 0.57 o 2 4 8 9.22 8.93 0.13 o 3 4 8 57.09 55.52 0.31 o 4 4 8 665.13 643.01 3.78 o 0 5 8 40.50 38.21 0.44 o 1 5 8 459.10 452.66 1.88 o 2 5 8 95.52 88.86 0.49 o 3 5 8 122.18 113.28 0.58 o 4 5 8 24.76 21.66 0.26 o 5 5 8 351.47 351.32 2.21 o 0 6 8 1071.76 1076.14 7.00 o 1 6 8 99.49 98.91 0.62 o 2 6 8 5.67 6.43 0.20 o 3 6 8 7.02 6.43 0.21 o 4 6 8 6.05 6.45 0.18 o 5 6 8 12.06 14.92 0.18 o 0 7 8 106.97 111.86 0.80 o 1 7 8 3.96 3.12 0.18 o 2 7 8 9.83 9.43 0.22 o 3 7 8 54.94 54.08 0.40 o 4 7 8 35.21 38.48 0.36 o 0 8 8 21.91 22.29 0.33 o 1 8 8 20.35 23.16 0.26 o 2 8 8 28.72 34.49 0.32 o 0 1 9 0.07 0.59 0.07 o 1 1 9 188.73 212.98 0.75 o 0 2 9 97.88 109.42 0.54 o 1 2 9 1494.28 1584.31 4.27 o 2 2 9 322.37 327.55 1.12 o 0 3 9 156.97 157.27 0.58 o 1 3 9 511.83 487.93 1.23 o 2 3 9 16.71 14.85 0.11 o 3 3 9 14.37 14.53 0.21 o 0 4 9 4.40 3.00 0.13 o 1 4 9 154.89 158.28 0.60 o 2 4 9 31.72 31.69 0.25 o 3 4 9 2.27 2.36 0.13 o 4 4 9 1.37 1.15 0.18 o 0 5 9 8.02 7.73 0.26 o 1 5 9 332.97 332.86 1.44 o 2 5 9 56.66 55.97 0.36 o 3 5 9 114.13 115.60 0.59 o 4 5 9 117.84 119.76 0.59 o 5 5 9 151.94 159.05 1.08 o 0 6 9 2.94 4.43 0.23 o 1 6 9 147.66 139.83 0.75 o 2 6 9 137.02 137.27 0.75 o 3 6 9 4.66 4.45 0.19 o 4 6 9 37.72 38.47 0.31 o 5 6 9 21.83 19.42 0.20 o 0 7 9 154.15 151.37 1.01 o 1 7 9 104.22 102.91 0.59 o 2 7 9 40.72 40.31 0.35 o 3 7 9 0.80 1.05 0.17 o 4 7 9 22.97 24.38 0.31 o 0 8 9 13.61 13.32 0.40 o 1 8 9 1.22 0.96 0.13 o 2 8 9 3.58 2.75 0.20 o 0 1 10 36.70 36.65 0.19 o 1 1 10 0.37 0.73 0.06 o 0 2 10 196.97 198.15 0.68 o 1 2 10 156.75 138.31 0.38 o 2 2 10 96.45 101.74 0.38 o 0 3 10 367.79 378.65 1.42 o 1 3 10 984.01 984.35 2.90 o 2 3 10 71.71 76.43 0.28 o 3 3 10 1.50 2.54 0.15 o 0 4 10 23.32 25.13 0.27 o 1 4 10 39.00 35.89 0.24 o 2 4 10 82.94 85.58 0.48 o 3 4 10 188.66 175.12 0.79 o 4 4 10 57.16 60.14 0.53 o 0 5 10 40.94 43.54 0.46 o 1 5 10 98.38 98.66 0.52 o 2 5 10 195.49 189.88 0.86 o 3 5 10 0.68 0.61 0.14 o 4 5 10 75.34 73.00 0.44 o 5 5 10 50.75 54.73 0.47 o 0 6 10 72.25 67.14 0.57 o 1 6 10 60.35 58.83 0.43 o 2 6 10 61.33 59.41 0.45 o 3 6 10 54.07 49.60 0.41 o 4 6 10 7.95 8.74 0.18 o 5 6 10 6.91 5.70 0.22 o 0 7 10 5.00 3.72 0.22 o 1 7 10 108.92 114.54 0.62 o 2 7 10 18.12 17.85 0.26 o 3 7 10 18.90 19.06 0.23 o 4 7 10 30.25 33.04 0.32 o 0 8 10 41.81 53.68 0.57 o 1 8 10 22.66 25.99 0.33 o 0 1 11 791.45 837.28 3.15 o 1 1 11 35.93 40.10 0.22 o 0 2 11 1.91 1.59 0.09 o 1 2 11 103.54 105.69 0.30 o 2 2 11 164.75 152.80 0.64 o 0 3 11 257.93 274.13 1.14 o 1 3 11 307.27 308.00 0.97 o 2 3 11 66.30 65.13 0.33 o 3 3 11 81.09 86.28 0.62 o 0 4 11 19.13 20.68 0.29 o 1 4 11 75.92 76.86 0.38 o 2 4 11 362.01 344.44 1.45 o 3 4 11 104.86 102.56 0.55 o 4 4 11 72.55 68.38 0.62 o 0 5 11 61.32 61.99 0.53 o 1 5 11 20.17 17.29 0.25 o 2 5 11 29.01 27.97 0.28 o 3 5 11 136.27 128.17 0.68 o 4 5 11 7.47 7.74 0.19 o 5 5 11 403.46 419.80 2.94 o 0 6 11 0.86 0.76 0.17 o 1 6 11 91.30 89.63 0.52 o 2 6 11 66.16 62.61 0.46 o 3 6 11 16.54 15.24 0.27 o 4 6 11 59.10 58.14 0.37 o 5 6 11 25.08 26.31 0.38 o 0 7 11 2.65 3.58 0.20 o 1 7 11 203.19 204.03 0.97 o 2 7 11 38.07 37.50 0.31 o 3 7 11 9.45 12.12 0.22 o 0 0 12 2147.07 2223.46 22.55 o 0 1 12 73.84 81.39 0.36 o 1 1 12 111.88 116.01 0.51 o 0 2 12 24.93 29.09 0.20 o 1 2 12 42.87 41.01 0.18 o 2 2 12 0.11 0.17 0.13 o 0 3 12 648.24 654.37 3.70 o 1 3 12 27.31 26.74 0.21 o 2 3 12 546.21 556.08 2.27 o 3 3 12 2.07 3.38 0.22 o 0 4 12 28.96 28.81 0.35 o 1 4 12 510.13 506.47 1.99 o 2 4 12 411.69 401.79 1.73 o 3 4 12 38.72 38.43 0.32 o 4 4 12 33.35 37.57 0.51 o 0 5 12 2.96 3.16 0.23 o 1 5 12 112.25 115.97 0.58 o 2 5 12 48.75 43.86 0.33 o 3 5 12 50.24 44.70 0.35 o 4 5 12 10.64 9.23 0.21 o 5 5 12 14.67 13.04 0.30 o 0 6 12 0.13 0.43 0.15 o 1 6 12 21.69 23.35 0.27 o 2 6 12 91.72 87.27 0.49 o 3 6 12 25.23 27.15 0.29 o 4 6 12 12.38 14.62 0.20 o 0 7 12 39.81 43.24 0.46 o 1 7 12 24.22 27.96 0.34 o 2 7 12 57.41 62.96 0.39 o 3 7 12 4.22 1.32 0.15 o 0 1 13 12.78 11.11 0.14 o 1 1 13 25.92 27.14 0.23 o 0 2 13 314.54 307.73 1.37 o 1 2 13 444.48 427.78 1.68 o 2 2 13 21.86 20.72 0.44 o 0 3 13 14.62 18.83 0.28 o 1 3 13 22.50 21.85 0.21 o 2 3 13 39.13 38.98 0.33 o 3 3 13 2.99 2.55 0.20 o 0 4 13 12.91 14.97 0.30 o 1 4 13 803.98 805.50 3.43 o 2 4 13 160.88 154.74 0.74 o 3 4 13 49.14 44.38 0.37 o 4 4 13 1.28 1.12 0.24 o 0 5 13 65.71 64.73 0.53 o 1 5 13 20.13 19.72 0.24 o 2 5 13 266.22 243.37 1.10 o 3 5 13 35.96 35.63 0.32 o 4 5 13 44.66 41.19 0.36 o 5 5 13 0.01 0.15 0.18 o 0 6 13 211.91 208.88 1.37 o 1 6 13 56.09 52.61 0.39 o 2 6 13 9.03 9.77 0.18 o 3 6 13 56.54 56.69 0.38 o 4 6 13 15.68 14.69 0.25 o 0 7 13 231.60 244.37 1.75 o 1 7 13 45.04 52.32 0.38 o 2 7 13 8.06 7.82 0.19 o 0 1 14 646.55 653.18 3.67 o 1 1 14 0.66 1.79 0.15 o 0 2 14 101.63 103.31 0.81 o 1 2 14 31.02 28.91 0.24 o 2 2 14 64.64 62.23 0.60 o 0 3 14 1.41 1.72 0.19 o 1 3 14 339.25 334.43 1.40 o 2 3 14 143.42 136.31 0.70 o 3 3 14 75.92 75.59 0.67 o 0 4 14 58.75 61.82 0.49 o 1 4 14 358.11 349.37 1.52 o 2 4 14 18.13 21.69 0.28 o 3 4 14 16.42 16.59 0.27 o 4 4 14 4.77 6.80 0.33 o 0 5 14 5.39 5.75 0.23 o 1 5 14 34.08 30.81 0.30 o 2 5 14 109.85 116.74 0.62 o 3 5 14 1.12 1.07 0.15 o 4 5 14 37.03 37.53 0.37 o 5 5 14 49.63 53.54 0.61 o 0 6 14 2.96 3.78 0.20 o 1 6 14 17.68 17.86 0.24 o 2 6 14 14.51 14.69 0.22 o 3 6 14 68.61 63.83 0.57 o 4 6 14 43.41 45.38 0.43 o 0 7 14 7.37 6.82 0.31 o 1 7 14 50.11 52.49 0.37 o 0 1 15 266.98 264.81 1.68 o 1 1 15 5.27 3.96 0.21 o 0 2 15 65.07 63.97 0.53 o 1 2 15 76.63 73.91 0.42 o 2 2 15 58.42 58.47 0.55 o 0 3 15 78.48 79.62 0.65 o 1 3 15 226.58 213.65 0.98 o 2 3 15 203.64 209.80 0.99 o 3 3 15 52.04 47.24 0.52 o 0 4 15 4.98 6.22 0.22 o 1 4 15 152.73 144.46 0.73 o 2 4 15 113.77 108.46 0.64 o 3 4 15 0.24 0.51 0.13 o 4 4 15 0.20 0.16 0.18 o 0 5 15 0.88 1.26 0.18 o 1 5 15 68.40 66.74 0.42 o 2 5 15 71.15 64.13 0.46 o 3 5 15 30.70 26.03 0.31 o 4 5 15 4.17 3.37 0.18 o 0 6 15 11.73 11.22 0.25 o 1 6 15 81.49 86.98 0.53 o 2 6 15 121.15 117.29 0.67 o 3 6 15 0.26 0.12 0.12 o 0 7 15 18.34 20.79 0.41 o 0 0 16 1187.07 1234.54 16.44 o 0 1 16 52.57 53.92 0.49 o 1 1 16 60.58 62.14 0.56 o 0 2 16 3.86 5.31 0.23 o 1 2 16 44.52 43.51 0.35 o 2 2 16 127.05 119.85 0.93 o 0 3 16 110.96 108.66 0.88 o 1 3 16 3.16 3.60 0.26 o 2 3 16 232.17 224.50 1.07 o 3 3 16 43.85 40.12 0.46 o 0 4 16 78.46 76.81 0.64 o 1 4 16 62.79 57.12 0.40 o 2 4 16 24.75 22.98 0.27 o 3 4 16 20.07 17.70 0.24 o 4 4 16 47.80 53.99 0.65 o 0 5 16 0.10 0.26 0.14 o 1 5 16 105.34 103.08 0.56 o 2 5 16 27.18 27.20 0.30 o 3 5 16 2.11 0.87 0.14 o 4 5 16 54.55 63.47 0.48 o 0 6 16 0.26 0.27 0.13 o 1 6 16 6.69 5.88 0.18 o 2 6 16 7.82 8.08 0.21 o 0 1 17 223.43 215.64 1.34 o 1 1 17 7.97 7.71 0.28 o 0 2 17 6.70 7.40 0.27 o 1 2 17 17.68 18.28 0.24 o 2 2 17 108.76 109.24 0.85 o 0 3 17 24.46 26.99 0.48 o 1 3 17 2.07 2.43 0.18 o 2 3 17 45.06 45.74 0.41 o 3 3 17 60.44 59.78 0.58 o 0 4 17 384.29 385.43 2.72 o 1 4 17 41.97 37.37 0.34 o 2 4 17 112.56 105.97 0.62 o 3 4 17 8.37 8.78 0.19 o 4 4 17 43.96 43.38 0.51 o 0 5 17 9.04 9.13 0.24 o 1 5 17 8.76 7.85 0.19 o 2 5 17 112.16 105.01 0.61 o 3 5 17 0.55 0.23 0.12 o 0 6 17 10.46 11.76 0.28 o 1 6 17 8.61 9.04 0.18 o 2 6 17 32.33 35.92 0.56 o 0 1 18 2.26 1.78 0.24 o 1 1 18 3.27 3.02 0.26 o 0 2 18 38.76 39.42 0.49 o 1 2 18 66.01 65.13 0.47 o 2 2 18 379.23 374.01 3.18 o 0 3 18 215.23 214.11 1.88 o 1 3 18 214.84 209.89 1.46 o 2 3 18 11.94 13.48 0.24 o 3 3 18 4.38 4.23 0.28 o 0 4 18 126.53 125.56 1.02 o 1 4 18 95.64 91.33 0.57 o 2 4 18 131.58 127.75 0.72 o 3 4 18 22.79 20.55 0.27 o 4 4 18 8.94 8.52 0.32 o 0 5 18 1.29 0.81 0.13 o 1 5 18 68.78 64.19 0.43 o 2 5 18 52.08 53.43 0.40 o 3 5 18 46.02 45.86 0.39 o 0 1 19 21.57 22.60 0.38 o 1 1 19 123.47 121.04 1.22 o 0 2 19 213.10 212.19 1.85 o 1 2 19 20.83 21.76 0.28 o 2 2 19 158.35 164.74 1.42 o 0 3 19 0.01 0.08 0.18 o 1 3 19 13.40 15.14 0.27 o 2 3 19 111.11 107.83 0.87 o 3 3 19 5.85 4.95 0.24 o 0 4 19 57.70 60.05 0.59 o 1 4 19 61.56 66.24 0.48 o 2 4 19 51.53 50.45 0.39 o 3 4 19 23.28 25.22 0.27 o 0 5 19 4.21 4.44 0.45 o 1 5 19 33.29 32.54 0.40 o 2 5 19 30.50 27.26 0.34 o 0 0 20 329.48 337.42 7.17 o 0 1 20 37.54 36.83 0.50 o 1 1 20 11.65 11.54 0.30 o 0 2 20 10.22 9.81 0.28 o 1 2 20 123.71 124.76 0.72 o 2 2 20 93.38 97.18 1.54 o 0 3 20 9.22 8.27 0.29 o 1 3 20 68.55 71.53 0.61 o 2 3 20 119.52 116.33 0.96 o 3 3 20 25.23 23.10 0.36 o 0 4 20 4.41 4.80 0.22 o 1 4 20 5.83 6.14 0.19 o 2 4 20 14.58 13.88 0.23 o 3 4 20 16.76 17.26 0.39 o 0 5 20 0.01 -0.15 0.28 o 0 1 21 82.41 84.26 0.99 o 1 1 21 1.09 1.40 0.17 o 0 2 21 0.49 0.21 0.19 o 1 2 21 93.61 95.22 0.76 o 2 2 21 84.61 81.14 1.10 o 0 3 21 227.67 238.39 2.39 o 1 3 21 59.15 56.67 0.47 o 2 3 21 16.92 14.46 0.30 o 3 3 21 22.52 23.55 0.51 o 0 4 21 48.63 53.46 0.78 o 1 4 21 19.68 20.05 0.25 o 0 1 22 0.03 0.05 0.14 o 1 1 22 19.27 18.36 0.41 o 0 2 22 6.87 6.03 0.27 o 1 2 22 77.64 79.37 0.63 o 2 2 22 27.85 30.34 0.57 o 0 3 22 36.08 34.82 0.55 o 1 3 22 79.62 80.87 0.57 o 2 3 22 75.05 80.63 0.86 o 0 1 23 2.53 3.00 0.20 o 1 1 23 6.83 7.12 0.26 o 0 2 23 45.88 46.81 0.71 o 1 2 23 97.44 100.02 1.22 o 2 2 23 8.14 9.16 0.43 o 0 0 24 0.03 0.06 0.38 o 0 1 24 4.60 5.97 0.32 o