#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/94/2219431.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2219431_Fobs loop_ _publ_author_name 'Chu, Chao-Xia' 'Zhou, Hu' 'Liu, Lang' 'Yuan, Ai-Hua' _publ_section_title ; Tris[tris(ethane-1,2-diamine)cobalt(II)] bis[octacyanidomolybdate(V)] dihydrate ; _journal_coeditor_code SI2095 _journal_issue 9 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1154 _journal_page_last m1155 _journal_volume 64 _journal_year 2008 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 94.138 _cell_angle_gamma 90.000 _cell_length_a 9.2113 _cell_length_b 30.5439 _cell_length_c 11.4022 _exptl_crystal_F_000 1398.00 _reflns_d_resolution_high 0.8107 _[local]_cod_data_source_file si2095Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' G0353 in P21/n' _shelx_refln_list_code 4 _shelx_F_calc_maximum 336.36 _shelx_F_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 16029.03 15486.89 199.00 o 4 0 0 231.58 379.86 312.47 o 6 0 0 3183.88 3200.46 324.96 o 8 0 0 86.51 157.91 284.78 o 10 0 0 316.74 307.54 30.97 o 2 1 0 16003.62 16067.00 181.49 o 3 1 0 59.24 54.65 26.53 o 4 1 0 23495.31 22187.10 476.31 o 5 1 0 2310.98 2094.63 31.34 o 6 1 0 90.80 131.04 35.95 o 7 1 0 1548.39 1690.70 174.81 o 8 1 0 1922.04 2054.05 97.90 o 9 1 0 109.62 213.68 47.94 o 10 1 0 34.94 57.05 142.64 o 11 1 0 77.96 92.75 35.91 o 2 2 0 125.00 159.08 49.93 o 3 2 0 9216.69 9015.38 73.95 o 4 2 0 3377.68 3298.90 114.34 o 5 2 0 4742.43 4583.72 48.60 o 6 2 0 9297.37 9291.18 148.39 o 7 2 0 1029.23 1192.27 102.12 o 8 2 0 258.03 268.36 42.06 o 9 2 0 609.41 665.25 75.65 o 10 2 0 193.35 237.65 60.45 o 11 2 0 35.22 42.76 138.25 o 2 3 0 2600.67 2641.67 113.50 o 3 3 0 170.73 225.82 32.99 o 4 3 0 247.07 388.59 161.36 o 5 3 0 5892.92 6063.68 169.94 o 6 3 0 1627.84 1549.28 58.62 o 7 3 0 422.26 809.21 147.53 o 8 3 0 210.41 321.64 78.61 o 9 3 0 1.01 3.10 9.93 o 10 3 0 3.29 3.63 39.35 o 11 3 0 340.77 331.98 87.66 o 1 4 0 14244.29 15018.33 127.48 o 2 4 0 7238.09 7110.63 92.87 o 3 4 0 11246.63 11302.79 186.59 o 4 4 0 3328.39 3735.99 185.70 o 5 4 0 7196.86 6916.80 78.70 o 6 4 0 5171.48 5545.53 147.79 o 7 4 0 1804.25 1957.53 197.16 o 8 4 0 1241.58 1212.93 123.13 o 9 4 0 189.94 184.93 75.18 o 10 4 0 306.35 241.70 79.97 o 11 4 0 0.38 19.92 166.23 o 1 5 0 1243.16 1705.19 164.39 o 2 5 0 275.61 360.36 73.82 o 3 5 0 221.67 317.12 79.88 o 4 5 0 12167.48 11872.47 289.55 o 5 5 0 7302.56 6861.70 280.37 o 6 5 0 179.65 279.11 71.22 o 7 5 0 4001.39 3846.19 144.51 o 8 5 0 204.43 261.89 58.12 o 9 5 0 126.93 139.01 14.42 o 10 5 0 164.84 173.56 61.37 o 11 5 0 32.07 129.84 189.93 o 0 6 0 113139.65 110526.81 350.08 o 1 6 0 315.85 429.04 57.27 o 2 6 0 875.58 831.29 10.12 o 3 6 0 4.50 90.62 36.13 o 4 6 0 2170.27 2072.57 39.19 o 5 6 0 5397.82 5210.14 201.56 o 6 6 0 5284.95 5068.50 77.37 o 7 6 0 5330.03 5043.41 85.22 o 8 6 0 129.90 139.42 43.56 o 9 6 0 287.05 258.05 37.02 o 10 6 0 207.71 220.50 55.04 o 11 6 0 157.73 126.41 115.20 o 1 7 0 253.50 361.76 136.63 o 2 7 0 6326.78 6395.40 97.58 o 3 7 0 11824.65 11298.43 247.51 o 4 7 0 17435.83 17844.76 203.29 o 5 7 0 20655.68 19861.13 201.53 o 6 7 0 55.58 166.73 64.84 o 7 7 0 1859.63 1758.90 30.51 o 8 7 0 1832.88 2153.02 85.67 o 9 7 0 1.28 73.12 76.45 o 10 7 0 231.52 202.82 36.52 o 11 7 0 192.11 251.18 51.17 o 0 8 0 83.14 595.89 172.04 o 1 8 0 216.89 268.61 36.55 o 2 8 0 1076.93 1631.97 149.98 o 3 8 0 9759.30 9424.72 77.02 o 4 8 0 844.61 1259.96 122.09 o 5 8 0 65.26 83.44 48.05 o 6 8 0 5288.02 5076.26 112.66 o 7 8 0 3933.79 3706.85 76.04 o 8 8 0 250.73 338.31 61.14 o 9 8 0 1251.37 1438.86 113.83 o 10 8 0 664.55 736.82 89.49 o 11 8 0 81.42 71.04 24.11 o 1 9 0 45812.20 44721.06 433.75 o 2 9 0 2582.51 2618.25 106.71 o 3 9 0 492.14 502.63 28.54 o 4 9 0 652.89 614.16 78.77 o 5 9 0 9125.34 9696.98 540.24 o 6 9 0 15042.89 13659.73 173.46 o 7 9 0 932.74 1350.15 119.20 o 8 9 0 435.36 454.85 51.09 o 9 9 0 634.94 627.90 62.33 o 10 9 0 133.01 212.92 98.92 o 11 9 0 686.39 695.51 72.14 o 0 10 0 4458.98 4596.29 110.86 o 1 10 0 753.98 747.78 47.71 o 2 10 0 810.55 802.27 55.50 o 3 10 0 14316.89 13445.03 742.23 o 4 10 0 7338.17 6988.85 129.00 o 5 10 0 2973.05 3250.44 91.92 o 6 10 0 6895.46 6532.44 28.25 o 7 10 0 1325.33 1243.90 102.04 o 8 10 0 161.65 203.81 79.36 o 9 10 0 1214.47 1308.07 58.57 o 10 10 0 1076.08 959.82 62.19 o 1 11 0 8650.65 8646.74 87.33 o 2 11 0 15735.89 15446.47 110.07 o 3 11 0 2020.92 2042.80 42.65 o 4 11 0 863.21 878.52 67.23 o 5 11 0 5654.26 5457.82 103.19 o 6 11 0 5624.02 5538.20 124.46 o 7 11 0 4396.32 4234.28 80.39 o 8 11 0 2243.21 1970.32 187.58 o 9 11 0 739.88 977.20 170.89 o 10 11 0 14.58 88.59 61.20 o 0 12 0 9589.32 9285.97 66.48 o 1 12 0 1180.74 1123.50 14.22 o 2 12 0 4534.20 4349.17 106.04 o 3 12 0 3707.18 3591.49 57.49 o 4 12 0 581.56 590.74 33.31 o 5 12 0 2132.59 2123.71 80.48 o 6 12 0 3564.05 3394.10 109.81 o 7 12 0 2383.44 2331.70 225.86 o 8 12 0 481.78 667.38 141.30 o 9 12 0 26.21 44.18 94.61 o 10 12 0 957.13 1174.86 117.58 o 1 13 0 1072.02 1034.84 28.58 o 2 13 0 9924.43 9603.03 111.68 o 3 13 0 4303.60 4340.13 93.15 o 4 13 0 966.25 918.15 11.86 o 5 13 0 4434.31 4241.45 94.65 o 6 13 0 40.52 68.25 34.53 o 7 13 0 190.23 236.24 110.83 o 8 13 0 1384.46 1359.18 275.61 o 9 13 0 1750.46 1695.41 210.42 o 10 13 0 11.14 7.16 82.18 o 0 14 0 860.27 1034.21 167.28 o 1 14 0 5384.05 5251.70 122.44 o 2 14 0 8.69 119.04 48.31 o 3 14 0 3381.93 3678.96 145.94 o 4 14 0 2144.44 1932.09 212.12 o 5 14 0 201.37 279.85 38.54 o 6 14 0 5495.19 5235.45 124.39 o 7 14 0 2233.25 2175.16 145.51 o 8 14 0 686.43 647.24 13.67 o 9 14 0 2.81 54.21 69.72 o 10 14 0 820.63 754.76 49.63 o 1 15 0 5913.55 5895.83 62.40 o 2 15 0 2041.28 1974.10 133.14 o 3 15 0 549.30 554.09 70.88 o 4 15 0 19.11 92.94 43.63 o 5 15 0 979.95 1004.76 77.39 o 6 15 0 967.30 1099.25 52.70 o 7 15 0 83.95 153.10 40.77 o 8 15 0 950.58 962.94 132.73 o 9 15 0 2383.84 2522.56 90.37 o 10 15 0 17.26 67.39 59.83 o 0 16 0 87.48 165.50 112.78 o 1 16 0 2.98 18.06 15.64 o 2 16 0 1650.48 1657.41 155.90 o 3 16 0 4637.39 4629.91 56.66 o 4 16 0 5207.83 5245.07 87.17 o 5 16 0 691.19 885.37 97.51 o 6 16 0 2110.84 2037.08 39.84 o 7 16 0 225.30 370.67 92.06 o 8 16 0 130.72 217.74 89.44 o 9 16 0 140.62 131.52 126.93 o 10 16 0 979.02 799.87 36.24 o 1 17 0 191.64 209.25 25.35 o 2 17 0 8143.07 7859.20 125.78 o 3 17 0 80.99 120.01 45.94 o 4 17 0 6.37 16.67 140.69 o 5 17 0 61.39 49.44 9.24 o 6 17 0 1032.97 1311.67 80.61 o 7 17 0 257.51 355.54 81.26 o 8 17 0 1993.31 1655.95 89.61 o 9 17 0 331.29 395.19 49.06 o 10 17 0 21.47 48.38 148.94 o 0 18 0 10391.79 9860.75 275.59 o 1 18 0 242.57 241.13 14.87 o 2 18 0 1977.08 2049.63 114.45 o 3 18 0 194.61 256.64 28.82 o 4 18 0 719.58 709.08 66.38 o 5 18 0 285.91 323.69 36.06 o 6 18 0 503.80 616.47 112.42 o 7 18 0 236.94 260.18 68.07 o 8 18 0 2380.14 2624.90 87.00 o 9 18 0 143.89 246.30 57.34 o 1 19 0 22.21 148.31 43.12 o 2 19 0 167.64 269.51 47.53 o 3 19 0 4440.61 4195.00 107.61 o 4 19 0 202.63 284.22 49.36 o 5 19 0 1588.88 1718.26 161.86 o 6 19 0 11.25 21.33 54.48 o 7 19 0 1182.99 1134.05 41.04 o 8 19 0 832.05 810.96 177.38 o 9 19 0 751.99 898.89 73.38 o 0 20 0 6.71 81.10 70.72 o 1 20 0 1038.93 1021.89 100.82 o 2 20 0 50.22 101.34 40.53 o 3 20 0 2129.21 1997.52 52.00 o 4 20 0 22.40 25.59 28.87 o 5 20 0 2125.11 2112.79 140.06 o 6 20 0 333.75 387.95 48.73 o 7 20 0 3039.12 2702.54 188.92 o 8 20 0 154.35 216.34 78.68 o 9 20 0 323.58 387.24 118.34 o 1 21 0 1796.77 1733.11 42.98 o 2 21 0 269.98 364.96 57.30 o 3 21 0 0.20 3.89 8.65 o 4 21 0 67.39 88.15 43.57 o 5 21 0 689.11 651.18 30.28 o 6 21 0 25.21 90.76 171.01 o 7 21 0 108.36 134.01 33.53 o 8 21 0 302.59 312.90 48.40 o 9 21 0 1899.46 1909.37 113.19 o 0 22 0 6.39 140.65 141.91 o 1 22 0 1.74 6.72 23.74 o 2 22 0 463.51 526.04 58.62 o 3 22 0 145.37 204.99 50.03 o 4 22 0 7136.38 6650.34 96.95 o 5 22 0 1115.76 1071.72 34.61 o 6 22 0 1109.72 1373.49 75.92 o 7 22 0 911.09 882.16 37.33 o 8 22 0 76.35 106.50 42.68 o 9 22 0 446.61 488.53 72.05 o 1 23 0 1555.96 1893.67 108.59 o 2 23 0 754.45 783.74 36.17 o 3 23 0 18.70 45.06 62.52 o 4 23 0 42.37 143.00 97.02 o 5 23 0 95.33 93.36 16.32 o 6 23 0 1623.97 1549.93 279.94 o 7 23 0 355.11 465.93 127.69 o 8 23 0 1414.68 1673.02 157.00 o 0 24 0 2503.30 2538.30 66.68 o 1 24 0 441.96 436.71 55.08 o 2 24 0 24.10 38.79 30.20 o 3 24 0 1158.36 1137.45 81.53 o 4 24 0 2877.91 2797.14 42.94 o 5 24 0 95.37 157.71 107.15 o 6 24 0 272.16 285.84 48.47 o 7 24 0 742.07 696.07 29.27 o 8 24 0 474.41 587.41 100.85 o 1 25 0 60.80 72.13 13.13 o 2 25 0 5.26 37.38 40.77 o 3 25 0 6463.76 6224.12 91.91 o 4 25 0 27.18 29.36 36.78 o 5 25 0 2720.01 2844.25 76.75 o 6 25 0 686.03 587.56 45.71 o 7 25 0 391.90 481.70 150.08 o 8 25 0 605.36 611.45 46.49 o 0 26 0 750.31 864.66 156.01 o 1 26 0 575.28 656.51 56.38 o 2 26 0 1731.17 1691.09 71.48 o 3 26 0 797.81 827.36 43.05 o 4 26 0 63.57 132.91 53.56 o 5 26 0 181.97 332.48 76.42 o 6 26 0 20.07 52.55 52.52 o 7 26 0 1631.92 1621.53 100.54 o 8 26 0 77.28 96.38 25.62 o 1 27 0 861.74 974.71 102.90 o 2 27 0 1455.24 1576.81 69.15 o 3 27 0 366.69 385.15 36.51 o 4 27 0 214.88 435.33 152.04 o 5 27 0 881.98 858.27 36.25 o 6 27 0 60.83 107.91 30.29 o 7 27 0 30.40 76.07 63.92 o 0 28 0 1076.27 1097.39 320.65 o 1 28 0 352.49 355.59 30.89 o 2 28 0 95.17 86.54 35.32 o 3 28 0 312.02 295.23 47.15 o 4 28 0 2096.55 1945.87 232.60 o 5 28 0 357.79 332.98 63.46 o 6 28 0 1456.04 1345.95 188.03 o 7 28 0 292.60 483.40 171.02 o 1 29 0 1372.27 1346.94 107.26 o 2 29 0 850.75 846.97 55.05 o 3 29 0 579.96 607.82 83.80 o 4 29 0 199.66 259.38 35.01 o 5 29 0 64.78 75.95 25.41 o 6 29 0 469.54 495.31 34.06 o 7 29 0 36.23 41.34 37.72 o 0 30 0 3446.42 3144.25 194.13 o 1 30 0 515.79 431.76 67.09 o 2 30 0 62.03 71.51 19.37 o 3 30 0 1074.09 997.86 23.89 o 4 30 0 140.40 121.02 52.37 o 5 30 0 259.31 282.48 86.46 o 6 30 0 27.55 130.83 62.78 o 1 31 0 1944.59 1964.31 66.67 o 2 31 0 83.57 102.29 38.49 o 3 31 0 134.56 123.12 100.59 o 4 31 0 337.89 387.82 41.49 o 5 31 0 1078.33 1312.24 114.56 o 6 31 0 573.58 472.93 52.18 o 0 32 0 1421.17 1327.73 116.35 o 1 32 0 492.63 613.90 102.29 o 2 32 0 2429.82 2510.55 104.54 o 3 32 0 223.47 232.38 23.97 o 4 32 0 26.40 61.00 89.82 o 5 32 0 207.70 212.08 82.29 o 1 33 0 1079.79 1039.15 112.23 o 2 33 0 1357.72 1304.36 111.15 o 3 33 0 191.45 211.30 25.51 o 4 33 0 1028.96 916.67 118.97 o 5 33 0 224.71 232.95 44.83 o 0 34 0 957.21 1118.96 81.89 o 1 34 0 1.43 11.87 25.66 o 2 34 0 237.07 264.94 37.71 o 3 34 0 442.23 380.68 60.38 o 4 34 0 430.91 466.63 56.97 o 1 35 0 886.16 960.12 94.27 o 2 35 0 921.83 914.46 109.38 o 3 35 0 298.29 310.80 72.77 o 4 35 0 1059.90 1017.80 84.10 o 0 36 0 539.44 640.78 209.72 o 1 36 0 262.34 270.07 32.12 o 2 36 0 186.58 276.85 70.69 o 3 36 0 792.74 751.67 98.78 o 1 37 0 264.40 257.69 82.26 o 2 37 0 28.52 89.33 181.38 o -11 0 1 316.44 404.47 271.97 o -9 0 1 2803.09 3075.84 273.96 o -7 0 1 5.60 15.36 31.06 o -5 0 1 11.84 247.46 225.62 o -3 0 1 132.80 256.26 62.53 o 3 0 1 3381.88 3361.93 167.91 o 5 0 1 3311.07 3645.07 223.51 o 7 0 1 10805.27 11783.83 264.76 o 9 0 1 22.87 33.23 182.66 o 11 0 1 2116.13 1788.74 26.32 o -11 1 1 521.99 783.51 84.89 o -10 1 1 638.02 587.05 49.95 o -9 1 1 268.51 320.82 49.02 o -8 1 1 879.04 1064.66 100.49 o -7 1 1 1002.34 1053.15 39.97 o -6 1 1 1055.84 1706.21 156.72 o -5 1 1 6370.68 5891.60 61.08 o -4 1 1 1029.01 1108.98 19.18 o -3 1 1 229.77 385.61 99.85 o -2 1 1 55.72 84.51 42.02 o 1 1 1 3620.00 3600.98 69.13 o 2 1 1 4056.91 3849.54 113.20 o 3 1 1 1202.28 1218.04 80.30 o 4 1 1 29.51 44.42 49.16 o 5 1 1 926.02 914.22 39.26 o 6 1 1 16.69 24.62 26.44 o 7 1 1 1573.12 1828.40 105.13 o 8 1 1 9.23 91.86 118.14 o 9 1 1 1033.03 1020.22 95.44 o 10 1 1 788.26 764.90 134.70 o 11 1 1 485.98 741.25 105.94 o -11 2 1 352.56 440.67 183.67 o -10 2 1 1796.05 1561.54 115.08 o -9 2 1 1465.43 1629.44 110.96 o -8 2 1 5.34 37.29 65.46 o -7 2 1 2033.93 2127.04 163.79 o -6 2 1 3670.60 3557.18 112.49 o -5 2 1 2328.31 2504.34 125.20 o -4 2 1 10624.63 11314.59 389.98 o -3 2 1 16287.62 17280.78 280.30 o -2 2 1 14318.37 13918.87 83.99 o -1 2 1 6442.97 6826.42 115.18 o 1 2 1 4900.58 4854.35 67.94 o 2 2 1 1014.04 1041.42 79.66 o 3 2 1 11.43 145.18 53.60 o 4 2 1 7284.59 7093.86 72.70 o 5 2 1 374.96 399.31 97.94 o 6 2 1 10.06 90.10 50.25 o 7 2 1 628.99 602.93 70.75 o 8 2 1 2570.26 2701.27 98.97 o 9 2 1 319.69 295.19 62.53 o 10 2 1 1939.00 2269.10 143.68 o 11 2 1 1007.17 1102.13 163.79 o -11 3 1 0.62 9.21 104.29 o -10 3 1 1793.21 1978.90 88.08 o -9 3 1 52.78 110.92 67.69 o -8 3 1 1915.03 1934.68 95.44 o -7 3 1 682.23 712.34 195.36 o -6 3 1 18.81 70.08 90.22 o -5 3 1 0.50 13.97 15.66 o -4 3 1 2812.93 2573.40 68.29 o -3 3 1 10984.04 10856.78 80.37 o -2 3 1 2038.40 2301.96 180.29 o -1 3 1 7141.52 6981.12 31.02 o 1 3 1 4960.22 4885.72 64.89 o 2 3 1 2766.41 3158.40 173.59 o 3 3 1 1709.86 1955.69 87.78 o 4 3 1 9187.90 8890.60 161.30 o 5 3 1 1796.21 1840.84 76.06 o 6 3 1 10451.74 9821.19 143.30 o 7 3 1 231.74 246.82 25.58 o 8 3 1 1963.06 2257.93 206.78 o 9 3 1 35.54 75.33 41.69 o 10 3 1 642.45 613.18 179.80 o 11 3 1 6.26 8.80 40.41 o -11 4 1 1.42 32.61 82.34 o -10 4 1 1169.68 1217.16 87.51 o -9 4 1 799.13 684.43 86.64 o -8 4 1 614.38 658.30 56.62 o -7 4 1 558.73 630.22 70.86 o -6 4 1 4147.78 4352.36 119.18 o -5 4 1 594.94 597.96 214.60 o -4 4 1 6808.02 6555.85 131.02 o -3 4 1 40651.16 39525.16 245.83 o -2 4 1 384.75 531.32 56.99 o -1 4 1 3338.97 3426.78 60.91 o 0 4 1 1066.93 1056.37 53.72 o 1 4 1 25753.37 25395.77 135.80 o 2 4 1 2079.71 2305.79 210.43 o 3 4 1 2390.66 2528.95 88.25 o 4 4 1 8009.50 8031.80 142.57 o 5 4 1 287.23 286.30 63.63 o 6 4 1 4.85 107.37 151.37 o 7 4 1 24.81 96.14 80.10 o 8 4 1 888.40 948.43 88.83 o 9 4 1 146.38 184.37 34.23 o 10 4 1 1744.82 1505.57 64.26 o 11 4 1 807.72 928.30 114.56 o -11 5 1 660.60 734.46 64.10 o -10 5 1 1023.96 994.89 112.81 o -9 5 1 451.98 459.26 36.06 o -8 5 1 4497.20 4296.17 97.04 o -7 5 1 2626.74 2654.05 97.60 o -6 5 1 5133.60 5157.46 128.78 o -5 5 1 9708.51 9435.62 71.05 o -4 5 1 4819.07 4677.80 139.38 o -3 5 1 122.55 178.39 27.85 o -2 5 1 395.03 448.95 73.92 o -1 5 1 5105.95 5501.96 152.61 o 0 5 1 1850.57 1872.15 41.15 o 1 5 1 2.08 152.80 113.55 o 2 5 1 1449.09 1696.98 120.75 o 3 5 1 21745.37 20894.50 340.62 o 4 5 1 1014.28 1245.71 101.92 o 5 5 1 6489.85 6482.47 165.14 o 6 5 1 1441.64 1360.72 124.50 o 7 5 1 2544.19 2491.04 286.93 o 8 5 1 120.59 162.09 135.98 o 9 5 1 1252.26 1118.07 220.54 o 10 5 1 904.03 794.02 44.13 o 11 5 1 411.60 385.12 36.33 o -11 6 1 0.50 104.64 88.80 o -10 6 1 363.65 435.29 135.29 o -9 6 1 3062.90 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