#------------------------------------------------------------------------------ #$Date: 2009-05-03 21:56:13 +0300 (Sun, 03 May 2009) $ #$Revision: 691 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2219384.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2219384_Fobs loop_ _publ_author_name 'Gainsford, Graeme J.' 'Bhuiyan, M. Delower H.' 'Kay, Andrew J.' 'Robinson, Ward T.' _publ_section_title ; 2-{3-Cyano-5,5-dimethyl-4-[4-(pyrrolidin-1-yl)buta-1,3-dienyl]-2,5-dihydrofuran-2-ylidene}malononitrile dichloromethane solvate ; _journal_coeditor_code LH2664 _journal_issue 9 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o1715 _journal_volume 64 _journal_year 2008 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 93.482 _cell_angle_gamma 90.000 _cell_length_a 6.8755 _cell_length_b 16.8913 _cell_length_c 16.6677 _exptl_crystal_F_000 816.00 _reflns_d_resolution_high 0.7330 _[local]_cod_data_source_file lh2664Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' PITB_0m in P2(1)/c RElabelled STRIPPED DATASET' _shelx_refln_list_code 4 _shelx_F_calc_maximum 184.27 _shelx_F_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 3 0 0 199.06 262.36 42.89 o 4 0 0 33956.65 44267.11 2322.44 o 5 0 0 1016.82 893.91 71.17 o 6 0 0 5440.49 5323.09 295.19 o 8 0 0 424.22 469.11 69.91 o 9 0 0 280.98 147.52 136.36 o 1 1 0 2197.87 1172.77 44.62 o 2 1 0 4269.74 3886.23 75.41 o 3 1 0 190.37 235.50 17.91 o 4 1 0 3337.12 4778.89 139.35 o 5 1 0 757.02 670.35 45.56 o 6 1 0 1723.92 1769.75 81.69 o 7 1 0 69.18 117.98 35.19 o 8 1 0 327.58 434.07 59.38 o 9 1 0 7.52 1.73 90.65 o 1 2 0 20.19 16.18 2.36 o 2 2 0 11622.35 12587.96 230.00 o 4 2 0 2521.20 2218.12 57.34 o 5 2 0 352.23 398.72 20.42 o 6 2 0 535.86 608.46 30.79 o 7 2 0 96.20 29.54 43.99 o 8 2 0 194.96 168.88 50.74 o 9 2 0 18.40 45.25 56.09 o 1 3 0 2499.11 2432.57 37.55 o 2 3 0 182.81 183.02 10.68 o 4 3 0 169.48 222.93 22.94 o 5 3 0 132.13 127.57 18.38 o 6 3 0 68.01 39.75 21.21 o 7 3 0 4.56 14.30 24.98 o 8 3 0 0.79 -10.84 30.48 o 9 3 0 0.18 -6.91 53.89 o 0 4 0 114.67 137.31 9.58 o 1 4 0 74.86 71.95 5.18 o 2 4 0 532.13 382.70 8.80 o 5 4 0 3.84 -0.63 17.91 o 6 4 0 25.96 28.75 23.88 o 8 4 0 2.13 -27.34 27.34 o 9 4 0 1.06 -19.01 60.96 o 1 5 0 2071.81 1487.76 23.72 o 2 5 0 302.41 265.03 8.17 o 3 5 0 1176.00 1649.73 35.51 o 4 5 0 533.38 546.09 16.02 o 5 5 0 177.36 179.41 21.99 o 6 5 0 294.13 351.75 29.85 o 8 5 0 63.45 64.88 30.48 o 9 5 0 0.47 16.81 31.42 o 1 6 0 213.21 226.86 7.86 o 2 6 0 436.90 424.49 11.31 o 5 6 0 201.34 171.87 14.61 o 6 6 0 6.76 50.43 25.76 o 7 6 0 90.20 126.00 31.11 o 8 6 0 16.52 24.67 32.05 o 9 6 0 16.31 30.16 34.25 o 1 7 0 12805.01 13858.91 234.55 o 2 7 0 0.21 -4.40 4.40 o 3 7 0 2878.69 2754.63 51.37 o 4 7 0 0.82 1.41 10.05 o 5 7 0 859.53 707.43 31.58 o 6 7 0 11.01 15.55 26.39 o 7 7 0 22.70 -19.95 33.78 o 8 7 0 7.22 8.48 33.62 o 1 8 0 32.41 27.49 7.38 o 2 8 0 565.22 498.17 13.20 o 4 8 0 38.64 25.92 10.21 o 5 8 0 180.97 195.28 17.75 o 6 8 0 0.02 5.34 19.64 o 8 8 0 7.86 74.62 35.19 o 1 9 0 1850.00 1379.98 31.26 o 2 9 0 296.43 284.20 11.47 o 3 9 0 171.50 230.78 12.10 o 4 9 0 373.83 343.74 15.55 o 5 9 0 236.64 253.72 23.25 o 6 9 0 308.33 309.02 25.14 o 8 9 0 17.20 43.20 35.51 o 1 10 0 2.12 1.73 9.58 o 2 10 0 461.10 546.40 16.18 o 5 10 0 264.43 299.44 24.82 o 8 10 0 0.17 -15.24 37.08 o 1 11 0 104.35 106.67 15.87 o 2 11 0 435.10 379.87 17.28 o 4 11 0 531.46 643.80 27.65 o 5 11 0 37.16 24.19 21.52 o 6 11 0 269.75 296.14 27.02 o 7 11 0 12.66 21.37 24.19 o 8 11 0 19.62 12.57 38.33 o 0 12 0 3350.76 4481.33 149.56 o 1 12 0 309.40 301.48 20.11 o 2 12 0 1215.91 906.16 30.48 o 3 12 0 1039.56 1291.85 40.38 o 4 12 0 116.64 144.53 23.72 o 5 12 0 674.43 595.73 43.67 o 7 12 0 362.28 361.18 32.05 o 1 13 0 2075.51 1998.81 112.80 o 2 13 0 37.11 10.84 17.28 o 4 13 0 51.97 76.82 23.57 o 5 13 0 262.33 252.93 27.49 o 6 13 0 0.18 32.52 25.14 o 1 14 0 0.17 -15.55 18.38 o 2 14 0 44.52 73.52 17.44 o 5 14 0 68.95 52.63 24.67 o 6 14 0 79.18 98.19 27.49 o 7 14 0 60.63 126.00 30.01 o 1 15 0 276.51 282.47 21.37 o 2 15 0 28.96 37.55 19.48 o 5 15 0 0.69 27.34 25.29 o 6 15 0 163.10 178.31 29.54 o 0 16 0 1058.24 1249.59 68.97 o 1 16 0 28.96 32.05 18.54 o 2 16 0 216.48 168.41 22.78 o 5 16 0 131.77 55.14 26.86 o 6 16 0 15.92 58.60 35.98 o 1 17 0 475.60 442.09 27.18 o 2 17 0 36.24 29.85 21.84 o 3 17 0 601.24 495.34 40.22 o 5 17 0 22.41 34.72 28.12 o 6 17 0 37.55 48.23 30.32 o 0 18 0 62.11 56.56 30.01 o 1 18 0 2.87 -21.21 23.88 o 2 18 0 96.27 97.40 23.72 o 3 18 0 2.41 32.83 26.71 o 4 18 0 52.70 83.42 29.69 o 5 18 0 67.51 35.98 29.69 o 1 19 0 275.82 325.83 28.12 o 2 19 0 25.72 19.79 23.25 o 3 19 0 9.14 -4.56 27.18 o 4 19 0 29.94 51.69 30.48 o 5 19 0 40.74 45.72 30.63 o 1 20 0 4.87 8.80 23.57 o 2 20 0 128.54 98.03 31.11 o 3 20 0 11.37 40.38 30.32 o 1 21 0 49.93 48.86 32.36 o 2 21 0 2.57 24.51 30.95 o 0 22 0 1574.32 1982.94 123.01 o 1 22 0 68.64 56.40 33.62 o 2 22 0 1420.60 1135.38 56.40 o -9 1 1 4.75 31.58 53.73 o -8 1 1 636.68 923.60 104.32 o -7 1 1 20.03 32.36 31.73 o -6 1 1 1289.70 1883.18 89.86 o -5 1 1 188.40 166.21 16.34 o -3 1 1 111.02 155.06 11.63 o -2 1 1 1925.47 1875.33 32.05 o -1 1 1 1211.36 819.92 15.08 o 1 1 1 619.43 394.64 7.86 o 2 1 1 1647.96 1268.44 27.96 o 4 1 1 555.53 749.06 27.18 o 5 1 1 91.26 93.95 24.35 o 7 1 1 14.19 41.79 42.57 o 8 1 1 14.38 98.19 48.70 o 9 1 1 5.20 46.50 90.02 o -9 2 1 8.19 6.91 55.77 o -8 2 1 14.23 18.22 45.56 o -7 2 1 26.48 52.31 24.04 o -6 2 1 164.00 214.60 24.82 o -5 2 1 247.17 301.79 31.11 o -3 2 1 1541.05 1395.85 28.91 o -2 2 1 1067.63 863.59 17.44 o -1 2 1 9408.26 10356.48 159.46 o 0 2 1 103.92 127.88 6.91 o 1 2 1 8765.49 9608.36 138.41 o 2 2 1 1157.89 944.97 18.54 o 3 2 1 479.79 515.29 16.81 o 5 2 1 373.06 410.98 19.79 o 6 2 1 22.51 36.45 21.05 o 7 2 1 27.58 65.67 43.99 o 8 2 1 7.16 61.74 53.26 o 9 2 1 3.16 -3.46 92.06 o -9 3 1 86.78 24.04 56.40 o -8 3 1 3.64 -25.29 25.29 o -6 3 1 15.57 2.98 19.01 o -5 3 1 1079.91 910.88 34.09 o -3 3 1 194.36 257.18 10.05 o -2 3 1 250.23 276.50 14.45 o -1 3 1 396.69 363.85 8.80 o 0 3 1 3.59 -3.61 3.61 o 1 3 1 506.68 419.93 8.95 o 2 3 1 896.08 780.64 22.47 o 3 3 1 700.01 644.59 17.28 o 4 3 1 0.92 -5.97 11.63 o 5 3 1 47.81 54.51 15.87 o 6 3 1 40.60 54.51 19.17 o 8 3 1 19.04 18.70 47.13 o 9 3 1 13.19 6.91 55.61 o -9 4 1 1.71 -16.34 60.33 o -8 4 1 21.34 38.18 28.12 o -7 4 1 3.87 -23.09 25.76 o -6 4 1 9.87 34.41 23.72 o -5 4 1 79.12 47.76 18.70 o -4 4 1 867.17 877.89 21.37 o -3 4 1 1257.02 1187.53 24.82 o -2 4 1 5255.00 4660.43 77.45 o -1 4 1 7790.93 7719.99 118.93 o 0 4 1 5.55 0.16 6.13 o 1 4 1 4857.91 4236.57 61.11 o 2 4 1 2120.73 1759.70 30.16 o 4 4 1 119.90 104.32 14.61 o 5 4 1 179.74 203.45 21.21 o 6 4 1 2.15 9.58 19.64 o 8 4 1 4.69 -11.00 26.24 o 9 4 1 2.87 20.11 61.11 o -9 5 1 1.20 16.97 47.76 o -8 5 1 38.55 62.06 30.48 o -7 5 1 11.09 3.61 27.65 o -6 5 1 39.69 30.16 24.35 o -5 5 1 134.81 144.38 13.04 o -3 5 1 1153.31 1706.28 38.18 o -2 5 1 30.17 28.59 5.81 o -1 5 1 3446.46 3082.34 49.02 o 0 5 1 1365.88 2146.01 35.98 o 1 5 1 7519.46 7501.31 107.14 o 2 5 1 13.50 0.31 5.34 o 3 5 1 3726.21 5210.13 98.19 o 5 5 1 280.76 294.41 32.68 o 7 5 1 26.35 41.16 27.96 o 8 5 1 24.45 61.74 30.32 o 9 5 1 1.60 69.12 32.21 o -9 6 1 0.01 3.14 34.09 o -8 6 1 12.53 -19.79 31.89 o -7 6 1 5.03 18.54 30.32 o -6 6 1 321.85 474.76 29.06 o -5 6 1 100.42 77.61 13.04 o -4 6 1 702.54 690.93 19.79 o -2 6 1 981.19 646.00 16.18 o 1 6 1 1795.81 1322.64 24.51 o 2 6 1 1014.23 692.82 16.02 o 3 6 1 4556.58 5889.44 111.86 o 4 6 1 187.78 204.23 11.31 o 5 6 1 996.68 879.61 37.39 o 7 6 1 341.72 449.94 56.40 o 8 6 1 7.96 36.76 35.66 o -8 7 1 1.96 15.87 34.56 o -7 7 1 171.36 219.94 35.03 o -6 7 1 13.25 17.75 18.54 o -5 7 1 804.68 714.34 25.61 o -4 7 1 17.52 14.30 10.05 o -2 7 1 69.06 66.61 7.86 o -1 7 1 632.28 569.65 16.81 o 0 7 1 130.28 186.17 8.33 o 1 7 1 0.26 -5.97 5.97 o 2 7 1 133.25 121.91 8.17 o 3 7 1 73.85 69.44 8.33 o 4 7 1 228.45 293.78 13.35 o 5 7 1 1.34 -13.20 13.20 o 6 7 1 127.36 143.12 28.28 o 7 7 1 0.00 48.70 29.85 o 8 7 1 0.04 23.41 34.41 o -8 8 1 6.08 72.27 35.51 o -7 8 1 3.00 -15.55 23.72 o -6 8 1 5.78 6.91 20.11 o -5 8 1 22.90 35.03 15.71 o -4 8 1 5.34 13.82 11.94 o -3 8 1 682.51 712.61 19.01 o -2 8 1 46.40 11.78 7.86 o -1 8 1 4288.96 4009.56 79.02 o 1 8 1 3212.98 2651.72 56.71 o 2 8 1 25.49 17.91 7.07 o 3 8 1 890.16 715.76 19.01 o 5 8 1 451.01 417.73 19.64 o 7 8 1 125.84 178.15 46.03 o -8 9 1 15.50 29.06 35.82 o -7 9 1 2.30 -23.72 23.72 o -6 9 1 30.13 38.18 21.37 o -5 9 1 7.71 38.02 20.42 o -2 9 1 107.07 102.12 9.90 o -1 9 1 585.50 525.03 16.81 o 0 9 1 117.68 167.00 13.35 o 1 9 1 912.25 714.81 24.35 o 2 9 1 550.68 450.41 13.82 o 3 9 1 376.92 402.34 14.14 o 4 9 1 485.83 522.84 18.22 o 5 9 1 80.76 64.88 19.01 o 6 9 1 240.56 292.05 24.67 o 8 9 1 99.09 102.43 37.86 o -8 10 1 70.00 113.11 55.61 o -7 10 1 0.09 -14.45 22.47 o -6 10 1 300.01 401.71 31.58 o -5 10 1 15.97 3.77 22.15 o -4 10 1 452.56 490.79 21.21 o -2 10 1 464.85 413.34 15.40 o -1 10 1 0.90 -2.67 9.74 o 0 10 1 680.33 1010.48 30.79 o 1 10 1 5.72 17.28 9.90 o 2 10 1 0.11 -10.53 10.53 o 3 10 1 3.36 16.34 10.37 o 5 10 1 13.80 1.41 20.42 o 6 10 1 20.85 40.53 22.15 o 7 10 1 0.04 70.38 41.47 o 8 10 1 11.40 46.35 41.79 o -8 11 1 3.09 -29.69 29.69 o -7 11 1 15.14 44.77 24.98 o -6 11 1 13.99 14.45 22.94 o -5 11 1 148.05 156.63 23.72 o -4 11 1 353.34 555.04 26.55 o -3 11 1 2154.21 1852.70 44.93 o -2 11 1 1468.52 1127.84 28.44 o -1 11 1 3508.43 2528.56 67.87 o 1 11 1 3911.38 3175.19 89.39 o 2 11 1 3281.42 2616.06 53.41 o 3 11 1 1846.01 1519.18 33.31 o 4 11 1 1708.87 1467.80 41.00 o 5 11 1 291.10 307.29 26.39 o 6 11 1 622.81 671.77 49.33 o 8 11 1 45.04 98.66 59.38 o -8 12 1 0.93 4.56 27.34 o -6 12 1 100.04 134.01 26.24 o -5 12 1 305.08 276.50 27.02 o -4 12 1 45.13 82.48 21.05 o -2 12 1 8.42 -11.47 15.71 o -1 12 1 1085.45 1065.47 38.49 o 0 12 1 80.90 125.84 17.44 o 1 12 1 635.21 745.29 41.95 o 2 12 1 87.91 66.61 13.82 o 5 12 1 183.61 157.89 24.67 o 7 12 1 20.53 20.42 25.92 o -6 13 1 9.71 26.55 24.67 o -5 13 1 1468.65 1251.00 51.69 o -4 13 1 13.50 15.87 22.47 o -3 13 1 1761.27 2095.74 60.80 o -2 13 1 219.15 207.85 19.48 o -1 13 1 3953.06 3881.21 93.79 o 1 13 1 2408.81 2997.35 141.71 o 2 13 1 1012.05 823.37 26.86 o 3 13 1 473.64 607.83 25.92 o 4 13 1 471.09 478.85 31.26 o 5 13 1 182.73 158.36 26.08 o -6 14 1 374.53 408.62 43.67 o -5 14 1 422.03 433.76 33.78 o -4 14 1 983.92 908.68 43.05 o -3 14 1 805.87 737.44 31.73 o -2 14 1 1563.27 1083.38 35.19 o -1 14 1 975.12 1177.17 69.44 o 0 14 1 175.12 301.32 22.62 o 1 14 1 1661.64 1523.42 46.19 o 2 14 1 63.89 38.33 16.81 o 3 14 1 2400.28 1859.30 55.30 o 4 14 1 125.77 171.24 26.39 o 5 14 1 841.55 749.69 39.59 o 7 14 1 560.37 509.32 65.83 o -6 15 1 94.41 73.52 28.28 o -5 15 1 379.35 311.38 41.47 o -4 15 1 537.99 519.38 35.19 o -3 15 1 1431.09 1114.80 40.85 o -2 15 1 1605.73 1174.65 39.12 o -1 15 1 1161.42 1205.60 50.59 o 0 15 1 1882.85 2469.64 64.73 o 1 15 1 807.19 1110.24 45.40 o 2 15 1 2635.11 1914.92 57.81 o 3 15 1 330.74 499.11 27.34 o 4 15 1 1131.25 938.68 44.30 o 5 15 1 13.57 5.03 24.67 o 6 15 1 254.17 250.11 31.11 o 7 15 1 132.21 151.29 33.93 o -6 16 1 56.51 98.50 30.16 o -5 16 1 0.12 -25.45 25.45 o -4 16 1 256.20 335.26 31.89 o -3 16 1 112.76 115.16 22.62 o -2 16 1 405.64 361.81 26.55 o -1 16 1 694.40 709.16 29.22 o 0 16 1 11.87 18.22 18.22 o 1 16 1 588.34 609.56 34.41 o 2 16 1 6.76 -13.67 19.95 o 3 16 1 214.01 298.18 27.81 o 4 16 1 2.04 28.75 25.76 o 5 16 1 270.00 312.32 39.75 o 6 16 1 17.05 18.70 34.25 o -6 17 1 0.80 -28.44 28.44 o -5 17 1 49.44 17.28 27.81 o -4 17 1 68.19 94.26 28.12 o -2 17 1 119.14 116.26 23.25 o -1 17 1 0.60 11.31 19.32 o 1 17 1 0.95 15.24 19.17 o 2 17 1 91.38 70.22 22.15 o 4 17 1 4.01 6.13 26.39 o 5 17 1 8.62 52.00 28.12 o 6 17 1 0.07 30.79 29.54 o -5 18 1 22.31 0.47 29.06 o -4 18 1 84.61 109.03 29.69 o -3 18 1 25.82 16.81 26.39 o -2 18 1 468.05 435.80 29.69 o 0 18 1 964.96 1305.20 43.36 o 1 18 1 576.27 543.89 31.26 o 2 18 1 786.30 711.52 34.56 o 3 18 1 680.76 648.83 39.90 o 4 18 1 142.28 199.36 31.89 o 5 18 1 352.38 306.98 44.93 o -5 19 1 1.29 -24.98 29.69 o -4 19 1 0.96 2.36 30.01 o -3 19 1 0.48 21.68 27.65 o -2 19 1 27.42 54.20 23.72 o -1 19 1 151.66 131.97 26.55 o 0 19 1 37.66 9.43 24.04 o 1 19 1 139.91 144.38 24.67 o 2 19 1 233.24 221.36 25.76 o 3 19 1 44.26 75.72 29.38 o 4 19 1 249.78 245.86 34.56 o 5 19 1 6.71 -9.43 29.85 o -4 20 1 175.20 136.52 33.78 o -3 20 1 55.81 79.18 30.48 o -2 20 1 58.24 44.93 27.81 o -1 20 1 80.79 89.71 26.86 o 1 20 1 12.33 19.48 23.72 o 2 20 1 19.68 33.93 28.75 o 3 20 1 36.13 46.82 37.23 o 4 20 1 0.02 31.89 38.80 o -3 21 1 163.31 202.98 44.93 o -2 21 1 85.98 38.65 34.72 o -1 21 1 0.35 -30.01 30.01 o 0 21 1 95.55 141.39 36.92 o 1 21 1 14.30 -6.60 27.02 o 2 21 1 17.75 7.54 34.88 o -2 22 1 0.21 65.83 40.38 o 0 22 1 92.00 88.92 38.18 o 1 22 1 109.98 126.62 33.78 o 2 22 1 0.33 52.16 32.21 o 0 23 1 43.85 32.52 46.66 o -9 0 2 240.78 291.58 132.91 o -5 0 2 1611.10 1395.54 49.49 o -4 0 2 389.15 436.27 36.29 o -3 0 2 840.69 779.38 25.61 o -2 0 2 5739.15 6110.17 133.69 o -1 0 2 5590.77 5601.94 106.99 o 1 0 2 1256.32 1002.00 21.84 o 2 0 2 8131.77 9607.42 334.94 o 3 0 2 2504.71 1853.49 82.79 o 4 0 2 4226.74 4413.78 189.15 o 5 0 2 251.84 196.06 55.30 o 6 0 2 2752.40 2942.99 229.05 o 7 0 2 404.16 302.74 107.61 o 8 0 2 715.73 524.09 136.36 o 9 0 2 190.22 -18.85 125.52 o -9 1 2 14.61 -41.95 50.27 o -8 1 2 544.80 556.61 50.74 o -5 1 2 77.03 98.19 11.31 o -4 1 2 575.09 860.60 20.89 o -3 1 2 3205.87 2933.57 52.94 o -2 1 2 474.41 417.89 9.58 o -1 1 2 2454.24 2127.95 37.86 o 1 1 2 4696.40 4511.97 66.14 o 2 1 2 4737.18 4703.48 95.83 o 5 1 2 659.80 705.23 35.51 o 6 1 2 90.25 123.64 32.83 o 8 1 2 341.71 366.68 93.32 o 9 1 2 25.85 47.92 92.22 o -9 2 2 14.57 27.34 51.84 o -7 2 2 0.87 47.92 32.99 o -5 2 2 0.98 5.18 10.53 o -4 2 2 2124.55 1896.54 38.96 o -2 2 2 7285.21 7235.18 111.39 o -1 2 2 2063.59 1832.59 30.95 o 0 2 2 923.23 1434.34 22.31 o 1 2 2 3809.05 3333.39 47.44 o 2 2 2 197.32 224.97 6.91 o 3 2 2 210.95 210.67 10.53 o 4 2 2 663.89 603.11 27.18 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