#------------------------------------------------------------------------------
#$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $
#$Revision: 26848 $
#$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/94/2219491.hkl $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided by IUCr Journals, http://journals.iucr.org/.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_2219491_Fobs
loop_
_publ_author_name
'Kobayashi, Masayuki'
'Masaoka, Shigeyuki'
'Sakai, Ken'
_publ_section_title
;
Chlorido(dimethyl
sulfoxide-\kS)[2-(2-pyridyl)phenyl-\k^2^N,C^1^]platinum(II)
;
_journal_coeditor_code AT2633
_journal_issue 10
_journal_name_full 'Acta Crystallographica Section E'
_journal_page_first m1325
_journal_volume 64
_journal_year 2008
_space_group_IT_number 15
_symmetry_space_group_name_Hall '-C 2yc'
_symmetry_space_group_name_H-M 'C 1 2/c 1'
_cell_angle_alpha 90.000
_cell_angle_beta 124.512
_cell_angle_gamma 90.000
_cell_length_a 22.4139
_cell_length_b 10.0205
_cell_length_c 14.0574
_exptl_crystal_F_000 1744.00
_reflns_d_resolution_high 0.7800
_[local]_cod_data_source_file at2633Isup2.hkl
_[local]_cod_data_source_block I
#BEGIN Tags that were not found in dictionaries:
_shelx_title
' 070601_2 in C2/c 006 KENX'
_shelx_refln_list_code 4
_shelx_F_calc_maximum 1165.17
_shelx_F_squared_multiplier 1.000
#END Tags that were not found in dictionaries
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, y, -z+1/2'
'x+1/2, y+1/2, z'
'-x+1/2, y+1/2, -z+1/2'
'-x, -y, -z'
'x, -y, z-1/2'
'-x+1/2, -y+1/2, -z'
'x+1/2, -y+1/2, z-1/2'
loop_
_refln_index_h
_refln_index_k
_refln_index_l
_refln_F_squared_calc
_refln_F_squared_meas
_refln_F_squared_sigma
_refln_observed_status
2 0 0 2022.72 2079.96 75.81 o
4 0 0 118730.70 124696.25 2189.36 o
6 0 0 15047.21 16521.35 308.68 o
8 0 0 341535.88 350113.41 6076.70 o
10 0 0 2240.27 2297.06 78.92 o
12 0 0 75637.99 74357.41 1989.94 o
14 0 0 19726.15 20744.60 485.43 o
16 0 0 98518.52 96568.38 1898.90 o
18 0 0 39401.82 43087.07 935.63 o
20 0 0 76970.92 77607.66 2354.76 o
22 0 0 12819.04 12751.41 639.62 o
1 1 0 278809.41 279600.00 3939.81 o
3 1 0 123427.36 128429.69 1449.84 o
5 1 0 186779.84 193147.41 2166.66 o
7 1 0 147587.48 155518.94 1740.12 o
9 1 0 190596.94 191950.73 2142.83 o
11 1 0 46512.77 44229.91 555.24 o
13 1 0 99626.52 99847.34 1562.56 o
15 1 0 11619.33 11714.49 259.85 o
17 1 0 116010.24 114493.48 1806.72 o
19 1 0 23801.76 26368.68 530.06 o
21 1 0 46213.88 44234.66 1050.81 o
23 1 0 1003.69 1281.28 203.79 o
0 2 0 304809.25 343454.13 8130.33 o
2 2 0 1709.51 1162.66 59.35 o
4 2 0 169777.70 174151.06 2528.93 o
6 2 0 21755.65 21602.85 268.44 o
8 2 0 291579.22 298394.44 3332.79 o
10 2 0 16480.47 16415.98 217.28 o
12 2 0 255468.58 250285.28 3800.01 o
14 2 0 7414.68 7931.27 213.66 o
16 2 0 76089.96 73894.30 1200.77 o
18 2 0 11145.25 15763.17 570.13 o
20 2 0 66457.16 63684.89 1607.74 o
22 2 0 9248.86 9648.84 389.70 o
1 3 0 116856.63 121931.75 2042.52 o
3 3 0 86727.09 88003.30 1129.74 o
5 3 0 246616.52 251831.52 3121.73 o
7 3 0 73747.16 73903.85 854.12 o
9 3 0 148189.20 148180.88 1675.28 o
11 3 0 56324.52 56121.75 664.33 o
13 3 0 161167.73 160009.42 2473.12 o
15 3 0 8397.27 8973.87 232.88 o
17 3 0 67406.80 64627.59 1338.42 o
19 3 0 11361.26 12296.56 500.64 o
21 3 0 36910.00 36334.74 856.05 o
23 3 0 176.47 167.84 168.00 o
0 4 0 448844.91 503450.03 11972.80 o
2 4 0 1871.59 1871.29 104.81 o
4 4 0 241622.83 248851.22 3734.45 o
6 4 0 4273.38 4935.79 120.83 o
8 4 0 138191.11 135027.69 1848.67 o
10 4 0 5381.93 5343.71 114.30 o
12 4 0 104305.12 103352.95 1368.58 o
14 4 0 21664.49 21950.89 436.37 o
16 4 0 56850.56 55737.38 1175.78 o
18 4 0 24376.29 28838.12 2056.27 o
20 4 0 55884.94 54763.75 1196.68 o
22 4 0 16284.71 16604.03 505.96 o
1 5 0 167147.72 180626.70 3032.52 o
3 5 0 66010.09 65298.89 1233.45 o
5 5 0 115940.13 116509.77 1985.00 o
7 5 0 105631.13 105321.08 1361.76 o
9 5 0 57132.79 56220.93 687.91 o
11 5 0 5705.56 5483.59 220.81 o
13 5 0 88609.38 87162.60 1749.58 o
15 5 0 27383.71 27305.13 660.42 o
17 5 0 71713.45 69311.80 1612.48 o
19 5 0 3281.38 4674.78 311.13 o
21 5 0 75971.32 75345.48 1632.22 o
0 6 0 135274.00 155144.23 3725.61 o
2 6 0 5514.39 5558.82 245.58 o
4 6 0 217517.84 224661.69 3770.69 o
6 6 0 2872.64 3361.73 465.90 o
8 6 0 135696.20 134333.00 2081.48 o
10 6 0 29815.18 30509.19 419.64 o
12 6 0 137835.91 135144.91 3109.12 o
14 6 0 3441.74 3853.64 219.71 o
16 6 0 65813.52 64051.93 1368.54 o
18 6 0 11838.55 15606.67 1726.98 o
20 6 0 35164.32 33285.67 828.85 o
1 7 0 76530.98 80207.30 2695.90 o
3 7 0 33372.20 34853.57 687.35 o
5 7 0 155877.89 160672.84 2740.48 o
7 7 0 54433.48 55821.13 1026.77 o
9 7 0 79773.09 81065.40 1439.42 o
11 7 0 25707.43 25850.37 642.15 o
13 7 0 130933.73 127730.02 2542.24 o
15 7 0 35733.81 36392.71 873.50 o
17 7 0 41850.43 43044.59 1013.00 o
19 7 0 2083.89 7872.90 598.56 o
0 8 0 88105.45 94463.70 2365.82 o
2 8 0 357.73 341.25 109.42 o
4 8 0 195564.48 199077.22 3385.96 o
6 8 0 369.26 397.27 106.64 o
8 8 0 78742.24 79210.02 1424.35 o
10 8 0 6110.28 6133.74 191.40 o
12 8 0 108555.50 107589.30 1697.99 o
14 8 0 7619.01 7668.99 344.58 o
16 8 0 42472.61 43710.46 1161.59 o
18 8 0 9364.34 11233.23 1536.68 o
1 9 0 53078.07 55511.28 1054.76 o
3 9 0 88363.86 90960.80 1634.36 o
5 9 0 89645.63 89263.43 1606.99 o
7 9 0 48748.07 49098.14 947.48 o
9 9 0 28179.10 28056.27 602.39 o
11 9 0 7932.06 8061.39 286.20 o
13 9 0 65802.25 62138.08 1229.39 o
15 9 0 7955.54 8397.23 469.06 o
0 10 0 124918.49 142304.39 3528.19 o
2 10 0 68.63 96.58 123.94 o
4 10 0 88892.55 89653.32 1632.67 o
6 10 0 3649.82 3829.98 206.02 o
8 10 0 77593.52 80389.26 1478.53 o
10 10 0 5889.45 6092.00 384.56 o
12 10 0 56636.05 55067.35 1122.81 o
14 10 0 5581.61 5699.76 407.46 o
1 11 0 28525.18 30819.22 687.92 o
3 11 0 18472.01 18852.54 487.98 o
5 11 0 53269.58 54173.28 1066.49 o
7 11 0 19577.57 19463.51 812.56 o
9 11 0 63646.65 64450.30 1625.12 o
11 11 0 17793.03 17733.47 685.42 o
0 12 0 72445.51 78629.47 2111.55 o
2 12 0 9.19 195.72 134.40 o
4 12 0 44139.56 44391.57 928.01 o
6 12 0 3657.87 3604.62 226.63 o
8 12 0 62367.36 65399.61 1407.96 o
-23 1 1 827.50 514.51 175.32 o
-21 1 1 40.19 -22.93 136.52 o
-19 1 1 9.33 -5.53 79.85 o
-17 1 1 2450.64 2353.22 118.35 o
-15 1 1 1005.28 979.75 80.53 o
-13 1 1 4401.39 4184.20 126.22 o
-11 1 1 17.94 3.69 22.10 o
-9 1 1 4581.89 5037.93 83.41 o
-7 1 1 32914.49 34939.18 406.96 o
-5 1 1 35691.13 40085.59 511.50 o
-3 1 1 544.35 501.16 36.60 o
-1 1 1 1134.37 1446.47 43.28 o
1 1 1 9.62 -12.98 12.98 o
3 1 1 507.23 565.62 27.53 o
5 1 1 12010.71 11709.51 150.13 o
7 1 1 32055.37 34927.61 487.53 o
9 1 1 2357.77 2206.82 66.79 o
11 1 1 14.95 1.32 49.71 o
13 1 1 257.62 182.29 65.30 o
15 1 1 57.83 140.53 72.45 o
17 1 1 1630.77 1724.36 132.46 o
19 1 1 4216.61 3895.70 181.52 o
21 1 1 157.90 41.06 183.20 o
-24 2 1 316.22 261.37 185.63 o
-22 2 1 2.95 16.01 143.41 o
-20 2 1 658.43 734.28 127.04 o
-18 2 1 2451.99 2524.67 160.53 o
-16 2 1 840.84 1010.09 121.52 o
-14 2 1 170.83 262.05 60.88 o
-12 2 1 3201.92 3108.02 76.04 o
-10 2 1 6154.28 5708.18 110.87 o
-8 2 1 17145.58 17915.86 232.71 o
-6 2 1 3179.27 2828.80 73.18 o
-4 2 1 3765.46 3205.40 80.05 o
-2 2 1 391.69 -18.53 44.10 o
0 2 1 22492.47 23267.04 522.51 o
2 2 1 2655.91 2328.63 71.97 o
4 2 1 4351.89 4475.09 82.37 o
6 2 1 294.59 291.21 31.51 o
8 2 1 108.89 99.18 28.00 o
10 2 1 478.06 416.82 44.91 o
12 2 1 1095.74 1028.98 100.33 o
14 2 1 42.01 -24.58 67.62 o
16 2 1 398.67 435.88 101.25 o
18 2 1 894.09 1012.42 135.21 o
20 2 1 1688.41 1971.89 181.25 o
22 2 1 282.03 310.10 170.17 o
-23 3 1 12.72 -52.36 155.94 o
-21 3 1 3011.06 3433.05 218.47 o
-19 3 1 5277.18 4915.06 231.04 o
-17 3 1 11855.88 11327.52 346.41 o
-15 3 1 16.07 -4.35 87.33 o
-13 3 1 1469.26 1341.36 67.75 o
-11 3 1 1033.33 1094.24 50.80 o
-9 3 1 910.48 1201.16 49.96 o
-7 3 1 1468.48 1427.23 59.19 o
-5 3 1 6973.23 6932.09 163.22 o
-3 3 1 912.14 1028.11 69.74 o
-1 3 1 20645.57 22772.88 420.44 o
1 3 1 14779.07 14766.00 341.12 o
3 3 1 13193.52 13864.37 214.73 o
5 3 1 2.08 15.67 31.53 o
7 3 1 107.61 149.93 35.71 o
9 3 1 1578.68 1669.25 61.54 o
11 3 1 16003.67 15479.23 318.78 o
13 3 1 790.29 786.27 89.11 o
15 3 1 7016.31 6863.87 207.27 o
17 3 1 14.30 -59.07 97.92 o
19 3 1 460.80 609.07 130.08 o
21 3 1 22.89 -3.69 127.56 o
-22 4 1 8.04 -224.26 224.26 o
-20 4 1 7.54 6.86 173.72 o
-18 4 1 239.54 270.38 120.89 o
-16 4 1 7052.79 7051.47 660.94 o
-14 4 1 2457.80 2674.97 173.88 o
-12 4 1 1567.60 1776.75 70.01 o
-10 4 1 845.83 714.47 52.11 o
-8 4 1 3774.11 4156.81 138.58 o
-6 4 1 6445.88 7318.83 166.35 o
-4 4 1 26195.09 28136.32 525.96 o
-2 4 1 7348.84 7446.41 188.15 o
0 4 1 1039.66 981.79 117.66 o
2 4 1 868.15 596.10 95.55 o
4 4 1 6035.34 6527.52 141.69 o
6 4 1 762.45 824.74 83.74 o
8 4 1 0.22 -39.62 39.62 o
10 4 1 1205.51 1059.96 71.77 o
12 4 1 558.85 679.27 92.54 o
14 4 1 4770.95 4270.90 183.62 o
16 4 1 4941.98 4939.31 230.71 o
18 4 1 2381.48 2818.32 204.90 o
20 4 1 1511.51 1260.27 166.63 o
-21 5 1 796.30 812.00 161.63 o
-19 5 1 202.17 391.10 200.57 o
-17 5 1 127.23 180.43 121.78 o
-15 5 1 1081.90 1147.91 160.30 o
-13 5 1 10798.51 10215.43 240.96 o
-11 5 1 102.74 141.34 51.83 o
-9 5 1 241.86 333.13 58.51 o
-7 5 1 6859.49 7301.72 179.73 o
-5 5 1 966.91 973.72 84.31 o
-3 5 1 6874.34 7921.48 209.33 o
-1 5 1 1776.47 2100.64 118.12 o
1 5 1 144.14 270.46 71.45 o
3 5 1 882.95 1244.38 136.61 o
5 5 1 4679.76 4496.65 128.24 o
7 5 1 18950.82 19169.31 277.10 o
9 5 1 5319.67 5204.72 124.97 o
11 5 1 159.32 113.82 69.30 o
13 5 1 11.29 107.07 84.77 o
15 5 1 972.35 1063.86 149.98 o
17 5 1 1680.49 1839.44 179.86 o
19 5 1 857.10 928.20 157.46 o
-20 6 1 2746.23 3155.60 294.54 o
-18 6 1 1444.30 1751.09 300.07 o
-16 6 1 15.62 -127.14 127.14 o
-14 6 1 4494.47 4287.95 160.03 o
-12 6 1 4820.28 4756.07 153.41 o
-10 6 1 4265.74 4048.65 152.53 o
-8 6 1 4984.64 4950.12 242.43 o
-6 6 1 563.89 839.35 95.86 o
-4 6 1 462.12 404.17 136.61 o
-2 6 1 388.05 470.83 89.26 o
0 6 1 1030.29 1567.47 193.47 o
2 6 1 1071.89 1219.23 195.84 o
4 6 1 12239.44 12303.66 299.83 o
6 6 1 5681.76 5787.12 277.96 o
8 6 1 1036.91 1137.35 78.25 o
10 6 1 1745.78 1752.96 104.34 o
12 6 1 5.22 -58.93 98.76 o
14 6 1 2447.21 2741.81 199.41 o
16 6 1 1580.37 1504.24 174.11 o
18 6 1 597.84 919.60 203.73 o
-19 7 1 665.45 553.54 172.64 o
-17 7 1 21.47 117.84 145.60 o
-15 7 1 34.42 89.70 137.02 o
-13 7 1 127.69 96.47 82.32 o
-11 7 1 168.04 101.32 80.36 o
-9 7 1 10.86 17.28 117.66 o
-7 7 1 865.55 810.36 109.89 o
-5 7 1 4565.64 4273.74 189.60 o
-3 7 1 1203.60 1102.28 113.76 o
-1 7 1 5769.72 6162.44 220.27 o
1 7 1 2035.85 2631.06 180.04 o
3 7 1 1543.52 1381.60 127.14 o
5 7 1 539.47 607.71 110.41 o
7 7 1 53.37 -34.74 175.30 o
9 7 1 9.55 -67.04 67.04 o
11 7 1 366.19 608.96 92.80 o
13 7 1 134.93 272.00 135.25 o
15 7 1 150.89 214.00 139.90 o
17 7 1 7.18 40.12 235.32 o
-18 8 1 79.28 97.86 158.04 o
-16 8 1 411.97 254.73 150.54 o
-14 8 1 499.95 510.37 117.57 o
-12 8 1 127.84 196.02 175.37 o
-10 8 1 4118.04 4229.87 190.11 o
-8 8 1 3779.57 4125.97 193.97 o
-6 8 1 11228.73 10428.77 669.63 o
-4 8 1 416.65 443.69 171.36 o
-2 8 1 9217.06 9982.62 543.29 o
0 8 1 5902.07 6408.61 239.96 o
2 8 1 3094.06 2728.69 160.76 o
4 8 1 7798.96 7585.46 251.08 o
6 8 1 86.80 184.60 105.42 o
8 8 1 56.49 76.65 77.99 o
10 8 1 988.34 800.97 121.17 o
12 8 1 4.66 -62.68 139.35 o
14 8 1 278.65 162.44 169.78 o
16 8 1 1530.65 1884.01 220.31 o
-17 9 1 1064.13 1037.61 236.90 o
-15 9 1 1493.44 1445.08 255.85 o
-13 9 1 184.19 232.40 369.56 o
-11 9 1 2499.88 2613.88 193.47 o
-9 9 1 955.40 925.75 127.83 o
-7 9 1 33.93 186.65 111.08 o
-5 9 1 1725.45 1801.03 156.76 o
-3 9 1 675.07 648.17 123.94 o
-1 9 1 619.89 766.77 125.33 o
1 9 1 549.87 780.95 146.88 o
3 9 1 794.78 792.32 125.47 o
5 9 1 5632.21 5552.38 525.91 o
7 9 1 164.05 131.81 103.57 o
9 9 1 148.91 142.16 92.68 o
11 9 1 3744.69 4102.69 402.73 o
13 9 1 1855.72 1664.60 247.95 o
15 9 1 546.45 603.30 219.53 o
-14 10 1 12242.73 14021.26 552.76 o
-12 10 1 1786.09 2034.16 221.10 o
-10 10 1 1251.36 1305.99 150.62 o
-8 10 1 28.48 83.82 169.78 o
-6 10 1 2252.92 2454.59 179.11 o
-4 10 1 9361.82 9162.48 308.66 o
-2 10 1 1225.16 1179.44 146.29 o
0 10 1 611.31 480.24 130.62 o
2 10 1 371.11 201.80 115.48 o
4 10 1 1002.27 1253.70 146.24 o
6 10 1 3859.22 4257.19 214.67 o
8 10 1 473.91 620.93 108.68 o
10 10 1 1892.40 2128.37 179.21 o
12 10 1 342.44 404.31 203.73 o
-13 11 1 70.85 125.15 190.31 o
-11 11 1 1128.30 1642.49 221.10 o
-9 11 1 293.63 193.96 128.62 o
-7 11 1 2423.09 2599.46 187.25 o
-5 11 1 959.74 1074.18 145.71 o
-3 11 1 1388.54 1502.67 155.76 o
-1 11 1 26.07 17.87 126.78 o
1 11 1 77.92 39.95 121.05 o
3 11 1 2062.46 2427.52 363.24 o
5 11 1 2934.62 3266.23 287.44 o
7 11 1 51.64 12.31 116.50 o
9 11 1 34.12 63.25 135.03 o
11 11 1 5628.85 6695.65 783.34 o
-8 12 1 3797.65 4460.10 247.36 o
-6 12 1 5973.62 6191.57 299.28 o
-4 12 1 64.98 217.83 135.07 o
-2 12 1 2731.51 3002.18 216.84 o
0 12 1 993.14 1399.24 231.37 o
2 12 1 4546.85 4636.38 245.62 o
4 12 1 1191.99 1295.01 349.82 o
6 12 1 100.09 97.47 129.02 o
-24 0 2 35886.20 33794.23 1238.18 o
-22 0 2 19586.18 21025.45 854.41 o
-20 0 2 94453.77 91832.55 2710.11 o
-18 0 2 48564.34 49442.11 1550.89 o
-16 0 2 54669.05 53642.36 1089.97 o
-14 0 2 3844.07 3575.54 114.66 o
-12 0 2 123179.59 119573.37 1770.78 o
-10 0 2 15897.63 16144.92 273.04 o
-8 0 2 210994.00 218557.89 3195.51 o
-6 0 2 5802.48 5679.74 140.09 o
-4 0 2 370731.13 368532.03 13265.47 o
-2 0 2 4164.06 2662.68 292.96 o
0 0 2 390837.09 408290.06 8847.34 o
2 0 2 7650.87 7429.08 160.13 o
4 0 2 261683.86 255235.05 6609.44 o
6 0 2 2966.73 3041.77 162.67 o
8 0 2 114641.77 107789.98 2842.77 o
10 0 2 1300.77 1332.94 132.66 o
12 0 2 71023.91 69311.50 1899.92 o
14 0 2 34274.95 33111.97 1001.29 o
16 0 2 113460.48 109984.86 2167.04 o
18 0 2 13455.28 14335.31 422.29 o
20 0 2 40655.46 40691.11 1399.28 o
-25 1 2 40939.94 40353.78 1026.29 o
-23 1 2 4760.18 5639.29 301.22 o
-21 1 2 90014.61 88488.51 1871.09 o
-19 1 2 15125.46 17074.59 490.65 o
-17 1 2 82166.56 81735.27 1340.02 o
-15 1 2 12945.07 13046.20 265.95 o
-13 1 2 108676.05 107551.92 1220.53 o
-11 1 2 74810.98 76146.13 871.54 o
-9 1 2 178976.38 183183.52 2044.41 o
-7 1 2 46185.64 48118.30 614.47 o
-5 1 2 63888.29 66947.08 959.93 o
-3 1 2 235465.27 260698.28 10336.51 o
-1 1 2 246484.45 261680.20 4141.03 o
1 1 2 37656.43 38410.20 486.55 o
3 1 2 60887.20 63315.24 789.64 o
5 1 2 163280.67 161201.20 2325.55 o
7 1 2 107959.03 112906.14 1640.36 o
9 1 2 97319.16 95632.98 1798.52 o
11 1 2 24165.03 23545.85 430.28 o
13 1 2 73789.61 73631.96 1190.91 o
15 1 2 22832.28 25630.84 489.65 o
17 1 2 88050.71 84590.44 1497.04 o
19 1 2 10302.56 10648.52 308.79 o
21 1 2 40146.00 36859.37 929.67 o
-24 2 2 19797.96 19325.88 603.85 o
-22 2 2 7421.81 9139.46 369.32 o
-20 2 2 96669.56 94028.43 2628.77 o
-18 2 2 10743.20 11554.64 342.92 o
-16 2 2 115479.44 112290.63 2181.04 o
-14 2 2 3593.89 3844.92 99.16 o
-12 2 2 231525.73 229423.13 2566.41 o
-10 2 2 31874.31 31030.16 406.65 o
-8 2 2 177716.25 181967.64 2264.66 o
-6 2 2 27677.17 27586.48 374.37 o
-4 2 2 185150.38 186337.64 3724.05 o
-2 2 2 1088.81 807.01 157.14 o
0 2 2 202693.28 207336.23 2470.65 o
2 2 2 14288.55 14873.59 192.82 o
4 2 2 190771.36 196993.50 2203.86 o
6 2 2 16662.77 16359.14 213.08 o
8 2 2 243168.44 242523.61 2704.47 o
10 2 2 628.36 964.13 79.01 o
12 2 2 123867.76 120425.09 1885.51 o
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