#------------------------------------------------------------------------------ #$Date: 2009-05-03 21:56:13 +0300 (Sun, 03 May 2009) $ #$Revision: 691 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2219342.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2219342_Fobs loop_ _publ_author_name 'Fun, Hoong-Kun' 'Patil, P. S.' 'Rao, Jyothi N.' 'Kalluraya, B.' 'Chantrapromma, Suchada' _publ_section_title ; 4-Chloro-N'-[(Z)-4-nitrobenzylidene]benzohydrazide monohydrate ; _journal_coeditor_code HB2764 _journal_issue 9 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o1707 _journal_volume 64 _journal_year 2008 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 104.122 _cell_angle_gamma 90.000 _cell_length_a 16.3049 _cell_length_b 6.8783 _cell_length_c 12.7209 _exptl_crystal_F_000 664.00 _reflns_d_resolution_high 0.7696 _[local]_cod_data_source_file hb2764Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' patil123m in P2(1)/c (100K)' _shelx_refln_list_code 4 _shelx_F_calc_maximum 283.69 _shelx_F_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 247.81 62.61 11.88 o 2 0 0 1287.26 1531.27 18.63 o 3 0 0 77.01 75.62 4.47 o 4 0 0 442.34 451.47 8.05 o 5 0 0 3494.44 3921.06 50.15 o 6 0 0 280.91 272.11 10.38 o 7 0 0 2415.86 2771.10 38.27 o 8 0 0 4.79 7.29 2.96 o 9 0 0 184.73 239.87 8.52 o 10 0 0 3580.51 3940.12 54.45 o 11 0 0 158.55 222.85 9.31 o 12 0 0 1487.76 1698.21 29.44 o 13 0 0 6615.77 7820.80 95.72 o 14 0 0 3599.52 4456.04 59.89 o 15 0 0 252.71 382.13 16.19 o 16 0 0 250.73 286.47 13.39 o 17 0 0 915.69 1121.54 32.20 o 18 0 0 99.09 115.08 12.84 o 19 0 0 143.43 208.56 16.01 o 20 0 0 187.22 236.62 19.73 o 1 1 0 14.62 12.84 2.34 o 2 1 0 389.40 449.62 11.95 o 3 1 0 807.22 926.80 13.20 o 4 1 0 7.24 11.41 1.84 o 5 1 0 983.73 1091.09 12.23 o 6 1 0 18.07 41.57 2.65 o 7 1 0 1132.92 1316.32 15.52 o 8 1 0 759.42 911.94 11.78 o 9 1 0 250.16 274.76 6.51 o 10 1 0 61.00 73.64 4.33 o 11 1 0 89.68 143.81 6.29 o 12 1 0 1450.83 1708.81 21.89 o 13 1 0 243.11 323.83 9.05 o 14 1 0 1501.09 1832.18 24.12 o 15 1 0 1099.59 1275.93 19.28 o 16 1 0 348.06 394.37 11.68 o 17 1 0 227.52 297.58 12.44 o 18 1 0 43.78 63.06 7.97 o 19 1 0 2.50 -1.34 6.38 o 20 1 0 132.52 183.98 16.64 o 0 2 0 19860.14 24961.46 529.05 o 1 2 0 37.12 55.77 4.36 o 2 2 0 1063.97 1258.93 19.31 o 3 2 0 414.62 427.55 10.89 o 4 2 0 3.29 3.27 2.81 o 5 2 0 2513.85 2973.16 49.92 o 6 2 0 572.04 772.75 14.06 o 7 2 0 187.28 222.91 4.96 o 8 2 0 69.44 129.41 4.38 o 9 2 0 305.00 328.90 7.41 o 10 2 0 45.75 62.72 4.70 o 11 2 0 8.03 6.19 3.38 o 12 2 0 245.44 331.14 10.36 o 13 2 0 717.86 874.78 16.42 o 14 2 0 484.95 566.57 13.93 o 15 2 0 26.56 23.77 5.43 o 16 2 0 59.88 66.83 8.67 o 17 2 0 38.68 51.06 7.48 o 18 2 0 68.33 80.31 9.24 o 19 2 0 17.62 10.18 8.82 o 20 2 0 0.01 13.55 9.50 o 1 3 0 2003.95 2408.13 43.10 o 2 3 0 7.79 0.81 2.36 o 3 3 0 478.12 547.96 12.13 o 4 3 0 461.54 520.20 11.85 o 5 3 0 959.64 1229.40 26.80 o 6 3 0 577.56 686.94 17.97 o 7 3 0 1948.18 2195.03 36.41 o 8 3 0 290.46 380.25 9.37 o 9 3 0 41.40 40.39 5.24 o 10 3 0 200.25 241.23 10.96 o 11 3 0 644.61 654.26 18.80 o 12 3 0 821.36 956.35 24.47 o 13 3 0 621.03 682.82 22.79 o 14 3 0 474.15 539.79 20.81 o 15 3 0 6.84 12.89 6.14 o 16 3 0 0.41 1.30 6.82 o 17 3 0 77.31 74.01 12.06 o 18 3 0 65.81 73.74 15.31 o 19 3 0 10.77 6.09 13.39 o 0 4 0 7900.76 10114.43 181.81 o 1 4 0 1980.59 2469.84 46.38 o 2 4 0 167.09 223.80 8.86 o 3 4 0 255.87 283.90 9.74 o 4 4 0 380.99 486.49 12.79 o 5 4 0 2673.53 3237.42 51.28 o 6 4 0 960.14 1150.39 23.70 o 7 4 0 390.31 410.88 15.28 o 8 4 0 6.10 10.08 6.08 o 9 4 0 7.48 -0.84 5.91 o 10 4 0 1077.83 1243.87 38.30 o 11 4 0 88.07 111.16 12.28 o 12 4 0 672.64 861.23 30.15 o 13 4 0 526.78 569.66 24.78 o 14 4 0 450.98 524.64 25.02 o 15 4 0 8.54 9.41 8.47 o 16 4 0 254.05 270.55 36.56 o 17 4 0 539.21 630.45 30.13 o 18 4 0 17.40 25.91 13.26 o 1 5 0 300.35 389.31 12.36 o 2 5 0 0.51 0.91 4.00 o 3 5 0 77.69 93.07 7.93 o 4 5 0 59.76 81.57 7.62 o 5 5 0 231.01 273.71 12.20 o 6 5 0 641.03 792.59 23.41 o 7 5 0 56.18 52.60 10.54 o 8 5 0 278.38 342.01 24.34 o 9 5 0 39.84 37.33 15.29 o 10 5 0 109.75 120.39 18.32 o 11 5 0 69.85 77.88 15.57 o 12 5 0 186.61 206.50 22.84 o 13 5 0 312.46 427.55 30.95 o 14 5 0 72.05 61.30 15.36 o 15 5 0 0.20 -5.59 10.99 o 16 5 0 32.92 16.37 12.87 o 17 5 0 5.76 17.20 12.96 o 0 6 0 53.38 45.95 11.67 o 1 6 0 1759.00 2062.09 44.46 o 2 6 0 461.92 556.32 17.85 o 3 6 0 212.97 298.58 16.00 o 4 6 0 311.79 414.78 19.92 o 5 6 0 319.58 416.46 19.43 o 6 6 0 50.86 60.56 14.01 o 7 6 0 45.39 54.11 13.37 o 8 6 0 32.75 24.92 11.62 o 9 6 0 176.15 226.11 30.08 o 10 6 0 152.22 212.99 22.96 o 11 6 0 55.59 90.26 19.35 o 12 6 0 898.31 950.48 44.99 o 13 6 0 247.84 309.64 44.60 o 14 6 0 272.06 330.20 30.21 o 15 6 0 419.67 531.18 38.21 o 1 7 0 277.91 350.90 17.44 o 2 7 0 7.21 15.27 6.32 o 3 7 0 78.52 141.17 13.27 o 4 7 0 243.17 309.24 24.90 o 5 7 0 3.80 3.73 10.48 o 6 7 0 398.48 455.24 31.08 o 7 7 0 128.82 158.88 20.72 o 8 7 0 304.90 430.08 75.72 o 9 7 0 595.26 691.20 37.76 o 10 7 0 60.14 60.03 32.76 o 11 7 0 10.00 13.81 12.21 o 12 7 0 73.96 123.10 28.28 o 0 8 0 0.04 3.23 11.57 o 1 8 0 44.83 71.32 13.93 o 2 8 0 44.64 58.75 11.31 o 3 8 0 72.75 88.55 14.75 o 4 8 0 27.96 33.06 12.46 o 5 8 0 14.94 12.86 12.51 o 6 8 0 52.86 78.24 15.60 o 7 8 0 6.47 18.61 20.27 o 8 8 0 47.41 50.16 16.13 o 9 8 0 1.26 -4.24 12.72 o -20 1 1 25.54 36.37 12.25 o -19 1 1 311.32 315.33 14.24 o -18 1 1 59.17 52.60 7.12 o -17 1 1 152.92 160.76 10.89 o -16 1 1 283.66 263.79 9.91 o -15 1 1 261.73 283.30 11.33 o -14 1 1 226.04 219.92 9.17 o -13 1 1 338.71 330.24 8.62 o -12 1 1 1100.11 1049.96 15.37 o -11 1 1 0.20 5.74 2.44 o -10 1 1 78.13 74.12 4.04 o -9 1 1 362.96 348.97 7.13 o -8 1 1 1506.94 1307.34 15.03 o -7 1 1 741.70 620.19 8.54 o -6 1 1 3203.73 3030.63 27.37 o -5 1 1 4.47 7.47 1.76 o -4 1 1 426.26 373.55 5.42 o -3 1 1 813.22 832.82 10.39 o -2 1 1 4083.47 3994.29 61.57 o -1 1 1 1078.36 972.88 15.33 o 0 1 1 5.87 1.13 2.31 o 1 1 1 57.24 69.38 5.16 o 2 1 1 363.10 344.12 6.37 o 3 1 1 654.12 593.80 7.69 o 4 1 1 130.57 131.67 3.48 o 5 1 1 588.93 561.88 7.20 o 6 1 1 1733.68 1576.22 16.11 o 7 1 1 1466.10 1417.95 15.27 o 8 1 1 978.41 889.88 12.38 o 9 1 1 40.06 48.99 3.65 o 10 1 1 341.41 322.24 7.60 o 11 1 1 2220.67 2027.40 24.41 o 12 1 1 84.75 91.19 5.71 o 13 1 1 6.07 6.85 3.50 o 14 1 1 124.93 147.45 9.51 o 15 1 1 183.83 186.23 8.42 o 16 1 1 159.20 161.99 8.54 o 17 1 1 20.96 23.82 6.30 o 18 1 1 43.11 42.61 7.86 o 19 1 1 30.25 49.13 10.20 o 20 1 1 145.95 159.83 14.51 o -20 2 1 88.74 90.54 15.74 o -19 2 1 27.67 28.01 9.56 o -18 2 1 776.30 748.60 20.90 o -17 2 1 0.88 4.17 5.22 o -16 2 1 487.24 472.07 14.68 o -15 2 1 315.80 312.56 12.23 o -14 2 1 3010.29 2934.83 37.85 o -13 2 1 830.29 802.61 15.36 o -12 2 1 172.54 174.48 7.46 o -11 2 1 1454.99 1264.29 19.62 o -10 2 1 4.24 6.04 2.81 o -9 2 1 336.23 358.02 7.56 o -8 2 1 117.43 65.29 3.57 o -7 2 1 47.97 62.88 4.11 o -6 2 1 3570.77 3330.58 42.36 o -5 2 1 3190.22 3036.27 51.92 o -4 2 1 2134.70 1989.03 38.23 o -3 2 1 273.13 285.23 7.84 o -2 2 1 1221.81 1171.17 19.99 o -1 2 1 80479.82 74445.34 1118.98 o 0 2 1 519.95 506.58 17.74 o 1 2 1 634.45 621.22 16.36 o 2 2 1 409.35 386.15 10.94 o 3 2 1 367.18 330.43 10.39 o 4 2 1 1979.44 1660.93 30.87 o 5 2 1 4383.57 3842.53 50.80 o 6 2 1 1322.45 1322.25 19.87 o 7 2 1 2.20 6.60 2.01 o 8 2 1 149.48 144.10 5.54 o 9 2 1 1994.23 1832.06 22.63 o 10 2 1 1168.72 1101.75 17.31 o 11 2 1 581.57 551.70 11.94 o 12 2 1 4095.61 3660.73 44.13 o 13 2 1 5146.03 4832.44 56.32 o 14 2 1 8.45 21.81 4.97 o 15 2 1 618.57 530.27 16.68 o 16 2 1 195.44 182.98 10.74 o 17 2 1 310.71 311.59 15.67 o 18 2 1 16.81 16.13 6.62 o 19 2 1 161.74 150.03 14.68 o -19 3 1 188.25 178.83 25.73 o -18 3 1 23.83 5.95 8.61 o -17 3 1 8.11 6.35 7.74 o -16 3 1 103.92 85.66 11.72 o -15 3 1 169.78 152.16 13.84 o -14 3 1 224.22 211.30 15.02 o -13 3 1 91.83 92.09 10.34 o -12 3 1 367.96 353.77 14.35 o -11 3 1 10.05 5.01 4.89 o -10 3 1 157.05 124.71 8.91 o -9 3 1 639.75 563.08 13.89 o -8 3 1 452.83 377.54 13.52 o -7 3 1 739.78 785.75 18.91 o -6 3 1 1825.25 1633.27 29.13 o -5 3 1 0.11 2.23 2.27 o -4 3 1 47.57 44.87 3.97 o -3 3 1 122.72 202.27 7.97 o -2 3 1 1592.57 1748.42 29.74 o -1 3 1 285.53 253.40 8.22 o 0 3 1 19.72 44.12 5.70 o 1 3 1 13.54 6.33 2.72 o 2 3 1 602.46 538.08 16.82 o 3 3 1 179.76 209.57 9.60 o 4 3 1 165.57 153.80 8.75 o 5 3 1 13.66 29.90 5.32 o 6 3 1 1.56 -0.46 3.95 o 7 3 1 1565.20 1513.63 25.00 o 8 3 1 207.69 208.87 8.50 o 9 3 1 47.93 50.58 5.57 o 10 3 1 35.24 27.29 5.92 o 11 3 1 920.00 825.52 24.91 o 12 3 1 3.29 -5.02 5.10 o 13 3 1 50.34 44.62 8.72 o 14 3 1 8.16 10.58 7.21 o 15 3 1 103.24 101.32 9.00 o 16 3 1 27.13 28.14 10.18 o 17 3 1 50.26 47.69 8.07 o 18 3 1 0.02 10.84 13.52 o 19 3 1 117.76 114.94 21.54 o -18 4 1 25.72 23.45 11.96 o -17 4 1 103.97 83.83 12.64 o -16 4 1 52.14 47.81 11.77 o -15 4 1 29.35 18.28 8.62 o -14 4 1 984.52 850.58 40.06 o -13 4 1 957.59 885.05 31.30 o -12 4 1 41.21 36.41 8.98 o -11 4 1 622.75 571.44 22.64 o -10 4 1 548.35 411.92 21.30 o -9 4 1 5.92 5.14 6.70 o -8 4 1 10.70 4.39 5.69 o -7 4 1 106.42 122.89 8.61 o -6 4 1 409.19 374.68 12.27 o -5 4 1 18.94 37.10 6.71 o -4 4 1 195.51 183.96 8.15 o -3 4 1 0.53 0.30 2.79 o -2 4 1 301.05 283.45 11.91 o -1 4 1 1744.12 1735.67 28.72 o 0 4 1 7445.46 7235.17 103.77 o 1 4 1 1904.72 1710.12 31.27 o 2 4 1 507.55 492.55 13.92 o 3 4 1 89.48 84.20 6.81 o 4 4 1 761.71 723.71 17.77 o 5 4 1 329.05 363.57 12.43 o 6 4 1 8.75 15.22 5.52 o 7 4 1 24.74 18.18 5.61 o 8 4 1 101.86 108.65 12.26 o 9 4 1 1.87 10.67 7.13 o 10 4 1 27.86 30.75 10.51 o 11 4 1 400.91 357.70 43.36 o 12 4 1 183.83 162.29 14.97 o 13 4 1 1430.14 1259.27 39.61 o 14 4 1 755.05 632.43 34.73 o 15 4 1 76.84 74.76 13.40 o 16 4 1 117.71 97.34 13.15 o 17 4 1 338.92 294.04 34.16 o 18 4 1 2.20 21.12 14.32 o -17 5 1 115.26 106.65 20.32 o -16 5 1 30.85 38.19 15.12 o -15 5 1 7.18 18.24 12.12 o -14 5 1 262.20 245.88 33.83 o -13 5 1 92.00 69.14 15.89 o -12 5 1 217.74 206.52 21.83 o -11 5 1 39.60 24.62 10.47 o -10 5 1 112.97 92.76 15.63 o -9 5 1 24.78 33.23 11.48 o -8 5 1 74.70 84.40 12.21 o -7 5 1 1295.85 1239.00 37.27 o -6 5 1 34.93 28.13 8.19 o -5 5 1 323.79 309.71 17.86 o -4 5 1 394.11 403.60 13.91 o -3 5 1 13.54 10.00 4.34 o -2 5 1 985.83 864.54 20.89 o -1 5 1 37.25 22.59 4.73 o 0 5 1 709.53 662.74 18.08 o 1 5 1 1.94 -2.22 3.40 o 2 5 1 12.44 5.42 4.65 o 3 5 1 384.72 327.85 13.19 o 4 5 1 278.59 301.80 12.93 o 5 5 1 227.05 237.88 12.01 o 6 5 1 690.64 635.84 29.42 o 7 5 1 22.12 12.84 7.62 o 8 5 1 1302.42 1230.48 45.79 o 9 5 1 4.06 1.56 8.11 o 10 5 1 155.77 181.74 20.40 o 11 5 1 368.13 364.93 27.76 o 12 5 1 33.98 43.34 13.43 o 13 5 1 331.48 291.29 32.26 o 14 5 1 59.69 78.20 19.50 o 15 5 1 1.47 -4.17 11.53 o 16 5 1 62.23 37.35 16.94 o -15 6 1 21.39 13.31 13.29 o -14 6 1 54.58 62.75 25.06 o -13 6 1 745.89 706.09 42.42 o -12 6 1 1.29 -8.29 9.59 o -11 6 1 539.57 497.85 32.64 o -10 6 1 57.47 27.86 12.08 o -9 6 1 156.81 148.55 25.56 o -8 6 1 62.39 39.64 23.64 o -7 6 1 58.01 57.84 14.18 o -6 6 1 123.87 128.62 17.28 o -5 6 1 171.44 171.92 15.48 o -4 6 1 329.01 342.23 17.34 o -3 6 1 42.84 44.46 6.64 o -2 6 1 442.66 436.49 18.67 o -1 6 1 354.03 380.62 19.03 o 0 6 1 589.75 562.95 31.40 o 1 6 1 937.17 932.97 48.97 o 2 6 1 238.04 225.20 17.81 o 3 6 1 12.98 15.26 6.95 o 4 6 1 165.18 171.82 14.41 o 5 6 1 259.34 251.77 15.72 o 6 6 1 118.10 101.35 16.23 o 7 6 1 121.26 106.78 16.77 o 8 6 1 14.90 2.24 13.10 o 9 6 1 57.23 31.22 14.22 o 10 6 1 149.73 125.32 19.53 o 11 6 1 103.81 56.88 38.89 o 12 6 1 135.18 90.70 18.42 o 13 6 1 21.61 24.79 19.01 o 14 6 1 62.56 60.94 17.61 o -13 7 1 22.72 28.20 21.23 o -12 7 1 0.47 8.12 16.48 o -11 7 1 83.84 90.35 18.34 o -10 7 1 3.57 2.46 11.29 o -9 7 1 11.73 10.95 11.87 o -8 7 1 0.81 5.83 11.10 o -7 7 1 251.82 212.07 70.81 o -6 7 1 97.12 84.06 25.90 o -5 7 1 131.17 128.86 15.51 o -4 7 1 15.18 20.36 8.96 o -3 7 1 0.92 2.23 6.84 o -2 7 1 376.26 393.60 19.90 o -1 7 1 16.05 9.87 6.95 o 0 7 1 18.58 14.74 7.11 o 1 7 1 90.37 84.53 10.79 o 2 7 1 19.35 18.50 7.01 o 3 7 1 0.51 2.44 8.25 o 4 7 1 74.65 42.02 13.08 o 5 7 1 233.13 230.53 23.27 o 6 7 1 21.48 21.50 12.19 o 7 7 1 204.59 180.90 22.07 o 8 7 1 253.23 236.99 24.89 o 9 7 1 141.55 116.34 19.49 o 10 7 1 11.12 -1.82 11.71 o 11 7 1 63.36 45.86 16.31 o 12 7 1 140.00 83.91 19.52 o -9 8 1 5.37 32.69 30.42 o -8 8 1 45.74 31.36 19.50 o -7 8 1 25.65 34.85 16.13 o -6 8 1 483.68 483.17 36.60 o -5 8 1 32.99 28.06 13.79 o -4 8 1 242.59 293.26 30.56 o -3 8 1 473.28 472.91 26.79 o -2 8 1 79.48 48.48 12.43 o -1 8 1 6.42 19.68 8.57 o 0 8 1 442.71 386.77 34.22 o 1 8 1 456.72 503.27 38.09 o 2 8 1 39.57 36.20 12.00 o 3 8 1 37.02 32.57 11.63 o 4 8 1 270.13 213.86 24.21 o 5 8 1 64.70 59.30 27.44 o 6 8 1 49.67 66.69 17.01 o 7 8 1 148.30 118.56 20.76 o 8 8 1 114.21 70.53 18.41 o -21 0 2 2.84 31.27 14.72 o -20 0 2 89.19 76.24 13.58 o -19 0 2 709.89 716.55 22.27 o -18 0 2 528.08 551.14 18.96 o -17 0 2 215.95 334.09 82.77 o -16 0 2 204.93 233.41 14.62 o -15 0 2 3129.64 2980.74 47.03 o -14 0 2 241.09 279.69 13.60 o -12 0 2 567.80 815.92 23.27 o -11 0 2 1338.34 1255.58 22.63 o -10 0 2 331.72 606.69 31.52 o -9 0 2 118.65 430.75 28.25 o -8 0 2 362.69 570.85 41.16 o -7 0 2 2084.27 2072.49 32.85 o -6 0 2 7462.95 6821.32 100.75 o -5 0 2 4425.10 3933.76 47.04 o -4 0 2 2981.22 2681.66 32.89 o -3 0 2 22.81 23.33 2.05 o -2 0 2 14721.08 13637.02 205.78 o -1 0 2 5553.73 5005.56 77.06 o 0 0 2 641.35 663.90 12.68 o 1 0 2 0.40 0.10 1.68 o 2 0 2 2367.43 2214.59 32.79 o 3 0 2 3861.04 3660.20 47.37 o 4 0 2 10279.33 9182.17 113.48 o 5 0 2 108.94 123.07 11.30 o 6 0 2 1654.44 1853.86 62.42 o 7 0 2 1207.66 1225.82 23.15 o 8 0 2 1320.67 1284.18 24.68 o 9 0 2 1698.41 1625.70 30.10 o 10 0 2 42.89 46.06 13.03 o 11 0 2 2240.83 2078.97 42.13 o 12 0 2 10318.66 9375.63 134.41 o 13 0 2 1.24 33.80 8.39 o 14 0 2 952.88 1214.79 64.64 o 15 0 2 129.45 148.99 18.00 o 16 0 2 1070.64 1148.22 28.57 o 17 0 2 83.43 102.29 11.57 o 18 0 2 123.34 136.10 13.25 o 19 0 2 0.34 2.97 9.60 o -20 1 2 461.77 434.10 21.71 o -19 1 2 48.14 56.73 8.89 o -18 1 2 32.35 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