#------------------------------------------------------------------------------ #$Date: 2009-05-05 17:46:52 +0300 (Tue, 05 May 2009) $ #$Revision: 697 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2219359.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2219359_Fobs loop_ _publ_author_name 'Shen, Li' 'Liu, Qi' 'Shen, Hai-Jun' _publ_section_title ; Bis(1,2,3,4-tetrahydroquinolin-6-yl)methane ; _journal_coeditor_code HK2506 _journal_issue 9 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o1747 _journal_volume 64 _journal_year 2008 _space_group_IT_number 43 _symmetry_space_group_name_Hall 'F 2 -2d' _symmetry_space_group_name_H-M 'F d d 2' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 17.5146 _cell_length_b 29.6595 _cell_length_c 5.7678 _exptl_crystal_F_000 1200.00 _reflns_d_resolution_high 0.8119 _[local]_cod_data_source_file hk2506Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 1 in Fdd2' _shelx_refln_list_code 4 _shelx_F_calc_maximum 265.00 _shelx_F_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, z' 'x+1/4, -y+1/4, z+1/4' '-x+1/4, y+1/4, z+1/4' 'x, y+1/2, z+1/2' '-x, -y+1/2, z+1/2' 'x+1/4, -y+3/4, z+3/4' '-x+1/4, y+3/4, z+3/4' 'x+1/2, y, z+1/2' '-x+1/2, -y, z+1/2' 'x+3/4, -y+1/4, z+3/4' '-x+3/4, y+1/4, z+3/4' 'x+1/2, y+1/2, z' '-x+1/2, -y+1/2, z' 'x+3/4, -y+3/4, z+1/4' '-x+3/4, y+3/4, z+1/4' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 6276.94 5417.67 45.79 o 8 0 0 842.14 1429.12 32.29 o 12 0 0 3437.27 3112.41 59.29 o 16 0 0 401.12 355.15 24.36 o 20 0 0 0.16 -0.88 7.92 o 2 2 0 10251.53 10237.04 141.01 o 4 2 0 331.78 323.69 9.70 o 6 2 0 731.09 554.60 108.01 o 8 2 0 11.49 3.69 7.63 o 10 2 0 943.43 476.14 586.88 o 12 2 0 647.22 654.71 44.03 o 14 2 0 25.20 25.99 5.85 o 16 2 0 1.94 0.23 3.28 o 18 2 0 5.25 7.14 3.32 o 20 2 0 269.75 275.90 26.12 o 0 4 0 16433.08 16329.20 728.21 o 2 4 0 21130.89 20050.43 496.63 o 4 4 0 32465.47 30060.63 469.96 o 6 4 0 367.33 393.39 12.07 o 8 4 0 428.29 302.23 10.19 o 10 4 0 390.14 486.92 21.59 o 12 4 0 2592.76 3030.81 99.62 o 14 4 0 965.11 935.69 50.72 o 16 4 0 2.61 4.55 3.14 o 18 4 0 4.65 6.37 4.12 o 20 4 0 337.39 411.80 31.99 o 2 6 0 70224.48 58419.18 3905.06 o 4 6 0 5628.47 6037.23 160.12 o 6 6 0 426.70 405.06 14.06 o 8 6 0 3.77 5.69 1.68 o 10 6 0 181.34 178.58 6.63 o 12 6 0 1769.11 1945.39 55.12 o 14 6 0 3671.02 3670.27 141.20 o 16 6 0 14.55 14.70 4.66 o 18 6 0 13.42 10.93 4.70 o 20 6 0 98.48 82.77 16.44 o 0 8 0 6898.28 7705.80 273.41 o 2 8 0 12655.34 13814.81 467.17 o 4 8 0 234.59 270.09 8.80 o 6 8 0 46.66 36.62 2.48 o 8 8 0 33.62 44.63 4.55 o 10 8 0 2090.71 2362.77 66.22 o 12 8 0 1160.18 1104.72 21.84 o 14 8 0 2604.87 2680.33 86.00 o 16 8 0 1556.70 1573.34 43.90 o 18 8 0 4.16 2.87 3.84 o 20 8 0 14.26 14.68 8.51 o 2 10 0 7700.12 7357.52 249.37 o 4 10 0 87.67 75.78 3.88 o 6 10 0 1065.66 936.28 33.58 o 8 10 0 96.79 81.96 4.45 o 10 10 0 82.51 58.33 4.34 o 12 10 0 333.96 332.16 14.76 o 14 10 0 2988.58 3233.18 127.33 o 16 10 0 585.97 616.79 23.63 o 18 10 0 0.05 3.79 4.93 o 20 10 0 77.03 63.71 13.94 o 0 12 0 75.37 101.63 6.38 o 2 12 0 2647.44 3316.71 127.14 o 4 12 0 7574.79 8813.70 322.82 o 6 12 0 1449.03 1331.43 40.97 o 8 12 0 1557.94 1541.51 58.88 o 10 12 0 951.39 857.29 35.33 o 12 12 0 4039.79 4101.35 126.65 o 14 12 0 443.67 460.13 15.97 o 16 12 0 52.93 66.74 10.27 o 18 12 0 47.28 57.80 16.29 o 20 12 0 7.18 8.25 6.62 o 2 14 0 2239.28 3283.99 97.17 o 4 14 0 1769.82 2647.04 60.28 o 6 14 0 802.31 989.28 44.06 o 8 14 0 10.73 3.99 2.33 o 10 14 0 612.94 670.41 31.60 o 12 14 0 10306.84 10986.38 489.85 o 14 14 0 94.69 96.29 9.14 o 16 14 0 35.74 39.38 7.60 o 18 14 0 0.83 6.75 7.63 o 0 16 0 13907.99 14237.91 671.24 o 2 16 0 1033.02 998.43 37.21 o 4 16 0 178.86 208.35 6.78 o 6 16 0 17.81 28.99 3.88 o 8 16 0 1722.87 2037.25 104.89 o 10 16 0 959.40 947.80 32.92 o 12 16 0 2172.09 2362.86 111.93 o 14 16 0 170.46 179.68 18.24 o 16 16 0 148.50 132.53 28.91 o 18 16 0 137.49 88.92 20.11 o 2 18 0 1228.69 1470.92 47.15 o 4 18 0 17.66 21.39 3.27 o 6 18 0 567.47 666.66 29.63 o 8 18 0 3517.48 3634.68 83.63 o 10 18 0 52.57 44.32 5.67 o 12 18 0 57.70 54.94 5.92 o 14 18 0 17.89 16.35 5.20 o 16 18 0 10.55 15.82 5.63 o 18 18 0 113.88 84.01 13.50 o 0 20 0 7946.23 9022.64 498.81 o 2 20 0 1590.19 1564.31 117.30 o 4 20 0 77.50 62.10 19.99 o 6 20 0 176.24 154.73 7.74 o 8 20 0 630.68 581.24 15.08 o 10 20 0 847.97 861.05 35.09 o 12 20 0 2.90 3.99 2.98 o 14 20 0 5.94 5.65 3.45 o 16 20 0 7.50 4.84 5.60 o 18 20 0 281.23 284.66 20.64 o 2 22 0 207.59 162.47 7.38 o 4 22 0 71.79 56.68 5.44 o 6 22 0 13.78 27.15 4.46 o 8 22 0 46.00 54.16 8.35 o 10 22 0 541.65 450.52 14.62 o 12 22 0 823.86 791.43 48.89 o 14 22 0 0.88 5.07 3.58 o 16 22 0 169.44 183.94 18.64 o 0 24 0 161.81 147.53 10.22 o 2 24 0 96.42 113.22 6.86 o 4 24 0 97.35 91.75 6.97 o 6 24 0 603.48 476.41 22.24 o 8 24 0 21.26 24.40 4.79 o 10 24 0 23.54 31.03 5.61 o 12 24 0 67.17 55.35 7.19 o 14 24 0 123.96 173.81 17.96 o 16 24 0 32.24 27.11 8.80 o 2 26 0 154.79 129.47 10.58 o 4 26 0 448.92 384.21 16.01 o 6 26 0 802.75 643.57 43.16 o 8 26 0 452.98 368.48 13.67 o 10 26 0 297.31 300.19 12.97 o 12 26 0 15.63 12.22 4.24 o 14 26 0 226.71 291.24 16.53 o 0 28 0 180.09 167.89 19.37 o 2 28 0 52.31 53.72 9.75 o 4 28 0 4.04 4.79 3.57 o 6 28 0 8.07 7.70 5.53 o 8 28 0 36.59 42.57 6.37 o 10 28 0 57.52 68.02 7.98 o 12 28 0 10.76 5.62 4.39 o 2 30 0 135.55 136.61 14.51 o 4 30 0 1313.84 1220.21 36.63 o 6 30 0 355.00 333.93 22.12 o 8 30 0 24.89 24.37 5.45 o 10 30 0 20.13 27.94 5.85 o 12 30 0 236.69 311.03 28.25 o 0 32 0 7.97 4.99 8.51 o 2 32 0 83.90 72.72 12.13 o 4 32 0 80.18 89.87 13.24 o 6 32 0 422.51 369.22 22.63 o 8 32 0 12.61 18.85 6.17 o 10 32 0 11.98 16.00 5.96 o 2 34 0 2.26 0.29 5.98 o 4 34 0 361.32 358.42 22.62 o 6 34 0 116.35 151.11 20.11 o 0 36 0 182.35 203.99 27.59 o 2 36 0 51.79 53.53 12.03 o 1 1 1 9506.29 10034.04 359.26 o 3 1 1 13894.53 13524.38 333.37 o 5 1 1 1894.31 2164.51 52.92 o 7 1 1 2655.38 2760.60 73.10 o 9 1 1 4344.36 5309.97 160.53 o 11 1 1 549.06 584.16 15.50 o 13 1 1 16.54 25.10 3.07 o 15 1 1 40.25 52.77 3.89 o 17 1 1 2038.31 2127.45 75.40 o 19 1 1 135.46 172.54 9.47 o 21 1 1 23.22 20.73 5.97 o 1 3 1 55896.51 49000.60 1505.21 o 3 3 1 30095.55 27264.11 469.10 o 5 3 1 1142.08 1136.51 26.71 o 7 3 1 9402.20 9745.30 219.25 o 9 3 1 3.75 6.43 1.28 o 11 3 1 813.29 883.83 26.32 o 13 3 1 221.64 197.39 5.68 o 15 3 1 334.64 343.03 14.93 o 17 3 1 1083.37 1071.66 40.21 o 19 3 1 322.82 300.31 13.45 o 21 3 1 187.73 188.16 12.32 o 1 5 1 4793.75 5216.71 107.22 o 3 5 1 61212.82 53022.94 2312.86 o 5 5 1 6269.28 6286.52 135.17 o 7 5 1 5966.58 6051.69 105.23 o 9 5 1 1606.30 1495.77 32.13 o 11 5 1 192.84 215.31 6.58 o 13 5 1 242.71 196.75 9.62 o 15 5 1 211.20 231.18 8.18 o 17 5 1 292.63 282.27 18.52 o 19 5 1 400.79 412.13 15.24 o 21 5 1 126.52 154.96 13.50 o 1 7 1 9599.11 10014.13 209.80 o 3 7 1 28752.05 28239.73 655.89 o 5 7 1 1492.04 1444.65 38.12 o 7 7 1 1879.29 2089.20 47.39 o 9 7 1 331.23 292.78 9.54 o 11 7 1 202.74 141.19 4.69 o 13 7 1 146.12 125.55 5.40 o 15 7 1 1458.59 1364.60 48.62 o 17 7 1 507.77 483.75 19.60 o 19 7 1 121.00 143.96 9.88 o 1 9 1 1646.32 1482.91 43.43 o 3 9 1 1622.94 1893.34 32.79 o 5 9 1 5753.70 6575.15 156.55 o 7 9 1 3070.82 3251.20 80.31 o 9 9 1 681.86 520.34 21.74 o 11 9 1 40.88 25.11 3.86 o 13 9 1 831.58 883.56 22.27 o 15 9 1 1404.51 1276.37 31.97 o 17 9 1 95.90 74.61 7.00 o 19 9 1 3.03 2.79 3.35 o 1 11 1 41.78 49.51 3.27 o 3 11 1 2805.25 3151.60 66.56 o 5 11 1 23743.78 25682.96 596.89 o 7 11 1 2409.59 2403.14 65.20 o 9 11 1 36.30 48.29 2.89 o 11 11 1 1675.78 1672.65 51.28 o 13 11 1 3011.47 3022.45 96.17 o 15 11 1 484.85 475.77 16.58 o 17 11 1 47.91 53.47 6.28 o 19 11 1 72.47 67.20 7.50 o 1 13 1 1885.62 1948.15 39.94 o 3 13 1 4422.91 4525.18 97.23 o 5 13 1 4653.27 4840.39 100.45 o 7 13 1 1531.05 1570.36 40.18 o 9 13 1 414.99 435.43 12.38 o 11 13 1 1524.10 1504.15 57.66 o 13 13 1 179.02 169.24 8.26 o 15 13 1 1245.93 1262.32 47.22 o 17 13 1 26.30 33.86 5.46 o 19 13 1 25.34 22.44 5.77 o 1 15 1 839.68 1058.30 35.02 o 3 15 1 1175.13 1386.87 39.79 o 5 15 1 5038.41 5592.76 133.49 o 7 15 1 484.37 479.44 8.10 o 9 15 1 507.71 486.66 16.89 o 11 15 1 1333.99 1416.04 40.39 o 13 15 1 79.02 106.20 7.52 o 15 15 1 151.55 181.91 9.47 o 17 15 1 598.12 533.17 19.06 o 19 15 1 132.14 128.96 11.24 o 1 17 1 828.88 918.23 17.71 o 3 17 1 962.58 1157.67 26.96 o 5 17 1 101.32 114.49 3.89 o 7 17 1 389.18 361.93 13.54 o 9 17 1 2626.44 2549.76 63.14 o 11 17 1 1807.07 1930.81 77.39 o 13 17 1 75.69 82.08 6.24 o 15 17 1 59.51 52.07 6.27 o 17 17 1 334.71 327.19 15.31 o 1 19 1 150.02 148.51 8.91 o 3 19 1 259.22 214.60 11.34 o 5 19 1 36.24 42.06 3.62 o 7 19 1 527.27 513.18 10.03 o 9 19 1 5256.49 5168.65 143.37 o 11 19 1 117.36 125.90 6.59 o 13 19 1 124.19 121.73 10.42 o 15 19 1 235.05 254.52 10.16 o 17 19 1 308.84 334.47 13.51 o 1 21 1 562.69 632.61 18.44 o 3 21 1 492.86 444.03 11.76 o 5 21 1 9.42 8.78 2.28 o 7 21 1 482.51 602.22 14.69 o 9 21 1 569.95 528.64 14.84 o 11 21 1 501.39 500.57 14.03 o 13 21 1 3.75 9.40 3.20 o 15 21 1 18.54 33.12 5.20 o 17 21 1 194.91 246.88 13.65 o 1 23 1 59.20 45.86 3.91 o 3 23 1 1129.79 1057.87 21.56 o 5 23 1 447.09 398.27 10.70 o 7 23 1 114.99 98.73 5.86 o 9 23 1 490.92 501.87 15.60 o 11 23 1 173.86 171.86 8.24 o 13 23 1 182.70 197.47 8.55 o 15 23 1 33.90 56.00 6.34 o 1 25 1 821.25 811.66 16.24 o 3 25 1 1232.91 1209.28 20.46 o 5 25 1 113.13 111.10 5.94 o 7 25 1 681.40 573.21 20.70 o 9 25 1 21.66 26.92 4.40 o 11 25 1 1.27 1.43 2.77 o 13 25 1 82.08 88.98 6.79 o 15 25 1 100.56 108.23 8.50 o 1 27 1 450.03 424.69 17.84 o 3 27 1 506.80 472.43 42.59 o 5 27 1 52.98 51.68 6.17 o 7 27 1 653.16 573.19 19.44 o 9 27 1 65.00 81.38 7.56 o 11 27 1 14.21 14.46 4.27 o 13 27 1 93.93 102.37 8.98 o 1 29 1 51.82 55.18 7.25 o 3 29 1 228.15 172.98 33.19 o 5 29 1 1032.79 888.95 29.75 o 7 29 1 233.01 223.84 8.67 o 9 29 1 2.34 4.11 2.74 o 11 29 1 23.14 24.14 4.19 o 1 31 1 65.46 81.08 8.68 o 3 31 1 198.85 206.80 11.62 o 5 31 1 322.48 322.15 12.59 o 7 31 1 45.52 42.05 5.54 o 9 31 1 31.94 38.40 5.49 o 11 31 1 47.03 40.30 5.30 o 1 33 1 144.30 164.11 11.75 o 3 33 1 287.40 330.07 15.10 o 5 33 1 256.27 255.72 13.64 o 7 33 1 283.80 225.10 12.96 o 1 35 1 18.70 26.30 6.70 o 3 35 1 21.43 16.95 5.93 o 5 35 1 50.63 42.60 7.73 o 2 0 2 3174.94 3323.98 105.36 o 6 0 2 2057.91 1959.24 106.48 o 10 0 2 1875.68 1933.21 88.73 o 14 0 2 6.75 11.60 3.89 o 18 0 2 891.47 846.07 56.90 o 0 2 2 20195.37 20605.99 561.07 o 2 2 2 6937.16 6429.78 154.76 o 4 2 2 1071.14 1217.73 27.21 o 6 2 2 1920.37 1694.08 48.43 o 8 2 2 4526.76 4810.14 119.57 o 10 2 2 1230.22 1195.27 42.02 o 12 2 2 44.70 35.15 3.38 o 14 2 2 202.16 202.27 8.18 o 16 2 2 730.73 634.93 19.99 o 18 2 2 405.14 493.87 16.76 o 20 2 2 761.04 701.88 22.36 o 2 4 2 561.06 969.08 22.47 o 4 4 2 4590.34 5057.20 107.77 o 6 4 2 2441.57 2905.23 61.88 o 8 4 2 21.52 19.98 1.67 o 10 4 2 1377.51 1287.94 47.37 o 12 4 2 50.85 62.03 3.94 o 14 4 2 170.02 133.69 7.01 o 16 4 2 666.37 629.39 18.63 o 18 4 2 299.18 281.36 10.56 o 20 4 2 198.10 222.68 12.72 o 0 6 2 5096.51 5819.62 206.41 o 2 6 2 1024.54 1175.88 22.58 o 4 6 2 796.80 834.06 18.18 o 6 6 2 9859.51 10910.11 221.74 o 8 6 2 2041.07 2125.72 56.22 o 10 6 2 1239.68 1168.69 27.74 o 12 6 2 419.22 408.03 16.25 o 14 6 2 657.44 579.55 24.39 o 16 6 2 699.57 616.67 22.40 o 18 6 2 415.83 382.80 13.56 o 20 6 2 43.25 69.32 8.75 o 2 8 2 2577.01 2714.30 67.75 o 4 8 2 18125.85 18824.67 416.57 o 6 8 2 17605.24 18204.83 424.49 o 8 8 2 85.62 109.82 12.68 o 10 8 2 24.15 34.24 4.51 o 12 8 2 777.03 584.17 38.92 o 14 8 2 1464.56 1353.28 32.11 o 16 8 2 7.90 0.28 2.97 o 18 8 2 39.21 54.60 6.73 o 20 8 2 116.11 136.53 10.32 o 0 10 2 552.76 415.33 14.35 o 2 10 2 2676.00 3038.95 60.24 o 4 10 2 5321.44 6060.98 164.49 o 6 10 2 1070.48 840.65 17.80 o 8 10 2 1560.28 1804.64 41.86 o 10 10 2 243.83 186.36 7.76 o 12 10 2 767.40 764.07 19.02 o 14 10 2 381.19 390.41 12.58 o 16 10 2 18.00 13.96 4.17 o 18 10 2 39.34 49.68 6.49 o 2 12 2 873.33 856.80 15.29 o 4 12 2 2350.85 3061.88 58.57 o 6 12 2 2121.21 2366.57 55.37 o 8 12 2 2332.86 1919.81 92.16 o 10 12 2 189.46 184.95 6.43 o 12 12 2 1037.14 961.59 19.92 o 14 12 2 547.49 532.78 23.36 o 16 12 2 399.32 342.83 14.50 o 18 12 2 31.49 26.81 5.30 o 0 14 2 244.66 282.70 7.15 o 2 14 2 521.45 437.81 6.86 o 4 14 2 227.62 280.98 5.69 o 6 14 2 1423.29 1496.31 41.38 o 8 14 2 2673.56 2605.59 72.29 o 10 14 2 1262.57 1171.88 42.44 o 12 14 2 144.46 101.90 6.59 o 14 14 2 571.26 521.38 15.98 o 16 14 2 775.63 661.21 22.52 o 18 14 2 27.99 36.65 6.24 o 2 16 2 756.55 687.89 17.83 o 4 16 2 240.56 182.52 4.98 o 6 16 2 1567.63 1577.81 33.34 o 8 16 2 33.47 48.55 4.04 o 10 16 2 629.79 563.11 13.06 o 12 16 2 523.23 527.21 18.63 o 14 16 2 486.45 498.75 16.47 o 16 16 2 386.77 434.21 24.32 o 18 16 2 40.87 60.44 7.54 o 0 18 2 3020.55 2644.75 76.95 o 2 18 2 1234.05 1233.19 29.29 o 4 18 2 414.68 436.65 13.46 o 6 18 2 1003.79 1048.51 25.25 o 8 18 2 2043.90 2168.02 67.20 o 10 18 2 858.41 788.35 18.97 o 12 18 2 98.04 107.95 7.23 o 14 18 2 163.58 176.12 8.74 o 16 18 2 161.87 177.22 10.57 o 2 20 2 1316.04 1265.44 37.79 o 4 20 2 25.98 29.68 3.04 o 6 20 2 428.68 399.47 13.90 o 8 20 2 971.36 924.51 47.52 o 10 20 2 150.13 202.83 8.52 o 12 20 2 6.39 4.43 2.90 o 14 20 2 59.04 82.18 7.16 o 16 20 2 144.80 176.79 10.99 o 0 22 2 5766.84 5995.04 252.94 o 2 22 2 1269.26 1268.05 41.41 o 4 22 2 79.77 97.88 5.48 o 6 22 2 793.71 733.68 23.07 o 8 22 2 1427.97 1336.71 48.89 o 10 22 2 168.56 159.41 7.65 o 12 22 2 72.56 55.41 6.05 o 14 22 2 13.05 16.95 4.13 o 16 22 2 82.94 106.84 9.59 o 2 24 2 1328.19 1289.76 20.71 o 4 24 2 746.60 683.68 12.81 o 6 24 2 1284.54 1416.27 47.70 o 8 24 2 461.31 440.41 15.96 o 10 24 2 120.62 141.60 7.68 o 12 24 2 54.59 44.37 5.57 o 14 24 2 13.26 11.90 4.01 o 0 26 2 1326.47 1226.91 28.58 o 2 26 2 823.43 823.15 31.17 o 4 26 2 125.38 110.90 7.07 o 6 26 2 409.42 390.83 15.60 o 8 26 2 100.65 103.86 7.42 o 10 26 2 18.97 18.77 3.95 o 12 26 2 44.90 49.41 6.14 o 2 28 2 554.10 504.26 35.93 o 4 28 2 1402.91 1322.30 29.36 o 6 28 2 110.58 101.17 8.29 o 8 28 2 112.84 108.56 8.76 o 10 28 2 14.34 17.15 4.24 o 12 28 2 27.18 24.99 4.96 o 0 30 2 137.54 150.86 15.02 o 2 30 2 275.40 290.60 13.41 o 4 30 2 204.10 181.15 11.32 o 6 30 2 75.30 102.52 8.69 o 8 30 2 13.86 9.49 4.30 o 10 30 2 50.02 56.25 7.29 o 2 32 2 89.39 91.10 9.49 o 4 32 2 142.85 168.89 13.94 o 6 32 2 202.20 193.81 12.36 o 8 32 2 54.10 55.46 7.23 o 0 34 2 65.55 86.97 13.68 o 2 34 2 3.26 -1.08 4.39 o 4 34 2 31.84 33.34 8.09 o 1 1 3 2705.34 3459.50 44.90 o 3 1 3 1649.48 1505.33 56.97 o 5 1 3 282.84 244.24 7.34 o 7 1 3 1202.78 1140.94 43.42 o 9 1 3 1657.51 1801.28 52.67 o 11 1 3 313.83 321.40 8.43 o 13 1 3 371.36 370.40 13.21 o 15 1 3 22.38 19.25 3.60 o 17 1 3 42.35 53.44 6.41 o 19 1 3 42.23 56.66 7.27 o 1 3 3 953.60 914.79 43.92 o 3 3 3 1171.56 1440.02 26.41 o 5 3 3 922.79 916.58 22.08 o 7 3 3 295.20 266.78 11.02 o 9 3 3 4950.53 4706.63 105.14 o 11 3 3 1085.12 1054.23 32.03 o 13 3 3 424.50 378.51 16.37 o 15 3 3 223.27 205.47 8.77 o 17 3 3 49.68 62.62 6.98 o 19 3 3 46.92 34.47 5.36 o 1 5 3 6283.40 7346.64 124.86 o 3 5 3 124.43 116.69 3.92 o 5 5 3 262.75 294.29 8.29 o 7 5 3 199.36 160.01 6.46 o 9 5 3 880.43 789.05 25.62 o 11 5 3 2405.53 2329.24 56.04 o 13 5 3 120.88 137.27 7.35 o 15 5 3 268.37 235.56 9.41 o 17 5 3 12.98 20.01 4.34 o 19 5 3 42.96 55.48 7.99 o 1 7 3 7.78 7.80 1.47 o 3 7 3 1885.19 1873.46 34.27 o 5 7 3 185.56 177.90 5.05 o 7 7 3 493.53 526.83 22.43 o 9 7 3 1048.75 1072.61 29.48 o 11 7 3 3017.14 2943.29 85.76 o 13 7 3 15.85 31.42 4.44 o 15 7 3 26.85 28.69 4.55 o 17 7 3 8.55 12.10 3.83 o 19 7 3 4.90 0.24 3.96 o 1 9 3 386.21 407.92 8.25 o 3 9 3 1698.28 1783.66 33.16 o 5 9 3 248.33 309.43 6.69 o 7 9 3 268.35 234.85 7.00 o 9 9 3 299.16 253.15 8.90 o 11 9 3 1749.79 1634.07 40.92 o 13 9 3 1016.63 875.78 26.69 o 15 9 3 480.89 436.36 12.76 o 17 9 3 3.37 4.89 3.60 o 1 11 3 607.03 549.97 11.61 o 3 11 3 4695.23 4892.74 112.25 o 5 11 3 435.14 405.14 8.60 o 7 11 3 87.37 92.82 5.04 o 9 11 3 232.47 214.08 7.96 o 11 11 3 397.64 300.86 23.47 o 13 11 3 1639.59 1233.14 198.57 o 15 11 3 57.59 88.53 8.06 o 17 11 3 59.07 52.01 7.07 o 1 13 3 805.42 870.11 18.05 o 3 13 3 2432.77 2366.33 61.31 o 5 13 3 434.98 392.59 13.14 o 7 13 3 1011.95 932.60 30.17 o 9 13 3 1350.68 1188.74 36.67 o 11 13 3 643.38 667.29 21.77 o 13 13 3 178.69 189.01 9.62 o 15 13 3 276.04 284.59 12.09 o 17 13 3 39.88 56.16 7.24 o 1 15 3 236.32 207.06 7.95 o 3 15 3 1804.32 1954.37 29.57 o 5 15 3 626.86 668.22 19.41 o 7 15 3 286.73 309.70 11.99 o 9 15 3 483.36 422.79 17.09 o 11 15 3 599.31 508.87 14.61 o 13 15 3 61.11 64.17 6.98 o 15 15 3 29.59 25.10 5.29 o 17 15 3 93.14 115.32 9.81 o 1 17 3 1451.47 1260.21 25.22 o 3 17 3 2427.78 2355.44 74.31 o 5 17 3 532.44 524.76 26.32 o 7 17 3 190.90 201.49 8.86 o 9 17 3 755.61 671.27 24.81 o 11 17 3 638.80 478.91 20.70 o 13 17 3 80.16 75.43 7.52 o 15 17 3 81.92 73.96 8.02 o 1 19 3 1634.88 1644.32 38.85 o 3 19 3 702.30 678.13 21.28 o 5 19 3 19.43 7.09 2.55 o 7 19 3 257.28 263.32 9.25 o 9 19 3 508.07 496.27 20.82 o 11 19 3 263.12 236.82 10.77 o 13 19 3 259.60 257.75 11.79 o 15 19 3 78.61 78.21 8.25 o 1 21 3 3103.42 3134.46 52.13 o 3 21 3 461.06 454.42 12.54 o 5 21 3 319.24 326.37 9.48 o 7 21 3 115.45 110.32 7.07 o 9 21 3 269.05 283.16 10.28 o 11 21 3 382.10 336.20 12.88 o 13 21 3 68.65 72.00 7.89 o 15 21 3 117.40 163.51 11.21 o 1 23 3 324.42 361.27 9.68 o 3 23 3 88.54 102.66 7.43 o 5 23 3 221.68 216.51 10.94 o 7 23 3 175.53 154.67 8.28 o 9 23 3 13.84 14.76 3.97 o 11 23 3 356.53 357.14 15.04 o 13 23 3 78.81 84.35 8.51 o 1 25 3 712.61 683.79 18.43 o 3 25 3 800.09 820.97 27.51 o 5 25 3 244.31 220.93 10.16 o 7 25 3 136.06 163.60 8.04 o 9 25 3 162.22 204.29 9.61 o 11 25 3 318.79 330.58 13.14 o 1 27 3 45.04 55.16 7.07 o 3 27 3 289.23 272.98 11.17 o 5 27 3 149.15 177.22 9.69 o 7 27 3 60.84 54.86 6.84 o 9 27 3 17.13 33.78 5.13 o 11 27 3 62.93 53.22 6.48 o 1 29 3 232.12 227.07 14.12 o 3 29 3 393.54 404.43 15.81 o 5 29 3 143.08 160.73 10.25 o 7 29 3 63.72 80.61 8.29 o 9 29 3 1.68 0.63 4.13 o 1 31 3 160.19 180.67 19.37 o 3 31 3 209.66 207.74 12.14 o 5 31 3 100.76 132.80 11.27 o 1 33 3 8.96 15.51 7.94 o 0 0 4 1109.04 1283.30 70.16 o 4 0 4 431.84 471.40 25.74 o 8 0 4 6572.95 6960.38 369.98 o 12 0 4 141.74 122.29 9.04 o 16 0 4 106.30 117.31 12.07 o 2 2 4 480.84 513.20 17.88 o 4 2 4 663.76 658.56 28.26 o 6 2 4 3739.10 3760.11 98.20 o 8 2 4 1023.11 934.75 39.57 o 10 2 4 575.99 588.05 17.23 o 12 2 4 208.51 209.72 7.06 o 14 2 4 106.24 121.78 6.86 o 16 2 4 4.58 8.72 3.56 o 0 4 4 389.38 325.71 12.92 o 2 4 4 302.93 318.34 41.91 o 4 4 4 787.61 711.88 19.01 o 6 4 4 1439.38 1326.13 41.19 o 8 4 4 1498.75 1460.27 30.46 o 10 4 4 911.44 915.18 29.65 o 12 4 4 9.24 19.72 3.57 o 14 4 4 69.01 73.38 6.71 o 16 4 4 76.44 65.45 6.37 o 2 6 4 117.29 112.97 4.32 o 4 6 4 468.34 497.91 18.29 o 6 6 4 2134.64 2085.28 58.93 o 8 6 4 221.41 203.93 7.38 o 10 6 4 928.73 975.41 26.62 o 12 6 4 70.95 55.69 5.76 o 14 6 4 234.30 212.17 9.44 o 16 6 4 118.08 118.25 8.56 o 0 8 4 396.11 368.73 25.10 o 2 8 4 178.97 181.47 19.64 o 4 8 4 351.39 363.21 8.39 o 6 8 4 784.58 857.13 22.00 o 8 8 4 1158.92 1065.89 22.59 o 10 8 4 391.53 379.14 11.29 o 12 8 4 154.97 162.23 8.36 o 14 8 4 167.76 152.82 8.90 o 16 8 4 18.48 19.75 4.49 o 2 10 4 71.48 79.90 4.65 o 4 10 4 39.72 30.64 3.19 o 6 10 4 2575.94 2594.19 62.88 o 8 10 4 328.37 333.66 10.33 o 10 10 4 360.73 321.66 10.59 o 12 10 4 107.99 107.24 7.59 o 14 10 4 46.50 46.64 5.80 o 16 10 4 88.87 82.39 8.51 o 0 12 4 1584.02 1324.22 109.47 o 2 12 4 37.76 37.33 3.64 o 4 12 4 139.18 156.35 5.83 o 6 12 4 870.12 939.48 33.27 o 8 12 4 142.07 148.87 7.78 o 10 12 4 65.44 51.36 5.58 o 12 12 4 139.00 137.50 8.43 o 14 12 4 53.56 56.90 7.15 o 16 12 4 56.88 63.29 7.67 o 2 14 4 649.62 652.72 26.37 o 4 14 4 2139.59 1971.21 71.09 o 6 14 4 1049.95 966.41 23.43 o 8 14 4 31.30 19.97 4.01 o 10 14 4 131.95 123.12 7.90 o 12 14 4 26.43 29.54 4.84 o 14 14 4 84.81 97.32 8.97 o 0 16 4 688.37 671.53 18.71 o 2 16 4 1119.69 1180.99 21.74 o 4 16 4 654.22 589.55 70.12 o 6 16 4 313.48 289.19 9.27 o 8 16 4 174.62 170.14 8.33 o 10 16 4 255.20 222.29 10.11 o 12 16 4 38.95 32.99 5.72 o 14 16 4 116.32 159.20 11.10 o 2 18 4 8.02 8.92 2.83 o 4 18 4 955.80 959.41 19.95 o 6 18 4 635.31 559.91 25.22 o 8 18 4 127.61 124.94 11.54 o 10 18 4 342.16 285.01 12.01 o 12 18 4 59.41 51.17 6.85 o 14 18 4 73.85 110.08 9.73 o 0 20 4 66.87 64.25 10.17 o 2 20 4 775.54 750.20 17.99 o 4 20 4 191.86 206.84 7.94 o 6 20 4 84.99 71.47 6.26 o 8 20 4 161.09 148.34 9.72 o 10 20 4 400.39 428.60 16.03 o 12 20 4 69.46 43.70 6.74 o 2 22 4 131.09 104.40 7.85 o 4 22 4 88.57 92.08 7.64 o 6 22 4 96.60 100.42 7.46 o 8 22 4 238.49 250.33 13.74 o 10 22 4 94.77 95.60 8.84 o 12 22 4 153.47 167.15 11.41 o 0 24 4 41.25 33.45 8.50 o 2 24 4 27.33 28.03 5.02 o 4 24 4 27.23 32.21 6.00 o 6 24 4 108.31 123.41 9.19 o 8 24 4 70.73 70.03 7.43 o 10 24 4 55.92 26.31 5.52 o 2 26 4 289.08 335.08 14.37 o 4 26 4 73.19 73.05 8.43 o 6 26 4 16.38 38.05 6.55 o 8 26 4 59.12 107.39 10.80 o 0 28 4 225.43 249.19 26.42 o 2 28 4 21.31 22.35 5.68 o 4 28 4 103.02 99.22 9.91 o 6 28 4 157.37 164.52 12.28 o 2 30 4 79.94 85.26 11.12 o 1 1 5 245.25 243.91 10.67 o 3 1 5 103.13 85.13 4.81 o 5 1 5 1512.71 1372.84 33.01 o 7 1 5 272.52 269.42 8.26 o 9 1 5 54.59 49.50 4.65 o 11 1 5 389.64 436.07 13.91 o 13 1 5 14.31 10.72 3.35 o 15 1 5 23.23 32.44 5.60 o 1 3 5 25.89 30.95 4.30 o 3 3 5 202.51 200.08 7.68 o 5 3 5 835.23 721.74 44.20 o 7 3 5 2365.58 2393.06 60.14 o 9 3 5 367.45 377.97 12.44 o 11 3 5 99.28 81.90 6.41 o 13 3 5 143.69 151.03 9.26 o 15 3 5 156.94 192.75 10.44 o 1 5 5 3.68 7.59 2.92 o 3 5 5 335.03 299.46 10.46 o 5 5 5 558.93 569.13 30.57 o 7 5 5 64.64 61.87 5.92 o 9 5 5 444.26 430.27 12.55 o 11 5 5 247.65 237.04 11.84 o 13 5 5 26.09 50.90 5.75 o 15 5 5 5.88 6.93 3.59 o 1 7 5 461.52 430.44 12.25 o 3 7 5 981.23 1014.77 16.95 o 5 7 5 479.97 476.92 12.93 o 7 7 5 722.64 685.28 15.70 o 9 7 5 429.42 466.62 17.52 o 11 7 5 119.77 124.75 8.44 o 13 7 5 5.15 4.47 3.56 o 1 9 5 333.76 293.62 11.93 o 3 9 5 620.39 600.83 14.82 o 5 9 5 554.27 555.07 13.26 o 7 9 5 416.57 389.99 12.96 o 9 9 5 311.61 308.97 14.05 o 11 9 5 192.44 208.30 9.55 o 13 9 5 91.45 96.82 8.17 o 1 11 5 0.28 3.30 2.50 o 3 11 5 698.22 595.10 24.72 o 5 11 5 581.39 633.02 15.86 o 7 11 5 353.09 376.51 16.36 o 9 11 5 165.71 167.70 8.96 o 11 11 5 56.11 73.81 7.15 o 13 11 5 59.38 67.65 7.15 o 1 13 5 225.00 224.66 7.91 o 3 13 5 78.99 78.60 6.94 o 5 13 5 366.85 348.72 18.00 o 7 13 5 684.64 662.74 21.77 o 9 13 5 7.37 1.21 3.11 o 11 13 5 166.87 181.64 9.75 o 13 13 5 139.82 140.05 9.53 o 1 15 5 161.04 135.84 35.78 o 3 15 5 280.22 263.52 14.57 o 5 15 5 132.40 147.71 9.09 o 7 15 5 143.47 155.95 8.98 o 9 15 5 57.58 76.50 7.17 o 11 15 5 56.12 73.79 7.32 o 1 17 5 17.06 14.74 4.46 o 3 17 5 96.72 108.38 8.08 o 5 17 5 340.78 317.71 13.31 o 7 17 5 218.77 203.12 14.64 o 9 17 5 1.86 3.21 3.31 o 11 17 5 24.14 28.57 5.94 o 1 19 5 190.11 197.40 11.01 o 3 19 5 16.07 25.25 5.71 o 5 19 5 4.69 9.58 3.91 o 7 19 5 78.31 81.27 7.34 o 9 19 5 5.69 5.00 3.92 o 1 21 5 21.39 18.36 5.18 o 3 21 5 201.99 208.85 17.33 o 5 21 5 197.86 192.65 11.56 o 7 21 5 58.19 74.27 7.80 o 9 21 5 20.73 23.14 6.42 o 1 23 5 235.49 289.05 13.69 o 3 23 5 19.06 30.48 6.94 o 5 23 5 10.35 3.55 6.23 o 7 23 5 58.09 75.34 9.34 o 1 25 5 47.14 62.65 8.32 o 3 25 5 14.96 17.47 6.53 o 2 0 6 82.44 74.09 11.60 o 6 0 6 15.93 17.85 7.11 o 10 0 6 227.72 222.00 12.48 o 0 2 6 249.77 251.80 17.64 o 2 2 6 109.78 104.08 9.34 o 4 2 6 38.57 37.42 6.51 o 6 2 6 10.05 10.60 3.93 o 8 2 6 39.38 55.96 5.28 o 10 2 6 303.48 327.94 10.52 o 2 4 6 300.56 328.49 14.01 o 4 4 6 278.95 293.59 13.53 o 6 4 6 93.28 91.35 8.05 o 8 4 6 303.78 313.13 11.53 o 10 4 6 281.56 285.30 10.58 o 0 6 6 770.87 722.93 28.61 o 2 6 6 141.78 132.45 10.26 o 4 6 6 100.80 86.94 8.92 o 6 6 6 19.65 32.95 5.41 o 8 6 6 26.61 38.74 5.45 o 10 6 6 84.66 72.64 7.26 o 2 8 6 612.54 542.03 17.96 o 4 8 6 96.81 103.70 11.18 o 6 8 6 77.20 81.76 8.86 o 8 8 6 89.20 111.10 9.11 o 10 8 6 178.93 198.43 10.09 o 0 10 6 1841.41 1649.86 43.28 o 2 10 6 138.07 186.00 11.36 o 4 10 6 214.02 210.48 11.68 o 6 10 6 25.94 33.29 6.27 o 8 10 6 29.83 25.88 5.42 o 2 12 6 132.64 147.89 12.91 o 4 12 6 32.56 30.96 6.05 o 6 12 6 52.03 66.36 7.23 o 8 12 6 2.84 3.59 3.89 o 0 14 6 680.08 705.04 29.13 o 2 14 6 433.40 429.40 19.36 o 4 14 6 81.90 67.67 8.46 o 6 14 6 2.32 4.21 3.82 o 8 14 6 18.12 9.12 4.43 o 2 16 6 76.90 81.14 13.07 o 4 16 6 91.31 128.22 10.76 o 6 16 6 32.17 37.95 6.20 o 0 18 6 59.64 64.87 17.90 o 2 18 6 227.98 247.50 19.09 o 4 18 6 41.42 25.66 7.15 o 1 1 7 29.62 25.85 6.54 o 3 1 7 97.07 114.99 11.11 o 1 3 7 12.11 8.05 4.82 o 3 3 7 125.30 145.04 12.02 o 1 5 7 125.42 108.42 10.86 o