#------------------------------------------------------------------------------ #$Date: 2009-05-03 21:56:13 +0300 (Sun, 03 May 2009) $ #$Revision: 691 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2219374.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2219374_Fobs loop_ _publ_author_name 'Wang, Yan' 'Li, Yue-Qin' 'Shen, Ying-Zhong' _publ_section_title ; Poly[[tetraaqua(\m~6~-2,2'-diiodobiphenyl-4,4',5,5'-tetracarboxylato)dizinc(II)] dihydrate] ; _journal_coeditor_code IS2308 _journal_issue 9 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1203 _journal_page_last m1204 _journal_volume 64 _journal_year 2008 _space_group_IT_number 5 _symmetry_space_group_name_Hall 'C 2y' _symmetry_space_group_name_H-M 'C 1 2 1' _cell_angle_alpha 90.000 _cell_angle_beta 100.187 _cell_angle_gamma 90.000 _cell_length_a 10.9466 _cell_length_b 9.8135 _cell_length_c 11.3913 _exptl_crystal_F_000 780.00 _reflns_d_resolution_high 0.8107 _[local]_cod_data_source_file is2308Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' ' _shelx_refln_list_code 4 _shelx_F_calc_maximum 277.83 _shelx_F_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 7 -9 0 758.99 802.29 251.90 o 8 -8 0 463.29 481.05 192.31 o 7 -7 0 1654.15 1723.21 341.83 o 9 -7 0 284.23 314.20 183.10 o 8 -6 0 137.32 215.06 143.56 o 10 -6 0 416.96 418.21 168.47 o 7 -5 0 4766.14 4663.66 423.08 o 9 -5 0 199.74 219.94 151.68 o 11 -5 0 1263.75 1686.37 369.99 o 6 -4 0 11377.85 11649.68 602.39 o 8 -4 0 1198.98 1430.68 270.32 o 10 -4 0 1869.69 1675.54 367.83 o 12 -4 0 231.24 403.04 169.02 o 5 -3 0 10559.55 10081.94 495.67 o 7 -3 0 2400.00 2334.27 268.15 o 9 -3 0 1040.49 1053.64 285.49 o 11 -3 0 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